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    Salt Analysis 7

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    tiwarimradul22

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    Salt Analysis 7

    Uploaded by

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    5 views2 pages

    Salt Analysis 7

    Uploaded by

    tiwarimradul22

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    of 2

    EPERIMENT-7

    AIM:- To identify the presence of acidic and basic radical in the given inorganic compound.

    MATERIAL REQUIRED: - Given inorganic compound, Test tubes, Test tube holders, Beaker,
    Glass rod, Dropper, Water Bottle, and Burner

    OBSERVATION TABLE:-

    1. TEST FOR ACIDIC RADICAL:

    S.NO. EXPERIMENT OBSERVATION INFERENCE


    1. Given inorganic salt + Conc. H2SO4 Colourless or Yellowish gas Chloride (Cl-) may be
    and then heat strongly. with pungent smell is evolved present.
    out.

    2. Bring a glass rod dipped in NaOH White dense fumes appear. Chloride (Cl-) is
    solution to the mouth of test tube. confirmed.

    3. Silver Nitrate Test: To a given Curdy white ppt. which is Chloride (Cl-) is
    inorganic salt add 1 ml dilute HNO3 insoluble in conc. HNO3 confirmed.
    and boil. Add silver nitrate solution
    to it.
    4. Shake the ppt. with excess of White ppt. soluble. Chloride (Cl-) is
    NH4OH solution. confirmed
    5. MnO2 Test: Salt solution+ MnO2 + White ppt. soluble. Chloride (Cl-) is
    Conc. H2SO4 and then heat. confirmed.

    2. TEST FOR BASIC RADICAL:

    S.NO. EXPERIMENT OBSERVATION INFERENCE


    1. White. Cu , Ni2+, Fe3+, Co2+,
    2+

    Colour of Inorganic salt is observed. Mn2+ is absent.

    2. Smell Ammonical. NH4+ ( Zero group) may


    be present
    3. To a given inorganic salt in a test Formation of white fumes with NH4+ may be present
    tube add 1 ml conc. NaOH solution ammonical smell
    and then heat.
    4. To a given inorganic salt add water Formation of brown colour ppt. NH4+ confirmed.
    and then add Nessler’s reagent along
    the sides of a test tube
    5. Salt solution + Conc. HCl and then Dense white fumes appear. NH4+ may be present
    bring a glass rod dipped in HCl to
    the mouth of test tube.

    RESULT: - The given unknown inorganic compound contains:

    Acidic Radical: Chloride (Cl-) ion

    Basic Radical: Ammonium (NH4+) ion (Zero Group)

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