ORGANISATION INTERNATIONALE DE NORMALISATION MEXC(YHAPOflHAFI OPTAHM3A~MR I-IO CTAHflAPTM3A~MM
Copper and topper alloys - Selection and preparation
of samples for Chemical analysis -
Part 2 : Sampling iTeh STANDARD of wrought PREVIEW products and castings (standards.iteh.ai) Cuivre et al.iages de cuivre - Selec tion et prbparaISO 1811-2:1988 tion des &han tillons pour l’analyse chimique - https://standards.iteh.ai/catalog/standards/sist/421167f3-fb0d-4e01-ae34- Partie 2 : ichantillonnage des produits 46ed3f1f96b3/iso-1811-2-1988 corroytk et des produits moulks
Reference number ISO 181l-2: 1988 (E) ISO 1811-2 : 1988 (EI
Foreword ISO (the International Organization for Standardization) is a worldwide federation of national Standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Esch member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, govern- mental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are circulated to
the member bodies for approval before their acceptance as International Standards by iTeh STANDARD PREVIEW the ISO Council. They are approved in accordance with ISO procedures requiring at least 75 % approval by the member bodies voting. (standards.iteh.ai) International Standard ISO 181 l-2 was prepared by Technical Committee ISO/TC 26, Copper and topper alloys. ISO 1811-2:1988 https://standards.iteh.ai/catalog/standards/sist/421167f3-fb0d-4e01-ae34- Together with ISO 181 l-l and 181 l-3, it cancels and 46ed3f1f96b3/iso-1811-2-1988 replaces ISO Recommendation R 1811 : 1971, of which it constitutes a technical revision.
ISO 1811 consists of the following Parts, under the general title Copper and topper alloys - Selection and prepara tion of samples for Chemical analysis:
- Part 7 : Sampling of cast unwrought products
- Part 2 : Sampling of wrought products and castings
- Part 3 : Sampling of cathodes
0 International Organkation for Standardkation, 1988
Printed in Switzerland INTERNATIONAL §TANDARD ISO 1811-2 : 1988 (E)
Copper and topper alloys - Selection and preparation
of samples for Chemical analysis -
Part 2 : Sampling of wrought products and castings
1 Scope 3 Def initions
. This part of ISO 1811 specifies methods for the selection and For the purposes of this part of ISO 1811, the definitions for preparation of samples for Chemical analysis of topper and topper and topper alloys in ISO 197-1, for wrought products in topper alloys in the form of wrought products and castings.1) ISO 197-3 and for castings in ISO 197-4 apply.
The methods specified in this patt of ISO 1811 apply to topper
iTeh STANDARDIn addition, PREVIEW and topper alloys in the following forms, and are intended to the following definitions apply. determine compliance with the requirements for their Chemical composition : (standards.iteh.ai) 3.1 lot: Unless othewise agreed between supplier and pur- chaser, for the purpose of sampling, a lot shall be defined as a) wrought products, including plate, sheet, Strip,ISO rod, follows: 1811-2:1988 bar, tube, Profile, forgings, etc.; https://standards.iteh.ai/catalog/standards/sist/421167f3-fb0d-4e01-ae34- b) castings, including sand castings, chill 46ed3f1f96b3/iso-1811-2-1988 castings, die 3.1.1 lot of wrought products: Material of the same alloy castings, continuous castings, centrifugal castings. and of a particular form, such as plate, sheet, Strip, rod, bar, tube, Profile, wire or forgings, made during the same produc- tion sequence under uniform conditions. 2 Normative references Materials processed under different conditions shall be con- The following Standards contain provisions which, through sidered as separate lots. reference in this text, constitute provisions of this patt of ISO 1811. At the time of publication, the editions indicated 3.1.2 lot of castings: Material of a particular form produced were valid. All Standards are subject to revision, and Parties to by, for instance, sand casting, chill casting, die casting or cen- agreements based on this part of ISO 1811 are encouraged to trifugal casting from a Single melting furnace Charge or from a investigate the possibility of applying the most recent editions particular cycle of a continuous melting furnace. of the Standards listed below. Members of IEC and ISO main- tain registers of currently valid International Standards. 3.2 sampling unit: An individual wrought product or ISO 197-1 : 1983, Copper and topper alloys - Terms and casting selected from a lot. de finitions - Part 7: Ma teriak.
ISO 197-3 : 1983, Copper and topper alloys - Terms and 3.3 gross Sample: The total amount of all sampling units de finitions - Part 3: Wrought products. taken from a lot.
ISO 197-4 : 1983, Copper and topper alloys - Terms and 3.4 test Sample: A Sample prepared from the gross Sample de finitions - Part 4: Castings. and from which the test portions will be taken. ISO 181 I-1 : 1988, Copper and topper alfoys - Selection and preparation of samples for Chemical analysis - Part 1: Sam- 3.5 test Portion: The quantity of material taken from the pling of unwrought products. test Sample and on which the analysis is actually carried out,
1) Sampling theory is explained in annex A of ISO 1811-1.
ISO 1811-2 : 1988 (EI ,
4 Selection of sampling units 5 Sample preparation
Unless otherwise agreed between supplier and purchaser, the 5.1 Wrought products and castings shall be sampled either following number of sampling units shall be selected from a by sawing and milling the entire Cross-section, or by drilling en- Single lot. tirely through the sampling unit at several Points along its length. Products too thin to be handled conveniently for machining shall be sampled by clipping. 4.1 General procedure 5.2 Before sampling, the sampling units shall be clean and Sampling units shall be selected randomly from a lot. When free from scale, dirt, Oil, grease and other contaminants. lf sampling units are to be taken from final products, necessary, the sampling units may be cleaned in ethyl ether or arrangements shall be made for the necessary excess length or acetone, rinsed in ethanol, and dried. Scale and dirt may be amount of material to be provided. removed by suitable mechanical or Chemical treatment. If Chemical methods of cleaning are used, such operations shall By agreement between supplier and purchaser, sampling units not alter the metal surface in any way. taken at the time of casting, or broken tensile test pieces or other physical test pieces may be used as sampling units 5.3 The saw, drill, Cutter or other tool used for sampling shall instead of taking sampling units from the product. be thoroughly cleaned Prior to use. The Speed of sampling shall be so regulated that excessive heating and consequent Oxidation of the Sample is avoided. Lubricants shall not be 4.2 Wrought products used. Carbide-tipped tools are recommended; steel tools, if used, shall be made of magnetic material to assist in the subse- quent removal of extraneous iron. 4.2.1 Rods, bars, shapes, sheet, Strip, plate and wire 5.4 For alloys with magnetic phases, carbide-tipped tools The sampling units shall be taken from’ four individual lengths shall be used; magnetic cleaning shall not be used. Drillings, iTeh STANDARD PREVIEW of finished product. lf the lot consists of less than four lengths, millings, sawings or clippings of alloys with no magnetic phases one sampling unit shall be taken from each individual length. shall be treated carefully with a strong magnet to remove any (standards.iteh.ai) particles of iron introduced during sampling. The drillings, mill- ings, sawings or clippings shall be carefully examined, and any 4.2.2 Tu bes foreign material introduced in taking the Sample shall be ISO 1811-2:1988 removed. https://standards.iteh.ai/catalog/standards/sist/421167f3-fb0d-4e01-ae34- The sampling units shall be taken from each lot accordi ng to the schedule in table 1. 46ed3f1f96b3/iso-1811-2-1988 5.5 In certain cases a complete Cross-section from a sampling unit may be required for spectrometric examination. Esch Cross-section shall be taken and properly marked before using the remainder of the sampling unit in other sampling Table 1 - Sampling frequency - Tubes operations. Number of tubes Number of sampling to be takenl) 5.6 The gross Sample shall be prepared by thoroughly mixing equal masses sf drillings, millings, sawings or clippings taken 51 to 200 2 from each sampling unit. The Chips obtained by milling, drilling, 201 to 1 500 3 etc., shall be uniformly small in size. over 1 500 0,2 % of the number of tubes, to a maximum of IO pieces 5.7 The gross Sample shall weigh at least four times the 1
1) Esch sampling unit shall be taken from a different tube. amount required for the analysis, and shall be divided into four test samples of equal mass, each of which shall be placed in a Container and sealed: one for the supplier, one for the pur- chaser, one for reference purposesl if necessary, and one as reserve. 4.3 Castings 5.8 In the event of the Oxygen content of Cu-OFE (and At least one sampling unit shall be selected from each furnace Cu-KP if necessary) being determined, an additional group of Charge of molten metal, or during a two-hour period of con- test samples shall be taken from the selected sampling units. tinuous melting and casting, or at the beginning, middle and Esch test Sample for Oxygen determination shall consist of a end of each shift. When sampling units are cast, the liquid Single piece of adequate size, tut from the sampling unit by a metal shall be poured at a temperature above that of the li- method agreeable to both Producer and purchaser at a mutu- quidus, so that it is homogeneous, into a small chill mould. ally agreeable location in the sampling unit. Esch test Sample shall be tut into three test portions of approximately equal In cases in which several furnace charges are mixed in a ladle mass: one for the Producer, one for the purchaser, and one for Prior to pouring, one sampling unit shall be taken from the reference purposes, if necessary. Esch Party shall determine combined melts Prior to pouring the castings. Oxygen on his test Portion using an agreed procedure. iTeh STANDARD PREVIEW (standards.iteh.ai) This page intentionally lef? blank
ISO 1811-2:1988 https://standards.iteh.ai/catalog/standards/sist/421167f3-fb0d-4e01-ae34- 46ed3f1f96b3/iso-1811-2-1988 iTeh STANDARD PREVIEW (standards.iteh.ai) This page intentionally left blank
ISO 1811-2:1988 https://standards.iteh.ai/catalog/standards/sist/421167f3-fb0d-4e01-ae34- 46ed3f1f96b3/iso-1811-2-1988 iTeh STANDARD PREVIEW (standards.iteh.ai) This page intentionally left blank
ISO 1811-2:1988 https://standards.iteh.ai/catalog/standards/sist/421167f3-fb0d-4e01-ae34- 46ed3f1f96b3/iso-1811-2-1988 ISO 1811-2 : 1988 (EI
iTeh STANDARD PREVIEW
(standards.iteh.ai) ISO 1811-2:1988 https://standards.iteh.ai/catalog/standards/sist/421167f3-fb0d-4e01-ae34- 46ed3f1f96b3/iso-1811-2-1988
