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    MSC 3 Sem Chemistry Analytical Chemistry 1 Winter 2018

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    ehsthvt8
    The document discusses analytical chemistry topics like thermal and electroanalytical methods. It contains 5 units that cover principles and applications of techniques like DTA, DSC, coulometric titration, potentiometry, polarography and spectroscopy. Example calculations and analysis of methods are provided.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd

    MSC 3 Sem Chemistry Analytical Chemistry 1 Winter 2018

    Uploaded by

    ehsthvt8
    69 views2 pages
    The document discusses analytical chemistry topics like thermal and electroanalytical methods. It contains 5 units that cover principles and applications of techniques like DTA, DSC, coulometric titration, potentiometry, polarography and spectroscopy. Example calculations and analysis of methods are provided.

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    Msc 3 Sem Chemistry Analytical Chemistry 1 Winter 2018

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    The document discusses analytical chemistry topics like thermal and electroanalytical methods. It contains 5 units that cover principles and applications of techniques like DTA, DSC, coulometric titration, potentiometry, polarography and spectroscopy. Example calculations and analysis of methods are provided.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    69 views2 pages

    MSC 3 Sem Chemistry Analytical Chemistry 1 Winter 2018

    Uploaded by

    ehsthvt8
    The document discusses analytical chemistry topics like thermal and electroanalytical methods. It contains 5 units that cover principles and applications of techniques like DTA, DSC, coulometric titration, potentiometry, polarography and spectroscopy. Example calculations and analysis of methods are provided.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 2

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    com/

    AV -207 4

    M.Sc. Semester III


    (CBCS) Erlmiution
    CIIEMISTRY (New)
    Paper-X
    Analytical Chemistry I (Thcrmal and ElectroaDllytical Methods)
    Time : Three Hours] f\,laximum Niarks : 80
    :{.8. :-(i) All questions arc compulsory.
    (2) All questions carry cqual marks-
    (3) Ose of calculator is permitled.
    (4) l)rarv labellcd diagrams *'hcrever necessary.
    UNIT-I
    1. (a) l-xplain the principle D'l'-{.
    and technique in (:

    (b) Explain the $,orking principlc of DSC. 5

    (c) A mixlure containing MgO and Ii,lgCO. undergoes a maximum weight loss of 15.6% by
    dccomposition lbmring CO,. Cdculate the weight percentage ofeach ofthe two components
    in the mixlurc. 5

    OR
    (p) What are the thermal methods of analysis ? Give the classilicalion of rhermal melhods
    of analysis. 6
    (q) Ilxplain various factors atlecting DTA curves. 5

    (r) Discuss the principal and dilltrent q'pcs of themomctric titrations. 5

    UNIT II
    2. (a) Explain lhe principle analysis.
    and instrumentation in coulometlic 6

    (b) Discuss the various applications of high iiequency titration. 5

    (c) Explain the principlc involved in electrogravimetric cstimation of binary nrixture of


    melrli. 5

    OR
    (p) Explain Coulomclric titrations and gjve theiradvantages. 6

    (q) l)iscuss the various applications of high liequelcy titmtion. 5

    (r) F.xplain the principle and tcchnique in clcctrogmvimctric analysis. 5

    UNIT III
    3. (a) F.xplain construolion and r-r'orking of Glass elecrode. llow pH can be detenrlined by
    this electrode ? 6

    (b) u/hat are ion seleclive elcctodes ? Fixplain working of sodium ion selective clectrode.
    5

    (c) Civc explanatory nole on bio-scnsors. 5

    OR

    wPz-10281 (Conld.)

    http://www.sgbauonline.com/
    http://www.sgbauonline.com/
    (p) \Vrir.e brief flotcs on .

    (i) ELcctochemical Sensor


    (ii) Potentionrelric Sens(,r. 6

    (q) What are the applicrlions ol chcmical sensors in agricultrue al:'d biotechnolog)' ? 5

    t) Gi\'3 the principLe inr o1r eil in ion scleclivc ele!trodcs- \\'hat are their advanlagcs and
    lirnrLatron:

    \l l-I\/ t
    I (r) Iixylain types oi current: rn polarogralph]. 6

    (b) Wrile short note on 'Su,rporling cleclrol)'tc" in polarography. 5

    (c) Explain thc principl: of cyclic volramelry and gile its appllcarions. 5

    OR
    (p) Define "Polarographic N{axilna". Hou is it renroved ? 6

    (q) Calculate the dillusion coellicient of an ion that gires dillusion cunent of l0 +A in
    a crll $'ith folloning properties. n- 2 t - 3.02 s, m:4.3 mg/s, C = 10 mM.

    G) What are ampelonletric titfations 1 Lxflain its principle and methodology. 5

    U\I1'-\'
    5. (u) Discuss the applicalioDs of spectrophotoIrrctr] in biomolccular anal.vsis $ith suitable
    example. 6

    (b) Wbat is meant b,v :L-ssa), ? Discuss il assay.


    hrief mcthod ol dry 5

    (c) Discuss thc priociplc and nalure 01'various types of ge1s. 5

    oR
    (p) IIo.x will Jou detemrure llv qui ti{ ol \iiliunin B from lbod stull by s}rectrofluolotnetJ ?
    Explain in brief. 6
    (q) Di-c,r.. rarious appli.. i, ns ol'ulrra(er triru[,rl:.r' j
    (r) \\irite brief account lxl lrcavy mctal toxicity and rheir remed-v. j

    \\,PZ 102E4 125

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