ABB - NAV 500 Sodium SWAS
ABB - NAV 500 Sodium SWAS
ABB - NAV 500 Sodium SWAS
A B B M E A S U R E M E N T & A N A LY T I C S | O P E R AT I N G I N S T R U C T I O N | O I/A S O 5 5 0 - E N R E V. G
Navigator 500
Sodium analyzer
—
Navigator 500 Introduction
sodium analyzer
The Navigator 500 sodium analyzer is designed to
provide continuous monitoring and control of power
station boiler feed water / steam condensate.
Commisioning Instruction
Navigator 550 CI/ASO550-EN
Sodium wet-section
Commisioning Instruction
Navigator 540 CI/AWT540-EN
Transmitter
Navigator 500
Sodium analyzer Contents
Contents
1 Health & Safety ................................................................ 3 5 Calibration ..................................................................... 21
1.1 Safety precautions ................................................... 3 5.1 Accessing the Configuration level menus ............... 21
1.2 Potential safety hazards ........................................... 3 5.2 Performing a calibration for the first time –
1.2.1 Navigator 550 sodium wet-section – single-stream wet-section ...................................... 22
electrical ....................................................... 3 5.3 Performing a calibration for the first time –
1.2.2 Navigator 550 sodium wet-section – multi-stream wet-section ....................................... 23
chemical reagents ......................................... 3 5.4 Calibration parameters – offset and slope .............. 24
1.2.3 Navigator 540 transmitter – electrical ............ 3 5.5 Calibration options ................................................. 24
1.3 Safety standards ...................................................... 3 5.5.1 Scheduled calibration ................................. 24
1.4 Safety conventions ................................................... 4 5.5.2 Monitoring calibration progress .................. 24
1.5 Symbols ................................................................... 4 5.5.3 Abort calibration ......................................... 24
1.5.1 Navigator 550 sodium wet-section ............... 4 5.5.4 Process calibration procedure .................... 25
1.5.2 Navigator 540 transmitter ............................. 5 5.5.5 Grab sample .............................................. 28
1.6 Product recycling and disposal (Europe only) ........... 5 5.6 Calibration timings ................................................. 28
1.6.1 End-of-life battery disposal ........................... 5 5.6.1 Recovery period ......................................... 28
1.7 Restriction of Hazardous Substances (RoHS) ........... 5 5.7 Regeneration procedure ........................................ 28
OI/ASO550–EN Rev. G 1
Navigator 500
Sodium analyzer Contents
2 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 1 Health & Safety
Warning. To ensure safe use when handling chemicals, the following points must be observed:
Review the Material Safety Data Sheets prior to handling containers, reservoirs, and delivery systems that contain chemical
reagents and standards.
Protective eye wear and hand wear must always be used when contact with chemicals is possible.
Normal safety precautions must be taken to avoid the possibility of an accident occurring when operating in conditions of
high pressure and / or temperature.
Chemicals must be stored away from heat, protected from temperature extremes and powders kept dry.
When disposing of chemicals ensure that no two chemicals are mixed.
Safety advice concerning the use of the equipment described in this manual or any relevant Material Safety Data Sheets (where
applicable) may be obtained from the Company, together with servicing and spares information.
Warning. To ensure safe use when operating this equipment, the following points must be observed:
Up to 240V AC may be present. Be sure to isolate the supply before removing the terminal cover.
Normal safety precautions must be taken to avoid the possibility of an accident occurring when operating in conditions of
high pressure and / or temperature.
Safety advice concerning the use of the equipment described in this manual or any relevant Material Safety Data Sheets (where
applicable) may be obtained from the Company, together with servicing and spares information.
OI/ASO550–EN Rev. G 3
Navigator 500
Sodium analyzer 1 Health & Safety
Warning. In this manual, a warning is used to indicate a condition which, if not met, could cause serious personal injury and / or
death. Do not proceed beyond a warning until all conditions have been met.
Caution. A caution is used to indicate a condition which, if not met, could cause minor or moderate personal injury and / or
damage to the equipment. Do not proceed beyond a caution until all conditions have been met.
Note. A note is used to indicate important information or instructions that should be considered before operating the equipment.
1.5 Symbols
1.5.1 Navigator 550 sodium wet-section
Symbols that appear on this product are shown below:
This symbol, when noted on a product, indicates a potential hazard which could cause serious personal injury and / or
death.
The user should reference this instruction manual for operation and / or safety information.
This symbol identifies a risk of chemical harm and indicates that only individuals qualified and trained to work with
chemicals should handle chemicals or perform maintenance on chemical delivery systems associated with the
equipment.
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems. In
conformity with European local and national regulations, European electrical equipment users must now return old or
end-of-life equipment to the manufacturer for disposal at no charge to the user.
4 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 1 Health & Safety
Protective earth.
This symbol, when noted on a product, indicates a potential hazard which could cause serious personal injury and / or
death.
The user should reference this instruction manual for operation and / or safety information.
This symbol, when noted on a product enclosure or barrier, indicates that a risk of electrical shock and / or electrocution
exists and indicates that only individuals qualified to work with hazardous voltages should open the enclosure or remove
the barrier.
Note. For return for recycling, please contact the equipment manufacturer or supplier for instructions on how to return end-of-life
equipment for proper disposal.
OI/ASO550–EN Rev. G 5
Navigator 500
Sodium analyzer 2 Overview
2 Overview
2.1 Navigator 550 sodium wet-section
The Navigator 550 sodium wet-section has been designed for use with an ABB Navigator 540 transmitter to provide continuous
monitoring and control of power station boiler feed water / steam condensate. Sampling points include mixed bed outlets in water
treatment plants, extraction pump discharge, boiler feed, boiler drum and steam.
The wet-section contains a sodium ion responsive electrode and a silver / silver chloride reference electrode housed in an acrylic
flowcell. The electrode pair measures the sodium concentration in the sample. The flowcell houses a temperature sensor for
temperature compensation, sample stream valves and calibration valves.
The measurement range specification is 0.01 ppb to 10,000 ppb. The correct pH value of the sample is achieved by pre-treatment
with an alkaline vapor*. Calibration is achieved by exposing the sensor to calibration solution* with the low and high calibration valves.
A calibration can be initiated manually when required, or automatically with programmable daily frequency ranges, from 1 to 7 days
and 1 to 8 weeks.
*For information about reagent solutions, contact the local ABB representative.
Reagent bottle
Calibration solution 1 bottle
Calibration solution 2 bottle
Bottle carrier
Quick-disconnect (QD)
couplings to solution bottles
Constant-head unit
Reagent tube to entrainment T-piece Navigator 500 Regeneration solution tubing (optional) to
Calibration + Regeneration valve
Fig. 2.1 Sodium wet-section main components (multi-stream version without flowmeters shown)
6 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 2 Overview
Mounting bracket
Display
Keypad
Transmitter door lock
OI/ASO550–EN Rev. G 7
Navigator 500
Sodium analyzer 3 Installation
3 Installation
3.1 Installing the wet-section
3.1.1 Sample requirements 3.1.2 Location
Ensure the sampling point is as close as possible to the For general location requirements refer to Fig. 3.1. Install in a
wet-section and provides a thoroughly-mixed representative clean, dry, well ventilated and vibration-free location giving easy
sample. access. Avoid rooms containing corrosive gases or vapors, for
example, chlorination equipment or chlorine gas cylinders.
Sample must contain less than 10 ppm suspended solids
with a particle size no greater than 60 µm. (If particle sizes Select a location away from strong electrical and magnetic
exceed 60 µm, use a 60 µm filter.) fields. If this is not possible, particularly in applications where
mobile communications equipment is expected to be used,
Sample temperature must be within the range 5 to 55 °C
screened cables within flexible, earthed metal conduit must be
(41 to 131 °F).
used.
Sample flow rates must be within the range 100 to 400
The standard solution and reagent containers are mounted at
ml/min (6.10 to 24.4 to cu in./min.).
the top of the wet-section panel. Standard solution containers
Sample must not exceed 1.5 bar gauge (21.75 psi). are connected via quick-disconnect (QD) couplings. If the
transmitter has to be mounted directly above the wet-section,
allow at least 270 mm (11 in.) separation between the two units
for access to solution containers.
55 °C
(131 °F)
Max. Navigator 500
Navigator 500
0 °C
(32 °F)
Min.
Humidity
0 to 95 %
8 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 3 Installation
Note. Clearance – the enclosure doors can open 180°. If mounting in a confined area, allow sufficient clearance for
door opening.
Dimensions in mm (in.)
Ø 7 (0.27)
Navigator 500
(26.30)*
668
384.8
384.8 CTRS
(15.15) 480
480
(18.90)
2 Holes Ø 7
(0.27)
80.2 (3.15)
18
210 (8.27) 110.5
110.5 281 290218.7 (0.7)
(4.35) (11.06 in.) (11.41 in.)
185
*When installing, allow a further 60 mm (2.36 in.) min. to remove the bottle carrier assembly,
or 135 mm (5.31 in.) min. to remove the calibration solution bottle from the carrier.
210 (8.27)
OI/ASO550–EN Rev. G 9
Navigator 500
Sodium analyzer 3 Installation
Note.
Sample inlet tubing to the base of the wet-section is customer-supplied.
Sample inlet tubing must have sufficient wall thickness to withstand the highest sample pressure. Keep tubing lengths
short.
Keep sample drains as short as possible and vertical to enable the sample to drain freely.
Where particulate matter is present (for example, magnetite in boiler samples) it is recommended that a 60 micron sample
filter is fitted to the sample inlet line.
3. Ensure the wet-section internal sample stream drain tubing and sample outlet tube is routed through the drain outlets at the
base of the wet-section and through the funnel E – refer to Fig. 8.5, page 65 (multi-stream) or Fig. 8.7, page 67
(single-stream) for tubing location details at the base of the wet-section enclosure.
4. Connect the flowcell drain tubing (customer-supplied) to the barbed connector at the base of the wet-section F.
Navigator 500
10 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 3 Installation
Nav
igat
or 500
Entrainment
T-piece
To constant-head unit
Calibration + Regeneration
valve assembly
To flowcell
OI/ASO550–EN Rev. G 11
Navigator 500
Sodium analyzer 3 Installation
186 +1.1
–0
(7.32 +0.04
–0 )
Avoid vibration
40 (1.57)**
40 (1.57)
Panel cut-out dimensions*
12 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 3 Installation
Fixing centers
194 62
(7.64) (2.44)
66 Ø6.4
(2.40) (0.25)
98 (3.85)
66 (2.6)
Fig. 3.9 Transmitter wall-mount option
Note.
Maximum length of cable from transmitter to
single-stream wet-section(s) = 30 m (92 ft.).
Multi-stream wet-sections cannot be connected.
Transmitter
30 m (92 ft.)
Maximum length of cable –
transmitter to (last) single-stream
Pipe diameters: wet-section
max. 62 (2.44) / min. 45 (1.77) Pipe-mount kit
– optional
L1 L2 L3 L4
Vertical Horizontal
configuration configuration
Multiple wet-sections connected in series
L1 + L2 + L3 + L4 = <30 m (92 ft.)
Fig. 3.8 Transmitter pipe-mount options
OI/ASO550–EN Rev. G 13
Navigator 500
Sodium analyzer 3 Installation
Note.
For single wet-section systems, the Modbus cable is connected to the wet-section at the factory – only transmitter
connections are required.
If additional wet-sections are added they must be connected in series – refer to Appendix C, page 78.
The following procedure is required only when connecting additional wet-sections to an existing analyzer.
Warning. Isolate power supplies to the transmitter and wet-section before attempting to access the wet-section PCB.
Note. When refitting the cover, ensure that the O-ring seal D in the PCB housing is located correctly in its groove.
14 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 3 Installation
OI/ASO550–EN Rev. G 15
Navigator 500
Sodium analyzer 3 Installation
16 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 3 Installation
I/O MODULE 3
F E
J
H
OI/ASO550–EN Rev. G 17
Navigator 500
Sodium analyzer 3 Installation
COMMUNICATIONS
RS485 SMART SENSOR
INTERFACE MODULE ANALOGUE OUTPUT BOARD
CM40/0215 ISS.1 CM40/0235
(shown fitted)
MODULE
COM
COM
N/C
N/C
+
–
+
–
SK4 SK5
SK5
Optional SK2
FUSE RATING
SCREEN
GREEN
BLACK
~100 – 240V
WHITE
RED
3.15A (T)
50/60 Hz
communications module I/O MODULE 2 I/O MODULE
I/O MODULE 3
(shown fitted)
DIO COM
DIO1
DIO2
DIO3
DIO4
DIO5
DIO6
COM
COM
COM
COM
+24V
N/C
N/C
N/C
N/C
+ – + –
N/C
N/C
N/C
N/C
INT
1 2 3 4 5 N L
(Ethernet)
3 and 4 (optional)
Analog outputs
SK1
COMMUNICATIONS
CM40/0215 ISS.1
COM
COM
N/C
N/C
+
+
–
–
SK4 SK5
Relay connections
5 and 6 (optional)
5 6
SK2
FUSE RATING
~100 – 240V
SCREEN
GREEN
BLACK
WHITE
3.15A (T)
50/60 Hz
RED
I/O MODULE 3
DIO COM
COM
COM
COM
COM
DIO1
DIO2
DIO3
DIO4
DIO5
DIO6
+24V
N/O
N/O
N/O
N/O
+ – + –
N/C
N/C
N/C
N/C
1 2 3 4 5 N L
INT
Comms. connections Digital I/O Analog output Relay connections Mains supply 100 V to 240 V
(Ethernet) connections connections 1 and 2 1 to 4 (standard) AC ±10 % (90 V min. to 264 V
(standard) max.) 50 / 60 Hz
Wet-section terminal connections Fuse 3.15 A Type T 100 to 240 V, 50/60 Hz
N/O COM
Load L N
DIO 1 – 6 Load
COM N/C L
N Load
N/C
Load L
18 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 4 Setup
4 Setup
This section describes how to set the analyzer up for first-time 7. Remove the supplied O-ring J (temporarily secured to
use. the top of the right-hand chamber) and fit it over the
reference electrode body.
If multiple wet-sections are to be connected to a transmitter, an
additional setup procedure is required – see Appendix C, page 8. Carefully position the reference electrode centrally in the
78. right-hand chamber K so that the ceramic plug L is
between 5 and 10 mm (0.2 to 0.4 in.) from the bottom of
Caution. Do not attempt to setup the analyzer unless the the chamber.
wet-section and transmitter are fully installed and ready for 9. Ensure O-ring M is fitted at the top of reference
operation. electrode.
10. Connect black-sleeved reference electrode connector N
4.1 Setting-up the wet-section to the top of reference electrode and tighten.
4.1.1 Fitting the electrodes
OI/ASO550–EN Rev. G 19
Navigator 500
Sodium analyzer 4 Setup
4.1.2 Fitting and filling the reservoir (option) 4.1.3 Sensor panel
1. Fill the reagent solution container with appropriate
Note. The reservoir is supplied partially-assembled. solution.
Assemble only immediately before using the wet-section (to 2. Open the shut-off valve upstream of the wet-section panel
avoid the possibility of solution drying out if the wet-section and adjust it until sample is overflowing from the overflow
is stored for any length of time). pipe of the constant-head unit.
The maximum and minimum flow rates are 400 to 100
Referring to Fig. 4.2: ml/min (24.4 to 6.10 cu in./min).
1. Push reservoir A into clip B. 3. Ensure that sample is passing from the constant-head unit
2. Slide the lower end of the reservoir tube C onto to the flowcell and that the entrainment of reagent is
reference electrode filler tube D. operating; the entrainment should be regular, not
intermittent.
Note. Ensure the reservoir tube is not kinked and Allow at least one hour before carrying out a calibration.
does not contain air bubbles.
4. If the wet-section is a multiple wet-section configuration,
3. Remove filler cap E from the reservoir A. check / set the DIP switches on the wet-section PCB –
see Appendix C, page 78.
4. Fill the reservoir with 3.5 KCI solution and squeeze the
reservoir tube C repeatedly to expel any bubbles. 5. Start-up the transmitter as described in the Section 4.2.
5. Unscrew filler plug G 1 turn from the fully-closed position 6. Perform a two-point calibration:
to avoid creating a vacuum. – for single-stream wet-sections refer to Section 5.2,
6. Ensure O-ring F is in place and replace filler cap E. page 22
– for multi-stream wet-sections refer to Section 5.3,
page 23
20 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 5 Calibration
5 Calibration
This section describes how to calibrate the analyzer once it is 5.1 Accessing the Configuration level menus
operational. Calibrations are initiated via the Cal prompt The configuration level menus are used to configure the
displayed on Operator pages, or via the Calibration Level and wet-section(s) and set parameter values – see Fig. 7.1, page 42
Advanced Level menus or as a Scheduled calibration. for an overview of menus.
To enter Configuration Level menus:
Note.
1. Press the key (below the icon).
Calibration menus can be accessed from the
Advanced level only – refer to Section 5.1 to access Navigator 10 : 34: 52
2012–04–15
4.28
Allow at least 1 hour for the wet-section to stabilize Data Views
before running a calibration. Logs ppb
Alarm Acknowledge
Manual Hold
Autoscroll 21.7 °C
Media Card
Enter Configuration
Access Level
Read Only
Calibrate
Advanced
Service
Back Select
Note.
Refer to Section 7, page 42, for menu
descriptions.
Refer to Section 6.1, page 29, for details of menu
navigation and parameter selection / adjustment.
OI/ASO550–EN Rev. G 21
Navigator 500
Sodium analyzer 5 Calibration
PV 2.93 ppb
21.7 °C
Na
CAL
SS1 100 ppb
Sodium 1
Back Select
Exit Yes
Exit Select
22 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 5 Calibration
5.3 Performing a calibration for the first time – 4. Press the key (below the Yes prompt on the Sodium
multi-stream wet-section Three Stream / Start Calibration page).
To perform a quick calibration from an Operator page:
The Calibration page is displayed with a bar graph to
1. Press the key (below the Cal prompt). indicate calibration progress:
Navigator 10 : 34: 52
2012–04–15 Sodium Three Stream
PV 2.93
Tag 1 09:57 30/01
The Calibrate page is displayed: At the end of the calibration, and if the calibration is
successful, the Active Slope, Active Offset, Last Slope and
Menu
Last Offset values in the Signals View are updated – see
Section 6.6, page 33 for details of View modes.
Calibrate
Note. The Active Slope and Active Offset values are
not updated if the calibration fails. The Calibration Log
is updated with the Active Slope and Active Offset
values.
Exit Select
Back Select
3. Press the key (below the Select prompt on the Back Select
Calibrate / Sodium Three Stream page).
The Sodium Three Stream / Start Calibration page is 6. Press the key (below the Back prompt on the
displayed: Calibrate / Sodium Three Stream page).
The Calibrate page is displayed:
Sodium Three Stream
Menu
Start Calibration
Calibrate
Exit Yes
Exit Select
OI/ASO550–EN Rev. G 23
Navigator 500
Sodium analyzer 5 Calibration
5.4 Calibration parameters – offset and slope 5.5.2 Monitoring calibration progress
A mV offset is calculated after a single-point or a two-point If the Calibration page is exited by press the key (below the
calibration. This value represents the difference in millivolt output OK prompt) before the calibration has completed, progress can
of the electrode pair compared to the ideal output. The slope is be monitored from the View mode – see Fig. 5.1.
calculated when a two-point calibration is performed and is an
indication of the quality of the electrode pair. A two-point 2012–08–16
Navigator 10:52:35
calibration can fail if the slope value is outside the pass criteria
S1
set in the software – refer to Table A.2, page 75, for a PV 2.93 ppb
description of the calibration pass limits.
SS1 100 ppb
5.5 Calibration options Low Calibration
Single-point or two-point calibrations can be performed
depending on the operating conditions. A single-point
calibration (low and high) adjusts the mV offset only, a two-point Calibrating CAL
calibration adjusts the mV offset and the slope (sensitivity) of the
electrode.
Fig. 5.1 Calibration view
Note. Perform a low-point calibration weekly and a At the end of the calibration, and if the calibration is successful,
two-point calibration monthly. However, a suitable schedule the Active Slope, Active Offset, Last Slope and Last Offset
must be set to suit the operating conditions and values in the Signals View are updated – see Section 6.6,
applications. page 33 for details of View modes.
5.5.1 Scheduled calibration Note. The Active Slope and Active Offset values are not
Automatic calibrations can be performed with a frequency of 1
updated if the calibration fails. The Calibration Log is
day to 8 weeks. Perform calibrations frequently to ensure
updated with the Active Slope and Active Offset values.
accurate readings and verify the performance of the
wet-section.
5.5.3 Abort calibration
To set up a scheduled calibration: Calibrations can be stopped manually by pressing the key
1. Access the configuration level Calibrate menu – (below the Abort prompt) while the Calibration page is displayed
see Section 5.1, page 21. (see page 22).
2. Configure the schedule at the Sensor 1 (4) (single-stream) The calibration valve closes enabling the sample to flow past the
or Sensor Three Stream / Scheduled Calibration / Type, sensor again. A calibration recovery period commences and the
Frequency, Interval and Time of Next Cal. menu options. Calibration Log displays Cal Aborted – see Section 6.7.1, page
35.
If the pressure switch on the constant-head unit detects there is
no solution present during the calibration, the calibration is
stopped automatically. The Diagnostic Log (see Section 6.7,
page 34) displays a Cal Failed diagnostic and No Low Cal or No
High Cal depending on the valve that was energized. The
Calibration Log displays a Cal Aborted entry – see Section
6.7.1, page 35.
24 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 5 Calibration
21.7 °C
Na Sodium 1
CAL
Navigator 10 : 34: 52
2012–04–15 Back Select
Operator Pages
– If a multi-stream wet-section is connected, the
4.28
Data Views
Logs ppb Calibrate / Sodium Three Stream page is displayed:
Alarm Acknowledge
Manual Hold
Autoscroll 21.7 °C Calibrate
Media Card
Enter Configuration Sodium Three Stream
Back Select
OI/ASO550–EN Rev. G 25
Navigator 500
Sodium analyzer 5 Calibration
Sensor Calibration
Scheduled Calibration
Calibration Setup PV 2.93 ppb
Restore Defaults
Sample Collection
Back Select
Abort Start
Process Calibration When sufficient sample has been collected in the sample
vessel, the collected sample must be analyzed using a
laboratory method or another analyzer to determine the
Start Procedure concentration of sodium in the sample.
13. Press the key (below the Stop prompt) to stop the
procedure manually.
Sample Complete
Abort Continue
26 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 5 Calibration
14. Press the key (below the Continue prompt). When the calculation is finished, a new page showing the
new reading and process calibration offset values is
The next Process Calibration page displayed shows an
displayed
average of the reading obtained:
Process Calibration
Process Calibration
Process Calibration
AVG 2.93 ppb
New 00 3.00
Next Continue
Back Select
Once the new value has been entered, press the key
17. Press the key (below the Back prompt).
(below the Continue prompt).
The Calibrate page is displayed:
The process calibration offset is calculated and a page
with a moving time bard is displayed for the duration of the Menu
calculation:
Calibrate
Process Calibration
Abort 18. Press the key (below the Exit prompt) to exit the
configuration level menu.
OI/ASO550–EN Rev. G 27
Navigator 500
Sodium analyzer 5 Calibration
28 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
Navigation key – left At menu level, selects the highlighted menu item, edit a selection or return to the previous
A and menu level.
Operator Level access key When Operator page is displayed, opens or closes the Operator menu.
Toggles the view between Operator pages, Diagnostic View and Calibration Log screens.
B View key
Note. Not enabled in Configuration mode.
C Up key Used to navigate up menu lists, highlight menu items and increase displayed values.
D Down key Used to navigate down menu lists, highlight menu items and decrease displayed values.
Toggles between:
Operator pages (1 to 5) when an Operator page is selected at the Group key.
View screens (Alarms, Outputs, Signals, Chart and Diagnostic) when the Diagnostic
E Group key View screen is selected at the Group key.
Log screens (Alarm, Audit, Diagnostic and Calibration) when the Calibration Log
screen is selected at the Group key.
Navigation key – right At menu level, selects the highlighted menu item, operation button or edits a selection.
F and
Cal shortcut key At Operator page level, used as a shortcut key to access the Calibrate level.
OI/ASO550–EN Rev. G 29
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
Note. Operator menus cannot be accessed directly from the Configuration level.
Referring to Fig. 6.2, Operator menus A are accessed from any Operating, View or Log page by pressing the key B.
To select Operator sub-menus (indicated by the arrow) press the key C.
Autoscroll
Manual hold
In
Enter Configuration Configuration CAL
A
B C
Autoscroll (enabled on Operator pages only) – displays Operator pages sequentially when multiple wet-sections are fitted.
Media Card – displays the status of the SD Card / USB stick (enabled only media module is fitted).
Enter Configuration – enabled on all pages – enters Configuration parameters via the Access Level – refer to Section 6.9.2,
page 39 for access levels and password security options.
CAL shortcut – initiates a calibration directly from an Operator Page, press the key C (below the CAL prompt). This shortcut
opens the Calibrate page, bypassing the Configuration level menus.
30 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
Instrument tag
Navigator 2012–04–15
10 : 29: 17 Time and date
(user-assignable)
TAG 1 TAG 2
Wet-section tag 2.77 ppb 4.28 ppb
Process value (PV)
(user-assignable) Na
No UNa Na Parameter ID
TAG 3
Autoscroll icon –
scrolls each page
6.93 ppb 8.82 ppb Unit of measure
Na Na
sequentially when enabled
In Configuration CAL Display icon –
see Section 6.10, page 40
Display icon – Diagnostic message or alarm tag –
see Section 6.10, page 40 see Appendix A, page 72 for diagnostic messages
*The highest priority diagnostic or alarm is displayed. Other active diagnostic / alarm states can be viewed on the Diagnostics
View – see page 33.
OI/ASO550–EN Rev. G 31
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
Fig. 6.5 shows an overview of Operator Pages 2 to 5. Each Operator Page displays the process value (PV) and temperature from a
single wet-section. Fixed, color-coded, user-assignable tags (one for each connected wet-section) and color-coded bargraphs aid
identification of each wet-section.
The bargraph indicates the PV (minimum and maximum values on the chart are configurable in the Sensor Setup level). If the PV is
above the maximum specified range of the wet-section, the bargraph flashes to indicate the value is out of range.
When multiple wet-sections are connected, and if Autoscroll is selected from the Operator Menu (see Fig. 6.2, page 30), the display
scrolls through each available Operator Page consecutively.
Color-coded
wet-section tag
wet-section 1 = red
Process value (PV)
wet-section 2 = green
wet-section 3 = blue Unit of measure
wet-section 4 = violet
Product tag Time / date
Navigator 2012–04–15
10 : 34: 52
(user-set)
Tag 1
Color-coded wet
4.28
section bargraph
Parameter ID
LLDO
ppb wet-section 1 = red
wet-section 2 = green
Sodium
Hydrazine 21.7 °C
wet-section 3 = blue
wet-section 4 = violet
Sodium
Temperature /
Operator Menu In Configuration CAL temperature unit
icon
Autoscroll
icon Diagnostic icon / Cal shortcut prompt
diagnostic message
32 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
01 Temp Failure S3
O2 NV Error S3
O3 Calibrating S3
O4 Recovery S3
CAL
2012–04–25
Alarms View 10 : 31: 27
2012–04–15
Outputs View 10 : 31: 27
CAL
OI/ASO550–EN Rev. G 33
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
CAL
Color-coded trace
(1 for each wet-section) Process value
2012–04–15
Chart View 10 : 31: 27
Wet-section ID
(color-coded)
Trace
time / date
CAL
2012–04–25
Audit Log 10 : 31: 27
Log icon
No. Event Date Time
01 Power Failure 07:04:13 14:03:24
02 Power Recovery 07:04:13 14:17:03
03 Power Failure 08:04:13 14:21:54
04 Power Recovery 08:04:13 14:26:31
34 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
Cal Failed Calibration procedure failed due to high / low slope or out of calibration solution or sample
temperature error during a calibration procedure.
Coefficients The Slope and mV Offset are displayed – refer to Section 5.4, page 24 for a description of
(Slope and mV Offset) these coefficients.
OI/ASO550–EN Rev. G 35
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
36 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
6.8.2 SD card / USB stick insertion and removal 6.8.3 Archive file types
To access the SD card / USB stick: All archive files created by the transmitter (except for
configuration files) are assigned filenames automatically. Each
1. Ensure the transmitter is offline.
type of archived file is assigned a different file extension.
2. Use a large Pozi-drive screwdriver to release the door
Archive files are created as text format data files.
catch A.
The file type and extension for Data text files is '.DOO'
3. Open the door and insert the SD card / USB stick B.
<ddmmyy><hhmmss><monitor tag>.DOO
The red LED C is lit when the SD card / USB stick is in
use by the transmitter.
The file type and extension for Event log files (containing
4. To remove the SD card / USB stick, if the red LED is lit, historical entries from the Audit, Calibration, Diagnostic and
press button D and wait until the LED goes out. Alarm logs is '.AOO’.
5. Pull the SD card / USB stick out of its socket. The SD card <ddmmyy><hhmmss><monitor tag>.AOO
/ USB stick can then be inserted into an appropriate card
reader USB port on the PC and the data downloaded.
Note.
The 'monitor tag' is set in the Device Setup level (see
page 42) when the user has access at Advanced level
– see Section 6.9, page 39.
The time and date are formatted according to the
format set in Display / Date & Time level – see
page 42.
The transmitter's internal clock can be configured to
adjust automatically at the start and end of Daylight
Saving periods – see page 42.
OI/ASO550–EN Rev. G 37
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
38 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
Note. When the transmitter is powered-up for the first time, the Calibrate and Advanced levels are not password protected.
Protected access to these levels can be allocated as required.
Access Level
Logout
Access levels – Read Only
scroll to level and press
Calibrate
Select key to enter
Advanced
Service
Level Access
Logout Displayed after Calibrate or Advanced level are accessed. Logs the user out of current level. If
passwords are set, a password must be entered to access these levels again after selecting Logout.
Read Only View all parameters in read-only mode.
Calibrate Enables access and adjustment of Calibrate parameters (refer to Section 5, page 21 for calibration
details).
Enter Password
Cursor / Password
character indicator Cursor – scroll characters using the
(maximum 6 characters) / keys;
press to accept character; press
to accept password while last
character is highlighted
OI/ASO550–EN Rev. G 39
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
40 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 6 Operation overview – transmitter
Media full
Alarm acknowledged
OI/ASO550–EN Rev. G 41
Navigator 500
Sodium analyzer 7 Menu descriptions
7 Menu descriptions
7.1 Menu overview
Refer to Section 7.1.1, page 43 Refer to Section 7.1.2, page 46 Refer to Section 7.1.3, page 48
Menu Menu Menu
Calibrate Sensor Setup Device Setup
Refer to Section 7.1.4, page 50 Refer to Section 7.1.5, page 52 Refer to Section 7.1.6, page 54
Menu Menu Menu
Display Input/Output Process Alarm
Refer to Section 7.1.7, page 55 Refer to Section 7.1.8, page 56 Refer to Section 7.1.9, page 57
Menu Menu Menu
42 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 7 Menu descriptions
7.1.1 Calibrate
Menu Used to calibrate the wet-section, regenerate the wet-section, set up calibration parameters,
process calibrations and initiate Grab Sample routines.
Calibrate
Access to the Calibrate menu is permitted via the Calibrate and Advanced levels only.
Exit Select
Sensor Calibration
Low Calibration Performs a single-point offset calibration using the low standard 15 min.
calibration solution. The default calibration time is 15 minutes and is
followed by a Recovery period.
The active offset value is adjusted after this calibration. This calibration
adjusts for any drift in the reading and should be performed weekly or
as required.
Note: During the calibration the sample is directed to drain via the
sample stream valve.
High Calibration Performs a single-point span calibration using the high standard 15 min.
calibration solution. The default calibration time is 15 minutes and is
followed by a Recovery period.
The active offset value is adjusted after this calibration.
Note: During the calibration the sample is directed to drain via the
sample stream valve.
Two-Point Cal Performs a two-point calibration. 30 min.
Runs both a low calibration and a high calibration. The total default
calibration time is 30 minutes and is followed by a Recovery period.
The active offset value and slope are calculated after this calibration.
This calibration compensates for any drift in the reading and changes
in the sensitivity and should be performed weekly or as required.
If the slope is calculated to be less than 80 % or greater than 110 %
the calibration has failed, a Cal Failed diagnostic appears and the offset
and slope are not updated.
Note: During the calibration the sample is directed to drain via the
sample stream valve.
Regeneration Cycle Displayed only if Regeneration Fitted is enabled.
Performs a regeneration automatically followed by a two-point
calibration. The regeneration procedure energizes the regeneration
valve (if fitted) for 1 minute to expose the electrode to the regeneration
solution.
A regeneration recovery period is then initiated, which last for 2 hours.
The recovery period is followed by a two-point calibration.
Refer to Section 5.7, page 28 for more details of the Regeneration
procedure.
OI/ASO550–EN Rev. G 43
Navigator 500
Sodium analyzer 7 Menu descriptions
Process Calibration Performs a process calibration. This calibration can be used to adjust
the concentration value on the wet-section to a value that has been
determined in the laboratory. It should only be used to make minor
adjustments to the reading.
A large discrepancy between the lab and wet-section readings could
be due to errors in calibration solutions or indicate problems with the
wet-section.
A Process Calibration can not be initiated on a multi-stream transmitter
unless one stream only is enabled.
Note: There is no recovery period after a process calibration.
Grab Sample Performs a Grab Sample routine. The Grab Sample function can be
used to measure the sodium concentration of an external sample, for
example, from another point in the process.
Note: During a grab sample routine the sample connected to the
wet-section is directed to drain via the sample stream valve.
Scheduled Calibration
Off
Low Standard Cal.
High Standard Cal.
Two-Point Cal.
Regeneration Cycle
Off
Selectable options: Daily, 2, 3, 4, 5, 6, 7 days.
Daily
Selectable options: Weekly, 2, 3, 4, 5, 6, 7, 8 weeks.
Weekly
Time of Next Cal. Selects the time and date of the next and subsequent scheduled 2000.01.01
calibrations. 00:00:00
Scheduled calibrations are not performed until the date / time set is
reached. The date of the next scheduled calibration is updated
automatically according to the frequency set. For example, if
Frequency is 5 days and Time of Next Cal. is12:00:00 2013-01-05, it
is updated automatically to: 12:00:00 2013-01-10.
Note: If the scheduled calibration cannot be run, or is not successful,
the next scheduled calibration date is updated according to the
Frequency set and a Missed Scheduled Cal. diagnostic message is
created. Parameters are not enabled if Frequency is Off.
44 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 7 Menu descriptions
Calibration Setup
Low Std Solution Sets the low standard calibration solution value between 50 and 100 ppb
10,000 ppb.
High Std Solution Sets the high standard calibration solution value between 50 and 1000 ppb
10,000 ppb.
Recovery Time Sets the recovery time in minutes (between 10 and 60 minutes). 15 min.
This value can be adjusted to ensure the wet-section has adequate
time to reach a stable reading after a calibration.
The default setting is 15 minutes, but this may need to be extended if
the process concentration is very low; especially if a high calibration
has been carried out.
Grab Sample Time Sets the grab sampling time in minutes. 15 min.
OI/ASO550–EN Rev. G 45
Navigator 500
Sodium analyzer 7 Menu descriptions
Menu Used to set the wet-section tag, measurement units, operational and stream ranges and filter type
and enable / disable the Flow Meter (optional) and Manual Valve Control functions.
Sensor Setup
Exit Select
Sodium 1 – 4 The identity of the sodium wet-section being set up (if a sodium
multi-steam wet-section, Sodium only is displayed).
Filter Time Sets the filter (input) time (5 to 100 seconds). 5 seconds
Wetting Routine Enables / disables the wetting routine. The wetting routine is initiated
when a No Samples situation is detected. It energizes the high
calibration solution valve for 1 minute every 24 hours.
The wetting routine is terminated if sample returns.
46 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 7 Menu descriptions
Sample Time Sets the how long each stream is sampled. 15 min.
Sequence Sets the order in which the streams are sampled, a maximum of 8 1,2,3,1,2,3,1,2,1
entries are permitted. A 0 indicates the end of the sequence. (3-stream)
An example sequence for streams 1 to 3 is: 1,2,3,1,2,3,0 where the 3
streams are sampled consecutively.
Stream 1 (3) Enables / Disables the selected stream (disabled streams are not sampled).
Man. Valve Control The solenoid valve can be energized manually. The current
concentration value is shown for reference. When the Man. Valve
Control parameter is exited, the valve returns to the closed state.
Note: Press the key to open the valve manually, press the key
to close the valve manually.
Low Standard Valve Enables the Low Standard Valve for manual control.
High Standard Valve Enables the High Standard Valve for manual control.
Regeneration Valve If fitted, enables the Regeneration Valve for manual control.
Reset to Defaults Resets all wet-section parameters to their default values. Disabled
OI/ASO550–EN Rev. G 47
Navigator 500
Sodium analyzer 7 Menu descriptions
Exit Select
1 0 100
2 0 1000
3 0 10000
The range spans can be changed to suit end-user’s requirements.
Continued on next page…
48 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 7 Menu descriptions
Relay operation
Relays 3 and 4 are used for the range changing functionality.
Connect Relay 3 – N/O to Relay 4 – COM
The range selection outputs can be determined as shown in the
following table:
Range Voltage-free contact
SK1
COMMUNICATIONS
COM
COM
N/C
N/C
+
–
+
–
SK4 SK5
SK5
SK2
FUSE RATING
SCREEN
GREEN
BLACK
~100 – 240V
WHITE
RED
3.15A (T)
50/60 Hz
COM
COM
COM
COM
+24V
N/C
N/C
N/C
N/C
+ – + –
N/C
N/C
N/C
N/C
INT
1 2 3 4 5 N L
COM
N/O
N/O
N/C
N/C
Relay 3 Relay 4
OI/ASO550–EN Rev. G 49
Navigator 500
Sodium analyzer 7 Menu descriptions
7.1.4 Display
Menu Used to select the display language, setup Operator page templates (1 to 5), enable diagnostic,
view and log functions, set the device’s display brightness / contrast and set the time and date.
Display
Exit Select
Page 1 (to 5) Template Page 1 template cannot be set, this defaults to the number of
wet-sections connected.
Chart View The chart can be configured to display the trend for 1, 2, 3 or 4 PV
and / or temperature values. The engineering ranges for the values
are configured in the Sensor Setup menu – see page 46.
Note: This menu is displayed only when Chart View is Enabled at the
Operator Functions / Chart View.
Channel 1 (to 4)
Source Selects the signal (PV and temperature) to be displayed on the chart.
Chart Duration Selects the chart duration from 1, 2, 4, 8, 12, 16, 20 and 24 hours.
View/Log Enables Enables / disables the following View and Log functions:
View functions:
Diagnostics View / Signals View / Chart View / Alarm View / Analog
OP View – refer to Section 6.6, page 33 for examples of Operator
Pages in View mode.
Log functions:
Calibration Log / Alarm Log / Audit Log / Diagnostics Log – refer to
Section 6.7, page 34 for examples of Operator Pages in Log mode.
50 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 7 Menu descriptions
Date & Time Sets / formats the device’s date, local time and daylight saving start /
end times:
Date & Time Sets the device date and time in the format: (date format set at Date 01.01.2000
Format menu) XX–XX–XXXX / time (fixed format) HR:MINS:SEC.
DS Region Selects the geographical region daylight saving hours are based on:
Off – daylight saving is disabled.
Europe – selects standard daylight saving start and end times
automatically.
USA – selects standard daylight saving start and end times
automatically.
Custom – used to set custom daylight saving start and end times
manually for regions other than Europe or USA.
Note: The DS Start Time / Occur / Day / Month and Time menus
(below) are activated only when Custom is selected at the DS
Region menu.
DS Start Time Sets the daylight saving start time and end time, selected from
DS End Time 1-hour increments.
DS Start Occur Selects the day within the month that daylight starts / ends – for
DS End Occur example, to set daylight saving to start (or end) on the second
Monday of the selected month, select Second.
DS Start Day Sets the day of the month daylight saving starts / ends.
DS End Day
Note: The DS Start Occur / DS End Occur parameters must be
valid within the month for the selected day.
OI/ASO550–EN Rev. G 51
Navigator 500
Sodium analyzer 7 Menu descriptions
7.1.5 Input/Output
Menu Input/Output level enables configuration of analog outputs, digital inputs and outputs and relays.
Input/Output
Exit Select
Analog Outputs The analog outputs can be configured to retransmit the process
variable and temperature values and have a configurable range from 0
to 22 mA.
Analog Output 1 to 4 Analog Outputs 3 and 4 are available only if an option board is fitted –
see page 18.
Elec Low The maximum and minimum engineering range output value 4 mA
Elec High (0 to 22 mA range). 20 mA
Eng Low The maximum and minimum engineering range output value. 0
Eng High 10,000
If the Output Type selection is logarithmic the Eng Low value is set
automatically to 2, 3 or 4 decades below the Eng High value.
Output Failure When enabled, the current output can be driven to a preset value if a Enabled
Failure category diagnostic state occurs for the selected source – see
page 72.
Failure Current Sets a preset value the current output is driven to when a Failure 22.0
category diagnostic state is present. – see page 72.
Note: Active only if Output Failure is Enabled.
52 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 7 Menu descriptions
Relays
Relay 1 to 6 Relays 5 and 6 are available only if an option board is fitted – see
page 18.
OI/ASO550–EN Rev. G 53
Navigator 500
Sodium analyzer 7 Menu descriptions
Exit Select
Hysteresis
Trip point
Hysteresis
Process variable
Alarm on
High process
Alarm off Alarm on
Low process Alarm off
Process Variable
Trip point Trip point
Hysteresis Hysteresis
Process
variable Alarm on Alarm latched Alarm On Alarm latched
Alarm acknowledged by operator Alarm off Alarm acknowledged by operator Alarm off
High latch alarm Low latch alarm
54 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 7 Menu descriptions
Menu Used to set the card on / off status, select the process data to be logged, enter file configuration
selection and save details and to format the media card.
Media Card
Media Card level menus are enabled only if an optional media card module is fitted.
Exit Select
Process Data
Channel 1 to 6 Selects the source to be logged – refer to Section 7.2, page 58 for
sources.
Save Configuration
Select File Name (8) Enables a user-selected filename to be specified for the current
configuration to be saved.
Load Configuration
Select File (8) Selects the configuration file to be loaded from a list of previously
saved files.
OI/ASO550–EN Rev. G 55
Navigator 500
Sodium analyzer 7 Menu descriptions
7.1.8 Communication
Menu Communication level menus are enabled only if an optional communications module is fitted.
Communication Ethernet and Email menus enabled only if a Ethernet communications module is fitted.
Exit Select
56 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 7 Menu descriptions
Menu Displays read-only factory-set details for the transmitter and connected wet-section(s).
Device Info
Exit Select
Transmitter
Input/Output
Sensor 1 – 4
OI/ASO550–EN Rev. G 57
Navigator 500
Sodium analyzer 7 Menu descriptions
58 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 8 Maintenance
8 Maintenance
8.1 Chemical solutions 8.1.2 Standard solutions
The reagents and calibration solutions detailed in this section The following instructions refer to the preparation of 100 µg l-1
are required to keep the wet-section operating. Solutions should and 1 mg l-1 sodium, STANDARD SOLUTION 1 (LOW) and 2
be stored in plastic bottles and, where possible, should be (HIGH) respectively. Alternative concentrations can be prepared
freshly made. within the measuring range selected by appropriate dilution of
the stock solution.
8.1.1 Reagent solutions
Two alternative reagent solutions may be used, depending on It is not advisable to prepare static sodium solutions of less than
the required lower limit of measurement. Concentrated 50 µg l-1 because low concentration solutions rapidly become
ammonia solution, that provides adjustment of sample pH to a contaminated and change in concentration.
minimum of 10.7 (if fresh 35 % w/v ammonia solution is used) is Although the HIGH and LOW standard solutions are typically
suitable for measurements of sodium ion to approximately 0.5 one decade apart in sodium concentration, any concentration
µg kg-1. At concentrations below this, hydrogen ion interference difference can be used if the HIGH solution is at least five times
becomes significant and a reagent of di-isopropylamine (DIPA) the concentration of the LOW solution. It is necessary to have a
should be used. This adjusts the sample pH between 11.2 and significant change in electrode output to achieve an accurate
11.5 and enables measurements to be made down to 0.1 µg calibration.
kg-1.
For all practical purposes, ‘µg l-1’ can be considered equal to
1. Concentrated ammonia solution – 1 liter (0.22 US gal.). ‘µg kg-1’ (‘ppb’) and ‘mg l-1’ equal to ‘mg kg-1’ (‘ppm’).
Warning. This reagent must only be handled under a To prepare stock solution (1000 mg l-1 sodium ions):
fume hood. It causes burns and is irritating to the 1. Dissolve 2.543 (±0.001) g of analytical reagent grade
eyes, respiratory system and skin. Wear rubber gloves sodium chloride in approximately 100 ml high purity water.
and eye protection. In warm weather pressure Transfer this solution to a one liter volumetric flask and
increases in the bulk container of ammonia and the make up to the one liter mark with more high purity water
cap must be released with care. to give a stock solution of 1000 mg l-1 sodium ions. Store
in a plastic container.
A 35 % w/v solution (s.g. 0.88) is recommended, but 2. Pipette 10 ml of this solution to a one liter volumetric flask.
lower concentrations, to a minimum of 30 % w/v (s.g. Make up to the one liter mark with high purity water to give
0.89), can be used. a solution of 10 mg l-1 sodium ions.
2. Di-isopropylamine – 1 liter (0.22 US gal.). 3. Pipette 10 ml of the 10 mg l-1 solution into a one liter
volumetric flask and make up to the one liter mark with
Warning. DIPA is an extremely inflammable and high purity water to give the LOW standard solution of
irritating colorless liquid with an ammoniacal odor. 100 µg l-1 sodium ions. Transfer this solution to the bottle
Handle with care at all times. labelled STANDARD SOLUTION 1 (LOW).
The following points must also be noted: 4. Transfer 100 ml of the 10 mg l-1 solution to a one liter
volumetric flask and make up to the mark with high purity
Avoid breathing vapor and avoid contact with
water to give the HIGH standard solution of 1 mg l-1
skin and eyes.
sodium ions. Transfer this solution to the bottle labelled
Work under a fume hood, wearing rubber STANDARD SOLUTION 2 (HIGH).
gloves and eye protection.
Keep away from sources of ignition. Note. High purity water = water containing less than
No smoking 2 µg l-1 sodium ions and a specific conductivity of less than
approximately 0.2 µS cm-1.
In the event of a fire, extinguish with water spray,
foam, dry powder or carbon dioxide.
8.1.3 Salt bridge solution
If a spillage occurs, shut off all possible sources This solution is required for refilling the double junction silver /
of ignition and instruct others to keep at a safe silver chloride reference electrode at extended intervals. The
distance. Mop up spillage with plenty of water, solution supplied with the electrode (3.5 M potassium chloride)
diluting greatly. Ventilate the area well to should be used for refilling using the plastic pipette provided.
evaporate any remaining liquid and dispel vapor.
Effluent from the wet-section contains DIPA (if
this reagent is used). Contact with it should also
be avoided.
OI/ASO550–EN Rev. G 59
Navigator 500
Sodium analyzer 8 Maintenance
60 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 8 Maintenance
8.2.3 12-Monthly
1. Check the condition of all plastic tubing; replace it as 8.3 Automatic regeneration
required – refer to Section 8.6, page 65 for multi-stream The regeneration valve is energized for 1 minute. The analyzer
wet-sections or Section 8.7, page 67 for single-stream then starts a 2-hour regeneration recovery period. After the
wet-sections. recovery period a two-point calibration is initiated automatically.
2. Clean the flowcell and the Pt1000 temperature A scheduled regeneration does not commence if the No
compensator to remove any deposits. Samples diagnostic (see Appendix A.1, page 72) is active.
Referring to Fig.8.2: It is not advisable to perform a manual regeneration procedure
(see Section 8.4, page 63) if the No Samples diagnostic is
a. Remove the Pt1000 temperature compensator A by
active.
unscrewing the compensator sleeve B and
withdrawing the Pt1000 temperature compensator
from the flowcell C. Note. If it is detected that no regeneration solution is
present, the regeneration valve is de-energized
b. Clean the Pt1000 temperature compensator A and automatically and a recovery period is initiated. A two-point
flowcell C using high purity water. calibration is initiated after the recovery period.
c. When replacing the Pt1000 temperature compensator,
ensure that the O-ring D is in place below the flange To start an automatic regeneration:
on the compensator, and the skid washer E is in
place above the flange. 1. Press the key (below the icon).
Navigator 10 : 34: 52
2012–04–15
Tag 1
2.93 ppb
21.7 °C
Na
CAL
Navigator 10 : 34: 52
2012–04–15
Operator Pages
4.28
Data Views
Logs ppb
Alarm Acknowledge
Manual Hold
Autoscroll 21.7 °C
Media Card
Fig. 8.2 Cleaning the flowcell and Pt1000 temperature Enter Configuration
compensator
Access Level
Read Only
Calibrate
Advanced
Service
Back Select
OI/ASO550–EN Rev. G 61
Navigator 500
Sodium analyzer 8 Maintenance
4. If the Calibrate page is not displayed, use the / 7. Press the key (below the Select prompt).
keys to scroll to the Calibrate page:
The Sensor Calibration page is displayed:
Menu
Sensor Calibration
Calibrate
Low Calibration
High Calibration
Two-Point Cal
Regeneration Cycle
Process Calibration
Exit Select
Back Select
Start Procedure
Back Select
No Yes
– If a multi-stream wet-section is connected, the
Calibrate / Sodium Three Stream page is displayed: Press the key (below the Yes prompt) to start the
regeneration procedure.
Calibrate
Back Select
Sensor 1
Sensor Calibration
Scheduled Calibration
Calibration Setup
Restore Defaults
Back Select
62 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 8 Maintenance
OI/ASO550–EN Rev. G 63
Navigator 500
Sodium analyzer 8 Maintenance
64 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 8 Maintenance
Note. Tubes B, C and D use QD couplings at the solution bottles, all other tubing connections are to barbed connectors.
To flowcell
Key to tubing
Multi-stream configuration –
wet-sections without regeneration option. *
Multi-stream configuration –
wet-sections with regeneration option
*For inlet tube routing on wet-sections with flowmeters, refer to item Fig. 8.6, page 66, item M.
Fig. 8.5 Physical arrangement, all plastic tubing – sodium multi-stream wet-section without flowmeters
OI/ASO550–EN Rev. G 65
Navigator 500
Sodium analyzer 8 Maintenance
*For inlet tube routing on wet-sections without flowmeters, refer to Fig. 8.5, page 65, item M.
Fig. 8.6 Physical arrangement, inlet tubing only – sodium multi-stream wet-section with flowmeters
66 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 8 Maintenance
Note. Tubes B, C and D use QD couplings at the solution bottles, all other tubing connections are to barbed connectors.
To flowcell
Key to tubing
Single-stream configuration –
wet-sections without regeneration option.
Single-stream configuration –
wet-sections with regeneration option
OI/ASO550–EN Rev. G 67
Navigator 500
Sodium analyzer 8 Maintenance
0212397
A Reagent tubing 550 (21.6) 3 1
/32 in. ID x 5/32 in. OD
0212189
H Sample outlet tubing 280 (11) 1 1
/4 in. ID x 3/8 in. OD
0212206
I Constant-head to entrainment 'T' piece tubing 100 (4) 1
1 mm ID x 1 mm wall
J Entrainment 'T' piece to flowcell chamber tubing Factory-made
K Drain tubing – same length for wet-sections with / without flowmeters 145 (5.7) 0212362* 1*
3
Inlet tubing – same length for single-stream wet-sections with / /32 in. ID x 5/32 in. OD
L 145 (5.7) Tygon 1*
without flowmeters
68 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 9 Specification – analyzer
9 Specification – analyzer
Operation Environmental data
Measuring range Ambient operating temperature:
0.01 to 10,000 ppb 0 to 55 ºC (32 to 131 ºF)
Units of measure Ambient operating humidity:
ppb, µg/l, µg/kg Up to 95 % RH non-condensing
Accuracy Storage temperature:
±5 % of reading or ±0.1 ppb, whichever is the greater (applies only – 20 to 70 °C (–4 to 158 °F) without sensor
when sample is within ±5 °C of calibration temperature) 0 to 55 °C (41 to 131 °F) with sensor
Repeatability
±5 % of reading or ±0.1 ppb, whichever is the greater (applies within
Approvals, certification and safety
a ±5 °C [±9 °F] variation)
CE mark
Response time
cULus
1 to 100 ppb <4 mins;
General safety
100 to 1 ppb <4 mins for a 90 % step change
EN61010-1
Multi-stream measurement
Pollution degree 2
Sample time programmable between 10 and 60 min.
Insulation class 1
Resolution
0.001 ppb
Temperature compensation EMC
5 to 55 °C (41 to 131 °F) automatic using a Pt1000 Emissions & immunity
AutoCal frequency Meets requirements of IEC61326 for an industrial environment and
Programmable from 1 to 7 days or 1 to 8 weeks domestic emissions
Sample temperature
5 to 55 °C (41 to 131 °F) Maintenance
Sample pressure Periodic calibration:
1.5 bar gauge (21.7 psi) maximum User-defined
Sample flow rate
100 to 400 ml/min DS/ASO550–EN Rev. E
Sample connections
1
/4 ID flexible tubing to barbed connector
OI/ASO550–EN Rev. G 69
Navigator 500
Sodium analyzer 10 Specification – transmitter
10 Specification – transmitter
Operation Relay outputs
Display 4 standard
89 mm (3.5 in) color 1/4 VGA TFT, liquid crystal display (LCD) with 2 optional
built-in backlight and brightness / contrast adjustment
Fully-programmable. Contacts rated at 2A @ 110 / 240 V. Standard
Language relays are changeover. Optional relays are normally closed (N/C).
English, German, French, Italian, Spanish
Keypad
6 tactile membrane keys:
Digital inputs / outputs
6 standard, user-programmable as input or output
Group select / left cursor, view select / right cursor, menu key,
up, down, enter key Minimum input pulse duration: 125 ms
No of inputs Input – volt-free or 24 VDC (conforms to IEC 61131-2)
Up to 4 single-stream or 1 multi-stream wet-section Output – open-collector, 30 V, 100 mA max.
(conforms to IEC 61131-2)
Mechanical data
Protection Connectivity / communications
IP66 / NEMA 4X Ethernet (optional)
Dimensions TCP/IP, HTTP
Height – 194 mm (7.64 in) minimum (excluding glands)
Width – 214 mm (8.42 in) – excluding glands Data logging
Depth – 98 mm (3.85 in) door closed – minimum (excluding fixing Storage
brackets) Measurement value storage (programmable sample rate)
Weight – 1.5 kg (3.3 lb) Audit Log*, Alarm Log*, Calibration log, Diagnostics log,
Materials of construction Configuration changes
Glass-filled polycarbonate Chart view
On local display
Historical review
Security
Of data
Password protection
Data transfer
Calibrate and Advanced – user-assigned
Service level access – factory-set Secure digital (SD) card interface / USB stick – Windows-compatible
FAT file system, data and log files in Excel and DataManager Pro
compatible formats
Electrical
*Audit Log and Alarm Log data are stored in the same log file.
Power supply ranges
100 to 240 V AC max., 50 / 60 Hz ± 10 %
(90 to 264 V AC, 45/65 Hz) DS/ASO550–EN Rev. F
Power consumption
<10W
Analog outputs
2 standard
2 optional
Galvanically isolated from the rest of the circuitry, 500 V for 1 minute.
Range-programmable source and range 0 to 22 mA, maximum
load 750 @ 20 mA
70 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer 11 Specification – wet-section
11 Specification – wet-section
Mechanical data
Protection
IP54
Dimensions
Height – 668 mm (26.30 in), including solution bottles
Width – 290 mm (11.41 in) – door shut
Depth – 185 mm (7.28 in) door closed – minimum
(excluding fixing brackets)
Weight – 4.5 kg (10 lb)
Electrical
Power supply ranges (supplied by transmitter)
24 V DC max.
Power consumption
8 W max.
DS/ASO550–EN Rev. E
OI/ASO550–EN Rev. G 71
Navigator 500
Sodium analyzer Appendix A – Troubleshooting
Appendix A – Troubleshooting
A.1 Diagnostic messages
The transmitter is programmed to display diagnostic messages Diagnostic Icon NAMUR Status
to provide information on servicing requirements and any other
conditions that develop during operation. Failure
All diagnostic messages displayed on the transmitter are added
to the transmitter's Audit Log.
Check function
The tables below show icon types, diagnostic messages and
possible causes / suggested remedial action.
Out of specification
Note. The diagnostic icons in the following tables conform
to NAMUR 107.
Maintenance required
Wet-section failure (temporary or permanent failure of analog to digital converter for wet-section 1, 2, 3, 4).
ADC Failure
(S1, S2, S3, S4) Cycle power to the transmitter.
If problem persists replace electronics inside wet-section, contact local service organization.
72 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer Appendix A – Troubleshooting
Calibrating.
Calibrating
Displayed during calibration of wet-section (1, 2, 3, 4).
(S1, S2, S3, S4)
On a multiple wet-section setup, this inhibits other wet-sections being calibrated.
Wet-section(s) performing a recovery stage after calibration, regeneration, or after exiting Man.Valve Control –
Recovery
see page 47.
(S1, S2, S3, S4)
During the recovery period, outputs and alarms are held if Hold Outputs is enabled – see page 45.
Flow Error
(S1, S2, S3, S4) Sample flow rate is less than 50 mlmin.(3.05 cu in.min.)
Displayed only if Increase the sample flow to the wet-section.
flowmeter is fitted
Missed Cal.
Missed last schedule calibration.
(S1, S2, S3, S4)
PV Range Process value (PV) measured is out of the specified range of the wet-section.
(S1, S2, S3, S4) 0 to 10,000 ppb.
OI/ASO550–EN Rev. G 73
Navigator 500
Sodium analyzer Appendix A – Troubleshooting
74 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer Appendix A – Troubleshooting
OI/ASO550–EN Rev. G 75
Navigator 500
Sodium analyzer Appendix A – Troubleshooting
A.3 Checking the temperature input A.4 Incorrect or erratic flow rate readings
1. Check that the wet-section responds to a temperature Incorrect or erratic flow rate readings may be due to a blockage
input. Disconnect the Pt1000 temperature compensator in the flowmeter. Stop the flow of sample to the wet-section,
leads in the wet-section PCB (see Section 3.4.3, page 15) remove the flowmeter and back-flush it with water or air. Re-
and connect a suitable resistance box to the wet-section connect the flowmeter, start the sample flow and check the flow
PCB inputs. reading. If the problem persists a replacement flowmeter may be
required – see page 82.
Note. Resistance boxes have an inherent residual
resistance which may range from a few milliohms up A.5 Erratic sodium readings
to 1 ohm. This value must be taken into account when If the sodium reading appears noisy/erratic carry out the
simulating input levels, as should the overall tolerance following checks:
of the resistors within the box. check the entrainment of reagent is regular and not
intermittent
2. Check that the transmitter displays the correct values as check the reagent has not become exhausted – either
set on the resistance box – see Table A.3. Incorrect check the pH of the sample exiting the flow cell (see
readings usually indicate an electrical calibration problem. Section A.2, page 75 for ideal pH values) or install a fresh
bottle of reagent solution.
Temperature °C (°F) Resistance
check the flow cell stud terminal (Fig. 2.1, page 6) is
0 (32) 1000.0 connected securely to a suitable earth (for example, the
earth stud on the transmitter).
10 (50) 1039.0
20 (68) 1077.9
30 (86) 1116.7
40 (104) 1155.4
50 (122) 1194.0
60 (140) 1232.4
76 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer Appendix B – Multi-stream sodium wet-section
0.1 5 20 Upscale
0.1 50 15 Upscale
5 50 10 Upscale
50 50 10 Upscale
5 0.1 35 Downscale
50 0.1 40 Downscale
50 5 10 Downscale
500 50 10 Downscale
The stream sequence is normally set to sample each stream in turn – for example, on a three stream wet-section the sequence would
be set to 1, 2, 3. However, greater priority could be given to a particular stream (for example, stream 1) by programming the
sequence 1, 2, 1, 3 or 1, 1, 1, 2, 3.
If only 1 stream is enabled the wet-section functions as a single-stream version and continuously measures the sodium
concentration. This is useful for troubleshooting as there is a concentration update every second.
OI/ASO550–EN Rev. G 77
Navigator 500
Sodium analyzer Appendix C – Multiple wet-section setup
2 OFF ON OFF ON
3 ON OFF ON OFF
4 ON ON ON ON
Terminals G and W
SW1.1 SW1.2
OFF position ON position
ON
B R Scr 1 3 5 7 9 1 1 13 15 17 19 21 23 25 27 29 31 33 3
G W 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36
1 2
SW1
SW1
1 2
ON
D5
D4
Note. The total cable length between the transmitter and the last wet-section must not exceed 30 m (98 ft.).
78 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer Appendix D – Spare parts and consumables
AWRS5000101 General purpose sodium measurements AW500 040 Flowmeter upgrade kit
for concentrations above 0.5 ppb.
Sodium reagent –
ammonia Provides up to 30 days of continuous
operation.
Shelf life 18 months – also available as a kit
(AWRK5000111, see below).
AWRK5000114
Sodium 6 x 1 liter bottles 100 ppb.
standards kit 6 x 1 liter bottles 1000 ppb.
OI/ASO550–EN Rev. G 79
Navigator 500
Sodium analyzer Appendix D – Spare parts and consumables
1048880 Sodium electrode cable assembly AW501 053 Solenoid valve – Multi-stream Cal / Stream
switch
Port configuration W.R.T
electrical connector
N/O
T
IN/OU
AW501 037 Reservoir-fed electrode upgrade kit N / C
N/C
T
IN/OU
N/O
80 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer Appendix D – Spare parts and consumables
AW501 057 Sodium electrode sleeve and O-ring AW501 062 Pressure switch assembly (2 in.set point)
including O-ring and fasteners
LOW
OI/ASO550–EN Rev. G 81
Navigator 500
Sodium analyzer Appendix D – Spare parts and consumables
AW501 066 Entrainment tube and connecting tubing AW501 070 Calibration solution bottle kit assembly –
includes hazard labels: Calibration Solution 1
and Calibration Solution 2
82 OI/ASO550–EN Rev. G
Navigator 500
Sodium analyzer Appendix D – Spare parts and consumables
OI/ASO550–EN Rev. G 83
Navigator 500
Sodium analyzer Appendix D – Spare parts and consumables
84 OI/ASO550–EN Rev. G
Acknowledgements
Microsoft, Windows and Excel are registered trademarks of
Microsoft Corporation in the United States and/or other
countries.
ABB Inc.
Measurement & Analytics
125 E County Line Road
Warminster, PA 18974
USA
Tel: +1 215 674 6000
Fax: +1 215 674 7183
abb.com/measurement
—
OI/ASO550-EN Rev. G 03.2019
We reserve the right to make technical changes or modify the contents of this document
without prior notice. With regard to purchase orders, the agreed particulars shall prevail.
ABB does not accept any responsibility whatsoever for potential errors or possible lack of
information in this document.
We reserve all rights in this document and in the subject matter and illustrations contained
therein. Any reproduction, disclosure to third parties or utilization of its contents – in
whole or in parts – is forbidden without prior written consent of ABB.
3KXA835550R4201