MenAMI Silitrace 02

AMI Silitrace
Version 6.31 and higher
Operator’s Manual
A-96.250.811 / 091017
Customer Support
SWAN and its representatives maintain a fully trained staff of technical specialists
around the world. For any technical question, contact your nearest
SWAN representative, or the manufacturer:
SWAN ANALYTISCHE INSTRUMENTE AG
Studbachstrasse 13
8340 Hinwil
Switzerland
Internet: www.swan.ch
E-mail: [email protected]
Document Status
Title: Monitor AMI Silitrace Operator’s Manual
ID: A-96.250.811
Revision Issue
00 Okt. 2015 First Edition
01 Aug. 2016 Update to FW Release 6.20, Mainboard Rev. 2.5
02 Mar. 2017 Update to FW Release 6.30 (includes multi-channel

capability)
© 2017, SWAN ANALYTISCHE INSTRUMENTE AG, Switzerland, all rights reserved
subject to change without notice.

AMI Silitrace
Table of Contents
1. Safety Instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
1.1. Warning Notices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.2. General Safety Regulations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2. Product Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2.1. Description of the System. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2.2. Instrument Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
2.3. Instrument Overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
3. Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
3.1. Installation Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
3.2. Mounting of Instrument Panel. . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
3.3. Connect Sample and Waste . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.3.1 AMI Silitrace . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.3.2 AMI Silitrace Dual-Stream . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
3.4. Electrical Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
3.4.1 Connection Diagram . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
3.4.2 Power Supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
3.5. Relay Contacts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
3.5.1 Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
3.5.2 Alarm Relay. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
3.5.3 Relay 1 and 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
3.6. Signal Outputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
3.6.1 Signal Output 1 and 2 (current outputs) . . . . . . . . . . . . . . . . . . 26
3.7. Interface Options . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
3.7.1 Signal Output 3 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
3.7.2 Profibus, Modbus Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
3.7.3 HART Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
3.7.4 USB Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
4. Instrument Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
4.1. Start-up Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
4.2 Prepare Reagents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
4.3. Prepare Standard . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
4.4. Switch on Power . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.5. Adjust Sample Flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.6. Activate the Peristaltic pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
4.7. Programming . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
4.7.1 AMI Sample Sequencer (Option) . . . . . . . . . . . . . . . . . . . . . . . 36
4.8. Final Tests . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
A-96.250.811 / 091017 1
AMI Silitrace
5. Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
5.1. Keys . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
5.2. Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
5.3. Software Structure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
5.4. Changing Parameters and values. . . . . . . . . . . . . . . . . . . . . . . . . 44
5.5. Grab Sample Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
6. Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
6.1. Maintenance Table . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
6.2. Stop of Operation for Maintenance . . . . . . . . . . . . . . . . . . . . . . . . 47
6.3. Refill or Replace Reagents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
6.4. Calibration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
6.5. Verification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
6.6. Zero. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
6.7. Replace the Pump Tubes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
6.8. Fill System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
6.9. Clean the Photometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
6.10. Longer Stop of Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
7. Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
7.1. Error List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
7.2. Replace the reaction chamber . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
7.3. Replace the 6-Way Valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
7.4. Replace the Cuvette . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67
7.5. Replace the Reagent Tubes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
7.6. Cleaning the solenoid valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
7.7. Replacing Fuses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
8. Program Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
8.1. Messages (Main Menu 1) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
8.2. Diagnostics (Main Menu 2) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
8.3. Maintenance (Main Menu 3) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
8.4. Operation (Main Menu 4) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
8.5. Installation (Main Menu 5). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77
9. Program List and Explanations . . . . . . . . . . . . . . . . . . . . . . . . . 79
1 Messages. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
2 Diagnostics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
3 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83
4 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
5 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87
2 A-96.250.811 / 091017
AMI Silitrace
10. Safety Data sheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105

11. Default Values. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 106
12. Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 109
13. Notes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 111
A-96.250.811 / 091017 3
AMI Silitrace
Safety Instructions
AMI Silitrace - Operator’s Manual

This document describes the main steps for instrument setup, oper-
ation and maintenance.
1. Safety Instructions
General The instructions included in this section explain the potential risks
associated with instrument operation and provide important safety
practices designed to minimize these risks.
If you carefully follow the information contained in this section, you
can protect yourself from hazards and create a safer work environ-
ment.
More safety instructions are given throughout this manual, at the
respective locations where observation is most important.
Strictly follow all safety instructions in this publication.
Target Operator: Qualified person who uses the equipment for its intended
audience purpose.
Instrument operation requires thorough knowledge of applications,
instrument functions and software program as well as all applicable
safety rules and regulations.
OM Location The AMI Operator’s Manual shall be kept in proximity of the instru-
ment.
Qualification, To be qualified for instrument installation and operation, you must:
Training  read and understand the instructions in this manual as well as
the Material Safety Data Sheets.
 know the relevant safety rules and regulations.
4 A-96.250.811 / 091017
AMI Silitrace
Safety Instructions
1.1. Warning Notices

The symbols used for safety-related notices have the following sig-
nificance:
DANGER
Your life or physical wellbeing are in serious danger if such

warnings are ignored.
 Follow the prevention instructions carefully.
WARNING
Severe injuries or damage to the equipment can occur if such

warnings are ignored.
CAUTION
Damage to the equipment, minor injury, malfunctions or incor-

rect process can be the consequence if such warnings are ig-
nored.
Mandatory The importance of the mandatory signs in this manual.

Signs
Safety goggles
Safety gloves
A-96.250.811 / 091017 5
AMI Silitrace
Safety Instructions
Warning Signs The importance of the warning signs in this manual.
Electrical shock hazard
Corrosive
Harmful to health
Flammable
Warning general
Attention general
1.2. General Safety Regulations

Legal The user is responsible for proper system operation. All precau-
Requirements tions must be followed to ensure safe operation of the instrument.
Spare Parts Use only official SWAN spare parts and disposables. If other parts
and are used during the normal warranty period, the manufacturer’s
Disposables warranty is voided.
Modifications Modifications and instrument upgrades shall only be carried out by
an authorized Service Technician. SWAN will not accept responsi-
bility for any claim resulting from unauthorized modification or alter-
ation.
6 A-96.250.811 / 091017
AMI Silitrace
Safety Instructions
WARNING
Risk of Electrical Shock

If proper operation is no longer possible, the instrument must be
disconnected from all power lines, and measures must be taken
to prevent inadvertent operation.
 To prevent from electrical shock, always make sure that the
ground wire is connected.
 Service shall be performed by authorized personnel only.
 Whenever electronic service is required, disconnect instru-
ment power and power of devices connected to.
– relay 1,
– relay 2,
– alarm relay
WARNING
For safe instrument installation and operation you must read

and understand the instructions in this manual.
WARNING
Only SWAN trained and authorized personnel shall perform the

tasks described in this document.
Download The current Safety Data Sheets (SDS) for the above listed Re-
MSDS agents are available for downloading at www.swan.ch.
A-96.250.811 / 091017 7
AMI Silitrace
Product Description
2. Product Description
2.1. Description of the System

Application The AMI Silitrace is a complete monitoring system for the automatic,
Range continuous measurement of the dissolved silica content in water
steam cycles or demineralizer plants.
Photometrical The determination of silica is done by the photometric analysis of
Detection of molybdate blue at 815 nm.
Silica Silica and ortho-phosphates react at low pH with ammonium mo-
lybdate to the yellow colored molybdosilic acid respectively molyb-
dophosphoric acid. The molybdophosphoric acid is destroyed with
oxalic acid before the molybdosilic acid is reduced with iron-(II)-am-
monium-sulfate to the heteropolyblue complex.
Especially the reaction speed of the first reaction step to the molyb-
dosilic acid is relatively slow. It is the most time consuming part of
the whole reaction. As the reaction speed increases with increasing
temperature, it is time saving to heat up the sample. The AMI Sili-
trace therefore uses a thermostatic reaction chamber with a con-
stant temperature of 45 °C.
At 45 °C the complete reaction only needs 150 s (2.5 min). Be-
cause the reaction time plays an important role in the color devel-
opment, the pump speed is adjusted constantly. Due to the
automatic heating and reaction time regulation a very high preci-
sion is achieved.
Instrument The AMI Silitrace is available in two variants:
variants  AMI Silitrace
 AMI Silitrace Dual-Stream
Both instruments are identical except that the AMI Silitrace Dual-
Stream includes a channel selector valve.
Sample If measurement of more than two sample streams is required, the
Sequencer AMI Silitrace can be connected to a Sample Sequencer, which al-
lows to measure up to six sample streams.
Automatic A calibration, verification or zero measurement can be performed
calibration and automatically according to a programmed time schedule or started
verification manually.
8 A-96.250.811 / 091017
AMI Silitrace
Product Description
Grab sample Easy to use grab sample function.

Signal Two signal outputs programmable for measured values (freely scal-
Outputs able, linear, bilinear, log) or as continuous control output (control
parameters programmable).
Current loop: 0/4–20 mA
Maximal burden: 510 Ohm
Third signal output available as an option. The third signal output
can be operated as a current source or as a current sink (selectable
via switch).
Relays Two potential-free contacts programmable as limit switches for
measuring values, controllers or timer for system cleaning with au-
tomatic hold function. Both contacts can be used as normally open
or normally closed.
Maximum load: 1 A/250 VAC
Alarm Relay One potential free contact.
Alternatively:
 Open during normal operation, closed on error and loss of
power.
 Closed during normal operation, open on error and loss of
power.
Summary alarm indication for programmable alarm values and in-
strument faults.
Input One input for potential-free contact to freeze the measuring value
or to interrupt control in automated installations (hold function or re-
mote-off)
Communica-  USB Interface for logger download
tion Interface  Third signal output (can be used in parallel to the USB interface)
(optional)  RS485 with Fieldbus protocol Modbus or Profibus DP
 HART interface
Safety No data loss after power failure. All data is saved in non-volatile
Features memory.
Over voltage protection of in- and outputs.
Galvanic separation of measuring inputs and signal outputs.
A-96.250.811 / 091017 9
AMI Silitrace
Product Description
Fluidic The sample enters at the sample inlet [N] and flows through the
flow meter [P], where the flow rate is measured, to the 6-way valve
[I]. A part of the sample overflows into the sample outlet [O].
The peristaltic pump [S] sucks the sample from the 6-way valve and
pumps it into the reaction chamber [D]. In the reaction chamber a
coil is wrapped around a heating device. It has 4 inlets to allow dos-
ing of the necessary reagents.
In the reaction chamber the sample is preheated to 45°C, eliminat-
ing temperature deviations of the sample. In a first step Ammoni-
ummolybdate [J] and sulfuric acid [K] are added, to form the
yellowish molybdosilic acid and molybdophosphoric acid.
Afterwards the oxalic acid [L] is added to mask the molybdophos-
phoric complex. At last the reducing agent ammonium ferrous (II)
sulfate [M] is added. The color of the sample turns to blue. As silica
is only present in trace amounts, the blue color can not be seen.
Afterwards the colored sample flows into the thermostatic cuvette
[E] until it is filled completely. Now the intensity of the color is mea-
sured at 815 nm. The color development is proportional to the silica
concentration in the sample.reaction chamber.
As the level of the sample in the cuvette increases, the sample
overflows into the siphon tube [G] and eventually the cuvette is
drained spontaneously through the siphon tube. The sample is led
via the aeration and drain tube [T] into the sample outlet [O].
Dosing, mixing and filling of the photometer are determined by the
rotating speed of the peristaltic pump [S]. This speed is adjusted
automatically and guarantees the correct timing of the measure-
ment.
The solenoid valve [R] is used for the zero measurement. It switch-
es off the supply of reagent 1, which is responsible for coloring the
sample. A zero can be started automatically or manually.
For a calibration or a verification the standard [B] is used. Both, cal-
ibration and verification can be started automatically or manually.
When a calibration or a verification is started, the 6-way valve is ro-
tated to position 5 and standard is pumped through the photometer.
NOTICE: The fluidic scheme shows the single-stream variant of
the AMI Silitrace. The dual-stream variant is fitted with a
different flow cell block and a channel selector valve (see AMI
Silitrace Dual-Stream, p. 34).
10 A-96.250.811 / 091017
AMI Silitrace
Product Description
T B
05 13
C
D
S
12
1B
2 03
03
3 3
4 4
04 04
05 I 12
12
4
5 3 F
1B 7
6 2 11
1 11
02
R G
01
04
04
1A H
03 1A 2 3 4
E
02 1 2 3 4 11
1 2 01 3 4
Q
J
P K
L
O M
N
A Grab sample bottle K Reagent 2

B Standard bottle L Reagent 3
C Photometer module M Reagent 4
D Reaction chamber N Sample inlet
E Cuvette O Sample outlet
F Cuvette de-aeration P Flow meter
G Sample outlet (siphon tube) Q Flow regulating valve
H Inlet from reaction chamber R Zero calibration valve
I 6-way valve S Peristaltic pump
J Reagent 1 T Aeration and drain tube
A-96.250.811 / 091017 11
AMI Silitrace
Product Description
2.2. Instrument Specification
Power Supply Voltage: 100–240 VAC (± 10%)

50/60 Hz (± 5%)
DC version not available
Power consumption: max. 50 VA
Transmitter Electronics housing Aluminium with a protection degree of
specifications IP 66 / NEMA 4X
Ambient temperature: -10 to +50 °C
Limit range of operation: -25 to +65 °C
Storage and transport: -30 to +85 °C
Humidity: 10–90% rel., non condensing
Display: backlit LCD, 75 x 45 mm
Sample Flow rate: min. 3 l/h
requirements Temperature: 5 to 50 °C
Inlet pressure: 0.15 to 2 bar
Outlet pressure: pressure free
On-site The analyzer site must permit connections to:
requirements Sample inlet: Serto PVDF 6 mm (1/8”),
for tubing 4x6 mm
Sample outlet: Tube 15 x 20 mm
(1/2”) hose nozzle which must end in a
pressure free waste of sufficient capacity
Ambient temperature 5 to 50 °C
Silica Measuring range 0.5 to 1’000 ppb
measurement Reproducibility: ± 0.5 ppb or ± 5%, whichever is greater
Cycle time: 3 min
12 A-96.250.811 / 091017
AMI Silitrace
Product Description
Dimensions Panel: stainless steel

Dimensions: 400x850x150 mm
Screws: 8 mm
Weight: 16.0 kg
400 mm / 15¾”
13 mm / ½”
374 mm / 14¾”
13 mm / ½”
Exit Enter
AMI SILITRACE
OzoneSiO
Trace Monitor
2
Process Analyzer
824 mm / 32 7/16”
850 mm / 33½”
4 x dia. 10 mm / /”
2L 2L 2L 2L
A-96.250.811 / 091017 13
AMI Silitrace
Product Description
2.3. Instrument Overview

A
Q C
P
F
O
H
N
I
M
L
K J
A Panel I Flow meter

B Standard bottle J Sample inlet
C Grab sample bottle K Sample outlet
D Solenoid valve for zero L Reagent 4
calibration M Reagent 3
E Photometer module N Reagent 2
F 6-way valve O Reagent 1
G Flow regulating valve P Peristaltic pump
H Flow cell Q Transmitter
14 A-96.250.811 / 091017
AMI Silitrace
Installation
3. Installation
3.1. Installation Checklist
Check Instrument’s specification must conform to the National Electri-

cal Code, all state and local codes, and all plant codes and stan-
dards for electrical equipment.
On site  100–240 VAC (± 10%), 50/60 Hz (± 5%) power outlet with
requirements ground connection and 50 VA.
 Sample line with sufficient sample flow and pressure (see
Instrument Specification, p. 12).
Installation  Mounting of Instrument Panel, p. 16.
 Connect Sample and Waste, p. 17.
Electrical NOTICE: Do not switch on the Instrument until all electrical
Wiring connections are made.
 Connect all external devices like limit switches, current loops
and pumps.
 Electrical Connections, p. 19.
 Connect power cord, see Power Supply, p. 22.
Start-up  Proceed according to Start-up Procedure, p. 29.
A-96.250.811 / 091017 15
AMI Silitrace
Installation
3.2. Mounting of Instrument Panel

The first part of this chapter describes the preparing and placing of
the instrument for use.
 The instrument must only be installed by trained personnel.
 Mount the instrument in vertical position.
 For ease of operation mount it so that the display is at eye
level.
 For the installation a kit containing the following installation
material is available:
– 4 Screws 8x60 mm
– 4 Dowels
– 4 Washers 8.4/24 mm
Mounting re- The instrument is only intended for indoor installation.

quirements For dimensions see Dimensions, p. 13.
16 A-96.250.811 / 091017
AMI Silitrace
Installation
3.3. Connect Sample and Waste
3.3.1 AMI Silitrace
2L 2L 2L 2L
OXYCON ON-LINE SILCA OXYCON ON-LINE SILCA OXYCON ON-LINE SILCA OXYCON ON-LINE SILCA
AMI SILICA REAGENT 3 AMI SILICA REAGENT 4
B
C
D
E
F
A Sample inlet D Compression ferrule

B Hose nozzle E Holder
C Knurled nut F 1/2” tube
Sample inlet Use a plastic tube (FEP, PA, or PE 4 x6 mm) to connect the sample.
1 Slide the knurled nut [C] and the compression ferrule [D] over
the plastic tube.
2 Push the plastic tube into the screw connection at the sample
inlet.
3 Tighten the knurled nut well.
Waste Push the 1/2” tube [F] over the hose nozzle [B] and place it into a
pressure free drain of sufficient capacity.
A-96.250.811 / 091017 17
AMI Silitrace
Installation
3.3.2 AMI Silitrace Dual-Stream
2L 2L 2L 2L
OXYCON ON-LINE SILCA OXYCON ON-LINE SILCA OXYCON ON-LINE SILCA OXYCON ON-LINE SILCA
AMI SILICA REAGENT 1 AMI SILICA REAGENT 2 AMI SILICA REAGENT 3 AMI SILICA REAGENT 4
A1
A2
B
C
D
E
F
A1 Sample inlet channel 1 D Compression ferrule
A2 Sample inlet channel 2 E Holder
B Hose nozzle F 1/2” tube
C Knurled nut G Channel selector valve
Sample inlet Use two plastic tubes (FEP, PA, or PE 4 x6 mm) to connect the sam-
ple streams.
1 Slide the knurled nut [C] and the compression ferrule [D] over
the plastic tube.
2 Push the plastic tube into the screw connection at the sample
inlet.
3 Tighten the knurled nut well.
Waste Push the 1/2” tube [F] over the hose nozzle [B] and place it into a
pressure free drain of sufficient capacity.
18 A-96.250.811 / 091017
AMI Silitrace
Installation
3.4. Electrical Connections
WARNING
Risk of electrical shock.

Do not perform any work on electrical components if the trans-
mitter is switched on. Failure to follow safety instructions could
result in serious injury or death.
 Always turn off AC power before manipulating electric parts.
 Grounding requirements: Only operate the instrument from a
power outlet which has a ground connection.
 Make sure the power specification of the instrument corre-
sponds to the power on site.
Cable In order to comply with IP66, use the following cable thicknesses
thicknesses
A B C
A PG 11 cable gland: cable Øouter 5–10 mm

B PG 7 cable gland: cable Øouter 3–6.5 mm
C PG 9 cable gland: cable Øouter 4–8 mm
NOTICE: Protect unused cable glands
Wire  For Power and Relays: Use max. 1.5 mm2 / AWG 14
stranded wire with end sleeves.
 For Signal Outputs and Input: Use 0.25 mm2 / AWG 23
stranded wire with end sleeves.
A-96.250.811 / 091017 19
AMI Silitrace
Installation
WARNING
External Voltage.
External supplied devices connected to relay 1 or 2 or to the
alarm relay can cause electrical shocks
 Make sure that the devices connected to the following con-
tacts are disconnected from the power before resuming in-
stallation.
– relay 1
– relay 2
– alarm relay
WARNING
To prevent from electrical shock, do not connect the instrument

to the power unless the ground wire (PE) is connected.
 Do not connect unless specifically instructed to do so.
WARNING
The mains of the AMI Transmitter must be secured by a main

switch and appropriate fuse or circuit breaker.
20 A-96.250.811 / 091017
AMI Silitrace
Installation
3.4.1 Connection Diagram
CAUTION
Use only the terminals shown in this diagram, and only for the
mentioned purpose. Use of any other terminals will cause short
circuits with possible corresponding consequences to material
and personnel.
A-96.250.811 / 091017 21
AMI Silitrace
Installation
3.4.2 Power Supply

WARNING
Risk of electrical shock
Do not perform any work on electrical components if the trans-
mitter is switched on. Failure to follow safety instructions could
result in serious injury or death.
 Always turn off AC power before manipulating electric parts.
 Installation and maintenance of electrical parts must be per-
formed by professionals.
A
B
C
A Power supply connector

B Neutral conductor, Terminal 2
C Phase conductor, Terminal 1
D Protective earth PE
NOTICE: The protective earth wire (Ground) has to be
connected to the grounding terminal.
Installation The installation must meet the following requirements.
requirements  Fuse 1.6 AT
 Mains cable to comply with standards IEC 60227 or IEC
60245; flammable rating FV1
 Mains equipped with an external switch or circuit-breaker
– near the instrument
– easily accessible to the operator
– marked as interrupter for AMI Silitrace
22 A-96.250.811 / 091017
AMI Silitrace
Installation
3.5. Relay Contacts
3.5.1 Input
NOTICE: Use only potential-free (dry) contacts.
The total resistance (sum of cable resistance and resistance of
the relay contact) must be less than 50 Ω.
Terminals 16/42
For programming see “Program List and Explanation” 5.3.4, p. 102.
3.5.2 Alarm Relay

NOTICE: Max. load 1 A/250 VAC
Alarm output for system errors.
Error codes see Error List, p. 58.
NOTICE: With certain alarms and certain settings of the AMI

transmitter the alarm relay does not switch. The error, however,
is shown on the display.
Terminals Description Relay connection

NC1) 10/11 Active (opened) during normal 1) 11
Normally operation.
0V
Closed Inactive (closed) on error and 10
loss of power.
12
NO 12/11 Active (closed) during normal 11

Normally operation. 0V
Open Inactive (opened) on error and 10
loss of power.
12
1) usual use
A-96.250.811 / 091017 23
AMI Silitrace
Installation
3.5.3 Relay 1 and 2

NOTICE: Max. load 1 A/250 VAC
Relay 1 and 2 can be configured as normally open or as normally
closed. Standard for both relays is normally open. To configure a
Relay as normally closed, set the jumper in the upper position.
NOTICE: Some error codes and the instrument status may
influence the status of the relays described below.
Relay Jumper
config. Terminals pos. Description Relay configuration
Normally 6/7: Relay 1 Inactive (opened) during
Open 8/9: Relay 2 normal operation and loss 6
of power.
Active (closed) when a pro-
0V
grammed function is
7
executed.
Normally 6/7: Relay 1 Inactive (closed) during
Closed 8/9: Relay 2 normal operation and loss 6
of power.
Active (opened) when a
programmed function is 0V
executed. 7
A
B
A Jumper set as normally open (standard setting)

B Jumper set as normally closed
For more information see Program List and Explanations, p. 79.
24 A-96.250.811 / 091017
AMI Silitrace
Installation
CAUTION
Risk of damage of the relays in the AMI Transmitter due to

heavy inductive load.
Heavy inductive or directly controlled loads (solenoid valves,
dosing pumps) may destroy the relay contacts.
 To switch inductive loads > 0.1 A use an AMI relay box avail-
able as an option or suitable external power relays.
Inductive load Small inductive loads (max 0.1A) as for example the coil of a power
relay can be switched directly. To avoid noise voltage in the
AMI Transmitter it is mandatory to connect a snubber circuit in par-
allel to the load.
A snubber circuit is not necessary if an AMI relaybox is used.
A A AC or DC power supply
B C B AMI Transmitter
C External power relay
D E D Snubber
E Power relay coil
Resistive load Resistive loads (max. 1A) and control signals for PLC, impulse
pumps and so on can be connected without further measures
A B A AMI Transmitter
B PLC or controlled pulse pump
C C Logic
Actuators Actuators, like motor valves, are using both relays: One relay con-
tact is used for opening, the other for closing the valve, i.e. with the
2 relay contacts available, only one motor valve can be controlled.
Motors with loads bigger than 0.1A must be controlled via external
power relays or an AMI relay box.
A A AC or DC power supply
B C B AMI Transmitter
C Actuator
A-96.250.811 / 091017 25
AMI Silitrace
Installation
3.6. Signal Outputs
3.6.1 Signal Output 1 and 2 (current outputs)

NOTICE: Max. burden 510 Ω.
If signals are sent to two different receivers, use signal isolator
(loop isolator).
Signal output 1: Terminals 14 (+) and 13 (-)
Signal output 2: Terminals 15 (+) and 13 (-)
For programming see Program Overview, p. 73, Menu Installation.
3.7. Interface Options

A AMI Transmitter
A B Slot for interfaces
C Screw terminals
The slot for interfaces can be used to expand the functionality of

the AMI instrument with either:
 Third signal output
 a Profibus or Modbus connection
 a HART connection
 an USB Interface
26 A-96.250.811 / 091017
AMI Silitrace
Installation
3.7.1 Signal Output 3

Terminals 38 (+) and 37 (-).
Requires the additional board for the third signal output 0/4–20 mA.
The third signal output can be operated as a current source or as a
current sink (switchable via switch [A]). For detailed information see
the corresponding installation instruction.
NOTICE: Max. burden 510 Ω.
A
Third signal output 0/4 - 20 mA PCB
A Operating mode selector switch
3.7.2 Profibus, Modbus Interface

Terminal 37 PB, Terminal 38 PA
To connect several instruments by means of a network or to config-
ure a PROFIBUS DP connection, consult the PROFIBUS manual.
Use appropriate network cable.
NOTICE: The switch must be ON, if only one instrument is
installed, or on the last instrument in the bus.
OFF
ON
Profibus, Modbus Interface PCB (RS 485)

A On - OFF switch
A-96.250.811 / 091017 27
AMI Silitrace
Installation
3.7.3 HART Interface

Terminals 38 (+) and 37 (-).
The HART interface PCB allows for communication via the HART
protocol. For detailed information, consult the HART manual.
HART Interface PCB
3.7.4 USB Interface

The USB Interface is used to store Logger data and for Firmware
upload. For detailed information see the corresponding installation
instruction.
The optional third signal output 0/4 – 20 mA PCB [B] can be
plugged onto the USB interface and used in parallel.
USB Interface
A USB interface PCB
B Third signal output 0/4 - 20 mA PCB
28 A-96.250.811 / 091017
AMI Silitrace
Instrument Setup
4. Instrument Setup
4.1. Start-up Procedure

The following table lists all necessary steps for a successful com-
missioning of the AMI Silitrace. Additionally, the expected result
and corrective actions are specified for each step.
NOTICE: It is important to verify the result of each step before
proceeding with the next step. We recommend to work exactly
in the order given in the table.
Prerequisites  Analyzer has been mounted, connected to the sample and waste
line and connected to power (see Installation, p. 15)
 Optional: AMI Sample Sequencer has been installed (see
manual of the AMI Sample Sequencer)
Step Expected result Corrective action

Prepare Reagents  31, n/a n/a
Prepare Standard  31
Switch on Power  33  The AMI transmitter  Check electrical wiring
starts up  Check fuses
 The main screen is
displayed
Adjust Sample Flow  33  The flow is indicated on  Check sample line
(approx. 5–10 l/h) the main screen  Check wiring of flow
sensor
Activate the Peristaltic  The tubes are filled  Tighten connections to
Pump  35,  The liquid moves with a the pump tubes
Fill System  35 speed of approximately  Check if occlusion
1 cm every 5 s frames are snapped
properly
 Check if occlusion
frames and pump tubes
are aligned in a 90°
angle to the rotor.
Programming  36 n/a n/a
A-96.250.811 / 091017 29
AMI Silitrace
Instrument Setup
Step Expected result Corrective action

Resolve all pending errors  No errors are displayed  As soon as the reaction
apart from E008 chamber has reached its
“SilTrace temp low” operating temperature,
E008 automatically
disappears
 If there are other
pending errors, resolve
them according to the
Error List  58
Visual check of the reac-  No air bubbles in the  Tighten all tube
tion chamber  37 reaction chamber connections
Check photometer raw  The photometer’s raw  Cuvette blocked

value  38 value follows a fill/empty  Cuvette not snapped
pattern completely
 While the photometer is
being filled, an unstable
raw value is normal
 Once the cuvette is
completely filled, the raw
value must remain
stable
Check P2P period  38  P2P period is different  Wait until the system is
from “0 Sec” free from air bubbles.
 Wait until the cuvette
has been emptied twice
Perform a zero calibra-  The raw value is close to  Clean cuvette / flush
tion  53 2.2 V system with ammonia
solution  57
 Perform a cuvette factor
determination  84
 Check if the zero
calibration valve is
switching
Perform a standard cali-  The calibration factor is  Check programmed
bration  51 between 0.5 and 2.0 concentration of
standard
 Repeat calibration with
fresh standard solution
30 A-96.250.811 / 091017
AMI Silitrace
Instrument Setup
4.2 Prepare Reagents

See Refill or Replace Reagents, p. 48
1 Insert suction lances into containers.

 Make sure that the numbers on suction lances correspond to
the numbers on the containers.
4.3. Prepare Standard

Following standard solutions are available:
 100 ppb standard in a 250 ml bottle
 100 ppm stock solution in a 100 ml bottle
Standard Ready for use.
100 ppb
Stock solution From the stock solution you can produce your own standard. Stan-
100 ppm dards from 10 to 1000 ppb can be used for the AMI Silitrace.
SWAN does not recommend to mix your own standard!
By default the instrument is programmed for a standard of 100 ppb.
NOTICE: If you prepare a standard different from 100 ppb,
program the standard concentration in menu <Installation>/
<Sensors>/<Meas. Parameters>/<Cal./Verif.>/<Standard>.
Make the following dilution to obtain a standard of 100 ppb:
1 Put a 250 ml bottle on to a balance, set balance to 0 g.
2 Fill in 250 μg stock solution 100 ppm.
3 Fill up to 250 g with demineralized water.
4 Mark the bottle with the correct concentration.
5 Program the instrument accordingly, see 5.1.1.1.1, p. 87.
A-96.250.811 / 091017 31
AMI Silitrace
Instrument Setup
Standard During a calibration or verification approximately 15 ml standard is

consumption consumed. Therefore a standard bottle lasts for 3 months at default
interval settings.
The default interval settings are:
Start time: 06:00:00
Monday: Verification
All other days: Off
Screw the standard bottle to the right bottle holder.
Grab
Standard
Sample
32 A-96.250.811 / 091017
AMI Silitrace
Instrument Setup
4.4. Switch on Power

Open the sample tap and switch on the instrument.
INIT
R1
R2 0.0 ppb
5.0 l/h 0.0 °C
After switching on, the instrument starts to warm up the reaction

chamber. During the warm-up phase, the display shows <INIT>
and alarm E008 is active.
NOTICE: The duration of the warm-up phase depends on the
ambient temperature at the operating site.
After the reaction chamber has reached its operating temperature,
the instrument changes to <RUN> and is ready for operation.
4.5. Adjust Sample Flow

AMI Silitrace A Flow regulating valve
A B Overflow
1 Open the flow regulating valve (A).

2 Adjust the sample flow to 5–10 l/h
A-96.250.811 / 091017 33
AMI Silitrace
Instrument Setup
AMI Silitrace A1 Flow regulating valve for

Dual-Stream C channel 1
A2 Flow regulating valve for
channel 2
B Overflow
C Channel selector valve
A1
A2
1 Open the flow regulating valves (A1 and A2).

2 Adjust the sample flow to 5–10 l/h.
34 A-96.250.811 / 091017
AMI Silitrace
Instrument Setup
4.6. Activate the Peristaltic pump

The occlusion frames of the peristaltic pump are opened during
transport and storage. This prevents the pump tubes from sticking
together at the pressure points.
1 Turn the occlusion frames [B] clockwise until they snap in to ac-
tivate the peristaltic pump.
NOTICE: Make sure the occlusion frames and pump tubes are
aligned in a 90° angle to the rotor.
A Turn to lock
A B Occlusion frame
C Rotor
B D Pump tube
C
D
Fill System Select <Maintenance>/<Service>/<Fill system>. This activates the

reagent pump and fills all tubes from the container to the cuvette
outlet.
A-96.250.811 / 091017 35
AMI Silitrace
Instrument Setup
4.7. Programming
Program all parameters for external devices (interface, recorders,
etc.). Program all parameters for instrument operation (limits,
alarms). See Program List and Explanations, p. 79.
4.7.1 AMI Sample Sequencer (Option)

AMI Sample Select mode “AMI” in the firmware of the AMI Sample Sequencer.
Sequencer
AMI Analyzer Set the firmware of the AMI Analyzer according to your require-
ments.
1 Navigate to menu <Installation>/
Multi-Channel 5.1.2.2
<Sensors>/<Multi-Channel>.
Channels 1
Channel Selection internal 2 Navigate to <Channels> with
Switching time 20 Min the[ ] or[ ] key.
3 Press [Enter].
4 Set <Channels> according to the
Multi-Channel 5.1.2.2 number of available channels
Channels Save? 6 (1–6) with the [ ] key.
Channel Selection
Yes internal
Switching No
time 20 Min
5 Confirm with [Enter].
6 Press [Exit], choose <Save> “Yes”
Confirm with [Enter].
Channels 6
With the AMI Sample Sequencer connected, the AMI Silitrace can
be operated in the following 3 different modes.
 internal
 fieldbus
 external
1 Navigate to menu <Installation>/
Multi-Channel 5.1.6 <Sensors>/<Multi-Channel>.
Channel Selection
Channels 6
internal internal
Channel Selection 2 Navigate to <Channel Selection>
fieldbus with the [ ] or[ ] key.
Switching time
external 20 Min
3 Press [Enter].
Internal, see chap. 9, Mode Internal, p. 89

Fieldbus, see chap. 9, Mode Fieldbus, p. 89
External, see chap. 9, Mode External, p. 89
36 A-96.250.811 / 091017
AMI Silitrace
Instrument Setup
4.8. Final Tests

Pending errors Resolve all pending errors, see Troubleshooting, p. 58.
Visual check Carefully pull out the cuvette [C] from the photometer module and
of reaction open the cover [B]. Check that there are no air bubbles in the reac-
chamber tion chamber [D].
If this check fails:
 check if all tube connections are tight
A Cover fixing screws
A B Photometer module cover
C Cuvette
B
C
D Reaction chamber
Close the cover again and snap in the cuvette.
A-96.250.811 / 091017 37
AMI Silitrace
Instrument Setup
Photometer Select <Diagnostics>/<Sensors>/<SilTrace>/<Photometer>.

raw value Check if the photometer raw value follows a fill/empty pattern. See
example below:
2.5
1.5
FOME raw [V]
0.5
While the cuvette is being filled, an unstable raw value is normal.

Once the cuvette is completely filled, the raw value must remain
stable.
 check if the cuvette is blocked
 check if the cuvette is snapped in properly
P2P Cycle Select <Diagnostics>/<Sensors>/<Cycle diagnostics>.
Check whether the analyzer has already performed a valid mea-
surement cycle. This can be recognized by a P2P period not equal
to "0 sec".
 wait until all air bubbles have left the system
 wait until the cuvette has been emptied twice
Zero Manually start a zero calibration (Zero, p. 53), then review the raw
Calibration value in <Diagnostics>/<Sensors>/<History>/<Zero History>. The
raw value must be close to 2.2 V.
 check if the zero calibration valve is switching (reagent 1 is led
into the waste)
 clean the photometer using an ammonia solution (see Clean the
Photometer, p. 57)
 perform a cuvette factor determination (see 3.4.3, p. 84)
38 A-96.250.811 / 091017
AMI Silitrace
Instrument Setup
Standard Manually start a standard calibration (Calibration, p. 51), then re-

Calibration view the calibration factor in <Diagnostics>/<Sensors>/<Cal. His-
tory>. The calibration factor must be between 0.5 and 2.0.
 Check if the programmed concentration matches the reference
value of the standard solution
 Repeat the calibration with a new standard solution
A-96.250.811 / 091017 39
AMI Silitrace
Operation
5. Operation
5.1. Keys
A B C D
Exit Enter
A to exit a menu or command (rejecting any changes)

to move back to the previous menu level
B to move DOWN in a menu list and to decrease digits
C to move UP in a menu list and to increase digits
to switch between display 1 and 2
D to open a selected sub-menu
to accept an entry
Program
RUN 14:10:45 Main Menu 1
Access, Exit Enter
R1 Messages
1.4 ppb Diagnostics
R2
Maintenance
Exit Operation
9 l/h 25.4°C Installation
40 A-96.250.811 / 091017
AMI Silitrace
Operation
5.2. Display
A B C D E
RUN 15:20:18
R1
4.7 ppb F
15:10:52
R2
I 5 l/h 45.1 °C
G
H
A INIT Warming up the reaction chamber

RUN normal operation
HOLD input closed or cal delay: Instrument on hold (shows
status of signal outputs).
OFF input closed: control/limit is interrupted (shows status
of signal outputs).
GRAB A grab sample measurement is in progress.
B ERROR Error Fatal Error
C Reagent low, indicates remaining reagents in % (17% = 340 ml)

D Keys locked, transmitter control via Profibus
E Time
F Process value with time stamp
G Reaction chamber temperature
H Sample flow
I Relay status
Relay status, symbols

upper/lower limit not yet reached
upper/lower limit reached
control upw./downw. no action
control upw./downw. active, dark bar indicates control intensity
motor valve closed

motor valve: open, dark bar indicates approx. position
timer
timer: timing active (hand rotating)
channel selection (Dual-Stream variant) or controlled via Profibus
A-96.250.811 / 091017 41
AMI Silitrace
Operation
Display when
operating with
two or more RUN 15:21:18
sample streams R1
4.7
15:10:52
ppb
F
Si1
4.5
R2 15:20:52
Si2 ppb ~
5 l/h 45.1 °C
F Process values with time stamp

Si1 –Si6: Sample streams 1 to 6, according to the number of
available channels.
Up to 3 process values can be displayed on one screen. Toggle
screens with the [ ] key.
Active measurement
Position of valve
~ No sample flow
n Measurement not valid
x Sample stream inactive (only visible if a Sample Sequencer is
connected to the AMI Silitrace and measuring mode
<internal> is selected).
42 A-96.250.811 / 091017
AMI Silitrace
Operation
5.3. Software Structure
Main Menu 1
Messages
Diagnostics
Maintenance
Operation
Installation
Menu Messages 1
Messages 1.1
Pending Errors Reveals pending errors as well as an event history
Maintenance List (time and state of events that have occurred at an
Message List earlier point of time).
It contains user relevant data.
Menu Diagnostics 2
Diagnostics 2.1
Identification Provides user relevant instrument and sample data.
Sensors
Sample
I/O State
Interface
Menu Maintenance 3
Maintenance 3.1
Calibration For instrument calibration, relay and signal output
Verification simulation, and to set the instrument time.
Zero It is used by the service personnel.
Service
Simulation
Menu Operation 4
Operation 4.1
Grab Sample User relevant parameters that might need to be
Sensors modified during daily routine. Normally password
Relay Contacts protected and used by the process-operator.
Logger Subset of menu 5 - Installation, but process-related.
Menu Installation 5
Installation 5.1
Sensors For initial instrument set up by SWAN authorized
Signal Outputs person, to set all instrument parameters. Can be
Relay Contacts protected by means of password.
Interface
A-96.250.811 / 091017 43
AMI Silitrace
Operation
5.4. Changing Parameters and values

Changing The following example shows how to change the logger interval:
parameters 1 Select the parameter you want to
Logger
Sensors 5.1.2
4.4.1
change.
Sensor
Log type
interval FOME
30 min
Disinf.logger Free chlorine 2 Press [Enter]
Clear no
Temperature NT5K
Standards
3 Press [ ] or [ ] key to
Logger 4.1.3
highlight the required parameter.
Log interval Interval. 30min
5 min
Clear logger no 4 Press [Enter] to confirm the selec-
10 min tion or [Exit] to keep the previous
30 min parameter).
1 Hour
The selected parameter is

Logger 4.1.3
highlighted but not saved yet.
Log interval 10 min
Clear logger no 5 Press [Exit].
Yes is highlighted.
Logger 4.1.3
Log interval
Save ?
6 Press [Enter] to save the new pa-
Clear logger no rameter.
Yes
No The system reboots, the new
parameter is set.
Changing 1 Select the value you want to

values Alarm Si 1 5.3.1.1.1
change.
Alarm High 1.00 ppm
Alarm Low 0.0 ppb 2 Press [Enter].
Hysteresis 5.0 ppb 3 Set required value with [ ] or
Delay 5 Sec
[ ] key.
4 Press [Enter] to confirm the new
Alarm Si 1 5.3.1.1.1
value.
Alarm High 0.70 ppm
Alarm Low 0.0 ppb 5 Press [Exit].
Hysteresis 5.0 ppb Yes is highlighted.
Delay 5 Sec
6 Press [Enter] to save the new val-
ue.
44 A-96.250.811 / 091017
AMI Silitrace
Operation
5.5. Grab Sample Measurement

NOTICE: The grab sample function is not suitable for quality
assurance of the instrument.
Select Menu 4.1 (<Operation>/<Grab Sample>) and follow the in-

structions on the display.
Relay status during grab sample measurement:
 Signal outputs are on hold
 All limits are switched off
1 Close the flow regulating valve.

Grab Sample 4.1.5
Connect the 2 Fill the sample into the grab sam-
Grab Sample bottle ple bottle and screw it to the left
to marked holder bottle holder.
3 Press [Enter].
<Enter> to continue
Grab
Standard
Sample
4 Enter an ID for the sample.

Grab Sample 4.1.5
This ID will be saved together
with the measuring result of the
Sample ID xxxx grab sample.
5 Press [Enter].
<Enter> to continue
A-96.250.811 / 091017 45
AMI Silitrace
Operation
Grab Sample 4.1.5

State xxxx
Progress
<Enter> to stop
Grab Sample 4.1.5

State xxxx
Cycle 1
Timer 10 sec
<Enter> to stop
Grab Sample 4.1.5

State xxxx
Cycle 1
Progress
<Enter> to stop
6 Press [Enter] to finish the grab

Grab Sample 4.1.5
sample measurement.
Operation completed
Sample ID xxxx The measuring value of the grab
Grab Sample xx.x ppb
sample is saved.
<Enter> to finish
46 A-96.250.811 / 091017
AMI Silitrace
Maintenance
6. Maintenance
6.1. Maintenance Table
Monthly or less Replace reagents.

frequent1)
Every 2–3 months Check standard solution and exchange if
necessary.
Semiannual Exchange pump tubes. Perform a calibra-
tion after exchanging the pump tubes.
By occurrence E020, FOME dirty. Clean the photometer
with 5% NH3 solution, see Clean the Pho-
tometer, p. 57.
1) The interval depends on the <Reagents saving> setting, see 4.2.3, p. 85.
NOTICE: A verification is performed automatically each week,

programmed by default on Monday at 06:00 AM. Make sure that
a standard bottle containing sufficient standard solution is
connected.
6.2. Stop of Operation for Maintenance

The prepare maintenance function will flush the complete analyzer
with water. It is recommended to start this function before starting
any maintenance.
1 Select <prepare maintenance>.

2 Follow the instructions on the display.
(Put suction lances into a bucket with high purity water).
3 Wait until the peristaltic pump has stopped.
4 Stop sample flow.
5 Put suction lances into an empty bucket.
6 Shut off power of the instrument.
A-96.250.811 / 091017 47
AMI Silitrace
Maintenance
6.3. Refill or Replace Reagents

The liquid level in container 4 is monitored. The following messag-
es are displayed:
Container almost Maintenance E065 - Reagents low and the
empty remaining reagent volume in % (starting at
17 % = 340 ml).
Container empty Error E022 - Reagent empty
WARNING
Health hazard
 For safe handling of the reagents you must read and under-
stand the Material Safety Data Sheets (MSDS).
 Only persons trained in handling dangerous chemicals are al-
lowed to prepare the reagents.
Canister setup A Suction lance without
A
level detector
B (containers 1-3)
B Suction lance with
level detector
(container 4)
C Level detector
D 2 L mark
C E Reagent container 1
F Reagent container 2
G Reagent container 3
H Reagent container 4
D 2L 2L 2L 2L I Holder
E
OXYCON ON-LINE SILCA OXYCON ON-LINE SILCA
OXYCON ON-LINE SILCA OXYCON ON-LINE SILCA AMI SILICA REAGENT 3 AMI SILICA REAGENT 4
F
G
H
I
48 A-96.250.811 / 091017
AMI Silitrace
Maintenance
Reagent Each 2 liter reagent canister will last for approximately 1 month of
consumption operation if reagent saving is switched off or up to three months if
reagent saving is switched on (see 4.2.3, p. 85).
NOTICE: Excessive use of the flush/fill function or frequent flow
interruptions will shorten this period.
Contents of the Reagent 1: Bags 1a and 1b for Canister 1
reagent set ammonium molybdate and sodium hydroxyde
Reagent 2: Bottle 2 for Canister 2
sulfuric acid 25%
Reagent 3: Bag 3 for Canister 3
oxalic acid dihydrate
Reagent 4: Bag 4a and bottle 4b for Canister 4
ammonium ferrous sulfate hexahydrate
sulfuric acid 25% containing detergent
WARNING
Sulfuric Acid is corrosive and causes severe burns.
 Read the Material Safety Data Sheets (MSDS) first.
 Only persons trained in handling dangerous chemicals are al-
lowed to prepare the reagents
 In case of contact with eyes, rinse immediately with plenty of wa-
ter eyelid wide open, summon medical advice. In case of acci-
dent or if you feel unwell, summon medical advice immediately.
NOTICE: Never prepare this reagent from concentrated sulfuric
acid packed in glass bottles!
Reagent 3:
H302: Harmful if swallowed H312: Harmful
in contact with skin
Warning
Reagent 4a:
H315: Causes skin irritation
H319: Causes serious eye irritation
Warning
H335: May cause respiratory irritation
Reagent 1b, Reagent 2, Reagent 4b:
H314: Causes severe skin burns and eye
damage
Danger
A-96.250.811 / 091017 49
AMI Silitrace
Maintenance
Preparation NOTICE: Please consider the following points when preparing

new reagents:
• Reagent 3, Oxalic Acid dissolves very slowly, we therefore
recommend to prepare Reagent 3 first.
• Reagent 1, add Sodium hydroxide (Reagent 1b) first.
• Before refilling rinse all containers well with demineralized
water.
Reagent 3 1 Fill canister 3 with approx. 1.5 liters of ultrapure water.

2 Add reagent 3 to canister 3.
3 Close the canister with a screw cover and shake well.
4 Fill up the canister to the 2 L mark, close it and shake again.

2 First add the content of bag 1b (sodium hydroxyde).
3 Close the canister with a screw cover and shake well until the
sodium hydroxyde is dissolved.
4 Add the content of bag 1a.

2 Add the bottle 2 (sulfuric acid 25%).
Reagent 4 1 Fill up the canister to the 2 L mark.

2 First add bag 4a.
4 Add bottle 4b, close the canister and mix again.
Some foam forms on the surface.
All canisters
Always replace the reagent filters (included with each reagent set)
when preparing new reagents.
Insert suction lances into the containers. Make sure that the num-
bers on the suction lances correspond to the numbers on the con-
tainers.
50 A-96.250.811 / 091017
AMI Silitrace
Maintenance
6.4. Calibration
Select Menu 3.1 <Maintenance>/<Calibration> and follow the in-
Relay status during calibration:
Calibration 4.1.5
Connect the
standard bottle
to marked holder
<Enter> to continue
Calibration 3.1.1
State xxxx
Progress
<Enter> to stop
Calibration 3.1.1
State Synchronize
Cycle 1
Timer 10 sec
<Enter> to stop
Calibration 3.1.1
State Measure
Cycle 1
Progress
<Enter> to stop
Press [Enter] to save the value in the
Calibration 3.1.1
calibration history or leave the menu
Operation completed with [Exit].
Factor xxxx
<Enter> to save
A-96.250.811 / 091017 51
AMI Silitrace
Maintenance
6.5. Verification
Select Menu 3.2 <Maintenance>/<Verification> and follow the in-
Relay status during verification:
Verification 4.1.5
Connect the
standard bottle
to marked holder
<Enter> to continue
Verification 3.2.1
State xxxx
Progress
<Enter> to stop
Verification 3.2.1
State Synchronize
Cycle 1
Timer 10 sec
<Enter> to stop
Verification 3.2.1
State Measure
Cycle 1
Progress
<Enter> to stop
Verification 3.2.1
verification history or leave the menu
Operation completed
with [Exit].
Current value xxx ppb
Reference value xxx ppb
Deviation xx.x%
<Enter> to save
52 A-96.250.811 / 091017
AMI Silitrace
Maintenance
6.6. Zero
Select Menu 3.2 <Maintenance>/<Zero> and follow the instructions
on the display.
Relay status during zero:
Zero 3.2.1
State xxxx
Progress
<Enter> to stop
Zero 3.2.1
State xxxx
Cycle 1
Timer 10 sec
<Enter> to stop
Zero 3.2.1
State xxxx
Cycle 1
Progress
<Enter> to stop
Zero 3.2.1
verification history or leave the menu
Operation completed
Zero 1.00 V
with [Exit].
<Enter> to save
A-96.250.811 / 091017 53
AMI Silitrace
Maintenance
6.7. Replace the Pump Tubes

The pump tubes [D] of the peristaltic pump are exposed to a mini-
mal wear. It is therefore recommended to exchange the pump
tubes semiannually.
NOTICE: it is highly recommended to replace all pump tubes at
once. Replacement of only one pump tube may lead to uneven
dosing.
CAUTION
Pollution of reagents possible.

If the occlusion frames are opened during operation, already
mixed reagents will flow back into the reagent canisters and pol-
lute the reagents.
 Never open the occlusion frames if the instrument is in opera-
tion.
 Proceed according to Stop of Operation for Maintenance, p.
47 before opening the occlusion frames.
Overview A Pump housing

B Occlusion frame
A
closed
B C Rotor
D Pump tube
C
E Pump inlet
D F Pump outlet
54 A-96.250.811 / 091017
AMI Silitrace
Maintenance
Dismount The pump tubes can easily be dismounted and mounted.

pump tubes Proceed as follows:
A Pump housing
B Occlusion frame open
A C Rotor
B D Pump tube
C E Pump inlet
D F Pump outlet
E
F
1 Switch off the instrument according to instructions in Stop of

Operation for Maintenance, p. 47
2 Open the occlusion frames [B] by turning them counter-clock-
wise.
3 Remove the occlusion frames [B] from the rotor [C] by pulling
the complete occlusion frame out of the holder.
4 Dismount all reagent and sample tubes from the occlusion
frame.
5 Remove all occlusion frames.
6 Install the new occlusion frames.
NOTICE: The tube nearest to the housing (sample tube) has a
diameter of 2.8 mm. All other tubes have a diameter of 0.64 mm.
Ø = 2.8 mm
Ø = 0.64 mm
Ø = 0.64 mm
Ø = 0.64 mm
Ø = 0.64 mm
A-96.250.811 / 091017 55
AMI Silitrace
Maintenance
7 Install the sample tube and all reagent tubes (see Replace the
Pump Tubes, p. 54).
8 Push the occlusion frames onto the rotor.
9 Lock the occlusion frames.
10 Put suction lances into the corresponding reagent container.
11 Start fill system, see Fill System, p. 56.
6.8. Fill System

Fill the reagent tubing:
 at first start-up
 after refilling the reagent containers
 after replacing the pump tubes
Service 3.2.2
Navigate to menu <Maintenance /
Service/Fill system>.
Fill System
Prepare Maintenance Press [Enter].
Fill System 3.2.2.5

The peristaltic pump is activated for
1.5 minutes.
Progress
<Enter> to stop
Fill System 3.2.2.5

Press [Exit] 4 times to return to the op-
erating display mode.
Progress
Done
56 A-96.250.811 / 091017
AMI Silitrace
Maintenance
6.9. Clean the Photometer

To clean the photometer, flush it with 5% ammonia solution.
1 Fill a beaker with 5% ammonia solution.

2 Place all suction lances in the beaker.
3 Navigate to menu <Maintenance>/<Service>/<Fill system>.
4 Press [Enter].
6.10. Longer Stop of Operation

1 Proceed according to chapter Stop of Operation for Mainte-
nance, p. 47.
2 Relax the occlusion frames of the Peristaltic pump.
See Replace the Pump Tubes, p. 54.
A-96.250.811 / 091017 57
AMI Silitrace
Troubleshooting
7. Troubleshooting
7.1. Error List
Error
Non-fatal Error. Indicates an alarm if a programmed value is ex-
ceeded. Such Errors are marked E0xx (bold and black).
Fatal Error (blinking symbol)
Control of dosing devices is interrupted.
The indicated measured values are possibly incorrect.
Fatal Errors are divided in the following two categories:
 Errors which disappear if correct measuring conditions are re-
covered (i.e. Sample Flow low).
Such Errors are marked E0xx (bold and orange)
 Errors which indicate a hardware failure of the instrument.
Such Errors are marked E0xx (bold and red)
HOLD 14:10:45 Error or fatal Error

R1 Error not yet acknowledged.
0.65 ppb
Check Pending Errors 1.1.5 * and
R2
take corrective action.
8 l/h 25.4°C Press [ENTER].
Main Menu 1 Navigate to menu Messages.

Messages Press [ENTER].
Diagnostics
Maintenance
Operation
Installation
Messages 1.1 Navigate to menu Pending Errors.

Pending Errors Press [ENTER].
Maintenance List
Message List
Pending Errors 1.1.5 Press [ENTER] to acknowledge the

Error Code E010 Pending Errors. The Error is reset and
saved in the Message List.
Sample Flow low
<Enter> to Acknowledge
58 A-96.250.811 / 091017
AMI Silitrace
Troubleshooting
Error Description Corrective action

E001 Si 1 Alarm high – Check process
– Check programmed value, see
5.3.1.x.1, p. 96
E002 Si 1 Alarm low – Check process
5.3.1.x.22, p. 96
E003 Si 2 Alarm high – Check process
5.3.1.x.1, p. 96
E004 Si 2 Alarm low – Check process
5.3.1.x.22, p. 96
E007 SilTrace Temp. high – Call service
E008 SilTrace Temp. low – If the error occurs when starting up:
No action necessary. Only wait until the
photometer has warmed up (20
minutes at room temperature), then this
error disappears automatically.
– If the error occurs during operation:
Check whether there are any other
errors and resolve them first (some
errors cause the heater to be switched
off).
E009 Sample Flow high – Check inlet pressure
– Re-adjust sample flow
5.3.1.32.2, p. 97
E010 Sample Flow low – Check inlet pressure
– Re-adjust sample flow
5.3.1.32.32, p. 97
E011 Absorbance too high – Check process
– Check tube connections for air
leakages
A-96.250.811 / 091017 59
AMI Silitrace
Troubleshooting

E012 Temp. Timeout – Check ambient temperature (min 5°C)
– Close the photometer lid
– Heater defective, call service.
E013 Case Temp. high – Check case/environment temperature
5.3.1.42, p. 97
E014 Case Temp. low – Check case/environment temperature
– Check programmed value, see 5.3.1.5,
p. 97
E015 Pump Speed high – Flow in reaction chamber too slow
– Check tubes for air leakages
– Replace pump tubing, see Replace the
Pump Tubes, p. 54
E016 Pump Speed low – Flow in reaction chamber too fast
– Check PeriClip pump tubing (tube
sizes)
– Check tube connections
E017 Control Timeout – Check control device or programming
in Installation, Relay contact, Relay 1
and 2 see 5.3.2 and 5.3.3, p. 98
E018 Reagent Pump – Check cable connection
– Check PeriClip version (Diagnostic/
Identification/Periphery)
– Call service
E019 SilTrace – Check cable connection
– Check Siltrace version (Diagnostic/
Identification/Periphery)
– Call service
E020 Photometer dirty – Cuvette dirty
– Clean cuvette lenses with a tissue
– Replace cuvette, see Replace the
Cuvette, p. 67.
60 A-96.250.811 / 091017
AMI Silitrace
Troubleshooting

E021 Signal Timeout – Unsuccessful peak detection can be
caused by:
1) interrupted light path
2) no water/too much air in the
reaction chamber
– Check if reaction chamber is clogged,
replace it if necessary, see Replace the
reaction chamber, p. 63.
– Check position of the cuvette (make
sure that it is pushed into the slot as far
as it will go)
– Check tube connections
E022 Reagent empty – Refill reagents, see Refill or Replace
Reagents, p. 48.
E023 Sequencer – Check Sample Sequencer connection.
– Make sure that the Sample Sequencer
is set to the mode “AMI” (menu
<Installation>/<Sequence>/<Mode>).
– This error message also appears
during programming of the Sample
Sequencer, as soon as the
<Installation> menu is entered.
E024 Input active – No action necessary.
– This message is displayed if “Fault =
Yes” is programmed, see 5.3.4, p. 102.
E025 Rovalve (6-way valve) – Check cable connection, see Electrical
Connections, p. 19.
– Replace the 6-way valve, see Replace
the 6-Way Valve, p. 65.
E026 IC LM75 – Call service
E028 Signal output open – Check wiring on signal outputs 1 and 2
E030 EEProm Frontend – Call service
E031 Cal. Recout – Call service
E032 Wrong Frontend – Call service
A-96.250.811 / 091017 61
AMI Silitrace
Troubleshooting

E033 Sample Flow 1 low – Check inlet pressure
(multi-channel instru- – Re-adjust sample flow
ments) – Check programmed value, see
5.3.1.32.2, p. 97
5.3.1.32.2, p. 97
5.3.1.32.2, p. 97
5.3.1.32.2, p. 97
5.3.1.32.2, p. 97
5.3.1.32.2, p. 97
E049 Power-on – None, normal status
E050 Power-down – None, normal status
62 A-96.250.811 / 091017
AMI Silitrace
Troubleshooting
7.2. Replace the reaction chamber

Replacing the reaction chamber may be necessary if:
Error 12, <Temp. time out> is shown.
Error 21, <Signal time out> is shown.
A Cover fixing screws
A B Photometer module cover
C Cuvette
D Connection panel
B
C
To replace the reaction chamber proceed as follows:

1 Shut down the Instrument according to Stop of Operation for
Maintenance, p. 47.
2 Pull the cuvette [C] out of the photometer unit.
3 Remove all tube connections from the connection panel [D].
4 Unscrew and remove the 4 cover fixing screws [A].
5 Remove the cover [B] from the photometer unit.
E E Cuvette housing
F Reaction chamber
G Fixing screw
H Insulating disc
F
G
H
6 Loosen the fixing screw [G] of the reaction chamber.
A-96.250.811 / 091017 63
AMI Silitrace
Troubleshooting
7 Remove the reaction chamber from the photometer housing.
Install the new 1 Insert the new reaction chamber into the photometer housing
reaction and tighten the fixing screw [G].
chamber 2 Put the cover [B] onto the photometer unit and tighten the 4
cover fixing screws [A].
3 Push the cuvette into the slot of the cuvette housing.
4 Connect all tubes to the connection panel according to the dia-
gram below.
2 4
03
1B 3 04
64 A-96.250.811 / 091017
AMI Silitrace
Troubleshooting
7.3. Replace the 6-Way Valve
CAUTION
Never loosen the 4 allen screws [D] visible on the 6-way valve
body.
Remove the Replacing the 6-way valve may be necessary if:

6-way valve Error 25 <Rovalve> is shown.
A 6-way valve body
B Valve fixing screw
C Allen key 2.5 mm
A D Valve body fixing screw
D
To remove the 6-way valve from the housing proceed as follows:

Maintenance, p. 47.
2 Switch the instrument off.
3 Disconnect all tubes from the 6-way valve.
4 Disconnect all blind plugs from the 6-way valve.
5 Unscrew the valve fixing screws [B] with the allen key [C].
6 Remove the 6-way valve.
A-96.250.811 / 091017 65
AMI Silitrace
Troubleshooting
Install the
6-way valve
A B C D E F G
A Blind plug E Positioning screw

B 6-way valve F Driving slot
C Fixing screw G Guiding hole
D Valve shaft with driving pin
Seal all unused Inputs with the enclosed blind plugs [A]. Proceed
as follows:
1 Make sure that the valve shaft with driving pin [D] is aligned with
the driving slot [F].
2 Install the 6-way valve so that the valve shaft with driving pin fits
into the driving slot of the motor shaft and the positioning screw
[E] fits into the guiding hole [G].
3 Attach the 6-way valve with the fixing screws [C] to the valve
housing, use the enclosed 2.5 mm Allen key.
4 Fit all tubes to the corresponding outputs/inputs of the 6-way
valve [B], see Replace the Reagent Tubes, p. 68.
5 Screw the blind plugs into the unused inputs of the 6-way valve.
6 Switch on the instrument and select <Maintenance>/
<Service>/<Fill System>.
7 Check all tube connections for leakage.
66 A-96.250.811 / 091017
AMI Silitrace
Troubleshooting
7.4. Replace the Cuvette

Replacing the cuvette may be necessary if:
Error 20 <FOME Dirty> is shown.
A A Photometer module
B Cuvette
B
A Photometer module
A B Cuvette
To exchange the cuvette proceed as follows:

Maintenance, p. 47.
2 Remove all tubes from the cuvette.
3 Pull the cuvette out of the photometer module.
4 Push the new cuvette as far as it will go into the slot of the pho-
tometer module.
5 Connect all tubes to the cuvette, see Replace the Reagent
Tubes, p. 68.
6 Switch on the instrument and select <Maintenance>/
<Service>/<Fill System>.
7 Perform a cuvette factor determination, see 3.4.3, p. 84.
A-96.250.811 / 091017 67
AMI Silitrace
Troubleshooting
7.5. Replace the Reagent Tubes

Tube numbering
A
05
B
13
12
1B
2 03
03
3 3
4 4
04 04
05 I 12
12
4
5 3
1B 7
6 2 11
1 11
02
S
01
04
04
1A
03 1A 2 3 4
T E
02 1 2 3 4 11
1 2 01 3 4
J
K
L
M
68 A-96.250.811 / 091017
AMI Silitrace
Troubleshooting
Nr. from to Length
1 Canister 1 [J] Peristaltic pump [T] inlet 2 1200 mm
2 Canister 2 [K] Peristaltic pump [T] inlet 3 1200 mm
3 Canister 3 [L] Peristaltic pump [T] inlet 4 1200 mm
4 Canister 4 [M] Peristaltic pump [T] inlet 5 1200 mm
1A Peristaltic pump [T] outlet 2 Solenoid valve [R] bottom 280 mm
1B Solenoid valve [S] top reaction chamber [D] 1B 125 mm
2 Peristaltic pump outlet 3 reaction chamber [D] 2 400 mm
01 Flow cell 6-way valve [I] 1 340 mm
02 6-way valve [I] 7 Peristaltic pump inlet 1 (diam.2.8) 340 mm
04 reaction chamber [D] 04 Cuvette [E] 04 160 mm
05 Standard bottle [B] 6-way valve [I] 5 800 mm
11 Cuvette [E] (Siphon tube) lower venting block 470 mm
Fix the siphon tube [A] to the

A lower venting block [C] using the
B two screws [B].
C
B
12 Cuvette [E] upper venting block 300 mm
13 Grab sample bottle [A] 6-way valve [I] 2 640 mm
A-96.250.811 / 091017 69
AMI Silitrace
Troubleshooting
7.6. Cleaning the solenoid valve

Disassemble The solenoid valve should be disassembled if it does not switch
the solenoid anymore or if it is clogged.
valve
1 Switch off the instrument according to instructions in Stop of
Operation for Maintenance, p. 47.
2 Loosen the nut (A).
3 Remove the solenoid coil (B) from

the valve body (C).
B
4 Loosen the fixing screws of the

valve body with a 2.5 mm Allen key
(D).
70 A-96.250.811 / 091017
AMI Silitrace
Troubleshooting
NOTICE: The O-rings inside the

valve body may stick on the flow
cell and fall down if the valve body
is removed.
5 Remove the valve body from the
flow cell.
E
6 Remove the base plate (G) with a

screw driver size 0 (F).
The membrane (H) is now

visible.
7 Clean base plate (G) and mem-
H brane (H) with clean water.
Assemble Assemble the solenoid valve in reverse order.
A-96.250.811 / 091017 71
AMI Silitrace
Troubleshooting
7.7. Replacing Fuses
WARNING
External Voltage.
External supplied devices connected to relay 1 or 2 or to the
alarm relay can cause electrical shocks.
 Make sure that the devices connected to the following con-
tacts are disconnected from the power before resuming in-
stallation.
– relay 1
– relay 2
– alarm relay
When a fuse has blown, find out the cause and fix it before replac-
ing it with a new one.
Use tweezers or needle-nosed pliers to remove the defective fuse.
Use original fuses provided by SWAN only.
A B C D E F G
A 1.6 AT/250V Instrument power supply

B 1.0 AT/250V Relay 1
C 1.0 AT/250V Relay 2
D 1.0 AT/250V Alarm relay
E 1.0 AF/125V Signal output 2
F 1.0 AF/125V Signal output 1
G 1.0 AF/125V Signal output 3
72 A-96.250.811 / 091017
AMI Silitrace
Program Overview
8. Program Overview
For explanations about each parameter of the menus see Program
List and Explanations, p. 79.
 Menu 1 Messages informs about pending errors and mainte-

nance tasks and shows the error history. Password protection
possible. No settings can be modified.
 Menu 2 Diagnostics is always accessible for everybody. No
password protection. No settings can be modified.
 Menu 3 Maintenance is for service: Calibration, verification,
zero, service, simulation of outputs and set time/date. Please
protect with password.
 Menu 4 Operation is for the user, allowing to set limits, alarm
values, etc. The presetting is done in the menu Installation
(only for the System engineer). Please protect with password.
 Menu 5 Installation: Defining assignment of all inputs and
outputs, measuring parameters, interface, passwords, etc.
Menu for the system engineer. Password strongly recom-
mended.
8.1. Messages (Main Menu 1)

Pending Errors Pending Errors 1.1.5* * Menu numbers
1.1*
Maintenance List Maintenance Code 1.2.5*
1.2*
Message List Number 1.3.1*
1.3* Date, Time
A-96.250.811 / 091017 73
AMI Silitrace
Program Overview
8.2. Diagnostics (Main Menu 2)

Identification Designation AMI Silitrace * Menu numbers
2.1* Version V6.31-10/17
Peripherals PeriClip
2.1.3* RoValve
SiliTrace
Factory Test Instrument 2.1.3.1*
2.1.4* Motherboard
Operating Time Years / Days / Hours / Minutes / Seconds 2.1.4.1*
2.1.5*
Sensors SilTrace Temp.
2.2* 2.2.1* PWM
Photometer Current value 2.2.1.3.1*
2.2.1.3* (Raw value)
Absorbance
FOME Mean
Case Temp. 2.2.2.1*
2.2.2* State Machine 2.2.2.2*
History Zero History Number 2.2.3.1.1*
2.2.3* 2.2.3.1* Date, Time
Zero
Cal. History Number 2.2.3.2.1*
2.2.3.2* Date, Time
Factor
Ver. History Number 2.2.3.3.1*
2.2.3.3* Date, Time
Meas. Value
Reference value
Deviation
Grab Sample Number 2.2.3.4.1*
Date, Time
Sample ID
Sample
74 A-96.250.811 / 091017
AMI Silitrace
Program Overview
Cycle diagnostics P2P period 2.2.4.1*

2.2.4* P2P counter
Pump speed
Adjust cycle
Sample Sample ID 2.3.1*
2.3* Sample flow Sample flow 2.3.2.1*
2.3.2* (Raw value)
I/O State Alarm Relay 2.4.1*
2.4* Relay 1 and 2 2.4.2*
Input
Signal Output 1 and 2
Interface Protocol 2.5.1* (only with RS485
2.5* Baud rate interface)
8.3. Maintenance (Main Menu 3)

Calibration * Menu numbers
3.1*
Verification
3.2*
Zero
3.3*
Service Fill System Progress
3.4* 3.4.1*
Prepare maintenance Progress
3.4.2*
Cuvette factor det. Progress
3.4.3*
Simulation Alarm Relay 3.5.1*
3.5* Relay 1 3.5.2*
Relay 2 3.5.3*
Signal Output 1 3.5.4*
Signal Output 2 3.5.5*
Magnetic valve 1 3.5.6*
Magnetic valve 2 3.5.7*
Rotary valve 3.5.8*
A-96.250.811 / 091017 75
AMI Silitrace
Program Overview
Pump 3.5.9*
Set Time (Date), (Time)
3.6*
8.4. Operation (Main Menu 4)

Grab Sample * Menu numbers
4.1*
Sensors Filter Time Const. 4.2.1*
4.2* Hold after Cal. 4.2.2*
Reagents saving 4.2.3*
Relay Contacts Alarm Relay Alarm Si 1 Alarm High 4.3.1.1.1*
4.3* 4.3.1* 4.3.1.1* Alarm Low 4.3.1.1.25*
Hysteresis 4.3.1.1.35*
Delay 4.3.1.1.45*
Relay 1and 2 Setpoint 4.3.x.102*
4.3.2* and 4.3.3* Hysteresis 4.3.x.202*
Delay 4.3.x.30*
Input Active 4.3.4.1*
4.3.4* Signal Outputs 4.3.4.2*
Output / Control 4.3.4.3*
Fault 4.3.4.4*
Delay 4.3.4.5*
Logger Log Interval 4.4.1*
4.4* Clear Logger 4.4.2*
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Program Overview
8.5. Installation (Main Menu 5)

Sensors Meas parameters Cal./Verif. Standard 5.1.1.1.1*
5.1* 5.1.1 5.1.1.1* Parameters Start time
5.1.1.1.2* Monday
Tuesday
Wednesday
Thursday
Friday
Saturday
Sunday
Background Background 5.1.1.2.1*
5.1.1.2*
Auto-Zero Auto-Zero 5.1.1.3.1*
5.1.1.3* Start time 5.1.1.3.2*
Cuvette Factor
5.1.1.4*
Multi-Channel Channels 5.1.2.1*
Channel Selection 5.1.2.2*
Switching time 5.1.2.3*
Signal Outputs Signal Output 1and 2 Parameter 5.2.1.1 - 5.2.2.1*
5.2* 5.2.1* - 5.2.2* Current Loop 5.2.1.2 - 5.2.2.2*
Function 5.2.1.3 - 5.2.2.3*
Scaling Range Low 5.2.x.40.10/10*
5.2.x.40 Range High 5.2.x.40.20/20*
Relay Contacts Alarm Relay Alarm Si 1 Alarm High 5.3.1.1.1*
5.3* 5.3.1* 5.3.1.1* Alarm Low 5.3.1.1.25
Hysteresis 5.3.1.1.35
Delay 5.3.1.1.45
Sample Flow Flow Alarm 5.3.1.2.1*
5.3.1.2* Alarm High 5.3.1.2.2*
Alarm Low 55.3.1.2.35*
Case Temp. high 5.3.1.3*
Case Temp. low 5.3.1.4*
Relay 1 and 2 Function 5.3.2.1–5.3.3.1*
5.3.2* and 5.3.3* Parameter 5.3.2.20–5.3.3.20*
Setpoint 5.3.2.302–5.3.3.302*
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Program Overview
Hysteresis 5.3.2.402–5.3.3.402* * Menu numbers

Delay 5.3.2.50–5.3.3.50*
Input Active 5.3.4.1*

5.3.4* Signal Outputs 5.3.4.2*
Output/Control 5.3.4.3*
Fault 5.3.4.4*
Delay 5.3.4.5*
Miscellaneous Language 5.4.1*
5.4* Set defaults 5.4.2*
Load Firmware 5.4.3*
Password Messages 5.4.4.1*
5.4.4* Maintenance 5.4.4.2*
Operation 5.4.4.3*
Installation 5.4.4.4*
Sample ID 5.4.5*
Line break detection 5.4.6*
Auto-Save 5.4.7*
Interface Protocol 5.5.1* (only with RS485
5.5* Device Address 5.5.21* interface)
Baud Rate 5.5.31*
Parity 5.5.41*
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Program List and Explanations
9. Program List and Explanations
1 Messages
1.1 Pending Errors
1.1.5 Provides the list of active errors with their status (active, acknowl-
edged). If an active error is acknowledged, the alarm relay is active
again. Cleared errors are moved to the Message list.
1.2 Maintenance List
1.2.5 Demands necessary maintenance, e.g. preparing new reagents.
1.3 Message List
1.3.1 Shows the error history: Error code, date/time of issue and status
(active, acknowledged, cleared). 65 errors are memorized. Then
the oldest error is cleared to save the newest error (circular buffer).
2 Diagnostics
In diagnostics mode, the values can only be viewed, not modified.
2.1 Identification
Designation: Designation of the instrument.
Version: Firmware of instrument (e.g. V6.31-10/17).
2.1.3 Peripherals:
2.1.3.1 PeriClip: Firmware of peristaltic pump (e.g. 1.06).
RoValve: Firmware of rotary valve (6-way valve) (e.g. 1.60).
SilTrace: Firmware of heater in the photometer module (e.g. 1.00).
2.1.4 Factory Test: Test date of the Instrument and Motherboard
2.1.5 Operating Time: Years / Days / Hours / Minutes / Seconds
2.2 Sensors
2.2.1 SilTrace (photometer module):
Temp. Temperature inside the reaction chamber in °C
PWM: Heating power in percent (100% at start-up)
2.2.1.3 Photometer:
Current value: Shows the photometer signal in ppb.
(Raw value): Shows the actual photometer signal in V.
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FOME mean
Absorbance: A = -log 10
zero
FOME Mean: Raw signal in V, measured during T2 (pump
stopped) to calculate the concentration.
2.2.2 Miscellaneous:
Case Temp: Shows the current temperature in °C inside the
transmitter.
State Machine: Shows the current process of the instrument.
WARMUP The instrument is heating up after start-up or recov-

ery from a fatal error.
WAITRDY The instrument has a fatal error i.e. pump and
heater off. The instrument will stay in this state until
the fatal error is acknowledged or self cleared.
WAITFLOW The instrument has a sample flow low (E010) alarm. In
this case, the pump stops but the heater stays on. It
remains in this state until the sample flow is re-estab-
lished.
FLUSH Before and after performing a zero, a calibration, a
verification or a grab sample measurement and
after recovering from an alarm, the instrument is
flushing.
Measurement cycle
FIND PEAK Step 1 of measurement (pump on):
The instrument is in measuring mode, waiting for
the peak.
WAIT T1 Step 2 of measurement (pump on):
The instrument is in measuring mode, peak found
and filling the photometer de-aeration tube and the
siphon tube. See Fluidic, p. 10.
WAIT T2 Step 3 of measurement (pump off):
The instrument is in measuring mode, waiting for
stabilization. FOME mean is recorded. After this
state, the instrument goes back to FIND PEAK.
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Calibration, verification, zero or grab sample procedure

CAL INIT A calibration, verification, zero or grab sample mea-
surement has been initiated.
CAL END A calibration, verification, zero or grab sample mea-
surement has finished or been aborted.
Service functions
FILL INIT Service function ‘Fill system’ or ‘Prepare mainte-
nance’ has been initiated (always manually).
FILL The instrument fills the system.
STOP The instrument has finished ‘fill system’ or ‘prepare
maintenance’. The pump stops, the heater is on.
2.2.3 History
2.2.3.1 Zero History
2.2.3.1.1 Number: Counter of zero calibrations.
Date, Time: Date and time when a zero was performed.
Zero: Measuring value in V of the sample without reagent 1,
which is responsible for coloring the sample. A too high value
may result in a FOME dirty error.
2.2.3.2 Cal. History
2.2.3.2.1 Number: Counter of standard calibrations.
Date, Time: Date and time when the standard calibration was
performed.
Factor: Correction factor of the calibration curve.
2.2.3.3 Verif. History
2.2.3.3.1 Number: Counter of verifications.
Date, Time: Date and time when the verification was performed.
Meas. Value: Measuring value of the sample in ppb.
Reference value: Silica concentration in ppb of the standard
solution used.
Deviation: Deviation between the two measurements in %.
2.2.3.4 Grab sample
Number: Counter of grab samples.
Date, Time: Date and time when the grab sample was measured.
Sample ID: ID assigned by the user.
Sample: Measuring result of the grab sample measurement.
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2.2.4 Cycle diagnostics

P2P Diagram Peak
P2P
Peak
2.5
1.5
FOME raw [V]
0.5
P2P period: interval between the last two peaks

P2P counter: shows the time of the current P2P period
Pump speed: shows the current speed code of the pump (0 – 30)
Adjust cycle: when the pump speed exceeds a given time limit 3
times, the pump speed will be readjusted. <Adjust cycles> shows
how many cycles are left before an adjustment.
(0 – 3)
2.3 Sample
Sample ID: Shows the assigned sample identification. This
identification is defined by the user to identify the location of the
sample.
2.3.2 Sample flow:
Sample flow: shows the current sample flow in l/h
(Raw value): shows the current sample flow in Hz
2.4 I/O State
Shows the actual status of all in- and outputs.
2.4.1 Alarm Relay: Active or inactive.
Relay 1 and 2: Active or inactive.
Input: Open or closed.
Signal Output 1 and 2: Actual current in mA
Signal Output 3 (option): Actual current in mA
2.5 Interface
2.5.1 Interface:
Only available if the optional interface is installed. Shows the pro-
grammed communication settings.
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3 Maintenance
3.1 Calibration
3.1.5 During calibration, a solution of known silica concentration (stan-
dard) is measured and the measuring value is compared with the
reference value of the standard (set in 5.1.1.1, p. 87). The instru-
ment then sets the calibration factor to adjust the photometer sensi-
tivity.
It is recommended to perform a calibration:
 at first start-up
 after replacing the pump tubes
 after replacing the cuvette
All calibrations are saved in the Calibration History.
3.2 Verification
3.2.5 During verification, a solution of known silica concentration (stan-
dard) is measured and the mesuring value is compared with the ref-
erence value of the standard. The deviation is expressed in
percent. Unlike a calibration, a verification does not change the cal-
ibration factor.
It is recommended to check the performance of the system by an
automatic weekly verification (default setting).
All verifications are saved in the Verification History.
3.3 Zero
3.3.5 To determine the electronic offset and light intensity of the photom-
eter the sample is measured without adding the color forming re-
agent 1.
It is recommended to program an automatic daily zero calibration
(default setting).
3.4 Service
3.4.1 Fill system
3.4.1.5 Activates the reagent pump and fills all tubes from the container to
the cuvette outlet.
3.4.2 Prepare Maintenance
All tubes are rinsed and emptied when starting this function.
NOTICE: Follow the instructions on the screen carefully,
otherwise the reagents in the canisters will be polluted with
already mixed reagents.
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3.4.3 Cuvette factor determination

The cuvette factor is unique for each combination of photometer
and cuvette. It is set at the factory and stored in a protected memo-
ry area (i. e. it is not deleted by a complete reset or an upgrade of
the firmware).
If the cuvette or photometer is replaced, the cuvette factor must be
determined again.
3.5 Simulation
To simulate a value or a relay state, select the
 alarm relay
 relay 1 and 2
 signal output 1 and 2
with the [ ] or [ ] key.

Press the [Enter] key.
Change the value or state of the selected item with the [ ] or
[ ] key.
 The value is simulated by the relay/signal output.
3.5.1 Alarm Relay: Active or inactive.
3.5.2 Relay 1: Active or inactive.
3.5.3 Relay 2: Active or inactive
3.5.4 Signal Output 1: Actual current in mA
3.5.5 Signal Output 2: Actual current in mA
3.5.6 Magnetic valve 1*: Active or inactive
3.5.7 Magnetic valve 2*: Active or inactive
3.5.8 Rotary valve: Position 1 to 6
3.5.9 Pump: Active or inactive
* Magnetic valve 1: Zero calibration valve
Magnetic valve 2: Channel selector valve (AMI Silitrace Dual-Stream)
At the absence of any key activities, the instrument will switch back
to normal mode after 20 min. If you quit the menu, all simulated val-
ues will be reset.
3.6 Set Time
Adjust date and time.
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4 Operation
4.1 Grab Sample
4.1.5 Starts a grab sample measurement. See Grab Sample Measure-
ment, p. 45.
4.2 Sensors
4.2.1 Filter Time Constant: Used to damp noisy signals. The higher the
filter time constant, the slower the system reacts to changes of the
measured value.
Range: 5–300 Sec
4.2.2 Hold after Cal: Delay permitting the instrument to stabilize again after
calibration. During calibration- plus hold-time, the signal outputs are
frozen (held on last valid value), alarm values, limits are not active.
Range: 0–6‘000 Sec
4.2.3 Reagents saving: Increases the duration of the T2 state (pump off) to
save reagents.
Range: No, Minimum, Medium, Maximum
On a single-channel instrument, the reagent saving mode has the
following effect on the measuring cycle and reagent lifetime:
Option Measuring cycle Reagent lifetime
No 2.8 min approx. 28 d
Minimum 5.3 min approx. 50 d
Medium 7.8 min approx. 75 d
Maximum 10.3 min approx. 100 d
On a multi-channel instrument, the reagent saving effect depends on
the switching time (see 5.1.2.3, p. 90). The faster the channels are
switched, the smaller the reagent saving effect is.
The following table shows the reagent saving effect for different
switching times if <Reagents saving> is set to <Maximum>. <Medi-
um> and <Minimum> correspond to 66% and 33% of the reagent
saving effect.
Switching time Measuring cycle Reagent lifetime
15 min 3.0 min approx. 28 d
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4.3 Relay Contacts

See Relay Contacts, p. 23
4.4 Logger
The instrument is equipped with an internal logger. The logger data
can be copied to a PC with an USB stick if the option USB interface
is installed.
The logger can save approx. 1500 data records. Records consists
of: Date, time, alarms, measured value(s), temperature, flow, ab-
sorbance and pump speed.
Range: 1 Second to 1 hour
4.4.1 Log Interval: Select a convenient log interval. Consult the table be-
low to estimate the max logging time. When the logging buffer is
full, the oldest data record is erased to make room for the newest
one (circular buffer).
Interval 1s 5s 1 min 5 min 10 30 1h Event

min min Driven
Time 25 min 2h 25 h 5d 10 d 31 d 62 d
4.4.2 Clear Logger: If confirmed with yes, the complete logger data is de-
leted. A new data series is started.
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5 Installation
5.1 Sensors
5.1.1 Meas. Parameters
5.1.1.1 Cal./Verif.
5.1.1.1.1 Standard: The default standard is 100 ppb.
During a calibration or verification 15 ml standard is consumed.
Therefore a standard bottle lasts for 3 months at default interval
settings. The default interval settings are:
Start time: 06:00:00
Monday: Verification
All other days: Off
Range: 10.0 ppb to 1.0 ppm (1000 ppb)
5.1.1.1.2 Parameters
5.1.1.1.2.1 Start time: Program the daily start time of a verification or calibra-
tion. Default setting is 06:00:00
5.1.1.1.2.2 Monday: Program a verification, a calibration or Off for this day. A ver-
ification or calibration will be started at the programed <start time>.
5.1.1.1.2.3 Tuesday: Same as Monday.
5.1.1.1.2.4 Wednesday: Same as Monday.
5.1.1.1.2.5 Thursday: Same as Monday.
5.1.1.1.2.6 Friday: Same as Monday.
5.1.1.1.2.7 Saturday: Same as Monday.
5.1.1.1.2.8 Sunday: Same as Monday.
NOTICE: If there is an overlap between a programmed zero
calibration and a programmed calibration/verification, the zero
calibration is prioritized and the calibration/verification is
skipped.
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5.1.1.2 Reag, Background

5.1.1.2.1 Reag. Background: Enter the known basic pollution of the reagents.
The entered value will be subtracted form the measuring value.
5.1.1.3 Auto-Zero
5.1.1.3.1 Auto-Zero: Activate or deactivate the automatic daily zero calibra-
tion.
NOTICE: The zero calibration is essential for a correct
measurement. Swan therefore strongly recommends to have
the option Auto-Zero activated.
If the option is deactivated, the zero calibration must be started
manually or via fieldbus at regular intervals.
5.1.1.3.2 Start time: Enter the start time of an auto zero measurement.
5.1.1.4 Cuvette Factor: Shows the current cuvette factor.
5.1.2 Multi-Channel
5.1.2.1 Channels: If a Sample Sequencer is connected, set the number of
active channels (up to 6).
Otherwise, set this parameter to 1 or 2 according to the instrument
variant.
5.1.2.2 Channel Selection: The following three operating modes can be
set:
 Internal
 Fieldbus
 External
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Mode Internal In the Mode Internal, the AMI Silitrace works as a master.
AMI Silitrace Dual-Stream
The instrument automatically switches between channel 1 and 2.
Sample Sequencer
The AMI Silitrace sequentially measures each single sample
stream of the Sample Sequencer.
Via an external PLC it can be defined which sample streams should
not be measured. In the example below, only the sample streams
2, 4 and 6 are measured, whereas the samples streams 1, 3 and 5
are switched off. Sample streams which are switched off are
marked with an “x” behind the measuring value on the AMI Silitrace
display.
CH1 9
CH2 10
1 mA sink, 5 V open
6 Inputs from PLC
CH3 11
Processor
CH4 12
CH5 13
CH6 14
GND 15
SEQUENCER
Mode Fieldbus The AMI Silitrace is controlled via fieldbus.

Mode External In the mode External, the AMI Silitrace works as a slave.
AMI Silitrace Dual-Stream
The instrument is switched between sample stream 1 and 2 via in-
put. Open: channel 1 is selected, closed: channel 2 is selected.
Sample Sequencer
The AMI Silitrace is controlled by the Sample Sequencer. The Sam-
ple Sequencer in turn is controlled via an external PLC. Each sample
stream to be measured has to be activated by closing the respective
contact.
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Example:
If sample stream 1 of the Sample Sequencer is active, the AMI Sili-
trace measures the sample stream 1 until the Sample Sequencer
changes to the next programmed channel. In the example below, the
sample stream 3 (CH3) highlighted in green will be measured as
soon as the switching time has elapsed.
CH1 9
CH2 10
1 mA sink, 5 V open
6 Inputs from PLC
CH3 11
Processor
CH4 12
CH5 13
CH6 14
GND 15
SEQUENCER
5.1.2.3 Switching time: Time after which the instrument switches to the
next channel. The switching time is valid for all three operating
modes (Internal, Fieldbus and External).
Range: 15–60 min, selectable in 5 min steps
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5.2 Signal Outputs

NOTICE: The navigation in the menu <Signal Output 1> and
<Signal Output 2> is identical. For reason of simplicity only the
menu numbers of Signal Output 1 are used in the following.
5.2.1 and 5.2.2 Signal Output 1 and 2: Assign process value, the current loop
range and a function to each signal output.
5.2.1.1 Parameter: Assign one of the process values to the signal output.
Available values:
 Sample Flow
 Si1
 Si2 (AMI Silitrace Dual-Stream)
5.2.1.2 Current Loop: Select the current range of the signal output. Make
sure the connected device works with the same current range.
Available ranges: 0–20 mA or 4–20 mA
5.2.1.3 Function: Define if the signal output is used to transmit a process
value or to drive a control unit. Available functions are:
 Linear, bilinear or logarithmic for process values.
See As process values, p. 92
 Control upwards or control downwards for controllers.
See As control output, p. 93
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As process The process value can be represented in 3 ways: linear, bilinear or

values logarithmic. See graphs below.
[mA]
20
(0 - 20 [mA])
(4 - 20 [mA])
B A
10 12
0/4 X
0.0 0.1 0.2 0.3 0.4 0.5
A linear X Measured value

B bilinear
[mA]
20
(0 - 20 [mA])
(4 - 20 [mA])
10 12
0/4 X
2 4 6
1 10 100 1’000 10’000
0 1 2 3 4
X Measured value (logarithmic)
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5.2.1.40 Scaling: Enter beginning and end point (Range low & high) of the
linear or logarithmic scale. In addition, the midpoint for the bilinear
scale.
Parameter Sample flow:

5.2.1.40.10 Range low: 0–50 l/h
5.2.1.40.20 Range high: 0–50 l/h
Parameter Si1:
5.2.1.40.11 Range low: 0.0 ppb to 1.00 ppm
5.2.1.40.21 Range high: 0.0 ppb to 1.00 ppm
Parameter Si2:
5.2.1.40.12 Range low: 0.0 ppb to 1.00 ppm
5.2.1.40.22 Range high: 0.0 ppb to 1.00 ppm
As control Signal outputs can be used for driving control units. We distinguish
output different kinds of controls:
 P-controller: The controller action is proportional to the devia-
tion from the setpoint. The controller is characterized by the
P-Band. In the steady-state, the setpoint will never be
reached. The deviation is called steady-state error.
Parameters: setpoint, P-Band
 PI-controller: The combination of a P-controller with an
I-controller will minimize the steady-state error. If the reset
time is set to zero, the I-controller is switched off.
Parameters: setpoint, P-Band, reset time.
 PD-controller: The combination of a P-controller with a
D-controller will minimize the response time to a fast change
of the process value. If the derivative time is set to zero, the
D-controller is switched off.
Parameters: setpoint, P-Band, derivative time.
 PID-controller: The combination of a P-, an I - and a D-con-
troller allows a proper control of the process.
Parameters: setpoint, P-Band, reset time, derivative time.
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Ziegler-Nichols method for the optimization of a PID controller:

Parameters: Setpoint, P-Band, Reset time, Derivative time
Y
B A
X
a
A Response to maximum control output Xp = 1.2/a

B Tangent on the inflection point Tn = 2L
X Time Tv = L/2
The point of intersection of the tangent with the respective axis will
result in the parameters a and L.
Consult the manual of the control unit for connecting and program-
ming details. Choose control upwards or downwards.
If Control upwards or Control downwards is active
5.2.1.43 Control Parameters
5.2.1.43.10 Setpoint: User-defined process value (Measured value or flow)
5.2.1.43.20 P-Band: Range below (upwards control) or above (downwards con-
trol) the set-point, within the dosing intensity is reduced from 100%
to 0% to reach the set-point without overshooting.
5.2.1.43 Control Parameters: if Parameters = Sample flow
5.2.1.43.10 Setpoint: 0–50 l/h
5.2.1.43.20 P-Band: 0–50 l/h
5.2.1.43 Control Parameters: if Parameters = Si1 or Si2
5.2.1.43.12 Setpoint: 0.0 ppb to 1.00 ppm
5.2.1.43.22 P-Band: 0.0 ppb to 1.00 ppm
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5.2.1.43.3 Reset time: The reset time is the time till the step response of a sin-
gle I-controller will reach the same value as it will be suddenly
reached by a P-controller.
Range: 0–9’000 sec
5.2.1.43.4 Derivative time: The derivative time is the time till the ramp re-
sponse of a single P-controller will reach the same value as it will
be suddenly reached by a D-controller.
Range: 0–9’000 sec
5.2.1.43.5 Control timeout: If a controller action (dosing intensity) is constantly
over 90% during a defined period of time and the process value
does not come closer to the setpoint, the dosing process will be
stopped for safety reasons.
Range: 0–720 min
5.2.4 Signal Sequencer: Only visible if a Sample Sequencer is
connected.
Assign process value, the current loop range and a function to the
signal output.
5.2.4.1 Parameter: Only the parameter “Si Sequencer” is available.
5.2.4.2 Current Loop: Select the current range of the signal output. Make
sure the connected device works with the same current range.
Available ranges: 0–20 mA or 4–20 mA
5.2.4.3 Scaling: Define the scaling of the signal output used to transmit a
process value. Available functions are:
Linear, bilinear or logarithmic for process values.
See As process values, p. 92.
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5.3 Relay Contacts

5.3.1 Alarm Relay: The alarm relay is used as cumulative error indicator.
Under normal operating conditions the contact is active.
The contact is inactive at:
 Power loss
 Detection of system faults like defective sensors or electronic
parts
 High case temperature
 Process values out of programmed ranges.
Program alarm levels for the following parameters:
 Si1
 Si2 (multi-channel instruments)
 Sample Flow
 Case Temperature high
 Case Temperature low
5.3.1.1/5.3.1.2 Alarm Si1 and Si2
5.3.1.x.1 Alarm High: If the measured value rises above the alarm high val-
ue, the alarm relay is activated and E001/E003, is displayed in the
message list.
Range: 0.0 ppb to 1.00 ppm
5.3.1.x.22 Alarm Low: If the measured value falls below the alarm low value,
the alarm relay is activated and E002/E004 is displayed in the
message list.
5.3.1.x.32 Hysteresis: Within the hyst. range, the relay does not switch. This
prevents damage of relays contacts when the measured value fluc-
tuates around the alarm value.
5.3.1.x.42 Delay: Duration, the activation of the alarm relay is retarded after
the measuring value has risen above/fallen below the programmed
alarm. Range: 0–28‘800 Sec
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5.3.1.32 Sample Flow: Define at which sample flow a flow alarm should be
issued.
5.3.1.32.1 Flow Alarm: Program if the alarm relay should be activated if there
is a flow alarm. Choose between yes or no. The flow alarm will al-
ways be indicated in the display, pending error list, saved in the
message list and the logger.
Available values: Yes or no
NOTICE: Sufficient flow is essential for a correct measurement.
We recommend to program yes.
5.3.1.32.2 Alarm High: If the measuring values rises above the programmed
value E009 will be issued.
Range: 0–50 l/h
5.3.1.32.32 Alarm Low: If the measuring values falls below the programmed
value E010 will be issued.
Range: 0–50 l/h
5.3.1.42 Case Temp. high: Set the alarm high value for temperature of
electronics housing. If the value rises above the programmed value
E013 is issued.
Range: 30–75 °C
5.3.1.5 Case Temp. low: Set the alarm low value for temperature of
electronics housing. If the value falls below the programmed value
E014 is issued.
Range: -10–20 °C
A-96.250.811 / 091017 97
AMI Silitrace
5.3.2 and 5.3.3 Relay 1 and 2: The contacts can be set as normally open or nor-
mally closed with a jumper. See Relay 1 and 2, p. 24.
The function of relay contacts 1 or 2 are defined by the user
NOTICE: The navigation in the menu <Relay 1> and <Relay 2>
is identical. For reason of simplicity only the menu numbers of
Relay 1 are used in the following.
1 First select the functions as:
- Limit upper/lower,
- Control upwards/downwards,
- Timer
- Fieldbus
- Channel Selection (AMI Silitrace Dual-Stream)
2 Then enter the necessary data depending on the selected func-
tion.
5.3.2.1 Function = Limit upper/lower:
When the relays are used as upper or lower limit switches, program
the following:
5.3.2.20 Parameter: select a process value:
 Sample flow
 Si1
5.3.2.300 Setpoint: If the measured value rises above respectively falls below
the set-point, the relay is activated.
5.3.2.400 Hysteresis: within the hysteresis range, the relay does not switch.
This prevents damage of relay contacts when the measured value
fluctuates around the alarm value.
5.3.2.50 Delay: Duration, the activation of the alarm relay is retarded after the
measuring value has risen above/fallen below the programmed alarm.
Range. 0–600 sec
5.3.2.1 Function = Control upwards/downwards:
The relays may be used to drive control units such as solenoid
valves, membrane dosing pumps or motor valves. When driving a
motor valve both relays are needed, relay 1 to open and relay 2 to
close the valve.
98 A-96.250.811 / 091017
AMI Silitrace
5.3.2.22 Parameter: Choose on of the following process values.

 Sample flow
 Si1
5.3.2.32 Settings: Choose the respective actuator:
 Time proportional
 Frequency
 Motor valve
5.3.2.32.1 Actuator = Time proportional
Examples of metering devices that are driven time proportional are
solenoid valves, peristaltic pumps.
Dosing is controlled by the operating time.
5.3.2.32.20 Cycle time: duration of one control cycle (on/off change).
Range: 0–600 sec.
5.3.2.32.30 Response time: Minimal time the metering device needs to react.
Range: 0–240 sec.
5.3.2.32.4 Control Parameters
Range for each Parameter same as 5.2.1.43, p. 94
5.3.2.32.1 Actuator = Frequency
Examples of metering devices that are pulse frequency driven are

the classic membrane pumps with a potential free triggering input.
Dosing is controlled by the repetition speed of dosing shots.
5.3.2.32.21 Pulse frequency: Max. pulses per minute the device is able to re-
spond to. Range: 20–300/min.
5.3.2.32.1 Actuator = Motor valve
Dosing is controlled by the position of a motor driven mixing valve.
5.3.2.32.22 Run time: Time needed to open a completely closed valve
Range: 5–300 sec.
5.3.2.32.32 Neutral zone: Minimal response time in % of the runtime. If the re-
quested dosing output is smaller than the response time, no
change will take place.
Range: 1–20%
A-96.250.811 / 091017 99
AMI Silitrace

5.3.2.1 Function = Timer:
The relay will be activated repetitively depending on the pro-
grammed time scheme.
5.3.2.24 Mode: Operating mode (interval, daily, weekly)
5.3.2.24 Interval
5.3.2.340 Interval: The interval can be programmed within a range
of 1–1’440 min.
5.3.2.44 Run Time: Enter the time the relay stays activated.
Range: 5–32’400 sec.
5.3.2.54 Delay: during run time plus the delay time the signal and control
outputs are held in the operating mode programmed below.
Range: 0–6’000 sec.
5.3.2.6 Signal Outputs: Select operating mode of the signal output:
Cont.: Signal outputs continue to issue the measured value.
Hold: Signal outputs hold the last valid measured value.
Measurement is interrupted. Errors, except fatal errors,
are not issued.
Off: Signal outputs are switched off (set to 0 or 4 mA).
Errors, except fatal errors, are not issued.
5.3.2.7 Output/Control: Select operating mode of the controller output:

Cont.: Controller continues normally.
Hold: Controller continues based on the last valid value.
Off: Controller is switched off.
5.3.2.24 daily
The relay contact can be activated daily, at any time of a day.
5.3.2.341 Start time: to set the start time proceed as follows:
1 Press [Enter], to set the hours.
2 Set the hour with the [ ] or [ ] keys.
3 Press [Enter], to set the minutes.
100 A-96.250.811 / 091017

AMI Silitrace
4 Set the minutes with the [ ] or [ ] keys.

5 Press [Enter], to set the seconds.
6 Set the seconds with the [ ] or [ ] keys.
Range: 00:00:00–23:59:59
5.3.2.44 Run Time: see Interval
5.3.2.54 Delay: see Interval
5.3.2.6 Signal Outputs: see Interval
5.3.2.7 Output/Control: see Interval
5.3.2.24 weekly
The relay contact can be activated at one or several days, of a
week. The daily starting time is valid for all days.
5.3.2.342 Calendar:
5.3.2.342.1 Start time: The programmed start time is valid for each of the pro-
grammed days. To set the start time see 5.3.2.341, p. 100.
Range: 00:00:00–23:59:59
5.3.2.342.2 Monday: Possible settings, on or off
to
5.3.2.342.8 Sunday: Possible settings, on or off
5.3.2.44 Run Time: see Interval
5.3.2.54 Delay: see Interval
5.3.2.6 Signal Outputs: see Interval
5.3.2.7 Output/Control: see Interval
5.3.2.1 Function = Fieldbus:
The relay will be switched via the Profibus input. No further param-
eters are needed.
5.3.2.1 Function = Channel Selection:
AMI Silitrace Dual-Stream:
Relay 2 can be used to indicate which channel is selected. No fur-
ther parameters are needed.
Relay 2 inactive Channel 1 is selected
Relay 2 active: Channel 2 is selected
A-96.250.811 / 091017 101

AMI Silitrace
5.3.4 Input: The functions of the relays and signal outputs can be de-
fined depending on the position of the input contact, i.e. no function,
closed or open.
AMI Silitrace Dual-Stream:
If <Channel Selection> (5.1.2.2, p. 88) is set to “external”, the input
is used to switch between channels 1 and 2.
5.3.4.1 Active: Define when the input should be active:
The measurement is interrupted during the time the input is active.
No: Input is never active.
When closed Input is active if the input relay is closed
When open: Input is active if the input relay is open
5.3.4.2 Signal Outputs: Select the operation mode of the signal outputs
when the relay is active:
Cont.: Signal outputs continue to issue the measured
value.
Hold: Signal outputs issue the last valid measured value.
Measurement is interrupted. Errors, except fatal
errors, are not issued.
Off: Set to 0 or 4 mA respectively. Errors, except fatal
errors, are not issued.
5.3.4.3 Output/Control: (relay or signal output):
Cont.: Controller continues normally.
Hold: Controller continues on the last valid value.
Off: Controller is switched off.
5.3.4.4 Fault:
No: No message is issued in pending error list and the
alarm relay does not close when input is active.
Message E024 is stored in the message list.
Yes: Message E024 is issued and stored in the mes-
sage list. The Alarm relay closes when input is
active.
5.3.4.5 Delay: Time which the instrument waits, after the input is deactivat-
ed, before returning to normal operation.
Range: 0–6‘000 sec
102 A-96.250.811 / 091017

AMI Silitrace
5.4 Miscellaneous
5.4.1 Language: Set the desired language.
Language
German
English
French
Spanish
5.4.2 Set defaults: Reset the instrument to factory default values in three
different ways:
Set defaults
no
Calibration
In parts
Completely
 Calibration: Sets calibration values back to default. All other
values are kept in memory.
 In parts: Communication parameters are kept in memory. All
other values are set back to default values.
 Completely: Sets back all values including communication
parameters.
5.4.3 Load Firmware: Firmware updates should be done by instructed
service personnel only.
Load Firmware
no
yes
5.4.4 Password: Select a password different from 0000 to prevent unau-
thorized access to the following menus:
5.4.4.1 Messages
5.4.4.2 Maintenance
5.4.4.3 Operation
5.4.4.4 Installation.
Each menu may be protected by a different password. If you forgot
the passwords, contact the closest SWAN representative.
5.4.5 Sample ID: Identify the process value with any meaningful text,
such as KKS number.
5.4.6 Line Break Detection: Define if message E028 should be issued in
case of a line break on signal output 1 or 2.
Choose between <Yes> or <No>.
A-96.250.811 / 091017 103

AMI Silitrace
5.4.7 Auto-Save: Determines whether the result of a manually started

procedure (e. g. grab sample measurement) is automatically saved
or discarded after 20 minutes without key input.
Choose between <Yes> or <No>.
The setting applies to the following procedures:

 grab sample measurement
 (zero) calibration
 verification
 cuvette factor determination
5.5 Interface
Select one of the following communication protocols. Depending on
your selection, different parameters must be defined.
5.5.1 Protocol: Profibus

5.5.20 Device address: Range: 0–126
5.5.30 ID-Nr.: Range: Analyzer; Manufacturer; Multivariable
5.5.40 Local operation: Range: Enabled, Disabled
5.5.1 Protocol: Modbus RTU
5.5.31 Baud Rate: Range: 1200–115 200 Baud
5.5.41 Parity: Range: none, even, odd
5.5.1 Protocol: USB-Stick:
Only visible if an USB interface is installed. No further settings are
possible.
5.5.1 Protocol: HART
104 A-96.250.811 / 091017

AMI Silitrace
Safety Data sheets
10. Safety Data sheets
Catalogue No.: A-85.420.860

Product name: AMI Silitrace Reagent 1a
Ammonium molybdate tetrahydrate.
Product name: AMI Silitrace Reagent 1b
Sodium hydroxide
Product name: AMI Silitrace Reagent 2
Sulphuric acid
Product name: AMI Silitrace Reagent 3
Oxalic acid dihydrate
Product name: AMI Silitrace Reagent 4a
Ammonium iron(II) sulfate hexahydrate
Product name: AMI Silitrace Reagent 4b
Sulphuric acid
Product name: Silica Standard, 100ppb
Calibration solution
Download The current Safety Data Sheets (SDS) for the above listed Re-
MSDS agents are available for downloading at www.swan.ch.
A-96.250.811 / 091017 105

AMI Silitrace
Default Values
11. Default Values

Operation:
Sensors: Filter Time Const.:...................................................................... 10 s
Hold after Cal.:......................................................................... 720 s
Reagents saving ...........................................................................no
Relay Contacts Alarm Relay .................................................. same as in Installation
Relay 1 and 2 ............................................... same as in Installation
Input.............................................................. same as in Installation
Logger: Logger Interval:............................................................ event driven
Clear Logger: ................................................................................no
Installation:
Sensors Meas. Parameters; Cal/Verif:...............................................100 ppb
Meas. Parameters; Parameters; Start time: .......................06:00:00
Meas. Parameters; Parameters; Monday: ...................... Verification
Meas. Parameters; Parameters; Tuesday: .................................. Off
Meas. Parameters; Parameters; Wednesday: ............................. Off
Meas. Parameters; Parameters; Thursday: ................................. Off
Meas. Parameters; Parameters; Friday: ...................................... Off
Meas. Parameters; Parameters; Saturday: ................................. Off
Meas. Parameters; Parameters; Sunday:.................................... Off
Meas. Parameters; Background: ..........................................0.0 ppb
Meas. Parameters; Auto Zero; Auto Zero: .............................. active
Meas. Parameters; Auto Zero; Start time: ..........................00:30:00
Multi-Channel; Channels ................................................................1
Multi-Channel; Channel Selection ........................................ internal
Multi-Channel; Switching time ............................................... 20 min
Signal Output Parameter: ...................................................................................Si1
1 and 2 Current loop: ......................................................................4–20 mA
Function: .................................................................................. linear
Scaling: Range low: ..............................................................0.0 ppb
Scaling: Range high:..........................................................0.50 ppm
Alarm Relay: Alarm Si1:
Alarm high:...........................................................................1.0 ppm
Alarm low: .............................................................................0.0 ppb
Hysteresis: ............................................................................5.0 ppb
Delay:.....................................................................................30 Sec
Sample Flow; Flow Alarm: .......................................................... Yes
Sample Flow; Alarm High ..................................................... 50.0 l/h
Sample Temp; Alarm Low: ...................................................... 3.0 l/h
106 A-96.250.811 / 091017

AMI Silitrace
Default Values
Case temp. high: ..................................................................... 65 °C

Case temp. low:......................................................................... 0 °C
Relay 1 and 2 Function:.......................................................................... limit upper
Parameter:................................................................................... Si1
Setpoint: ............................................................................ 1.00 ppm
Hysteresis:............................................................................ 5.0 ppb
Delay ......................................................................................... 30 s
If Function = Control upw. or dnw:
Parameter:...................................................................................Si1
Settings: Actuator: .......................................................... Frequency
Settings: Pulse Frequency: ..............................................120/min
Settings: Control Parameters: Setpoint:......................... 1.00 ppm
Settings: Control Parameters: P-band: ............................. 5.0 ppb
Parameter:................................................................... Sample flow
Settings: Actuator: .......................................................... Frequency
Settings: Pulse Frequency: ..............................................120/min
Settings: Control Parameters: Setpoint:............................50.0 l/h
Settings: Control Parameters: P-band: ..................................1 l/h
Common settings:
Settings: Control Parameters: Reset time:............................... 0 s
Settings: Control Parameters: Derivative Time: ....................... 0 s
Settings: Control Parameters: Control Timeout:................... 0 min
Settings: Actuator: ................................................ Time proportional
Cycle time: ............................................................................ 60 s
Response time: ..................................................................... 10 s
Settings: Actuator ......................................................... Motor valve
Run time: ............................................................................... 60 s
Neutral zone: ...........................................................................5%
If Function = Timer:
Mode:.................................................................................... Interval
Interval: ................................................................................ 1 min
Mode: ........................................................................................daily
Start time:........................................................................ 00.00.00
Mode:..................................................................................... weekly
Calendar; Start time: ....................................................... 00.00.00
Calendar; Monday to Sunday:.................................................. Off
Run time: ................................................................................... 10 s
Delay: .......................................................................................... 5 s
Signal output:............................................................................. cont
Output/Control: .......................................................................... cont
A-96.250.811 / 091017 107

AMI Silitrace
Default Values
Input: Active ............................................................................when closed

Signal Outputs ........................................................................... hold
Output/Control .............................................................................. off
Fault..............................................................................................no
Delay.......................................................................................... 10 s
Miscellaneous Language:............................................................................. English
Set default:....................................................................................no
Load firmware: ..............................................................................no
Password: ........................................................... for all modes 0000
Sample ID: ....................................................................... - - - - - - - -
Line Break Detection ....................................................................no
Auto-Save .....................................................................................no
Interface Protocol:....................................................... depending on interface
108 A-96.250.811 / 091017

AMI Silitrace
Index
12. Index
A I
Alarm Relay . . . . . . . . 9, 23 Input . . . . . . . . . . . . . 9, 23
Application Range . ...... 8 Instrument Overview . . . . 14
Interface
B HART . . . . . . .... 28
Background. ......... 88 Modbus . . . . . .... 27
Profibus . . . . . .... 27
USB . . . . . . . .... 28
C
Cable thicknesses . . . . . . 19
Calendar . . . . . . . . . . . 101 L
Changing parameters . . . . 44 Longer Stop of Operation. . 57
Changing values . . . . . . . 44
Cuvette factor . . . . . . 67, 84 M
Measuring Principle . ..... 8
D Modbus . . . . . . . . .... 27
Default Values . . . . . . . . 106 Mode External . . . . .... 89
Disassemble the solenoid valve 70 Mode Fieldbus . . . . .... 89
Mode Internal . . . . .... 89
Mounting . . . . . . . .... 16
E
Error List ........... 58
O
F
On-site requirements .... 12
Fill system .......... 83
P
P2P
G
counter . . . . . . . . . 82
Grab Sample . ........ 45
Diagram . . . . . . . . . 82
period . . . . . . . . . . 82
H Power Supply . . . . . . 12, 22
HART . . . . . . . ...... 28 Prepare Maintenance . . . . 83
History Profibus . . . . . . . . . . . . 28
Cal. History . ...... 81
Ver. History . ...... 81
R
Zero History . ...... 81
Reagent consumption. ... 49
Relays. . . . . . . . . . .... 9
A-96.250.811 / 091017 109

AMI Silitrace
Index
S T
Safety Features. . . . . .... 9 Technical Data . . . . . . . . 14
Sample Flow . . . . . . . . . 33 Terminals . . . 21, 23–24, 27
Sample requirements . . . . 12 Tube numbering . . . . . . . 68
Setup. . . . . . . . . . . . . . 29
Signal Outputs . . . . . . 9, 26 U
Silica measurement . . . . . 12 USB Interface . ........ 28
SilTrace . . . . . . . . . . . . 79
Software . . . . . . . . . . . . 43 W
Standard consumption . . . . 32
State Machine . . . . . . . . 80 Wire .............. 19
System, Description of . .... 8
110 A-96.250.811 / 091017

AMI Silitrace
Notes
13. Notes
A-96.250.811 / 091017 111

AMI Silitrace
SWAN
is represented worldwide by subsidiary companies
and distributors.
cooperates with independent representatives

all over the world.
SWAN Products
Analytical Instruments for:
High Purity Water
Feedwater, Steam and Condensate
Potable Water
Pool and Sanitary Water
Cooling Water
Waste Water and Effluents
Made in Switzerland
112 A-96.250.811 / 091017

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AMI Silitrace

Version 6.31 and higher

Title: Monitor AMI Silitrace Operator’s Manual

00 Okt. 2015 First Edition

01 Aug. 2016 Update to FW Release 6.20, Mainboard Rev. 2.5

02 Mar. 2017 Update to FW Release 6.30 (includes multi-channel

© 2017, SWAN ANALYTISCHE INSTRUMENTE AG, Switzerland, all rights reserved

subject to change without notice.

10. Safety Data sheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105

AMI Silitrace - Operator’s Manual

1.1. Warning Notices

Your life or physical wellbeing are in serious danger if such

Severe injuries or damage to the equipment can occur if such

Damage to the equipment, minor injury, malfunctions or incor-

Mandatory The importance of the mandatory signs in this manual.

Warning Signs The importance of the warning signs in this manual.

Electrical shock hazard

1.2. General Safety Regulations

Risk of Electrical Shock

For safe instrument installation and operation you must read

Only SWAN trained and authorized personnel shall perform the

2.1. Description of the System

Grab sample Easy to use grab sample function.

A Grab sample bottle K Reagent 2

2.2. Instrument Specification

Power Supply Voltage: 100–240 VAC (± 10%)

Dimensions Panel: stainless steel

2.3. Instrument Overview

A Panel I Flow meter

3.1. Installation Checklist

Check Instrument’s specification must conform to the National Electri-

3.2. Mounting of Instrument Panel

Mounting re- The instrument is only intended for indoor installation.

3.3. Connect Sample and Waste

3.3.1 AMI Silitrace

A Sample inlet D Compression ferrule

3.3.2 AMI Silitrace Dual-Stream

3.4. Electrical Connections

Risk of electrical shock.

A PG 11 cable gland: cable Øouter 5–10 mm

To prevent from electrical shock, do not connect the instrument

The mains of the AMI Transmitter must be secured by a main

3.4.1 Connection Diagram

3.4.2 Power Supply

A Power supply connector

3.5. Relay Contacts

3.5.2 Alarm Relay

NOTICE: With certain alarms and certain settings of the AMI

Terminals Description Relay connection

NO 12/11 Active (closed) during normal 11

3.5.3 Relay 1 and 2

A Jumper set as normally open (standard setting)

Risk of damage of the relays in the AMI Transmitter due to

3.6. Signal Outputs

3.6.1 Signal Output 1 and 2 (current outputs)

3.7. Interface Options

The slot for interfaces can be used to expand the functionality of

3.7.1 Signal Output 3

3.7.2 Profibus, Modbus Interface