Lampiran C

LC-
1000
LAMPIRAN C
PERHITUNGAN SPESIFIKASI ALAT
1. Tangki Isoamil Alkohol

Kode : T-01
Fungs : menampung sementara bahan baku isoamyl alkohol untuk persediaan 1
minggu.
Tipe : Silinder vertikal dengan tutup atas berbentuk standar dishead dan tutup
bawah berbentuk plat datar.
Kondisi Operasi : T = 30 oC (303 K)
P = 1 atm
Kapasitas : 6488,8600 kg/jam
Waktu Penyimpanan : 7 hari
= 7 x 24 jam
= 168 jam
Kapasitas tangki untuk memenuhi selama 1 minggu
=mxt
= 6488,8600 kg/jam x168 jam
= 1090128,4430 kg
Densitas ( ρ ¿ = 812,000 kg/m3
1. Volume Tangki (Vt)
Volume larutan dalam tangki (VL)
m
VL =
p
109128.443 kg
=
812.000 kg/ jam
= 1342,5230 m3
LC-
1000
Tangki dirancang dengan ketentuan :
a. 90% dari volume tangki terisi Isoamil Alkohol
b. Perbandingan Tinggi (H) 1.5 Diameter Tangki (ID)

Maka tangki berisi larutan Isoamil Alkohol (Vt)
100
Vt = (VL)
90
100
= (1342.523 m3)
90
Vt = 1491,692 m3
= 394063.2890 galon
Jumlah tangki yang dibutuhkan (n)

n = 2 buah
maka volume tangki per unit (Vt)
1491.692m 3
Vt =
2
= 745.8460 m3
2. Diameter Tangki
Volume tangki bola (Vt) = volume silinder (Vs) + Volume tutup ( Vh)
volume silinder (Vs)
Vs = Hs + As
Hs = 3/2 (D) = 1.5 D
As =1/4 phi r2
Vs = 1,5 D ((1/4)(π D2))
Vs = 1,178 D3
Dari Pers. 5.11 hal 88 Brownell & Young
Volume tutup ( Vh)
Dimana dalam f3 dan D dalam satuan inch.
Vh = 8,0297 x 10-10 x D3
LC-
1000
Maka :
Vt = Vs + Vh
Vt = 1,178 D3
745,846
D3 =
1,178
Dt =√ 633,415 m³
Dt = 8,5881 m
Hs = 1,5 D
Hs = 1,5 x 8,5881 m
= 12.8820 m
Tinggi Larutan dalam Silinder
90
Hl = (Hs)
100
Hl = 11.5940 m
3. Tebal Dinding Tangki
Untuk Internal Presure, tebal dinding (shell) dihitung dengan persamaan

sebagai berikut :
Dari Pers. 13.1 hal 254 Brownel & Young
Pr . dt
ts = +C
4. fE−Pr
Dimana :
pr = tekanan rancangan
Pr = P.operasi + (5% x PH)
jika :
PH = densitas . Hl.g
PH = 92353,8232 N/m2
Fk = 120658253 N/m2
LC-
1000
Maka :
Pr = 105942,6910 N/m2
Ri = jari jari dalam
Ri = Dt/2
Ri = 4,294 m
jika material yang digunakan adalah carbon steel SA-212 Grade B (tabel 13.1
brownell & young ) maka ( tabel 13.1 brownell& young,. Hal 521)
Allowwable Street (f)
f = 17500 psi
= 120658253N/m2
Efisiensi (E)
E = 80 %
Faktor Korosi (c)
C = 0,0032 m
Maka :
Pr . dt
ta = +C
4. fE−Pr
105942,691 N /m2 X 4,294 m
= + 0,0032 m
4 x 20658253 N /m2−105942,691 N /m2
= 0.008 m
4. Penentuan tebal tutup Atas (th) :
0,885. pr . Ro
th = +C
fE−0,1 Pr
dimana :
Ro = Diameter Luar selinder

Ro = 8,604 m
LC-
1000
N
0,885. x 105942.691 x 8,604 m
th = m2
+0,0032 m
0,8 x 120658253 N /m2−0,1 x 105942.691 N /m2
= 0,012 m
th = 0,4540 in
karena th = 0,454 in, maka tetabal tutup adalah
th = 7/6 in
= 0.438 x 0,0254
= 0,0111 m
BC = R- ICR
AB =ID/2 – ICR
AC = (BC2-AB2)1/2
B = r-AC
OA = th + B + Sf
dari tabel 5.6 brownell&young hal.88 untuk tebal tutup
th = 0,438 in
di dapat :
Strength flange (Sf) = 0.0381 in

LC-
1000
Brown radius (r) = OD shell

= 8,604 m
Knokcle radius (icr) = 0,008 m
Maka :
BC = 8.596 M
AB = 4.294 M
AC = 7.456 M
B = 1.148 M
OA = 1.197 M
Sehingga tinggi total tangki (Ht)
Maka :
Ht = Hs + OA
Ht = 14.079 m
5. Penentuan tutup bawah

Tebal tutu bawah (plat datar) dihitung dengan menggunakan pers. 3.16 hal. 45
brownell & young :
Pr . dt
ta = +C
2. fE
105942.691mN /m2 x 8,604 m

ts = +0,0032 m
2 x 0,8 x 20658253 N /m2
= 0,007912 m
2. Pompa (P-01)
Kode : P-01
Fungs : untuk memompa bahan baku isoamyl alkohol menuju ke reactor
LC-
1000
(R-01)
Tipe : Pompa sentrifugal
Material : stainless steel
Jumlah : 2 buah
P = 1 atm
Kapasitas yang akan di pompakan (m)

m = 6488,860 kg/jam
= 6488,860 kg/jam x 2,0246 x 1/3600
= 3,649 lb/s
Densitas ( ρ ¿ = 812,000 kg/jam
= 50,6914 lb/ft3
Viskositas (µ) = 3,4 cp
= 0,0022 lb/ft.s
Laju alir Volumetrik (Q)

Q = m/p
3 ,649 lb/s
=
0,00228lb / ft 3. s
= 0,0719 ft3/s
1. Diameter `dalam optimum pipa (Diopt)
Laju alir dalam pipa diasumsikan sebagai aliran turbulen (Nre> 2100),
maka dari pers. 14-15, peters & timmerhause, hal 496, maka diameter pipa
optimum
Di opt = 3.9(Q)^0.45 x (P)^0.13
= 1,9882 in
berdasarkan tabel 11 hal 884 kern, dipilih:
Nominal size pipe = 3 in
Shedule = 40
LC-
1000
inside diameter = 0,256 ft

outside diameter = 0,292 ft
luas permukaan air = 0,0512 ft2
kecepatan aliran dalam pipa (V)
V = Q/A
= 1.4046 ft/s
Pemeriksaan bilangan Reynold (Nre)

ρ .V . D
Nre =
μ
Nre = 7968,1468
Karena Nre > 2.100 maka asumsi benar
direncanakan :
Panjang pipa lurus (L)
L = 5m
= 16.40419948 ft
Tinggi pompa (H)
H = 5m
= 16.40419948 ft
12elbow
gate, open
Dipilih Le/Dpipa besi baja :
material
90 (Le/D)
Le/D
Le/D == 32
32 (tabel.1Peters
(tabel.1 Peters%%Timmehaus,
Timmehaus,hal
hal484)
484)
ε
Le
Le == 8.181330061
8.181330061ftft
= 0,00015 ft
ε /D = 0,00015 ft / 0,256 ft
LC-
1000
= 0,0006
f = 0.009502608
Friksi yang terjadi (F)

Friksi sepanjang pipa lurus dari sambungan
2. f .V . Ltot
F = (Pers. 9, Peter & Yimmerhaus, hal. 483)
gc . D
Dimana Ltot = (16,4042ft + 8,1813 ft + 3,5793 ft )
= 28.16486144 ft
F = 0.128397371 ft
Friksi karena adanya kontraksi dari tangki ke pipa:

Dimana :
K = 0,5
F = (k.V2) / (gc.2)
= 0.015331676 ft
Total friksi ( Σ F) = 0.143729047 ft
Penentuan kerja pompa (W)
p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
Jika diasumsikan bahwa pengaliran fluida tidak terjadi perubahan
diameter pipa, maka :
∆ V =V 2−V 1=0
Untuk aliran turbulen
a=1
jadi :
LC-
1000
W = 0 + (16,4042 ft) +(0) 0.143729047 ft

W = 16.54792905 lbf.ft/lbm
2. Penentuan daya Pompa (P)
ρ .Q . W
P =
550
= 0.10979589 hp
Jika :
Q = 0,071989795 ft3/s
= 32.31126521gal/ mnt
µ = 3,4 cp
= 0,34 gr/cm.s
µ / ρ = 0,418719212 cs
Berdasarkan gambar 14.36 peters & timmerhaus, hal 520
efisiensi pompa (ɳ ) = 55% = 0,55
maka :
Broke horse power (BHP) = p/ ɳ
= 0.199629 hp
Penentuan daya motor :
Berdasarkan gambar 14.38, peters & timmerhaus, hal. 521
Untuk BHP = 0,199629 hp
ɳ = 0,08
Daya motor = 0.249536113 hp
= 0,25hp
3. Tangki Asam Asetat
Kode : T-03
Fungs : menampung sementara bahan baku asam asetat untuk
LC-
1000
persediaan 1 minggu.
Tipe : Silinder vertikal dengan tutup atas berbentuk standar dishead
dan tutup bawah berbentuk plat datar.
Kondisi Operasi : T = 30 oC (303

K)
P = 1 atm
Kapasitas : 4393.243 kg/jam
= 7 x 24 jam
= 168 jam
=mxt
= 4393.243 kg/jam x168 jam
= 738065 kg
Densitas ( ρ ¿ = 1043 kg/jam
m
VL =
p
738065 kg
=
1043 kg/ jam
= 707,636 m3
c. 90% dari volume tangki terisi Isoamil Alkohol
d. Perbandingan Tinggi (H) 1.5 Diameter Tangki (ID)

LC-
1000
100
Vt = (VL)
90
100
= (707,636 m3)
90
Vt = 768,263 m3
= 207708.637 galon

n = 2 buah
768,263m 3
Vt =
2
= 393,1313 m3
2. Diameter Tangki
Vs = Hs + As
Hs = 3/2 (D) = 1.5 D
As =1/4 π r2
Vs = 1,5 D ((1/4)(π D2))
Vs = 1,175 D3
Volume tutup ( Vh)
Vh = 8,0297 x 10-10 x D3
Maka :
Vt = Vs + Vh
Vt = 1,175 D3
393,1313m ³
D3 =
1,175
LC-
1000
Dt =√ 333,8695402m ³
Dt = 6,9373 m
Hs = 1,5 D
Hs = 1,5 x 6,9373 m
= 10,40599 m
90
Hl = (Hs)
100
Hl = 9,365393 m

sebagai berikut :
Pr . dt
ts = +C
4. fE−Pr
Dimana :
jika :
PH = 95825,1153 N/m2
Fk = 120658253.000 N/m2
Maka :
Pr = 106116,2558 N/m2
Ri = Dt/2
Ri = 3,4686 m
LC-
1000
f = 17500 psi
= 120658253 N/m2
Efisiensi (E)
E = 80 %
Faktor Korosi (c)
C = 0,0032 m
Maka :
Pr . dt
ta = +C
4. fE−Pr
106116,2558 N /m 2 X 3,4686 m
= +0,0032 m
4 x 120658253 N /m 2−106116,2558 N /m2
= 0.007 m
0,885. pr . Ro
th = +C
fE−0,1 Pr
dimana :

Ro = 6,951 m
0,885. x 106116,2558 N / m2 x 6,951 m
+ 0,0032m
th = N
0,8 x 20658253 −0,1 x 106116,2558 N /m2
m2
= 0,00995 m
th = 0,39 in
th = 7/6 in
LC-
1000
= 0.438 x 0,0254
= 0,0111 m
BC = R- ICR
AB =ID/2 – ICR
AC = (BC2-AB2)1/2
B = r-AC
OA = th + B + Sf
th = 0,438 in
di dapat :

= 6,943 m
Knokcle radius (icr) = 0,315 in
= 0,0079 m
Maka :
BC = 6,943 M
AB = 3,47 M
AC = 6,024 M
LC-
1000
B = 0,93 M
OA = 0,98 M
Maka :
Ht = Hs + OA
Ht = 11,38 m

brownell & young :
Pr . dt
ta = +C
2. fE
106116,2558 N / m 2 x 8,604 m
ts = + 0,0032m
2 x 0,8 x 120658253 N / m2
= 0,00701 m
4. Pompa (P-02)
Kode : P-02
Fungs : untuk memompa bahan baku asam asetat menuju ke reactor
(R-01)
Jumlah : 2 buah
P = 1 atm

m = 4393,3421 kg/jam
= 4393,3421 kg/jam x 2,0246 x 1/3600
LC-
1000
= 2,47071 lb/s
= 65,1122 lb/ft3
= 0.0005 lb/ft.s

Q = m/p
2,47071lb/s
=
0,0005lb/ ft 3. s
= 0.0379 ft3/s
optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 1,3597 in
Shedule = 40
outside diameter =0,292 ft
luas permukaan air = 0.05125 ft2
V = Q/A
= 1.40468 ft/s

ρ .V . D
Nre =
μ
LC-
1000
Nre = 24465,361
direncanakan
L : = 5m
Panjang pipa lurus (L) = 16.40419948 ft
Tinggi pompa (H)
H = 5m
= 16.40419948 ft
21Dipilih
gate,
elbowopen
90 Le/D
material pipa besi baja :
(Le/D)
Le/D
Le/D = =327 (tabel.1
(tabel.1Peters
Peters%%Timmehaus,
Timmehaus,hal
hal484)
484)
ε
Le
Le = =8.181330061
3,57933 ft ft
= 0,00015 ft
ε /D = 0,00015 ft / 0,256 ft
= 0,0006
f = 0.0079418

2. f .V . Ltot
gc . D
= 28.16486144 ft
F = 0,02981 ft

Dimana :
K = 0,5
F = (k.V2) / (gc.2)
= 0.0042596 ft
LC-
1000
Total friksi ( Σ F) = 0,0340727 ft

p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
a=1
jadi :
W = 0 + (16,4042 ft) +(0) 0,0340727 ft
W = 16,43827 lbf.ft/lbm
ρ .Q . W
P =
550
= 0,073844 hp
Jika :
Q = 0,0379454 ft3/s
= 17,031094 gal/ mnt
µ = 0,75 cp
= 0,075 gr/cm.s
M/ ρ = 0,071908 cs
LC-
1000

maka :
= 0,13426 hp
ɳ = 0,8
Daya motor = 0.16782737 hp
= 0,2 hp
5. Tangki H2O
Kode : T-03
Fungs : menampung sementara bahan baku air untuk persediaan 1
minggu.
Tipe : Silinder vertikal dengan tutup atas berbentuk standar dishead
dan tutup bawah berbentuk plat datar.

P = 1 atm
Kapasitas (m) : 186,0099 kg/jam
= 7 x 24 jam
= 168 jam

M =mxt
= 168,0099 kg/jam x168 jam
= 31249,6681 kg
LC-
1000
m
VL =
p
31249,6681kg
=
1027 kg/ jam
= 30,429 m3
a. 90% dari volume tangki terisi Isoamil Alkohol

100
Vt = (VL)
90
100
= (30,429 m3)
90
Vt = 33,80901 m3
= 8931,3951 galon

n = 2 buah
33,429 m3
Vt =
2
= 16,9045 m3
2. Diameter Tangki
LC-
1000
Vs = Hs + As
Hs = 3/2 (D) = 1.5 D
As =1/4 π r2
Vs = 1,5 D ((1/4)(π D2))
Vs = 1,175 D3
Volume tutup ( Vh)
Vh = 8,0297 x 10-10 x D3
Maka :
Vt = Vs + Vh
Vt = 1,175 D3
16,9045m ³
D3 =
1,175
Dt =√ 14,35626 m³
Dt = 2,4304 m
Hs = 1,5 Dt
Hs = 1,5 x 2,4304 m
= 3,6456 m
90
Hl = (Hs)
100
Hl = 3,281 m

sebagai berikut :

LC-
1000
Pr . dt
ts = +C
4. fE−Pr
Dimana :
jika :
PH = 33056,2614 N/m2
Fk = 120658253.000 N/m2
Maka :
Pr = 102977,8131 N/m2
Ri = Dt/2
Ri = 3,4686 m
f = 17500 psi
= 120658253 N/m2
Efisiensi (E)
E = 80 %
Faktor Korosi (c)
C = 0,0032 m
Maka :
Pr . dt
ta = +C
4. fE−Pr
102977,8131 N /m 2 X 3,4686 m
= + 0,0032m
4 x 120658253 N /m 2−106297,8131 N /m2
= 0.0045 m
LC-
1000
0,885. pr . Ro
th = +C
fE−0,1 Pr
dimana :

Ro = 2,44m
0 , 885 . x 102977,8131 N /m2 x 2,44 m
th = +0,0032 m
0,8 x 120658253 N /m2−0,1 x 102977,8131 N /m2
= 0,00549 m
th = 0,22 in
th = 7/6 in
= 0.438 x 0,0254
= 0,0111 m
BC = R- ICR
AB =ID/2 – ICR
AC = (BC2-AB2)1/2
B = r-AC
LC-
1000
OA = th + B + Sf
th = 0,438 in
di dapat :

= 6,943 m
Knokcle radius (icr) = 0,315 in
= 0,0079 m
Maka :
BC = 6,943 M
AB = 3,47 M
AC = 6,024 M
B = 0,93 M
OA = 0,98 M
Maka :
Ht = Hs + OA
Ht = 11,38 m

brownell & young :
Pr . dt
ta = +C
2. fE
106116,2558 N / m 2 x 8,604 m
ts = + 0,0032m
2 x 0,8 x 120658253 N / m2
= 0,007013 m
LC-
1000
6. Pompa (P-03)
Kode : P-03
Fungs : untuk memompa bahan baku air menuju ke reactor
(R-01)
Jumlah : 2 buah
P = 1 atm

m = 186,0099kg/jam
= 186,0099 kg/jam x 2,0246 x 1/3600
= 0,10461 lb/s
= 64,1133 lb/ft3
= 0.00571 lb/ft.s

Q = m/p
0,10461lb /s
=
0,000571lb /ft 3. s
= 0,001632 ft3/s
optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
LC-
1000
= 0,37294 in
Shedule = 40
luas permukaan air = 0.006 ft2
V = Q/A
= 0,27194 ft/s

ρ .V . D
Nre =
μ
Nre = 2668,381
direncanakan
L : = 5m
Tinggi pompa (H)
H = 5m
= 16.40419948 ft
21Dipilih
gate, open Le/D
elbowmaterial pipa besi baja :
90 (Le/D)
Le/D
(tabel.1Peters
Peters%%Timmehaus,
Timmehaus,hal
hal484)
484)
ε
Le
Le = =2,797
1,223
ft ft
= 0,00015 ft
ε /D = 0,00015 ft / 0,08741 ft
= 0,001716
LC-
1000
f = 0.01132

2. f .V . Ltot
gc . D
= 20,4253 ft
F = 0,012159 ft

Dimana :
K = 0,5
F = (k.V2) / (gc.2)
= 0.000575 ft
p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
a=1
jadi :
LC-
1000
W = 0 + (16,4042 ft) +(0) 0,012734 ft

W = 16,41693 lbf.ft/lbm
ρ .Q . W
P =
550
= 0,003122hp
Jika :
Q = 0,001613 ft3/s
= 17,031094 gal/ mnt
µ = 0,85 cp
= 0,085 gr/cm.s
µ /ρ = 0,082765 cs
maka :
= 0,01 hp
Untuk BHP = 0,01 hp
ɳ = 0,8
Daya motor = 0,00709 hp
= 0,01 hp
7. Pompa (P-04)
Kode : P-04
Fungs : untuk memompa larutan yang terbentuk pada destilasi 3
(MD-03) menuju reaktor 1 (R-01)
LC-
1000

Material
BM.Xi : stainless
pl steel pl.xi miu miu.xi
Jumlah kg/m3
: 2 buah kg/m3 cp cp
0.1756 1027.0000 10.0111 1.7000 0.0166
Kondisi Operasi : T = 128 (401 K)
11.1698 1043.0000 194.0037 0.3500 0.0651
70.8916 P = 1
812.0000 atm 653.0482 0.2600 0.2091
Kapasitas
0.0000yang akan di pompakan0.0000
872.0000 (m) 0.2800 0.0000
m 82.2370 3754.0000 857.0631 2.5900 0.2908
= 7425,119 kg/jam
= 7425,119 kg/jam x 2,0246 x 1/3600
= 4,1752 lb/s
massa BM Mol fraksi

Komponen
(kg/jam) (kg/jam) (Kgmol) (Xi)
H2O 15.8532 18.0147 0.8800 0.0097
CH3COOH 1008.3749 60.0508 16.7920 0.1860
C5H11OH 6399.8909 88.1466 72.6051 0.8042
CH3COOC5H11 0.0000 130.1827 0.0000 0.0000
Total 7424.1190 90.2772 1.0000

= 64,1133 lb/ft3
= 0.00571 lb/ft.s

Q = m/p
4,1752llb/ s
=
857.0631lb /ft 3. s
= 0,0780 ft3/s
LC-
1000

optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 2,0762 in
Shedule = 40
V = Q/A
= 1,5226 ft/s

ρ .V . D
Nre =
μ
Nre = 1776,6451
direncanakan
L : = 5m
Tinggi pompa (H)
H = 5m
= 16.40419948 ft
21Dipilih
gate,
elbowopen
90 Le/D
(Le/D)
Le/D
(tabel.1Peters
Peters%%Timmehaus,
Timmehaus,hal
hal484)
484)
Le
Le = =8,1813
3,5793
ft ft
LC-
1000
ε = 0,00015 ft
ε /D = 0,00015 ft / 0,08741 ft
= 0,0000587
f = 0.0120

2. f .V . Ltot
gc . D
= 281646 ft
F = 0,1918 ft

Dimana :
k = 0,5
F = (k.V2) / (gc.2)
= 0,0180 ft
p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
LC-
1000

a=1
jadi :
W = 0 + (16,4042 ft) +(0) 0,02098 ft
W = 16,6140 lbf.ft/lbm
ρ .Q . W
P =
550
= 0,1261 hp
Jika :
Q = 0,0780 ft3/s
= 35,0249 gal/ mnt
µ = 0,2098 cp
= 0,0290 gr/cm.s
µ / ρ = 0,5434 cs
maka :
= 0,23 hp
Untuk BHP = 0,23 hp
ɳ = 0,8
= 0,5 hp
LC-
1000
8. Heater (He-01)
Kode : He-01
Fungsi : menaikan suhu larutan isoamyl alkohol dari tangki ke
reaktor (R-01)
Tipe : shell and tube (HE 1-2)
Material : Carbon steel
Tekanan : 1 atm
Jumlah : 1 unit
Sesuai hasil perhitungan neraca massa dan neraca panas dapat diketahui :
Beban panas heater (Q)
Q = 1533235,045 kJ/jam
= 1533235,045 kJ/jam x 0,23901
= 366458.5081 kkal/jam
= 1454217,298 btu/jam
Laju alir massa fluida panas (W)
W =528,4170 35 kg/jam
= 1164,9481 lb/jam
Laju alir massa fluida dingin (w)
w = 6488,8597 kg/jam
= 114305,3402 lb/jam
1. Beda suhu sebenarnya (∆ t ¿

Fluida panas (t) Fuida dingin (T) beda suhu
527 suhu tinggi 203 324
527 suhu rendah 86 441
0 Beda 117 117
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 379,498 oF
LC-
1000
T 1+T 2
Tc =
2
= 144,5 oF
2. UD dan A
Sesuai tabel 8 kern hal 840 fluida panas (steam) dan fluida dingin (heavy
organic) didapat :
UD = 6 Btu/hr.ft2.oF sampai 60 Btu/hr.ft2.oF
Trial UD = 40 Btu/hr.ft2.oF
Luas permukaan perpindahan panas (A)
Q
A =
U D x∆t
= 95,79854 ft2
direncanakan menggunakan tube dengan spesifikasi :
OD =3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Pitch triangular = 1 in
Panjang (L) = 10 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
LC-
1000
= 48,8021buah
Dari tabel 9 Kern hal. 842, dipilih nilai uyang mendekati
Nt = 52 buah
ID Shell = 10 in
= 0,833 ft
Passes (n) =2
A terkoreksi = Nt x l x a0
A terkoreksi = 52 x 10 ft x0,1963 ft2/ft
=102,076 ft2
Q
UD =
A terkoreksi x ∆ t
= 37,54008 Btu/hr.ft2.oF
= 38 Btu/hr.ft2.oF
Maka trial UD memenuhi.
3. Tube side (fluida dingin)
a. Luas Aliran (at)
Nt x At '
at =
1444 x n
= 0,05452 ft2
b. Kecepatan massa ( Gt)

w
Gt =
at
= 262349,5922 lb/hr.ft2
c. Bilangan Reynold (Nre)
¿
Ret = D x> µ ¿
LC-
1000
Pada tc = 144,5 oF
µ = 1,4 cp
=3,3867 lb/ft.jam
Konduktivitas panas (k)
k = 0,094 btu/ft2.jam
kapasitas panas (c)
c = o,62 lb/lb.oF
Ret = 4002,3116
d. Koefisien perpindahan panas bagian dalam (hi)
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
Dari gambar 24 Kern, hal 834, didapat :
JH = 16
hi = 81,982048 btu/jam.ft2.oF
hio = hi x (ID/OD)
=1093,0939 btu/jam.ft2.oF
4. Sheel side (fluida panas) :
a. Luas Aliran (at)
Nt x At '
at =
1444 x n
= 0,05452 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
B =ID shell (baffle maks)
LC-
1000
B = 10 in
Jadi
as = 0,17361 ft2
b. Kecepatan massa ( Gs)

w
Gs =
at
= 6710,1016 lb/hr.ft2
c. Bilangan Reynold (Res)
¿
Res = D x> µ ¿
De = 0,73 in
=0,06083 ft
Ret = 120,5287
d. Koefisien perpindahan panas bagian luar (ho)

ho = 1500 btu/jam.ft2.oF
e. Koefisien Perpindahan panas keseluruhan (Uc)

Uc = hio.ho / hio+ho
= 632,3106
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,0247
Rd desain > Rd minuman = 0,003, maka perancangan alat heater
memenuhi syarat yang digunakan.
5. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
dari Gambar. 26. Kern, hal 836, untuk
LC-
1000
Ret = 4002,3116
Didapat faktor friksi
f = 0,00029 ft2/in2
L = 10 ft
ID = 0,01566 ft
Dari gambar. 6 Kern, hal 809,didapat :
Spesifik gravity (s) = 0,887
Jumlah passes =2
Maka :
∆ Pt = 0,19564 psi
∆ Pt hitung < ∆ Pt maksium = 10 psi (aliran cairan), maka desain
heater memenuhi syarat untuk digunakan.
b. Sheel side
F x Gs ² x L x n
∆ Ps =
5,22 x 10¹ ° x D x s
Ret = 120,5287
f = 0,004 ft2/in2
(N+1) = 12 x(L/B)
= 12 ft
Diameter dalam shell (Ds)
Ds = 0,6667 ft
Diameter eqivalen (De)
De = 0,608ft
LC-
1000

Spesifik gravity (s) =1
Maka :
∆ Ps = 0,000227 psi
∆ Ps hitung < ∆ Ps maksium = 10 psi (aliran cairan), maka desain
9. Heater Asam Asetat (He-02)

Kode : He-02
Fungsi : menaikan suhu larutan Asam asetat dari tangki ke
reaktor (R-01)
Tekanan : 1 atm
Jumlah : 1 unit
Q = 1177045,0689 kJ/jam
= 1177045,0689 kJ/jam x 0,23901
= 281325,5419 kkal/jam
= 1116384,1480 btu/jam
W = 405.6662975kg/jam
= 894.3319195 lb/jam
w = 4393.243212kg/jam
LC-
1000
= 9685.343985lb/jam
0 Beda 117 117
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 379,498 oF
T 1+T 2
Tc =
2
= 144,5 oF
2. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 73.54332281ft2
OD =3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
LC-
1000
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 10 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
= 37.46475945 buah
Nt = 40 buah
ID Shell = 10 in
= 0,833 ft
Passes (n) =2
=37 ft2
Q
UD =
= 37,4647 Btu/hr.ft2.oF
= 38 Btu/hr.ft2.oF
a. Luas Aliran (at)

LC-
1000
Nt x At '
at =
1444 x n
= 0,0209 ft2

w
Gt =
at
= 461817,764l b/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 144,5 oF
µ = 0,55 cp
=1,3304lb/ft.jam
kapasitas panas (c)
c = 0,52 lb/lb.oF
Ret = 17933.55777
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH = 16
LC-
1000
hio = hi x (ID/OD)
a. Luas Aliran (at)
Nt x At '
at =
1444 x n
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
B = 10 in
Jadi
as = 0,17361 ft2
Kecepatan massa ( Gs)

w
Gs =
at
= 5151,3518 lb/hr.ft2
b. Bilangan Reynold (Res)
¿
Res = D x> µ ¿
De = 0,73 in
=0,06083 ft
Ret = 235,5310
LC-
1000
c. Koefisien perpindahan panas bagian luar (ho)

d. Koefisien Perpindahan panas keseluruhan (Uc)

= 513,8188
e. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,0243
q. Pressure drop
5. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 17933,5577
f = 0,00028 ft2/in2
L = 10 ft
ID = 0,0156 ft
Jumlah passes =4
Maka :
∆ Pt = 0,19564 psi
LC-
1000
6. Sheel side
F x Gs ² x L x n
∆ Ps =
5,22 x 10¹ ° x D x s
Ret = 17933,5577
f = 0,0022 ft2/in2
(N+1) = 12 x(L/B)
= 12 ft
Ds = 0,6667 ft
De = 0,608ft
Maka :
∆ Ps = 0,00007 psi
10. Heater Air (He-03)

Kode : He-03
Fungsi : menaikan suhu larutan air dari tangki ke reaktor (R-01)
Tekanan : 1 atm
LC-
1000
Jumlah : 1 unit
Q = 93149,9853 kJ/jam
= 93149,9853 kJ/jam x 0,23901
= 22263,7780 kkal/jam
= 88349,3501 btu/jam
W = 32,0474 kg/jam
= 70,6517 lb/jam
w = 168,0099 kg/jam
= 410,0774 lb/jam
0 Beda 117 117
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 379,498 oF
T 1+T 2
Tc =
2
= 144,5 oF
2. UD dan A
LC-
1000
organic) didapat :
Q
A =
U D x∆t
= 38,8008 ft2
OD =3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 10 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
= 19,7661 buah
Nt = 24 buah
LC-
1000
ID Shell = 8 in
= 0,6667 ft
Passes (n) =6
=47,1120 ft2
Q
UD =
= 4,9415 Btu/hr.ft2.oF
= 6 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
1444 x n
= 0,0084 ft2

w
Gt =
at
= 48883,4093 b/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 144,5 oF
µ = 0,49 cp
LC-
1000
=1,1854 lb/ft.jam
kapasitas panas (c)
c = 1 lb/lb.oF
Ret = 2130,7080
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH = 7,55
hio = hi x (ID/OD)
a. Luas Aliran (at)
Nt x At '
at =
144 x n
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
B = 8 in
LC-
1000
Jadi
as = 0,1111 ft2

w
Gs =
at
= 635.8658859 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
=0,06083 ft
Ret = 32,6331


= 549,4127
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,1648
5. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
LC-
1000

Ret = 2130,7080
f = 0,0004 ft2/in2
L = 10 ft
ID = 0,0516 ft
Jumlah passes =6
Maka :
∆ Pt = 0,0239 psi
b. Sheel side
F x Gs ² x L x n
∆ Ps =
5,22 x 10¹ ° x D x s
Ret = 32,6331
f = 0,0022 ft2/in2
(N+1) = 12 x(L/B)
= 12 ft
Ds = 0,6667 ft

LC-
1000
De = 0,608ft
Maka :
∆ Ps = 0,000006 psi
11. Cooler 4 (Cl-04)

Kode : Cl-04
Fungsi : menurunkan suhu larutan dari Destilasi 3 (MD-03), sebelum
masuk ke dalam Reaktor (R-01)

Tekanan : 1 atm
Jumlah : 1 unit
Q = 1555639,5977 kJ/jam
= 1555639,5977 kJ/jam x 0,23901
= 371813,4203 kkal/jam
= 1475467,1956 btu/jam
W = 7424,1190 kg/jam
= 16367,2128 lb/jam
w = 346,856842 kg/jam
= 764,6805 lb/jam
LC-
1000

262,6016 suhu tinggi 122 140,6016
59,6016 Beda 36 23,6016
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 128,4395 oF
(T 1−T 2)
R =
(t 1−t 2)
= 1,6556 oF
( t 1−t 2)
S =
(T 1−t 1)
= 0,2038 oF
2. UD dan A
organic) didapat :
UD = 5 Btu/hr.ft2. oF sampai 75 Btu/hr.ft2. oF
Trial UD = 50 Btu/hr.ft2. oF
Q
A =
U D x∆t
= 229,7527ft2
OD =3/4
= 0,75 in
= 0,0624 ft
LC-
1000
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 10 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
= 117,0416 buah
Nt = 118 buah
ID Shell = 15,25 in
= 1,2708 ft
Passes (n) =6
= 231,6340 ft2
Q
UD =
= 49,5939 Btu/hr.ft2.oF
= 50 Btu/hr.ft2.oF

LC-
1000
a. Luas Aliran (at)
Nt x At '
at =
1444 x n
= 0,0412 ft2

w
Gt =
at
= 18539,7922 b/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 104 oF
µ = 0,034 cp
=0,0822 lb/ft.jam
kapasitas panas (c)
c = 1 lb/lb.oF
Ret = 11646,20669
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
LC-
1000
JH = 5,9
hio = hi x (ID/OD)
a. Luas Aliran (as)

'
ID . c . B
as =
144 x pt
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
B = 15,25 in
Jadi
as = 0,4037 ft2

w
Gs =
at
= 40537,526 lb/hr.ft2

LC-
1000
¿
Res = D x> µ ¿
De = 0,73 in
=0,06083 ft
Ret = 29982,53336


= 342,8235
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,0170
Rd desain > Rd minuman = 0,003, maka perancangan alat cooler
5. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s

Ret = 11646,2066
f = 0,0004 ft2/in2
L = 10 ft
ID = 0,0516 ft
LC-
1000

Jumlah passes =6
Maka :
∆ Pt = 0,0034 psi
b. Sheel side
F x Gs ² x Ds x (n+1)
∆ Ps =
5,22 x 10¹ ° x De x s
Res = 29982,5336
f = 0,01 ft2/in2
(N+1) = 12 x(L/B)
= 7,8688 ft
Ds = 0,6667 ft
De = 0,608ft
Maka :
∆ Ps = 0,0135 psi
cooler memenuhi syarat untuk digunakan.
LC-
1000
12. Pompa (P-05)
Kode : P-05
Fungs : untuk memompa larutan yang terbentuk pada reaktor (R-01)
menuju MD-01
Jumlah : 2 buah
KondisiBM.Xi pl (386 K) pl.xi
Operasi : T = 95 miu miu.xi
kg/m3 kg/m3 cp cp
P = 1 atm
8.9247 1027.0000 508.7868 0.2650 0.1313
5.7660 1043.0000 100.1468 0.5000 0.0480
36.0142 812.0000 331.7599 0.4000 0.1634
0.0000 872.0000 0.0000 0.5500 0.0000
massa BM Mol fraksi
Komponen
50.7048 3754.0000 940.6935 1.7150 0.3427
H2O 1585.9565 18.0147 88.0369 0.4954
CH3COOH 1024.6380 60.0508 17.0629 0.0960
C5H11OH 6399.8909 88.1466 72.6051 0.4086
CH3COOC5H1
1 0.0000 130.1827 0.0000 0.0000
Total 9010.4853 177.7049 1.0000
LC-
1000
m = 18492,232 kg/jam
= 18492,232kg/jam x 2,0246 x 1/3600
= 10,3998 lb/s
= 58,7249 lb/ft3
= 0.0138 lb/ft.s

Q = m/p
4,1752llb/ s
=
857.0631lb /ft 3. s
= 0,1770 ft3/s

optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 2,0762 in
Shedule = 40
LC-
1000

V = Q/A
= 3,4554 ft/s

ρ .V . D
Nre =
μ
Nre = 3754,6095
direncanakan :

21Dipilih
gate,
elbowopen
90 Le/D
(Le/D)
Le/D
(tabel.1Peters
Peters%%Timmehaus,
Timmehaus,hal
hal484)
484)
Lε = 5m
Le
Le = =8,1813
3,5793
ft ft
= 16.40419948 ft
= 0,00015 ft
Tinggi pompa (H)
=
H = 5m
= 16.40419948 ft
ε /D
0,00015 ft / 0,08741 ft
= 0,0000587
f = 0.0107

2. f .V . Ltot
gc . D
LC-
1000

= 281646 ft
F = 0,8741 ft

Dimana :
k = 0,5
F = (k.V2) / (gc.2)
= 0,0927 ft
p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
a=1
jadi :
W = 0 + (16,4042 ft) +(0) + 0,9691 ft
ρ .Q . W
P =
550
LC-
1000
= 0,3285 hp
Jika :
Q = 0,1770 ft3/s
= 79,4852 gal/ mnt
µ = 0,3427cp
= 0,0342 gr/cm.s
µ / ρ = 0,5836 cs
maka :
= 0,6 hp
Untuk BHP = 0,6 hp
ɳ = 0,8
= 0,75 hp
13. Heater 4 (He-04)

Kode : He-04
Fungsi : menaikan suhu larutan dari reaktor (R-01) ke menara
destilasi (MD-01)
Tekanan : 1 atm
Jumlah : 1 unit
LC-
1000

Q = 4752956,1354 kJ/jam
= 4752956,1354 /jam x 0,23901
= 1136004.0459 kkal/jam
= 4508004,8555btu/jam
W = 685, 5999 kg/jam
= 1511,4736 lb/jam
w = 18492,2319 kg/jam
= 40767,9745 lb/jam

527 suhu tinggi 248,50472 278,49528
0 Beda 45,5072 45,5072
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 300,6739 oF
T 1+T 2
Tc =
2
= 225,7523 oF
2. UD dan A
organic) didapat :
LC-
1000
Q
A =
U D x∆t
= 24,1857 ft2
OD =3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 10 ft
3. Jumlah tube (Nt)

A
Nt =
a0 x L
= 109,1114 buah
Nt = 110 buah
ID Shell = 15,25 in
= 1,2708 ft
Passes (n) =8
LC-
1000

=215,93 ft2
Q
UD =
= 69,4345 Btu/hr.ft2.oF
= 70 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
1444 x n
= 0,0288 ft2

w
Gt =
at
= 1413747,943 lb/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 225,7526 oF
µ = 0,0385 cp
=0,09313lb/ft.jam
kapasitas panas (c)
c = 2,98 lb/lb.oF
LC-
1000
Ret = 784277,586
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH = 140
hio = hi x (ID/OD)
= 4069,2855 btu/jam.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
144 x n
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
B = 15,25
Jadi
as = 0,4037 ft2

LC-
1000
w
Gs =
at
= 3743,5476 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
=0,06083 ft
Res = 2445,1885


= 1095,9991
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.U d
= 0,0133
6. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret =784277,586
f = 0,000095 ft2/in2
LC-
1000
L = 10 ft
ID = 0,0156 ft
Jumlah passes =8
Maka :
∆ Pt = 5,6321 psi
b. Sheel side
F x Gs ² x L x n
∆ Ps =
5,22 x 10¹ ° x D x s
Res = 2445,1885
f = 0,001 ft2/in2
(N+1) = 12 x(L/B)
= 7,8688 ft
Ds = 0,6667 ft
De = 0,608ft
Maka :
LC-
1000
∆ Ps = 0,000116 psi
14. Pompa 6 (P-06)
Kode : P-06
Fungs : untuk memompa larutan yang terbentuk pada destilat destilasi
(MD-01) menuju CL-01
Jumlah : 2 buah
Kondisi Operasi : T = 100,04 (373,04 K)
P = 1 atm
massa BM Mol fraksi

Komponen
H2O 1570.0969 18.0147 87.1565 0.9970
CH3COOH 15.8596 60.0508 0.2641 0.0030
C5H11OH 0.0000 88.1466 0.0000 0.0000
CH3COOC5H1
1 0.0000 130.1827 0.0000 0.0000
total 1585.9565 87.4206 1.0000
BM.Xi Pl pl.xi Miu miu.xi

kg/m3 kg/m3 Cp cp
17.9603 1027.0000 1023.8974 0.2950 0.2941
0.1814 1043.0000 3.1510 0.3950 0.0012
0.0000 812.0000 0.0000 0.0000 0.0000
0.0000 872.0000 0.0000 0.0000 0.0000
18.1417 3754.0000 1027.0483 0.6900 0.2953
LC-
1000
m = 1585,9565 kg/jam
= 1585,9565 kg/jam x 2,0246 x 1/3600
= 0,8919 lb/s
= 64,11581 lb/ft3
= 0,0119 lb/ft.s

Q = m/p
0,8919lb /s
=
64,11581lb /ft 3. s
= 0,0139 ft3/s

optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 0,9783 in
Shedule = 80
outside diameter = 0,2917ft
V = Q/A
LC-
1000
= 0,8417 ft/s

ρ .V . D
Nre =
μ
Nre = 732,3913
Karena Nre < 2.100 maka asumsi benar
direncanakan :

21Dipilih
gate,
elbowopen
90 Le/D
(Le/D)
Le/D
(tabel.1Peters
Peters&&Timmehaus,
Timmehaus,hal
hal484)
484)
Lε = 5m
Le
Le = =5,1706
2,2621
ft ft
= 16,4041 ft
= 0,00015 ft
Tinggi pompa (H)
=
H = 5m
= 16.40419948 ft
ε /D
0,00015 ft / 0,08741 ft
= 0,0000587
f = 0,0139

2. f .V . Ltot
gc . D
= 23,8370 ft
F = 0,0904 ft
LC-
1000

Dimana :
k = 0,5
F = (k.V2) / (gc.2)
= 0,0055 ft
2. Penentuan kerja pompa (W)

p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
a=1
jadi :
W = 0 + (16,4042 ft) +(0) + 0,0959 ft
ρ .Q . W
P =
550
= 0,0267 hp
Jika :
Q = 0,0139 ft3/s
LC-
1000
= 6,2437 gal/ mnt

µ = 0,2953 cp
= 0,02953 gr/cm.s
µ / ρ = 0,4605 cs
maka :
= 0,05 hp
Untuk BHP = 0,05 hp
ɳ = 0,8
= 0,25 hp
15. Pompa 7 (P-07)
Kode : P-07
Fungs : untuk memompa larutan yang terbentuk pada bottom destilasi
(MD-01) menuju (MD-02)
Jumlah : 2 buah
Kondisi Operasi : T = 143,419 (416,419 K)
P = 1 atm
massa BM Mol fraksi

Komponen
H2O 15.8596 18.0147 0.8804 0.0054
CH3COOH 1008.7785 60.0508 16.7988 0.1030
LC-
1000
C5H11OH 6411.9310 88.1466 72.7417 0.4458

CH3COOC5H1
1 9469.7064 130.1827 72.7417 0.4458
total 16906.2755 163.1625 1.0000
BM.Xi Pl pl.xi miu miu.xi

kg/m3 kg/m3 cp cp
0.0972 1027.0000 5.5413 0.1300 0.0007
6.1827 1043.0000 107.3844 0.2950 0.0304
39.2978 812.0000 362.0087 0.2300 0.1025
58.0385 872.0000 388.7581 0.1800 0.0802
103.6162 3754.0000 863.6926 0.8350 0.2139

m = 16906,28kg/jam
= 16906,28 kg/jam x 2,0246 x 1/3600
= 9,5079 lb/s
= 53,9179 lb/ft3
= 0,00862 lb/ft.s

Q = m/p
9,5079lb/ s
=
53,9179lb/ft 3. s
= 0,1763 ft3/s

LC-
1000
optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 2,9995 in
Shedule = 40
V = Q/A
= 3,4407 ft/s

ρ .V . D
Nre =
μ
Nre = 5500,878
L = 5m
= 16,4041 ft
Tinggi pompa (H)

H = 5m
= 16.40419948 ft
1 elbow 90 (Le/D)
Le/D = 32 (tabel.1 Peters & Timmehaus, hal 484)
LC-
1000
Le = 5,1706 ft
2 gate, open Le/D

Le = 2,2621 ft
Dipilih material pipa besi baja :

ε = 0,00015 ft
ε /D = 0,00015 ft / 0,08741 ft
= 0,0000587
f = 0,0139

2. f .V . Ltot
gc . D
= 23,8370 ft
F = 0,0904 ft

Dimana :
k = 0,5
F = (k.V2) / (gc.2)
= 0,0055 ft

p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
LC-
1000
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
a=1
jadi :
W = 0 + (16,4042 ft) +(0) + 0,0959 ft
ρ .Q . W
P =
550
= 0,0267 hp
Jika :
Q = 0,0139 ft3/s
= 6,2437 gal/ mnt
µ = 0,2953 cp
= 0,02953 gr/cm.s
µ / ρ = 0,4605 cs
maka :
= 0,54 hp
LC-
1000
Untuk BHP = 0,54 hp

ɳ = 0,8
= 0,75 hp
16. Menara Destilasi (MD-01)
Kode : MD-01
Fungsi : Memisahkan produk isoamyl acetat dari campurannya ke dalam hasil
bawah menara
Tipe : Sieve Tray
Data-data yang diketahui dari perhitungan neraca massa

Suhu umpan masuk : 143,42 oC = 416,42 K
Suhu puncak menara : 128,135 oC = 401,14 K
Suhu dasar menara : 201,151 oC = 474,15 K
Tekanan puncak menara : 1 atm = 760 mmHg
Tekanan dasar menara : 1 atm = 760 mmHg
a. Aliran umpan
P = 760 mmHg
T = 416,42 K
FRAKSI
KOMPONEN MASSA BM MOL MOL
kg/jam kg/kgmol kmol/jam xi
H2O 15.8596 18.0147 0.8804 0.0054
CH3COOH 1,008.7785 60.0508 16.7988 0.1030
C5H11OH 6,411.9310 88.1466 72.7417 0.4458
CH3COOC5H11 9,469.7064 130.1827 72.7417 0.4458
TOTAL 16,906.2755 163.1625 1.0000
b. Aliran destilat
LC-
1000
P = 401,14 K
T = 760 mmHg
FRAKSI
KOMPONEN
MASSA BM MOL MOL
H2O 15.8596 18.0147 0.8804 0.0097
CH3COOH 1,008.7785 60.0508 16.7988 0.1859
C5H11OH 6,402.4613 88.1466 72.6343 0.8036
CH3COOC5H11 9.4697 130.1827 0.0727 0.0008
TOTAL 7,436.5690 90.3861 1.0000
c. Aliran Bottom (produk bawah)
P = 474,15 K
T = 760 mmHg
FRAKSI
KOMPONEN
MASSA BM MOL MOL
H2O - 18.0147 - -
CH3COOH - 60.0508 - -
C5H11OH 9.4697 88.1466 0.1074 0.0015
CH3COOC5H11 9,460.2367 130.1827 72.6689 0.9985
TOTAL 9,469.7064 72.7764 1.0000
1. Menentukan Jumlah plate minmum
Digunakan persamaaan Frensk (Van Winkle pers 4. 118 hal 236)
Xlk XHk
log .
Nm= Xhk XLk
log a
Dimana :
Nmin = jumlah plate minimum

LC-
1000
aav = Volatilitas relatif rata-rata
= ( α D +α B )
2
sehingga:
Nmin = 5,9239 = 6 plate
2. Menentukan jumlah plate teoritis
Digunakan metode gililand (pers. Hal 242 Van Winkle)
L
−
D D
L
( )
min
dan
N −Nmin
L N +1
+1
D
Dimana :
L/D = refluks operasi
(L/D)min = reflus minimum
N = jumlah plate teoritis
Nm = jumlah plate min
Dari perhitungan neraca massa MD-01 diketahui:
Rmin =(L/D)min = 0,4182
Roperasi = (L/D)0 = 0,5854
Maka :
L
−
D D
L
( )
min
= 0,1055
L
+1
D
Dengan mnggunakan metode grafik kondisi giiland fig 13-14 Perry’s

7th 1999 page 12-37 diperoleh harga :
LC-
1000
N −Nmin
=0,5399
N +1
N-M = 0,44 (N+1)

N-50N = 0.44 +NM
N = 14,21
= 15 plate
3. Menentukan jumlah plate aktual:
KOMPONEN A B C D
CH3COOH -3.8937 7.85E+02 6.67E-03 -7.56E-06
C5H11OH -7.9943 1.77E+03 1.15E-02 -8.93E-06
H2O -10.2158 1.79E+03 1.77E-02 -1.26E-05
CH3COOC5H11 -4.6434 8.29E+02 8.66E-03 -9.04E-06
Viskositas rata-rata umpan masuk kolom pada suhu 416,42 K

KOMPONEN XF miu (Cp) Xf.miu
CH3COOH 0.005 0.29 1.54E-03
C5H11OH 0.103 0.30 3.14E-02
H2O 0.446 1.91E-01 8.53E-02
CH3COOC5H11 0.446 2.45E-01 1.09E-01
total 0.2273
αAV-µAV = 1,45
maka dapat dihitung dan didapatkan efisiensi
Eo = 0,4575
Nteoritis+ 1
Naktual =
Eo
= 33,78 = 34 plate
LC-
1000
jadi, jumlah plate aktual sebanyak 34 plate
4. Menentukan plate umpan
Digunakan metode kik bride (Van Winkle hal311
[( ) ( )]
2
log = 0,206
X HK B ( X LK )B
× ×
X LK F D ( X HK ) D
Log Nr/Ns = 0,1301

Nr/Ns = 1,3494
Nr+Ns = 34 plate
Ns =14,47 = 15 plate
5. Menentukan diameter menara

a. Puncak menara
Dari perhitungan neraca massa dan neraca panas dapat diketahui komposisi uap
keluar puncak kolom (dapat dilihat perhitungan neraca panas) :
KOMPONEN MASSA BM MOL FRAKSI MOL xi.Bmi
kg/jam kg/kgmol kmol/jam xi kg/kgmol
H2O 25.1453 18.0147 1.3958 0.0097 0.1755
CH3COOH 1,599.4166 60.0508 26.6344 0.1859 11.1608
C5H11OH 10,151.0923 88.1466 115.1615 0.8036 70.8346
CH3COOC5H11 15.0142 130.1827 0.1153 0.0008 0.1048
TOTAL 11,790.6685 143.3071 1.0000 82.2756
BM rata-rata uap : zxi.Bmi = 82,2756 kg/kgmol
pv = (P. Bmi)/RT
Dimana
P= tekanan operasi uap keluar = 1 atm
LC-
1000
Bmi = Berat molekul rata-rata =

R = konstanta gas = 0.082 atm m3/kgmol.k
T = temperature = 401.14 k
Maka
Pv = 2.5013 kg/m3
= 0.15615 lb/ft3
Laju alir massa uap (m) = 7.2158 lb/detik
MASSA fraksi berat pi pi.xi

KOMPONEN
kg/jam kmol/jam (kg/m3)
H2O 15.8596 0.0021 1,027.0000 2.1902
CH3COOH 1,008.7785 0.1357 1,043.0000 141.4841
C5H11OH 6,402.4613 0.8609 812.0000 699.0856
CH3COOC5H11 9.4697 0.0013 872.0000 1.1104
TOTAL 7,436.5690 1.0000 3,754.0000 843.8703
dengan menggunakan pers (1) hal. 656 petersadisi 4 didapatkan kecepatan superfisial
uap keluar puncak kolom
( )
0,5
ρL −ρ V
Vm = Kv
ρV
LC-
1000
dimana :
vm = kecepatan supervisial uap : ft/detik
Kv = konstanta empiris
pv = densitas uap : lb/ft3
Pl = densitas liquid :ib/ft3
Maka :
Vm = 9,9850 ft/detik
Mnurut peters edisi 4 hal 658, kecepatan uap meninggalkan puncak kolom berkisar
65-80%kecepatan supervisial
Diambil :
V = 0,65 x Vm
= 6,4902 ft/detik
luas aliran uap keluar (A) :
A = m/pv V
= 13,8120 ft2
Diameter puncak kolom (D)
D = (4A/π)^1/2
= 4,1946 ft2
=1,2785 m
b. Bagian bawah menara

Neraca massa sekitar menara dasar (bottom)
L=V+B > (V=L-B)
dimana:
L = total cairan keluar dasar kolom
V = uap yang dibangkitkan reboiler
B = total produk bottom
LC-
1000
dari persamaan 5.31 van winkle hal 221

L/V =Klk
L = v.Klk = (L-B)Klk
dimana:
Klk = 3,9267
L = 163,1625 kgmol
Komponen liran cairan keluar dasar kolom (L) :

MOL BM MASSA pi pi.xi
fraksi
KOMPONEN (Kg/ berat
Kgmol kgmol) kg (kg/m3) (kg/m3)
1,027.000
H2O 0.8804 18.0147 15.8596 0.0009 0 0.9634
1,043.000
CH3COOH 16.7988 60.0508 1,008.7785 0.0597 0 62.2346
307.961
C5H11OH 72.7417 88.1466 6,411.9310 0.3793 812.0000 9
CH3COOC5H1 488.433
1 72.7417 130.1827 9,469.7064 0.5601 872.0000 1
16,906.275 3,754.000 859.593
TOTAL 163.1625 5 1.0000 0 0
Komposisi aliran uap yang dibangkitkan boiler (V)

V=L–B
massa BM mol BM rata-rata
fraksi berat
KOMPONEN (Kg/ mol
kg kgmol) kgmol kg/kgmol
H2O 15.8596 18.0147 0.8804 0.0054 0.0972
CH3COOH 1,008.7785 60.0508 16.7988 0.1030 6.1827
C5H11OH 6,411.9310 88.1466 72.7417 0.4458 39.2978
CH3COOC5H1
1 9,469.7064 130.1827 72.7417 0.4458 58.0385
16,906.275 163.162
TOTAL 5 5 1.0000 103.6162
LC-
1000
Densitas uap:
PV = P x Bm rata-rata / RT
Dimana :
P = 1 atm
Bmi
R = 0.082 atm m3/kgmol.k
T = 416.42 K
Pv = 3.03 kg/m3
= 0.19 lb/ft3
Laju massa uap :

m = 10,35 lb/detik
Maka kecepatan supervisial uap masuk pada dasar kolom :
Vm = Kv
Dimana
Di rencanakan menggunakan tray spacing (ts) = 18 in
kv = Dari fig. 16-6, hal. 657, Peters untuk ts = 24 in didapat Kv = 0,24 ft/s.
Vm = 4,0322 ft/s
luas aliran uap keluar (A)
A = m / (pv xV)
= 16,9316 ft2
Diameter dasar kolom (D) :
D =
= 4,6443 ft
= 1,4156 m
Digunakan kolom dengan diameter rata-rata : 1,3471 m
6. Menentukan tinggi kolom

Tinggi plate =(Naktual - 1)x ts
Dimana:
LC-
1000
ts = jarak plate = 18 in (0,4572cm)
Tinggi plate = 7,7531 m

Diambil ruang kosong diatas kolom masing-masing =
Jadi, tinggi menara = tinggi plate + (2x tinggi ruang kosong)
= 9,7532 m
7. Menentukan Tebal shell
Untuk internal pressure, tebal dinding (shell) dihitung dengan persamaan 13-1
brownell & young hal 254 :
ts = +C
Dimana :
P = tekanan desain, atm
R = jari jari , cm = 1/2 D
= 0.673522 m
f = tegangan yang diijinkan bahan konstruksi, atm
= 1190.5 atm
E = efisiensi pengelolaan
= 0.8
C = faktor korosi diambil 1/8 in
= 0.003175 m
diambil faktor keamanan desain 20%
Pdesain = 1.20 x Poperai
Maka
ts = 0,0041 m
= 0,0001 in
Digunakan tebal plate standar = 1/4 in = 0,0064
8. Menentukan tebal tutup
th = +C
dimana :
P = tekanan desain; atm
rc =crown radius; cm
LC-
1000
F = tegangan yang diijinkan bahan konstruks; atm

E = efisiensi pengelasan
C = factor korosi= 1/8 in (0,00318 m)
rc = OD SHELL = ID SHELL + 2. Ts
= 1,3598 m
= 135,98 cm
Bahan konstruksi tutup sama dengan shell, maka :
th = 0,0047 m
Digunakan tebal plate standar = 1/4 in = 0,0064 m
9. Condensor (CD-01)
1. Menentukan spesifikasi kondensor

panjang tube = 16 ft = 4.8768 m
OD = 3/4 in = 0.01905 m 0.0625 ft

BWG = 16
ID = 0.62 in = 0.05167 ft
outside surface = 0.1963 ft2
a't = 0.302 in2
pitch =1 in triangular
a) menghitung koefisien perpindahan panas dan faktor kekotoran
b) Menghitung ∆ T LMTD
dari perhitungan spesifikasi menara distilasi diperoleh data :
Q = 1555639,5977 kJ/jam
= 1555639,5977 kJ/jam x 0,23901
= 371813,4203 kkal/jam
= 1475467,1956 btu/jam
W = 7424,1190 kg/jam
= 16367,2128 lb/jam
LC-
1000

w = 346,856842 kg/jam
= 764,6805 lb/jam
212,07 suhu tinggi 122 90,072
212,07 suhu rendah 86 126,072
0 Beda 36 36
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 107,0652 oF
(T 1−T 2)
tc =
(t 1−t 2)
= 104 oF
( t 1−t 2)
Tc =
(T 1−t 1)
= 212,072 oF
3. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 49,6537 ft2
Jumlah tube (Nt)
LC-
1000
A
Nt =
a0 x L
= 15,8092 buah
Nt = 24 buah
ID Shell = 8 in
= 0,6666 ft
Passes (n) =4
A terkoreksi = 24 x 0,666 ft x 0,1963 ft2/ft
= 75,3792 ft2
Q
UD =
= 5 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
1444 x n
= 0,0126 ft2

w
Gt =
at
= 3261,3 lb/hr.ft2

LC-
1000
¿
Ret = D x> µ ¿
Pada tc = 104 oF
µ = 0,0075 cp
=0,0182 lb/ft.jam
kapasitas panas (c)
c = 1 btu/lb.oF
Ret = 0,0517
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH =5
hio = hi x (ID/OD)
= 10,0722 btu/jam.ft2.oF
a. Luas Aliran (as)

'
ID . c . B
as =
144 x pt
= 0,25 ft2
Dimana :
LC-
1000
C’ = Pt - OD
C’ = 0,25 in
B = 15,25 in
Jadi
as = 0,4037 ft2

w
Gs =
at
= 31467,9250 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Ret = 33660,9460
Koefisien perpindahan panas bagian luar (ho)

Koefisien Perpindahan panas keseluruhan (Uc)

= 9,7225
Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,06381
LC-
1000
6. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s

Ret = 9283,6423
f = 0,000135 ft2/in2
L = 16 ft
ID = 0,05167 ft
Jumlah passes =4
Maka :
∆ Pt = 0,20 psi
c. Sheel side
∆ Ps =
5,22 x 10¹ ° x De x s
Res = 33600,95
f = 0,000185 ft2/in2
LC-
1000
(N+1) = 12 x(L/B)
= 24 ft
Ds = 0,6667 ft
De = 0,608ft
Maka :
∆ Ps = 0,000462 psi
condensor memenuhi syarat untuk digunakan.
10. Akumulator (AC-01)

Kode : AC-01
Fungsi : menampung sementarakondensat yang keluar dari kondensor
distilat.
Tipe : silinder horizontal dengan tutup ellipsoidal
Laju alir massa (m) = 1585,9565 kg/jam
Densitas campuran ρ = 2070 kg/m3
Waktu tingal (t) = ½ jam
- Menghitung volume tangti (Vt)
Vt =mxt/ρ
= 0,38 m3
Tangki dirancang dengan kodisi
a. 90% air volume tangki terisi larutan
b. dipilih perbandingan panjang (L) : 3 Diameter (3D)
LC-
1000
maka
Vt = 0,43 m3
Diameter tangki (D)
D = (12x Vt / 10 π)^1/3
= 0,55 m
Panjang silinder (Hs)
Hs = 3D
= 3 x 0,55 m
= 1,64 m
Tinngi larutan dalam silinder (Hl)

Hl = 90/100 x (Hs)
= 1,47 m
- Tebal dinding tangki (ts)
ts = +C
Dimana :
p : tekanan disain
r : jari-jari tegak = 1/2 D 100 (0,27 m)
f : tegangan yang diizinkan bahan kosntruksi, atm
C : faktor korosi (0,0037 )
diambil factor keamanan desain 20%
Pdesain = 1.20 x Poperasi
Maka :
ts = 0,0035 m
= 0,1386 in
Digunakan tebal plat standar = 3/16 in = 0,1875
LC-
1000
- Tebal head (Tutup)

Dirancang tutup akumulator tipe ellipsoidal
PxDV
th = +C
2 x f x E−0,2 x Pt
dimana :
Kondisi tangki
D: diameter bahan konstruksi dan tekanan desain tutup atas sama dengan shell (dinding)
f : tegangan
th yang diizinkan bahan kosntruksi
E : efisiensi
= 0,00352 pengelasan
m
C : faktor korosi
V : faktor intensifikasi tegangan =
= ,1386 in
K : a/b untuk type ellipsoidaal, rasio tinggi tutup (a) dengan jari jari tangki
(b) = (2:1), maka K = 2
V : 1/6 (2+2) = 1
11. Reboiler (RB-01)

Kode : RB-01
Fungsi : menguapkan sebagian hasil bawah kolom distilasi.
Tipe : ketel
Q = 758381,76 kJ/jam
= 719297,33 lb/jam
W = 481,5336 kg/jam
= 1061,6001 lb/jam
w = 16906,2755 kg/jam
= 37271,9637 lb/jam
LC-
1000

527 suhu tinggi 290,1542 236,8458
527 suhu rendah 290,1542 236,8458
0 Beda 0 0
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 398,87 oF
menghitung Tc dan tc
T 1+T 2
Tc =
2
= 527 oF
tc = 290,1542 oF
2. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 90,6218 ft2
OD =3/4
= 0,75 in
= 0,0624 ft
BWG = 16
LC-
1000
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 16 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
= 28,8553 buah
Nt = 30 buah
ID Shell = 8 in
= 0,6667 ft
Passes (n) =2
= 94,224 ft2
Q
UD =
= 19,2354 Btu/hr.ft2.oF
= 20 Btu/hr.ft2.oF
a. Luas Aliran (at)

LC-
1000
Nt x At '
at =
1444 x n
= 0,0315 ft2

w
Gt =
at
= 1184804,146 lb/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 290,1542 oF
µ = 0,865 cp
= 2,0925 lb/ft.jam
k = 0,381btu/ft2.jam
kapasitas panas (c)
c = 3,07 lb/lb.oF
Ret = 111147,33
hi = hio
= 1500 btu/jam.ft2.oF
a. Luas Aliran (at)
IDxC ' xB
as =
144 x Pt
LC-
1000
Dimana :
C’ = Pt - OD
C’ = 0,94 in
B = 10 in
Jadi
as = 0,00289 ft2

w
Gs =
at
= 366888,3164 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Res = 10666,1452

∆ tw = 145,0076

= 581,6326
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
LC-
1000
= 0,0502 jam.ft2/btu
5. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 111147,33
f = 0,000085 ft2/in2
L = 16 ft
ID = 0,6667 ft
Jumlah passes =w
Maka :
∆ Pt = 0,1097 psi
c. Sheel side
F x Gs ² x L x n
∆ Ps =
5,22 x 10¹ ° x D x s
Ret = 10666,1452
f = 0,00035 ft2/in2
LC-
1000
(N+1) = 12 x(L/B)
= 18,0001 ft
Ds = 0,0516 ft
De = 0,73ft
Maka :
∆ Ps = 0,000575 psi
reboiler memenuhi syarat untuk digunakan.
17. Menara Destila 2 (MD-02)
Kode : MD-02
bawah menara
Tipe : Sieve Tray

a. Aliran umpan
P = 760 mmHg
LC-
1000
T = 416,42 K
FRAKSI
H2O 15.8596 18.0147 0.8804 0.0054
CH3COOH 1,008.7785 60.0508 16.7988 0.1030
C5H11OH 6,411.9310 88.1466 72.7417 0.4458
CH3COOC5H11 9,469.7064 130.1827 72.7417 0.4458
TOTAL 16,906.2755 163.1625 1.0000
b. Aliran destilat
P = 401,14 K
T = 760 mmHg
FRAKSI
KOMPONEN
MASSA BM MOL MOL
H2O 15.8596 18.0147 0.8804 0.0097
CH3COOH 1,008.7785 60.0508 16.7988 0.1859
C5H11OH 6,402.4613 88.1466 72.6343 0.8036
CH3COOC5H11 9.4697 130.1827 0.0727 0.0008
TOTAL 7,436.5690 90.3861 1.0000
P = 474,15 K
T = 760 mmHg
FRAKSI
KOMPONEN
MASSA BM MOL MOL
H2O - 18.0147 - -
CH3COOH - 60.0508 - -
C5H11OH 9.4697 88.1466 0.1074 0.0015
CH3COOC5H11 9,460.2367 130.1827 72.6689 0.9985
LC-
1000
TOTAL 9,469.7064 72.7764 1.0000
Xlk XHk
log .
Nm= Xhk XLk
log a
Dimana :
= ( α D +α B )
2
sehingga:
Nmin = 5,9239 = 6 plate
L
−
D D
L
( )
min
dan
N −Nmin
L N +1
+1
D
Dimana :

LC-
1000
Rmin =(L/D)min = 0,4182
Roperasi = (L/D)0 = 0,5854
Maka :
L
−
D D ( )
L
min
= 0,1055
L
+1
D

N −Nmin
=0,5399
N +1
N-M = 0,44 (N+1)

N-50N = 0.44 +NM
N = 14,21
= 15 plate
KOMPONEN A B C D
CH3COOH -3.8937 7.85E+02 6.67E-03 -7.56E-06
C5H11OH -7.9943 1.77E+03 1.15E-02 -8.93E-06
H2O -10.2158 1.79E+03 1.77E-02 -1.26E-05
CH3COOC5H11 -4.6434 8.29E+02 8.66E-03 -9.04E-06

CH3COOH 0.005 0.29 1.54E-03
C5H11OH 0.103 0.30 3.14E-02
H2O 0.446 1.91E-01 8.53E-02
LC-
1000
CH3COOC5H11 0.446 2.45E-01 1.09E-01

total 0.2273
αAV-µAV = 1,45
Eo = 0,4575
Nteoritis+ 1
Naktual =
Eo
= 33,78 = 34 plate
[( ) ( )]
2
log = 0,206
X HK B ( X LK )B
× ×
X LK F D ( X HK ) D
Log Nr/Ns = 0,1301

Nr/Ns = 1,3494
Nr+Ns = 34 plate
Ns =14,47 = 15 plate

a. Puncak menara
LC-
1000

H2O 25.1453 18.0147 1.3958 0.0097 0.1755
CH3COOH 1,599.4166 60.0508 26.6344 0.1859 11.1608
C5H11OH 10,151.0923 88.1466 115.1615 0.8036 70.8346
CH3COOC5H11 15.0142 130.1827 0.1153 0.0008 0.1048
TOTAL 11,790.6685 143.3071 1.0000 82.2756
pv = (P. Bmi)/RT
Dimana
Maka
Pv = 2.5013 kg/m3
= 0.15615 lb/ft3

KOMPONEN
H2O 15.8596 0.0021 1,027.0000 2.1902
CH3COOH 1,008.7785 0.1357 1,043.0000 141.4841
C5H11OH 6,402.4613 0.8609 812.0000 699.0856
CH3COOC5H11 9.4697 0.0013 872.0000 1.1104
TOTAL 7,436.5690 1.0000 3,754.0000 843.8703
LC-
1000
( )
0,5
ρL −ρ V
Vm = Kv
ρV
dimana :
Maka :
Diambil :
V = 0,65 x Vm
= 2,8611 ft/detik
A = m/pv V
= 16,1513 ft2
D = (4A/π)^1/2
= 4,5359 ft2
=1,3826 m
b. Bagian bawah menara

L=V+B > (V=L-B)
dimana:
LC-
1000
V = uap yang dibangkitkan reboiler

L/V =Klk
dimana:
Klk = 8,7146
L = 72,7764 kgmol

MOL BM MASSA fraksi pi pi.xi
KOMPONEN
Kgmol (Kg/kgmol) kg berat (kg/m3) (kg/m3)
H2O - 18.0147 - - 1,027.0000 -
CH3COOH - 60.0508 - - 1,043.0000 -
C5H11OH 0.1074 88.1466 9.4697 0.0010 812.0000 0.8120
CH3COOC5H11 72.6689 130.1827 9,460.2367 0.9990 872.0000 871.1280
TOTAL 72.7764 9,469.7064 1.0000 3,754.0000 871.9400

V=L–B
Massa BM mol BM rata-rata
fraksi berat
KOMPONEN (Kg/ mol
Kg kgmol) kgmol kg/kgmol
H2O - 18.0147 - - -
CH3COOH - 60.0508 - - -
C5H11OH 9.4697 88.1466 0.1074 0.0015 0.1301
CH3COOC5H11 9,460.2367 130.1827 72.6689 0.9985 129.9905
TOTAL 9,469.7064 72.7764 1.0000 130.1206
Densitas uap:
Dimana :
LC-
1000
P = 1 atm
Bmi
T = 474,15 K
Pv = 3.35 kg/m3
= 0.21 lb/ft3
Laju massa uap :

m = 5.80 lb/detik
Vm = Kv
Dimana
Vm = 3,0932 ft/s
A = m / (pv xV)
= 8,9879 ft2
D =
= 3,3799 ft
= 1,2063 m
Digunakan kolom dengan diameter rata-rata : 1,3471 m

Dimana:

LC-
1000

Diambil ruang kosong diatas kolom masing-masing = 1 m
= 16,9879 m
ts = +C
Dimana :
= 0.603193 m
= 1190.5 atm
= 0.8
= 0.003175 m
Maka
ts = 0,0040 m
= 0,0001 in
th = +C
dimana :
LC-
1000

= 1,2190 m
= 121,9 cm
th = 0,0046 m

OD =¾ in = 0.01905 m 0.0625 ft
BWG = 16
ID = 0.62 in = 0.05167 ft
a't = 0.302 in2
Pitch =1 in triangular
Q = 7436,5690 kJ/jam
= 16394,83 lb/jam
W = 2787,1238 kg/jam
= 6144,5573 lb/jam
w = 4196232,76 kJ/jam
LC-
1000
= 3979973,1206 lb/jam

262,64 suhu tinggi 122 140,643
262,64 suhu rendah 86 176,643
0 Beda 36 36
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 157,9598 oF
(t 1−t 2)
tc =
2
= 104 oF
T 1+T 2
Tc =
2
= 262,64 oF
3. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 335,4980 ft2
Jumlah tube (Nt)
A
Nt =
a0 x L
LC-
1000
= 106,9625 buah
Nt = 106 buah
ID Shell = 13,25 in
= 1,104 ft
Passes (n) =1
= 342,3472 ft2
Q
UD =
= 75 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
144 x n
= 0,2285 ft2

w
Gt =
at
= 26879,4052 lb/hr.ft2
¿
Ret = D x> µ ¿
LC-
1000
Pada tc = 104 oF
µ = 0,0075 cp
=0,0182 lb/ft.jam
kapasitas panas (c)
c = 1 btu/lb.oF
Ret = 76516,2128
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH = 175
hio = hi x (ID/OD)
a. Luas Aliran (as)

'
ID . c . B
as =
144 x pt
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
LC-
1000

B = 15,25 in
Jadi
as = 0,30ft2

w
Gs =
as
= 53789,5207 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Ret = 31083,8276

∆ Tw = 174,45 oF

= 155,6568
Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,0069
6. Pressure drop
LC-
1000
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 765116,21
f = 0,00016 ft2/in2
L = 16 ft
ID = 0,05167 ft
Jumlah passes =1
Maka :
∆ Pt = 3,47 psi
b. Sheel side
∆ Ps =
5,22 x 10¹ ° x De x s
Res = 31083,8276
f = 0,0002 ft2/in2
(N+1) = 12 x(L/B)
= 14,4905 ft

LC-
1000
Ds = 1,1041ft
De = 0,001458ft
Maka :
∆ Ps = 0,001458 psi

Kode : AC-02
Fungsi : menampung sementarakondensat yang keluar dari kondensor
distilat.
Vt =mxt/ρ
= 0,99 m3
c. 90% air volume tangki terisi larutan
d. dipilih perbandingan panjang (L) : 3 Diameter (3D)
maka
Vt = 1,1 m3
Diameter tangki (D)
LC-
1000
D = (12x Vt / 10 π)^1/3
= 0,75 m
Hs = 3D
= 3 x 0,75 m
= 2,25 m
Hl = 90/100 x (Hs)
= 2,02 m
ts = +C
Dimana :
p : tekanan disain
Maka :
ts = 0,0035 m
= 0,1436 in

PxDV
th = +C
2 x f x E−0,2 x Pt
dimana :
LC-
1000
Kondisi tangki
f : tegangan
E : efisiensi
m
C : faktor korosi
= ,1386 in
(b) = (2:1), maka K = 2
V : 1/6 (2+2) = 1
11. Reboiler (RB-02)

Kode : RB-02
Tipe : ketel
Q = 5250297,81 kJ/jam
= 719297,33 lb/jam
W = 9469,7964 kg/jam
w = 3333,6705 kg/jam

527 suhu tinggi 394,0718 132,9282
527 suhu rendah 394,0718 132,9282
0 Beda 0 0
LC-
1000
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 457,32 oF
T 1+T 2
Tc =
2
= 527 oF
tc = 394,0718 oF
2. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 90,6218 ft2
OD =3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
LC-
1000
Panjang (L) = 16 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
= 77,0426 buah
Nt = 82 buah
ID Shell = 12 in
= 0.9999 ft
Passes (n) =2
= 257,5456 ft2
Q
UD =
= 42,2794 Btu/hr.ft2.oF
= 45 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
1444 x n
= 0,0859 ft2

LC-
1000
w
Gt =
at
= 242796,57 lb/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 394,0718 oF
µ = 1,365 cp
= 1,365 lb/ft.jam
kapasitas panas (c)
c = 3,14 lb/lb.oF
Ret = 14433,7263
hi = hio
a. Luas Aliran (at)
IDxC ' xB
as =
144 x Pt
Dimana :
C’ = Pt - OD
C’ = 0,94 in
LC-
1000
B = 10 in
Jadi
as = 0,00651 ft2

w
Gs =
at
= 1128879,072 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Res = 20797,18179

∆ tw = 91,4643 oF

= 467,8899
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
5. Pressure drop
a. Tube side
LC-
1000
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 14433,73
f = 0,000085 ft2/in2
L = 16 ft
ID = 0,6667 ft
Jumlah passes =2
Maka :
∆ Pt = 0,01807 psi
b. Sheel side
F x Gs ² x L x n
∆ Ps =
5,22 x 10¹ ° x D x s
Res = 20797,18197
f = 0,00035 ft2/in2
(N+1) = 12 x(L/B)
= 12,0001 ft
Ds = 0,0516 ft
LC-
1000
De = 0,73ft
Maka :
∆ Ps = 0,003629 psi
18. Pompa 8 (P-08)
Kode : P-08
(MD-02) menuju (MD-03)
Jumlah : 2 buah
Kondisi Operasi : T = 128,135 (401, 135 K)
P = 1 atm
massa BM Mol fraksi

Komponen
H2O 15.8596 18.0147 0.8804 0.0097
CH3COOH 1008.7785 60.0508 16.7988 0.1859
C5H11OH 6402.4613 88.1466 72.6343 0.8036
CH3COOC5H11 9.4697 130.1827 0.0727 0.0008
total 7436.5690 90.3861 1.0000

kg/m3 kg/m3 cp cp
0.0972 1027.0000 10.0031 1.7000 0.0166
6.1827 1043.0000 193.8473 0.3500 0.0650
LC-
1000
39.2978 812.0000 652.5229 0.2600 0.2089

58.0385 872.0000 0.7018 0.2800 0.0002
103.6162 3754.0000 857.0750 2.5900 0.2908

m = 7436,569 kg/jam
= 16906,28 kg/jam x 2,0246 x 1/3600
= 4,1822 lb/s
= 53,5048 lb/ft3
= 0,0118 lb/ft.s

Q = m/p
9,5079lb/ s
=
53,9179lb/ft 3. s
= 0,07844 ft3/s

optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 2,9995 in
Shedule = 40
LC-
1000

V = Q/A
= 3,4407 ft/s

ρ .V . D
Nre =
μ
Nre = 5500,878
L = 5m
= 16,4041 ft
Tinggi pompa (H)

H = 5m
= 16.4042 ft
1 elbow 90 (Le/D)
Le = 8,1813 ft
2 gate, open Le/D

Le = 3,5793 ft

ε = 0,00015 ft
ε /D = 0,00015 ft / 0,08741 ft
= 0,0000587
f = 0,01207

LC-
1000

2. f .V . Ltot
gc . D
= 28,16486 ft
F = 0,1924 ft

Dimana :
k = 0,5
F = (k.V2) / (gc.2)
= 0,0055 ft

p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
a=1
jadi :
W = 0 + (16,4042 ft) +(0) + 0,0959 ft
LC-
1000
ρ .Q . W
P =
550
= 0,1263 hp
Jika :
Q = 0,0139 ft3/s
= 6,2437 gal/ mnt
µ = 0,2953 cp
= 0,02953 gr/cm.s
µ / ρ = 0,5434 cs
maka :
= 0,23 hp
Untuk BHP = 0,23 hp
ɳ = 0,8
= 0,50 hp
19. Pompa 9 (P-09)
Kode : P-09
(MD-02) menuju (CL-02)
Jumlah : 2 buah
LC-
1000

P = 1 atm
massa BM Mol fraksi

Komponen
H2O 0.0000 18.0147 0.0000 0.0000
CH3COOH 0.0000 60.0508 0.0000 0.0000
C5H11OH 9.4697 88.1466 0.1074 0.0015
CH3COOC5H11 9460.2367 130.1827 72.6689 0.9985
Total 9469.7064 72.7764 1.0000

kg/m3 kg/m3 cp cp
0.0000 1027.0000 0.0000 0.0000 0.0000
0.0000 1043.0000 0.0000 0.0000 0.0000
0.1301 812.0000 1.1987 0.0800 0.0001
129.9905 872.0000 870.7128 0.1300 0.1298
130.1206 3754.0000 871.9114 0.2100 0.1299

m = 9469,7064 kg/jam
= 9469,7064 kg/jam x 2,0246 x 1/3600
= 5,3256 lb/s
= 54,4310 lb/ft3
Viskositas (µ) = 0,1299cp
= 0,005238 lb/ft.s

Q = m/p
5,3256 lb/ s
=
54,4310lb / ft 3. s
= 0,09784 ft3/s
LC-
1000

optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 2,30388 in
Shedule = 40
V = Q/A
= 31,9091 ft/s

ρ .V . D
Nre =
μ
Nre = 5071,733
L = 5m
= 16,4041 ft
Tinggi pompa (H)

H = 5m
= 16.4042 ft
1 elbow 90 (Le/D) = 32 (tabel.1 Peters & Timmehaus, hal 484)

LC-
1000
Le/D
Le = 8,1813 ft
2 gate, open Le/D

Le = 3,5793 ft

ε = 0,00015 ft
ε /D = 0,00015 ft / 0,08741 ft
= 0,0000587
f = 0,01021

2. f .V . Ltot
gc . D
= 28,16486 ft
F = 0,254 ft

Dimana :
k = 0,5
F = (k.V2) / (gc.2)
= 0,028321 ft

p1=p2 = 1 atm
LC-
1000
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
a=1
jadi :
W = 0 + (16,4042 ft) +(0) + 0,0959 ft
W = 16,68747 lbf.ft/lbm
ρ .Q . W
P =
550
= 0,1263 hp
Jika :
Q = 0,0979 ft3/s
= 43,91467 gal/ mnt
µ = 0,1299 cp
= 0,01299 gr/cm.s
µ / ρ = 0,2386 cs
maka :
= 0,29 hp
LC-
1000

Untuk BHP = 0,29 hp
ɳ = 0,8
Daya motor = 0,367hp
= 0,50 hp
20. Pompa 10 (P-10)

Kode : P-08
(MD-03) menuju tangki UPL
Jumlah : 2 buah
P = 1 atm
massa BM Mol fraksi

Komponen
H2O 15.8596 18.0147 0.8804 0.0097
CH3COOH 1008.7785 60.0508 16.7988 0.1859
C5H11OH 6402.4613 88.1466 72.6343 0.8036
CH3COOC5H11 9.4697 130.1827 0.0727 0.0008
Total 7436.5690 90.3861 1.0000

kg/m3 kg/m3 cp cp
0.0972 1027.0000 10.0031 1.7000 0.0166
6.1827 1043.0000 193.8473 0.3500 0.0650
39.2978 812.0000 652.5229 0.2600 0.2089
58.0385 872.0000 0.7018 0.2800 0.0002
103.6162 3754.0000 857.0750 2.5900 0.2908
LC-
1000

m = 7436,569 kg/jam
= 16906,28 kg/jam x 2,0246 x 1/3600
= 4,1822 lb/s
= 53,5048 lb/ft3
= 0,0118 lb/ft.s

Q = m/p
9,5079lb/ s
=
53,9179lb/ft 3. s
= 0,07844 ft3/s

optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 2,9995 in
Shedule = 40
V = Q/A
= 3,4407 ft/s
LC-
1000

ρ .V . D
Nre =
μ
Nre = 5500,878
L = 5m
= 16,4041 ft
Tinggi pompa (H)

H = 5m
= 16.4042 ft
1 elbow 90 (Le/D)
Le = 8,1813 ft
2 gate, open Le/D

Le = 3,5793 ft

LC-
1000
ε = 0,00015 ft
ε /D = 0,00015 ft / 0,08741 ft
= 0,0000587
f = 0,01207

2. f .V . Ltot
gc . D
= 28,16486 ft
F = 0,1924 ft

Dimana :
k = 0,5
F = (k.V2) / (gc.2)
= 0,0055 ft

p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
LC-
1000

a=1
jadi :
W = 0 + (16,4042 ft) +(0) + 0,0959 ft
ρ .Q . W
P =
550
= 0,1263 hp
Jika :
Q = 0,0139 ft3/s
= 6,2437 gal/ mnt
µ = 0,2953 cp
= 0,02953 gr/cm.s
µ / ρ = 0,5434 cs
maka :
= 0,23 hp
Untuk BHP = 0,23 hp
ɳ = 0,8
= 0,50 hp
21. Pompa 11 (P-11)

LC-
1000
Kode : P-11
(MD-02) menuju (CL-02)
Jumlah : 2 buah
P = 1 atm
massa BM Mol fraksi

Komponen
H2O 0.0000 18.0147 0.0000 0.0000
CH3COOH 0.0000 60.0508 0.0000 0.0000
C5H11OH 9.4697 88.1466 0.1074 0.0015
CH3COOC5H11 9460.2367 130.1827 72.6689 0.9985
Total 9469.7064 72.7764 1.0000

kg/m3 kg/m3 cp cp
0.0000 1027.0000 0.0000 0.0000 0.0000
0.0000 1043.0000 0.0000 0.0000 0.0000
0.1301 812.0000 1.1987 0.0800 0.0001
129.9905 872.0000 870.7128 0.1300 0.1298
130.1206 3754.0000 871.9114 0.2100 0.1299

m = 9469,7064 kg/jam
= 9469,7064 kg/jam x 2,0246 x 1/3600
= 5,3256 lb/s
= 54,4310 lb/ft3
LC-
1000
Viskositas (µ) = 0,1299cp

= 0,005238 lb/ft.s

Q = m/p
5,3256 lb/ s
=
54,4310lb / ft 3. s
= 0,09784 ft3/s

optimum
Di opt = 3,9(Q)^0.45 x (P)^0.13
= 2,30388 in
Shedule = 40
V = Q/A
= 31,9091 ft/s

ρ .V . D
Nre =
μ
Nre = 5071,733
LC-
1000
L = 5m
= 16,4041 ft
Tinggi pompa (H)

H = 5m
= 16.4042 ft
1 elbow 90 (Le/D)
Le = 8,1813 ft
2 gate, open Le/D

Le = 3,5793 ft

ε = 0,00015 ft
ε /D = 0,00015 ft / 0,08741 ft
= 0,0000587
f = 0,01021

2. f .V . Ltot
gc . D
= 28,16486 ft
LC-
1000
F = 0,254 ft

Dimana :
k = 0,5
F = (k.V2) / (gc.2)
= 0,028321 ft

p1=p2 = 1 atm
∆p ∆g V²
W= +∆ H + +Σ F
p gc 2. a . gc
∆p
=0
p
∆H = 16,4042 ft
∆ V =V 2−V 1=0
a=1
jadi :
W = 0 + (16,4042 ft) +(0) + 0,0959 ft
W = 16,68747 lbf.ft/lbm
ρ .Q . W
P =
550
= 0,1263 hp
Jika :
LC-
1000
Q = 0,0979 ft3/s
= 43,91467 gal/ mnt
µ = 0,1299 cp
= 0,01299 gr/cm.s
µ / ρ = 0,2386 cs
maka :
= 0,00029 hp
ɳ = 0,8
= 0,01 hp

Kode : Cl-01
Fungsi : menurunkan suhu larutan dari Destilasi 1(MD-01), sebelum
masuk ke dalam tangki UPL
Tekanan : 1 atm
Jumlah : 1 unit
Q = 494749,3543 kJ/jam
= 494749,3543 kJ/jam x 0,23901
LC-
1000
= 118250,0432 kkal/jam
= 469251,6464 btu/jam
W = 1585,9565 kg/jam
= 3496,3996 lb/jam
w = 685,5999 kg/jam
= 1511,4736 lb/jam
212,072 suhu tinggi 122 90,072
95 suhu rendah 86 9
117,072 Beda 36 81,0072
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 35,1968 oF
(T 1−T 2)
R =
(t 1−t 2)
= 3,252 oF
( t 1−t 2)
S =
(T 1−t 1)
= 0,2856 oF
2. UD dan A
organic) didapat :
LC-
1000
Q
A =
U D x∆t
= 266,6438 ft2
OD =3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 10 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
= 135,8348 buah
Nt = 138 buah
ID Shell = 10 in
= 0,8333 ft
Passes (n) =4
= 231,6340 ft2
LC-
1000
Q
UD =
= 49,9392 Btu/hr.ft2.oF
= 50 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
144 x n
= 0,0713 ft2

w
Gt =
at
= 21197,1365 lb/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 104 oF
µ = 0,034 cp
=0,0822 lb/ft.jam
kapasitas panas (c)
c = 0,5871 lb/lb.oF
Ret = 13315,4801
LC-
1000
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH = 130
hi = 481,5541btu/jam.ft2.oF
hio = hi x (ID/OD)
= 6420,7217 btu/jam.ft2.oF
a. Luas Aliran (as)

'
ID . c . B
as =
144 x pt
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
B = 10 in
Jadi
as = 0,1736 ft2

w
Gs =
at
= 20139,2618 lb/hr.ft2
LC-
1000
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Res = 14895,4747


= 1215,9349
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,0191
5. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 13315,4801
f = 0,000185 ft2/in2
L = 10 ft
ID = 0,0516 ft
LC-
1000

Jumlah passes =4
Maka :
∆ Pt = 0,0013 psi
b. Sheel side
∆ Ps =
5,22 x 10¹ ° x De x s
Res = 14895,4747
f = 0,0003 ft2/in2
(N+1) = 12 x(L/B)
= 12 ft
Ds = 0,6667 ft
De = 0,608ft
Maka :
∆ Ps = 0,000153 psi
cooler memenuhi syarat untuk digunakan
LC-
1000

Kode : Cl-03
masuk ke tangki produk (T-04)
Tekanan : 1 atm
Jumlah : 1 unit
Q = 365432,8275 kJ/jam
= 365432,8275 kJ/jam x 0,23901
= 873424,4792 kkal/jam
= 3466010,3608 btu/jam
W = 9469,7064 kg/jam
= 20876,9148 lb/jam
w = 2303,4353 kg/jam
= 5078,1536 lb/jam
394,0718 suhu tinggi 122 272,0718
95 suhu rendah 86 9
299,0718 Beda 36 263,0718
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 77,1733 oF
LC-
1000
(T 1−T 2)
R =
(t 1−t 2)
= 8,3076 oF
( t 1−t 2)
S =
(T 1−t 1)
= 0,1168 oF
2. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 8,9823 ft2
OD = 3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 10 ft
LC-
1000
Jumlah tube (Nt)

A
Nt =
a0 x L
= 4,5758 buah
Nt = 24 buah
ID Shell = 8 in
= 0,6667 ft
Passes (n) =4
= 47,112 ft2
Q
UD =
= 5 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
144 x n
= 0,0125 ft2

w
Gt =
at
= 403,5618 lb/hr.ft2
LC-
1000
¿
Ret = D x> µ ¿
Pada tc = 104 oF
µ = 0,015 cp
= 0,03628 lb/ft.jam
kapasitas panas (c)
c = 0,5871 lb/lb.oF
Ret = 574,6156
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH = 2,5
hio = hi x (ID/OD)
a. Luas Aliran (as)
ID . c' . B
as =
144 x pt
= 0,25 ft2
Dimana :
LC-
1000
C’ = Pt - OD
C’ = 0,25 in
B = 8 in
Jadi
as = 0,1111ft2

w
Gs =
at
= 187,8922 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Res = 314,9976


= 71,6083
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,1860
LC-
1000
5. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 574,6156
f = 0,001 ft2/in2
L = 10 ft
ID = 0,0516 ft
Jumlah passes =4
Maka :
∆ Pt = 0,000027 psi
b. Sheel side
∆ Ps =
5,22 x 10¹ ° x De x s
Res = 314,9976
f = 0,0014 ft2/in2
(N+1) = 12 x(L/B)
= 15 ft
LC-
1000
Ds = 0,6667 ft
De = 0,608ft
Maka :
∆ Ps = 0,0000019 psi

Kode : Cl-03
masuk ke tangki produk (T-04)
Tekanan : 1 atm
Jumlah : 1 unit
Q = 365432,8275 kJ/jam
= 365432,8275 kJ/jam x 0,23901
= 873424,4792 kkal/jam
= 3466010,3608 btu/jam
W = 9469,7064 kg/jam
= 20876,9148 lb/jam
LC-
1000

w = 2303,4353 kg/jam
= 5078,1536 lb/jam
394,0718 suhu tinggi 122 272,0718
95 suhu rendah 86 9
299,0718 Beda 36 263,0718
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 77,1733 oF
(T 1−T 2)
R =
(t 1−t 2)
= 8,3076 oF
( t 1−t 2)
S =
(T 1−t 1)
= 0,1168 oF
7. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 8,9823 ft2
OD = 3/4
LC-
1000
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 10 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
= 4,5758 buah
Nt = 24 buah
ID Shell = 8 in
= 0,6667 ft
Passes (n) =4
= 47,112 ft2
Q
UD =
= 5 Btu/hr.ft2.oF
LC-
1000
a. Luas Aliran (at)
Nt x At '
at =
144 x n
= 0,0125 ft2

w
Gt =
at
= 403,5618 lb/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 104 oF
µ = 0,015 cp
= 0,03628 lb/ft.jam
kapasitas panas (c)
c = 0,5871 lb/lb.oF
Ret = 574,6156
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14

LC-
1000
JH = 2,5
hio = hi x (ID/OD)
a. Luas Aliran (as)
ID . c' . B
as =
144 x pt
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
B = 8 in
Jadi
as = 0,1111ft2

w
Gs =
at
= 187,8922 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
LC-
1000
= 0,06083 ft
Res = 314,9976


= 71,6083
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,1860
10. Pressure drop

a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 574,6156
f = 0,001 ft2/in2
L = 10 ft
ID = 0,0516 ft
Jumlah passes =4
Maka :
∆ Pt = 0,000027 psi
LC-
1000

b. Sheel side
∆ Ps =
5,22 x 10¹ ° x De x s
Res = 314,9976
f = 0,0014 ft2/in2
(N+1) = 12 x(L/B)
= 15 ft
Ds = 0,6667 ft
De = 0,608ft
Maka :
∆ Ps = 0,0000008 psi

Kode : Cl-05
masuk ke dalam UPL
LC-
1000

Tekanan : 1 atm
Jumlah : 1 unit
Q = 624,5299 kJ/jam
= 624,5299 kJ/jam x 0,23901
= 149,2689 kkal/jam
= 592,3438 btu/jam
W = 2,9803 kg/jam
= 6,5703 lb/jam
w = 0,3767 kg/jam
= 0,8305 lb/jam
262,6016 suhu tinggi 122 140,6061
59,6061 Beda 36 23,6061
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 128,4395 oF
(T 1−T 2)
R =
(t 1−t 2)
= 1,6556 oF
LC-
1000
( t 1−t 2)
S =
(T 1−t 1)
= 0,2038 oF
2. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 0,9223ft2
OD = 3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 10 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
LC-
1000
= 0,4699 buah
Nt = 24 buah
ID Shell = 15,25 in
= 1,2708 ft
Passes (n) =6
= 47,112 ft2
Q
UD =
= 5 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
144 x n
= 0,0083 ft2

w
Gt =
at
= 99,0118 lb/hr.ft2
¿
Ret = D x> µ ¿
LC-
1000
Pada tc = 104 oF
µ = 0,034 cp
= 0,0822 lb/ft.jam
kapasitas panas (c)
c = 0,5871 lb/lb.oF
Ret = 62,1967
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH =1
hio = hi x (ID/OD)
a. Luas Aliran (as)

'
ID . c . B
as =
144 x pt
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
LC-
1000

B = 15,25 in
Jadi
as = 0,4037ft2

w
Gs =
at
= 16,2731 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Res = 12,0360


= 71,7187
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
= 0,1860
5. Pressure drop
a. Tube side
LC-
1000
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 62,1967
f = 0,0004 ft2/in2
L = 10 ft
ID = 0,0516 ft
Jumlah passes =6
Maka :
∆ Pt = 0,000000098 psi
b. Sheel side
∆ Ps =
5,22 x 10¹ ° x De x s
Res = 12,0360
f = 0,001 ft2/in2
(N+1) = 12 x(L/B)
= 7,8688 ft
Ds = 0,6667 ft
LC-
1000
De = 0,608ft
Maka :
∆ Ps = 0,00000002 psi
26. Menara Destila 3 (MD-03)
Kode : MD-03
bawah menara
Tipe : Sieve Tray

a. Aliran umpan
P = 760 mmHg
T = 401,14 K
FRAKSI
H2O 15.8596 18.0147 0.8804 0.0097
CH3COOH 1,008.7785 60.0508 16.7988 0.1859
LC-
1000
C5H11OH 6,402.4613 88.1466 72.6343 0.8036

CH3COOC5H11 9.4697 130.1827 0.0727 0.0008
TOTAL 7,436.5690 90.3861 1.0000
b. Aliran destilat
P = 401,112 K
T = 760 mmHg
FRAKSI
KOMPONEN
MASSA BM MOL MOL
H2O 15.8596 18.0147 0.8804 0.0097
CH3COOH 1,008.7785 60.0508 16.7988 0.1860
C5H11OH 6,402.4518 88.1466 72.6341 0.8042
CH3COOC5H11 0.0095 130.1827 0.0001 0.0000
TOTAL 7,427.0993 90.3134 1.0000
P = 474,15 K
T = 760 mmHg
FRAKSI
KOMPONEN
MASSA BM MOL MOL
H2O - 18.0147 - -
CH3COOH - 60.0508 - -
C5H11OH 0.0095 88.1466 0.0001 0.0015
CH3COOC5H11 9.4602 130.1827 0.0727 0.9985
TOTAL 9.4697 0.0728 1.0000

LC-
1000
Xlk XHk
log .
Nm= Xhk XLk
log a
Dimana :
= ( α D +α B )
2
sehingga:
Nmin = 8,9239 = 9 plate
L
−
D D ( )
L
min
dan
N −Nmin
L N +1
+1
D
Dimana :
Rmin =(L/D)min = 0,4049
Roperasi = (L/D)0 = 0,5669

LC-
1000
Maka :
L
−
D D ( )
L
min
= 0,1033
L
+1
D

N −Nmin
=0,5399
N +1
N-M = 0,44 (N+1)

N-50N = 0.44 +NM
N = 20,85
= 21 plate
KOMPONEN A B C D
CH3COOH -3.8937 7.85E+02 6.67E-03 -7.56E-06
C5H11OH -7.9943 1.77E+03 1.15E-02 -8.93E-06
H2O -10.2158 1.79E+03 1.77E-02 -1.26E-05
CH3COOC5H11 -4.6434 8.29E+02 8.66E-03 -9.04E-06

CH3COOH 0.010 0.33 3.22E-03
C5H11OH 0.186 0.38 7.10E-02
H2O 0.804 2.15E-01 1.73E-01
CH3COOC5H11 0.001 2.79E-01 2.24E-04
total 0.2472
LC-
1000
αAV-µAV = 1,58
Eo = 44,57
Nteoritis+ 1
Naktual =
Eo
= 48,1151 = 49 plate
[( ) ( )]
2
log = 0,206
X HK B ( X LK )B
× ×
X LK F D ( X HK ) D
Log Nr/Ns = 0,1301

Nr/Ns = 1,3494
Nr+Ns = 49 plate
Ns =20,8528 = 21 plate
a. Puncak menara

H2O 24.8510 18.0147 1.3795 0.0097 0.1756
CH3COOH 1,580.6988 60.0508 26.3227 0.1860 11.1698
LC-
1000
C5H11OH 10,032.2799 88.1466 113.8136 0.8042 70.8915

CH3COOC5H11 0.0148 130.1827 0.0001 0.0000 0.0001
TOTAL 11,637.8446 141.5159 1.0000 82.2370
pv = (P. Bmi)/RT
Dimana
Maka
Pv = 2.500 kg/m3
= 0.15615 lb/ft3

KOMPONEN
H2O 15.8596 0.0021 1,027.0000 2.1930
CH3COOH 1,008.7785 0.1358 1,043.0000 141.6644
C5H11OH 6,402.4518 0.8620 812.0000 699.9759
CH3COOC5H11 0.0095 0.0000 872.0000 0.0011
TOTAL 7,427.0993 1.0000 3,754.0000 843.8345
LC-
1000
( )
0,5
ρL −ρ V
Vm = Kv
ρV
dimana :
Maka :
Diambil :
V = 0,65 x Vm
= 2,8616 ft/detik
A = m/pv V
= 15,9456 ft2
D = (4A/π)^1/2
= 4,5069 ft2
=1,3737 m
LC-
1000
b. bagian bawah menara

L=V+B > (V=L-B)
dimana:
V = uap yang dibangkitkan reboiler (0,0728)
L/V =Klk
dimana:
Klk = 6,7146
L = 0,0728 kgmol

MOL BM MASSA fraksi pi pi.xi
KOMPONEN
Kgmol (Kg/kgmol) kg berat (kg/m3) (kg/m3)
H2O - 18.0147 - - 1,027.0000 -
CH3COOH - 60.0508 - - 1,043.0000 -
C5H11OH 0.0001 88.1466 0.0095 0.0010 812.0000 0.8120
CH3COOC5H11 0.0727 130.1827 9.4602 0.9990 872.0000 871.1280
TOTAL 0.0728 9.4697 1.0000 3,754.0000 871.9400

V=L–B
massa BM mol BM rata-rata

fraksi berat
KOMPONEN (Kg/ mol
kg kgmol) kgmol kg/kgmol
H2O - 18.0147 - - -
CH3COOH - 60.0508 - - -
C5H11OH 0.0095 88.1466 0.0001 0.0015 0.1301
LC-
1000
CH3COOC5H11 9.4602 130.1827 0.0727 0.9985 129.9905

TOTAL 9.4697 0.0728 1.0000 130.1206
Densitas uap:
Dimana :
P = 1 atm
Bmi
T = 474,15 K
Pv = 3.35 kg/m3
= 0.21 lb/ft3
Laju massa uap :

m = 0,01 lb/detik
Vm = Kv
Dimana
Vm = 3,8664 ft/s
Diambil kecepata uap masuk (v) : 80 % kecepatan supervisal
V = 3,0931
A = m / (pv xV)
= 0,0089 ft2
D =
LC-
1000
= 0,1069 ft
= 0,0032 m
Digunakan kolom dengan diameter rata-rata : 0, 7031 m

Dimana:

Diambil ruang kosong diatas kolom masing-masing = 1 m
= 23,5410 m
ts = +C
Dimana :
= 0.35157 m
= 1190,5 atm
= 0.8
= 0.003175 m
Maka
ts = 0,0036 m
LC-
1000
= 0,0009 in
th = +C
dimana :
= 0,7158 m
= 71,58 cm
th = 0,0039 m

OD = 3/4 in = 0.01905 m 0.0625 ft

BWG = 16
ID = 0.62 in = 0.05167 ft
a't = 0.302 in2
Pitch =1 in triangular
LC-
1000
Q = 7427,0993 kJ/jam
= 16373,95 lb/jam
W = 2754,6384 kg/jam
= 6072,9393 lb/jam
w = 4147323,43 kJ/jam
= 39335984,4086 lb/jam

262,64 suhu tinggi 122 140,643
262,64 suhu rendah 86 176,643
0 Beda 36 36
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 157,9598 oF
(t 1−t 2)
tc =
2
= 104 oF
T 1+T 2
Tc =
2
= 262,64 oF
2. UD dan A
organic) didapat :
LC-
1000
Q
A =
U D x∆t
= 332,1198 ft2
Jumlah tube (Nt)
A
Nt =
a0 x L
= 105,7436 buah
Nt = 109 buah
ID Shell = 13,25 in
= 1,104 ft
Passes (n) =1
= 342,3472 ft2
Q
UD =
= 75 Btu/hr.ft2.oF
a. Luas Aliran (at)
Nt x At '
at =
144 x n
= 0,2285 ft2

w
Gt =
at
LC-
1000
= 26879,4052 lb/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 104 oF
µ = 0,0075 cp
=0,0182 lb/ft.jam
kapasitas panas (c)
c = 1 btu/lb.oF
Ret = 76524,3755
hi = JH. ( ) ( cK. μ )
K c .μ
D K
1/2 0.14
JH = 174
hio = hi x (ID/OD)
a. Luas Aliran (as)
ID . c' . B
as =
144 x pt
LC-
1000
= 0,25 ft2
Dimana :
C’ = Pt - OD
C’ = 0,25 in
B = 15,25 in
Jadi
as = 0,30ft2

w
Gs =
as
= 53721,0254 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Ret = 31044,8276

∆ Tw = 174,43 oF

= 155,6568
Dirt Factor (Rd)
LC-
1000
Rd = c-Ud / Uc.Ud
= 0,0069
7. Pressure drop
b. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 76524,3755
f = 0,00016 ft2/in2
L = 16 ft
ID = 0,05167 ft
Jumlah passes =1
Maka :
∆ Pt = 3,39 psi
c. Sheel side
∆ Ps =
5,22 x 10¹ ° x De x s
Res = 31083,8276

LC-
1000
f = 0,0002 ft2/in2
(N+1) = 12 x(L/B)
= 14,4905 ft
Ds = 1,1041ft
De = 0,0608 ft
Maka :
∆ Ps = 0,001454 psi
Kode : AC-03
Fungsi : menampung sementara kondensat yang keluar dari kondensor
distilat.
Vt =mxt/ρ
= 0,99 m3
a. 90% air volume tangki terisi larutan
LC-
1000
b. dipilih perbandingan panjang (L) : 3 Diameter (3D)

maka
Vt = 1,1 m3
Diameter tangki (D)
D = (12x Vt / 10 π)^1/3
= 0,75 m
Hs = 3D
= 3 x 0,75 m
= 2,25 m
Hl = 90/100 x (Hs)
= 2,02 m
ts = +C
Dimana :
p : tekanan disain
Maka :
ts = 0,00365 m
= 0,1436 in
LC-
1000

PxDV
th = +C
2 x f x E−0,2 x Pt
dimana :
Kondisi tangki
f : tegangan
E : efisiensi
m
C : faktor korosi
= ,1386 in
(b) = (2:1), maka K = 2
V : 1/6 (2+2) = 1
3. Reboiler (RB-03)
Kode : RB-03
Tipe : ketel
Q = 4148580,27kJ/jam
W = 9,4697 kg/jam
w = 481,5336 kg/jam

LC-
1000
527 suhu tinggi 394,0718 132,9282

527 suhu rendah 394,0718 132,9282
0 Beda 0 0
∆ t 2−∆ t 1
LMTD = ∆t2
ln
∆t1
= 457,32 oF
T 1+T 2
Tc =
2
= 527 oF
tc = 394,0718 oF
2. UD dan A
organic) didapat :
Q
A =
U D x∆t
= 90,6218 ft2
OD =3/4
= 0,75 in
= 0,0624 ft
BWG = 16
ID = 16
LC-
1000
= 0,62 in
= 0,0517 ft
ao = 0,1963 ft/ft
at = 0,302 in2
Panjang (L) = 16 ft
Jumlah tube (Nt)

A
Nt =
a0 x L
= 36,5356 buah
Nt = 37 buah
ID Shell = 8 in
= 0,6667 ft
Passes (n) =1
= 116,2096 ft2
Q
UD =
= 74,0384 Btu/hr.ft2.oF
= 75 Btu/hr.ft2.oF
a. Luas Aliran (at)

LC-
1000
Nt x At '
at =
14 4 x n
= 0,0776 ft2

w
Gt =
at
= 269,04 lb/hr.ft2
¿
Ret = D x> µ ¿
Pada tc = 394,0718 oF
µ = 1,365 cp
= 3,365 lb/ft.jam
kapasitas panas (c)
c = 3,14 lb/lb.oF
Ret = 15,9941
hi = hio
a. Luas Aliran (at)
IDxC ' xB
as =
144 x Pt
LC-
1000
Dimana :
C’ = Pt - OD
C’ = 0,94 in
B = 10 in
Jadi
as = 0,00289 ft2

w
Gs =
at
= 36688,3164 lb/hr.ft2
¿
Res = D x> µ ¿
De = 0,73 in
= 0,06083 ft
Res = 6759,1323

∆ tw = 91,4643 oF

= 467,8899
f. Dirt Factor (Rd)
Rd = c-Ud / Uc.Ud
LC-
1000
5. Pressure drop
a. Tube side
F x >² x L x n
∆ Pt =
5,22 x 10¹ ° x D x s
Ret = 15,9941
f = 0,000085 ft2/in2
L = 16 ft
ID = 0,6667 ft
Jumlah passes =2
Maka :
∆ Pt = 0,01807 psi
c. Sheel side
F x Gs ² x L x n
∆ Ps =
5,22 x 10¹ ° x D x s
Res = 20797,18197
f = 0,00035 ft2/in2
LC-
1000
(N+1) = 12 x(L/B)
= 12,0001 ft
Ds = 0,0516 ft
De = 0,73ft
Maka :
∆ Ps = 0,000509 psi
27. Tangki Isoamil Asetat (T-04)

Kode : T-04
Fungs : penampungan sementara produk selama 1 minggu
Tipe : Silinder vertikal dengan tutup atas berbentuk standar dishead dan
tutup bawah berbentuk plat datar.
P = 1 atm
= 7 x 24 jam
= 168 jam
=mxt
LC-
1000
= 9479,18 kg/jam x168 jam

= 1592502 kg
Densitas ( ρ ¿ = 872 kg/m3
m
VL =
p
1592502 kg
=
872 kg/ jam
= 1826,26 m3
a. 90% dari volume tangki terisi Isoamil Asetat

Maka tangki berisi larutan Isoamil Asetat (Vt)
100
Vt = (VL)
90
100
= (1 m3)
90
Vt = 2029,18 m3
= 536053 galon

n = 2 buah
1491.692m 3
Vt =
2
= 1014,59 m3
2. Diameter Tangki
LC-
1000
Vs = Hs + As
Hs = 3/2 (D) = 1.5 D
As =1/4 phi r2
Vs = 1,5 D ((1/4)(π D2))
Vs = 1,175 D3
Volume tutup ( Vh)
Vh = 8,0297 x 10-10 x D3
Maka :
Vt = Vs + Vh
Vt = 1,17 4D3
745,846
D3 =
1,175
Dt =√ 861,6481 m³
Dt = 9,5157 m
Hs = 1,5 D
Hs = 1,5 x 8,5881 m
= 14,2736 m
90
Hl = (Hs)
100
Hl = 12.8462 m

LC-
1000
sebagai berikut :
Pr . dt
ts = +C
4. fE−Pr
Dimana :
jika :
PH = 109891,116 N/m2
Fk = 120658253 N/m2
Maka :
Pr = 106819,5580 N/m2
Ri = Dt/2
Ri = 4,7478 m
f = 17500 psi
= 120658253N/m2
Efisiensi (E)
E = 80 %
Faktor Korosi (c)
C = 0,0032 m
Maka :
LC-
1000
Pr . dt
ta = +C
4. fE−Pr
106819,5580 N /m2 X 4,7578m
= + 0,0032m
4 x 120658253 N /m2−106819,5580 N /m2
= 0.0085 m
0,885. pr . Ro
th = +C
fE−0,1 Pr
dimana :

Ro = 8,604 m
N
0,885. x 105942.691 x 8,604 m
th = m2
+0,0032 m
0,8 x 120658253 N /m2−0,1 x 105942.691 N /m2
= 0,0125 m
th = 0,49 in
th = 7/6 in
= 0.438 x 0,0254
= 0,0111 m
LC-
1000
BC = R- ICR
AB =ID/2 – ICR
AC = (BC2-AB2)1/2
B = r-AC
OA = th + B + Sf
th = 0,438 in
di dapat :

= 8,604 m
Maka :
BC = 9,52 M
AB = 4,76 M
AC = 8,26 M
B = 1,27 M
OA = 1,32 M
LC-
1000
Maka :
Ht = Hs + OA
Ht = 15,60 m

brownell & young :
Pr . dt
ta = +C
2. fE
1106819,5580 N /m2 x 8,604 m
ts = +0,0032 m
2 x 0,8 x 120658253 N /m 2
= 0,0084 m
28. Tangki Penampung (T-05)

Kode : T-05
Fungs : menampung sementara hasil atas destilasi (MD-01) untuk persediaan
1 minggu
P = 1 atm
= 7 x 24 jam
= 168 jam
=mxt
= 1585,96 kg/jam x168 jam
LC-
1000
= 266441 kg
m
VL =
p
266441kg
=
4954 kg/m3
= 53,7829 m3
a. 90% dari volume tangki terisi

Maka tangki berisi larutan (Vt)
100
Vt = (VL)
90
100
= (1 m3)
90
Vt = 59,7588 m3
= 15786,6 galon

n = 2 buah
59,7588m 3
Vt =
2
= 29,8794 m3
1. Diameter Tangki
LC-
1000

Vs = Hs + As
Hs = 3/2 (D) = 1.5 D
As =1/4 phi r2
Vs = 1,5 D ((1/4)(π D2))
Vs = 1,175 D3
Volume tutup ( Vh)
Vh = 8,0297 x 10-10 x D3
Maka :
Vt = Vs + Vh
Vt = 1,17 4D3
59,7588
D3 =
1,175
Dt =√ 25,3753 m³
Dt = 2,9385 m
Hs = 1,5 D
Hs = 1,5 x 8,5881 m
= 4,4078 m
90
Hl = (Hs)
100
Hl = 3,9671 m

sebagai berikut :
LC-
1000
Pr . dt
ts = +C
4. fE−Pr
Dimana :
jika :
PH = 192795,023 N/m2
Fk = 120658253 N/m2
Maka :
Pr = 110964,023 N/m2
Ri = Dt/2
Ri = 1,4692 m
f = 17500 psi
= 120658253N/m2
Efisiensi (E)
E = 80 %
Faktor Korosi (c)
C = 0,0032 m
Maka :
Pr . dt
ta = +C
4. fE−Pr
LC-
1000
N
110964,023 X 1,4692 m
= m2
+0,0032 m
4 x 120658253 N /m 2−110964,023 N /m2
= 0.0049 m
0,885. pr . Ro
th = +C
fE−0,1 Pr
dimana :

Ro = 2,95 m
N
0,885. x 53,7829
x 8,604 m
th = m2
+0,0032 m
0,8 x 120658253 N /m2−0,1 x 53,7829 N /m 2
= 0,0125 m
th = 0,49 in
th = 7/6 in
= 0.438 x 0,0254
= 0,0111 m
LC-
1000
BC = R- ICR
AB =ID/2 – ICR
AC = (BC2-AB2)1/2
B = r-AC
OA = th + B + Sf
th = 0,4375 in
di dapat :
Strength flange (Sf) = 0.0381 m

= 8,604 m
Maka :
BC = 2,95 M
AB = 1,47 M
AC = 2,55 M
B = 0,39 M
OA = 0,44 M
Maka :
Ht = Hs + OA
Ht = 4,85 m

brownell & young :
Pr . dt
ta = +C
2. fE
LC-
1000
110964,023 N /m 2 x 8,604 m
ts = + 0,0032m
2 x 0,8 x 120658253 N / m2
= 0,0048 m
29. Tangki Penampung (T-05)
Kode : T-05
Fungs : menampung sementara hasil atas destilasi (MD-01) untuk persediaan
1 minggu
P = 1 atm
= 7 x 24 jam
= 168 jam
=mxt
= 2,9803 kg/jam x168 jam
= 500,6913 kg
m
VL =
p
266441kg
=
4954 kg/m3
= 0,1010 m3
LC-
1000
a. 90% dari volume tangki terisi

Maka tangki berisi larutan (Vt)
100
Vt = (VL)
90
100
= (1 m3)
90
Vt = 0,1122 m3
= 29,6659 galon

n = 2 buah
0,1010 m3
Vt =
2
= 0,056 m3
2. Diameter Tangki
Vs = Hs + As
Hs = 3/2 (D) = 1.5 D
As =1/4 phi r2
Vs = 1,5 D ((1/4)(π D2))
Vs = 1,175 D3
Volume tutup ( Vh)
Vh = 8,0297 x 10-10 x D3
Maka :
LC-
1000
Vt = Vs + Vh
Vt = 1,17 4D3
0,1122
D3 =
1,175
Dt =√ 0,0477 m ³
Dt = 0,363 m
Hs = 1,5 D
Hs = 1,5 x 8,5881 m
= 0,5439 m
90
Hl = (Hs)
100
Hl = 0,48954 m

sebagai berikut :
Pr . dt
ts = +C
4. fE−Pr
Dimana :
jika :
PH = 192795,023 N/m2
Fk = 120658253 N/m2
LC-
1000
Maka :
Pr = 23791,3452 N/m2
Ri = Dt/2
Ri = 0,1813 m
f = 17500 psi
= 120658253N/m2
Efisiensi (E)
E = 80 %
Faktor Korosi (c)
C = 0,0032 m
Maka :
Pr . dt
ta = +C
4. fE−Pr
N
23791,3452 X 1,4692 m
= m2
+ 0,0032 m
4 x 120658253 N /m 2−23791,3452 N /m2
= 0.0034m
0,885. pr . Ro
th = +C
fE−0,1 Pr
dimana :

Ro = 0,37 m
LC-
1000
N
0,885. x 23791,3452x 8,604 m
th = m2
+0,0032 m
0,8 x 120658253 N /m2−0,1 x 53,7829 N /m 2
= 0,00354 m
= 0,14 in
th = 7/6 in
= 0.438 x 0,0254
= 0,0111 m
BC = R- ICR
AB =ID/2 – ICR
AC = (BC2-AB2)1/2
B = r-AC
OA = th + B + Sf
th = 0,4375 in
di dapat :
Strength flange (Sf) = 0.0381 m

LC-
1000

= 8,604 m
Maka :
BC = 0,36 m
AB = 0,18 m
AC = 0,32 m
B = 0,05 m
OA = 0,09 m
Maka :
Ht = Hs + OA
Ht = 0,64 m

brownell & young :
Pr . dt
ta = +C
2. fE
23791,3452 N /m 2 x 8,604 m
ts = +0,0032 m
2 x 0,8 x 120658253 N / m2
= 0,0034 m
30. Reaktor (R-01)

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PERHITUNGAN SPESIFIKASI ALAT

1. Tangki Isoamil Alkohol

1. Volume Tangki (Vt)

Volume larutan dalam tangki (VL)

Tangki dirancang dengan ketentuan :

a. 90% dari volume tangki terisi Isoamil Alkohol

b. Perbandingan Tinggi (H) 1.5 Diameter Tangki (ID)

Jumlah tangki yang dibutuhkan (n)

3. Tebal Dinding Tangki

Untuk Internal Presure, tebal dinding (shell) dihitung dengan persamaan

Dari Pers. 13.1 hal 254 Brownel & Young

Ro = Diameter Luar selinder

karena th = 0,454 in, maka tetabal tutup adalah

Strength flange (Sf) = 0.0381 in

Brown radius (r) = OD shell

5. Penentuan tutup bawah

105942.691mN /m2 x 8,604 m

Kapasitas yang akan di pompakan (m)

Laju alir Volumetrik (Q)

inside diameter = 0,256 ft

Pemeriksaan bilangan Reynold (Nre)

Karena Nre > 2.100 maka asumsi benar

Panjang pipa lurus (L)

Friksi yang terjadi (F)

Friksi karena adanya kontraksi dari tangki ke pipa:

W = 0 + (16,4042 ft) +(0) 0.143729047 ft

2. Penentuan daya Pompa (P)

Kondisi Operasi : T = 30 oC (303

1. Volume Tangki (Vt)

Volume larutan dalam tangki (VL)

c. 90% dari volume tangki terisi Isoamil Alkohol

d. Perbandingan Tinggi (H) 1.5 Diameter Tangki (ID)

Jumlah tangki yang dibutuhkan (n)

3. Tebal Dinding Tangki

Untuk Internal Presure, tebal dinding (shell) dihitung dengan persamaan

Dari Pers. 13.1 hal 254 Brownel & Young

Ro = Diameter Luar selinder

karena th = 0,39 in, maka tetabal tutup adalah

Strength flange (Sf) = 0.0381 in

5. Penentuan tutup bawah

Kapasitas yang akan di pompakan (m)

Laju alir Volumetrik (Q)

Pemeriksaan bilangan Reynold (Nre)

Karena Nre > 2.100 maka asumsi benar

Friksi yang terjadi (F)

Friksi karena adanya kontraksi dari tangki ke pipa:

Total friksi ( Σ F) = 0,0340727 ft

2. Penentuan daya Pompa (P)

efisiensi pompa (ɳ ) = 55% = 0,55

Kondisi Operasi : T = 30 oC (303 K)

Kapasitas tangki untuk memenuhi selama 1 minggu

Densitas ( ρ ¿ = 1027 kg/jam

1. Volume Tangki (Vt)

Volume larutan dalam tangki (VL)

a. 90% dari volume tangki terisi Isoamil Alkohol

b. Perbandingan Tinggi (H) 1.5 Diameter Tangki (ID)

Jumlah tangki yang dibutuhkan (n)

3. Tebal Dinding Tangki