Dehydration of Milk

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The key takeaways are that dehydration/desiccation removes water from milk to extend its shelf life and reduce costs of transport and storage. The main methods discussed are cold methods like freezing and sublimation and hot methods like spray drying and drum drying.

The different methods of dehydrating milk discussed are cold methods like freezing out water & centrifuging and freezing milk & sublimation. Hot methods discussed include film roller or drum drying and spray drying.

The principal components of a spray dryer include a high pressure pump, a device for atomizing the feed stream, a heated air source with blower, a secondary collection vessel, and means for exhausting the moist air.

Dehydration / Desiccation

Dr . Mohammad Ashraf Paul

Division of Livestock Products


Technology
Faculty of Veterinary Sciences
& Animal Husbandry SKUAST - K
Alusteng , Ganderbal

Kashmir
Dehydration :
§Near complete removal of water from milk
to
§ a < 5 % level .
§Water in a liquid product – in this case
milk concentrate is removed , so that the
product takes on a solid form
§Microorganisms are unable to reproduce at
such a low water content thus shelf life of
the milk is extended
§Reduces weight and volume
§Reduces the cost of transporting and
storing the product .
§Skim milk powder has a maximum shelf life
of about three years while whole milk
powder has a maximum shelf life of six
months.
§Because the fat in the powder oxidises
during storage , with consequent
deterioration in flavour . However , the
 Dehydration /Desiccation Methods
 ‘According to Marco Polo’s accounts of his travels
in Asia, Mongolians produced milk powder by
drying milk in the sun’

Cold Methods:

v Freezing out water & centrifuging


v Freezing milk & Sublimation
• Produces very high quality powder
• Product is deep-frozen and the water
frozen in the product is evaporated
under vacuum
• Ensures high product quality as, among
other things, no protein denaturing
takes place compared to drying milk at
higher temperatures where the
proteins are denatured to a greater or
Hot Methods :
Film , roller or drum drying
Less common , used for a few special
products
Spray drying
§In spray drying , the milk is first
concentrated by evaporation and then dried
in a spray tower
§Although there are many types of driers ,
spray driers are the most widely used type
of air convection drier .
§It turns out more tonnage of dehydrated
products than all other types of driers
combined .
§It is limited to food that can be atomized ,
i . e . liquids , low viscosity pastes , and purees
§Drying takes place within a matter of
seconds at temperatures approximately 200 ° C .
§Evaporative cooling maintains low product
temperatures , however , prompt removal of the
Principal components include :
High pressure pump for introducing liquid
into the tower
Device for atomizing the feed stream
Heated air source with blower
Secondary collection vessel for removing
the dried food from the airstream
Means for exhausting the moist air
Atomizers :
Provide a large surface area for exposure
to drying
forces :
1 litre = 12 billion particles = > 300 ft
2 (30m 2 )

i. Compressed air
ii. Pressure spray
Rotary disc

iii. Centrifugal disc Pressure nozzles


Two - fluid nozzl
Powder Recovery systems :

Bag filters - very efficient ( 99 . 9 %)

Cyclone collector- efficient ( 99 . 5 %)

Wet scrubber - the most economical outlet
air cleaner . The principle of a wet
scrubber is to dissolve any dust powder
left in the airstream into either water
or the feed stream by spraying the wash
stream through the air . This also
recovers heat from the exiting air and
evaporates some of the water in the feed
stream
Two and Three Stage Drying Processes
In single stage spray drying , the rate of
evaporation is high in the first part of the
process , and it gradually decreases because
of the falling moisture content of the
particle surfaces
In order to complete the drying in one stage ,
a relatively high outlet temperature is
required during the final drying phase
resulting in high particle temperature and
thus heat damage .
Two stage drying process - is superior to
the traditional single stage drying in terms
of product quality and cost of production .
consists of a spray drier with an external
vibrating fluid bed placed below the drying
chamber .
The product can be removed from the drying
chamber with a higher moisture content , and
the final drying takes place in the external
Three stage drier : Here second stage is a
fluid bed built into the cone of the spray
drying chamber ( integrated fluid bed ). Thus it
is possible to achieve an even higher moisture
content in the first drying stage and a lower
outlet air temperature from the spray drier .
The inlet air temperature can be raised
resulting in a larger temperature difference
and improved efficiency in the drying process .
The exhaust heat from the chamber is used to
preheat the feed stream .
The third stage is again the external fluid
bed , for final drying and / or cooling the
powder . The results are as follows :
oHigher quality powders with much better
rehydrating properties directly from the drier
oLower energy consumption
oIncreased range of products can be spray
dried
oSmaller space requirements
 Roller drying Process summary:
Atmospheric / Vacuum

Milk
concentr
ate

Adjustable
pump

Feeding

Drying drum
Drying drum
cont
 .

Scraper

( Doctors
blade

)

Grinder

Sifter

Dried
product
Spray drying - Process summary :
The liquid food is generally
preconcentrated by evaporation to
economically reduce the water content
The concentrate is then introduced as a
fine spray or mist into a tower or
chamber with heated air .
As the small droplets make intimate
contact with the heated air, they flash
off their moisture , become small
particles , and drop to the bottom of the
tower and are removed .
The advantages of spray drying include a
low heat and short time combination which
leads to a better quality product .
 Skim Milk Powder manufacture
 Receiving milk

 Cooling@ 50C

Preheating (350C)
â
 Separation
â
 Pasteurization (710C /15s)
â
 Low heat SMP
High heat S M P
â
Condensing


L o w h e a t S M P. .

â
High heat SMP
â

 Reheating (630C)
P re h e a tin g 8 5 0 C / 2 0 m in .
â â
C o n d e n sin g

â

 R e h e a tin g ( 7 4 0 C )
â
 Filtration
R e m a in in g ste p s sa m e
 Whole Milk Powder
S ta n d a rd iz

a tio n
 Fat / SNF = 1 : 2 . 77

 Preheating
(71 0 C )

Filtration / Cl
arification
Homogenizati
on
2500 psi / 63 - 74 0 C – I
; 500psi - II

Heating
(93 0 C / 3min .)

Condensing
Preheating71 0
C

Pumping
( 2500psi )
Spray
Drying
(82 0 C outlet
temp .)
Cooling
(32 0 C )

Sifting

Vacuum + N 2

Packaging &
Storage @RT
 Instantiation :
 Process of making dried milk products
instant –soluble.
 Process:
1. Wetting of particle surface (steam, atomized
water or both in a tube or chamber or cyclone
2. Agglomeration (particles collide with each other
due to turbulence and adhere to form
clusters)
3. Re drying – with hot filtered air
4. Cooling
5. Sizing to exclude very large agglomerates &
very small particles
6. Sifting & packaging.

 PFA Standards:
• WMP :
• A product obtained from cow or buffalo
milk, or a combination thereof , or from
standardized milk, by the removal of
water. It may contain Cacl2,Citric acid and
sodium citrate , sodium salts of
orthophosphoricacid and poly phosphoric
acids , not exceeding 0.3% by weight of
the finished product , and 0.01% of
BHA(by Wt.) of the product. Such addition
need not to be declared on the label. Milk
powder should contain not more than 5%
moisture and not less than 26% fat. The
total acidity expressed as lactic should
not be more than 1.2%.The SPC may not
exceed 50000/g and coliform count may
not exceed 90/g. Max. solubility index
should be 15.0 for a roller dried and 2.0
for spray dried product.
Various uses of milk powder :
 Recombination of milk and milk products
 Reconstituted Milk and milk products
 In the bakery industry to increase the
volume of bread and improve its water -
binding capacity . The bread will then
remain fresh for a longer period of time
 Substitute for eggs in bread and
pastries
 Producing milk chocolate
 Producing various types of ready - cooked
foods in food and catering trade
 In baby foods
 Production of ice cream
 Animal feed , calf growth accelerator ,
pharmaceuticals , microbiological media
preparations
Typical properties of spray - dried
milk powder :
Characteristics WMP
SMP

Solubility (ml) 0.1 – 0.5


0.1 – 0.5

Scorched particles A
A
( standard disc grading )
Residual moisture
( max .%) 3.0
4.0

Bulk density ( g / ml ) 0 . 45 – 0 . 57
Composition of milk powder
Characteristics Whole
milk Skim milk

Fat , % solids content 26 – 29


1 . 25

Protein , % solids content 25 – 27


34 – 38

Lactose , % solids content 35 – 38


48 – 56

pH
6.6 – 6.7 6.6 –
6.7

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