Chemistry Half Yearly Lab Manual

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Experiment No,

Date )/44 Page No, 1

To detonmine,
one oqanic comhound..

let o ode dmonium Attrte Teat i

ENxtotment Observatio Infprence.


be
1|Orqonie Comhound Rod ax

coloun
Ntote aution

Estex Testiu

-OH breent
Compsund and Enuty,smell
Eonboxyle acid + two dbsented

heot

conc H,SOy
RcOoR

(Buttysnel)

Test in
Todolam
loc U 4 Lodie + Yolow pt -OH contirm

Na OH + Heot

Reudt kohal) þesent In 0c.

Teacher Signature
ExperimentNo, 9. No.2
Date 65 -24 Page

Am le deleine one in organic conakond.

Teat
Canbomy Guni
Obsexvoton

324DN Tet'u
0C + 2,4 DNP Yellow, orange Conlirm the

hydvazine

Sodiunm blsulhhite tesl'

oC1 sodium bttulphite


Contirm

Test or Ketonío Guoup

Obtervaion Inyenence

O-Ct m-dihitiobeNZeMe.

oH Con firm U the


+ Na
keaie

Red colown is
0.c4 Sadium nihopustide. Ketonie Srau
4 disklad water4 Na0H þroducad js tontmed

TeacherSignature
Experiment No. Date Page No. 3

NO)
Violet coloun
Reacon s

NO

Teacher
Experiment No, Date 1-94 Page No.

Aim •To delemine one

lest r Cankbony Gooti

&NaSeimat. Obenoion

,4 DN fest !
0C+ ,4 ON %dllauo, orange tpt

hydane.

oc t sodium bicalphite

Test tor tdehyde Gucufo '


Ohserwation Tntexene.

tet i

Soluhon tunt to
Gi yen O-C
CHO
ink colauy.

-CHO coniume
Sshuton'A of fahling

+ ting solution 8.

t 0'e heat

Teacher Signature
Experiment No, Date Page No. 5

Tollen'k teat

A mierot like loer df

A'oc+ Heat stler meto can bt.

doserved.

ARenediet 's tect ' ronge-xed


-CHO 4roue
OC + alcohol Benedid's AFheamana of

so| heot þpt af Cu.oxide

Reult--CHO (atchyli gnp) fcsent in oganz compoiund.


Experiment No,
Date 16/ 24 Page No. 6

Aim la detmine one camnfoand.

Conboy Conbound -
Staabeniment Obanvaton eente

AHehyte ond

net locmed kotome abynt


bydazine

Q:C + codium bisulbaita Crysalline. þet and


Aldeyde
ketomabsent

Tet on

Obsenvolion Treree
SN Experiment

00H may
Given o-c+ Blue

befresat

9.Codiara Hhydnogen Canbonale Tel -


Co, is dbserved. C00H
Experiment No. Date Page No.

3. Ester Test

O:C+ £honol t
' Sied smell of esten

Cone H,s0, +heot+


Na,COg
Experiment No. Date 23/4l24 Page No,8

0,(KMno4)

Chumitol

46H5Fe* Mn44H.0 +

inditatgo
End foiat! Colounlar to

Pactasotion
Weioh erocy 4-90 dMoh's sat on a wateh glate and dizrcve

beakon.

2 Tsanfo the solaion do a. 250 m me auuirg

Ad uyato do make the voluvne ezoatly 250


2s l.

i, Stosp the flask and shake to got a omo geneDus Colution.

Rine a beakan wla tht souton ond tranelerthe slation


ouk do Jhe beoken.

Moka's salt soluion KMnoy soluien i


Tb»ahion

Teacher Signature
Trtal Banette RendingFnal Banelle.
Vi)m

Oml
2OmL 9:2 mL 92 mL
3 OmL 9:2 mL 92mL

Coneordanb: Volume 9lm


Experiment No. Date Page No.

Mchu all solution.


a 20ml bibtte with

hette ut 0m0 d Nohi aßlsolukioyn in a fitakion


and
Volume

8Rinse and KMnOy solukion.

9.Note the ikil seadling


sital
i0.ld KMnOu sohution to Uohe 'e cale olution

La bermanent Jight oink calausk abp eant.

H. Note Jhe final hending


to get thiee concordant
42 Reheat dhe Atiation4-5 HneL

Concordant Voumee < mL

'
9:2

KMnOu Sdution
Calalaton
9
Nohr Salt v( mohr solt )
MCKMndu)
92
= 1200

0:02M

Malanity, x Malan
E-02 X 158
316gt
Teacher Signature
Experiment No, Date
Page No. h

1oecnutongi

bhunette shenld b nead.


SOppn menicua in Hhe

Do not heat the colution.


fitrokio

Romave the mnel fosm


am bwctte uile entoxenrg

Rexdt :Ahould

0-02 M
boe ocexaate.
Experiment No, 6 Date 20/+/ Page No. 11

Find he 40 KMnO4

Keguivcd omound oxadle acid for


M sohation

i000

y 280 =0 1889

Indiater KMnOy actsa o se nditotor.

Luanen to o 00nl beoke and dinalve in usten. Sir te

3. Ad wotee do moke the volume. exact 2s0 m

Staben and thake to g


and
SRiniea bealten usith Udhi soludion
tongen the lution

roion KMno, goletion


wwnn ngoatt 0xnlic acid dehon .
Teacher Signature
SoTntial Rendinga|Final Reodig lmit)

19-6 mL 19-6 mL

20-0m
Om 200m 200mL

CoNcarcht Vdume 10mL


Experiment No. Page No. 11
Date

KRinte. oa 20nd bibdte wl WA axalic acid. tolution.

Pipette. out 30.0 nd he dotior do a. titohon fok.

9. Rinse the buunetle aud


ond U A'ih KMnoy sduton.
t0Mote. Hhe inkl Jeadíng
Hlo ennan ent
sith
ink, clouu sthesn.
i. Repont the itaion 5 inner to
three tonordont eoadinge.

5
M(oale aid) X Vosalic aid

Mtu Y 2

O:01 M

Melaity KAnoa 0:01M


KMnO4

Teacher Signature
Experiment No, Date Page No. 13

Paeeouiong -
betuoen 60t6 0°c
Remove he ou am the bustte
choldnt be Sinpd. caith the erpeinental
koluton.

benemove d.
Page No. 14
Experiment No, Date 6/8/2l4

solt.
detewmine one anion and one cotior, dn

lest fan Anion

SN aeximevt
Obsemnliems

1Silven nitrate test

oolained which is
dd
souble in ammoniurm

dnc o slex uitate, otution. hydnonide.

Maqnee dloxide. Test


Maqnesc

tTo Nbineh o alt dakex in a tetA renich yellaw aat

dube,add

mangomeye diozide (MnO) and tml. evved.

ew Udnot cone H,son -Hest

Hhe contents.
stanch iodide
tifh Bsing- a molt stoeh iodide The conjsmed.
Meon. the mouth o the babea dtune ble
tost tube

Choride Telt
3.Cotomy
oMe a. 'small amount o salt.

otk asbd otausturm dithnsmste.Red vahsus evolved.

Take Jhe mixtune Jn the tert

tube and add cone H,SOy.

TeacherSignature
Experiment No. Date Page No. 15

Heat the eontents.

Yelouw eduion is

aOH obtained. Clconfimtd.


Koluton thkeo in a qad
detector.

cit To the tyellaus sutow., add tw

dil. acete add and obtoined

ed etote, outon.

est a Catton -
Ohteation.
GNahesignent
i Sodium hydoozido tert

to Heat Hhat oth tew dncbe Calouwlege go, with NH þreient


tore: Na 0H ina testybicol awlnomi al. Cmel
tohun
evolved .
tube.
tisWhite umer tet
|Buing a
fn|Dente white.
onmed.
ube in above test

aNeslen't Ragent tat

Phu the qas ormed n step


thrsak Nestle's eoqent
tskem
nmed.
in a qa deteator.

Caton- NH
Anion -Cl
Salt - NH,C Ammoritam cloride J
Teacher Signature
Page No. 16
Experiment No. 8 Date 6l8l:

Aim odelerwine ome anlon and oe eolom in given ot.

LCNA benixge vnt obconyaioi

1: Dil. H,So, tost


ti To ineh da solt in Hhe test Coloutlerc, odounles qo4

dube add uoth briskeesence


H,sOL umt lime watr millky:

tiih|Pasced the ahove gose though


Cimewaten dake. Lime woter tun

deotur.

QMaso4test
salt couton

Test tou Cotn i

ShsenyakisL
SNa EheuiMent

tet
4 Sodium hysazide
ieat he Uant oith few dahs dbulec qad willa NH þsaent.

cone NaoH soluton "in a Ommonie tmell evoled


Experiment No. Date Page No. 17

|Dente.site fumes

neon the. mouth


dest tube in. obove. test.

9Neslen't hesgent test

NH tonfmd.

token n aa deotedor.
qa

Keudt
Cotion i NH

: (NHa),Co, Ammonium Cabmate

Teacher Signature
Experiment No. Date 13924 Page No. 18

Aint o detenwine ne anlen ond one coisn sn


in aiven salt.

lest on Anion

Exoiment hsenvoion Inenenee


Ester Test

Take asmall quontty o he pleant


Sat ina ube.d conc:
test' mell esten CH,C00 itmed
confime

H,SOu and. het.dla add ethy


odeohol. Shake. Poux Jhectevts

waten. Slir.

2 eunic cleride Tegt

Take water exboct d e. sat. Reddich eolotused


CH,C00°cond
Ad meutrol dhlaide ol". Alkate.

oxtiens.
t one pont add, dil- Hol Reidish cdou disokpeatu. CH, t00
db |Ta seeond ont,add woter and bil Reddish baotun Ht. confimed

est on Cation
Experiment No. Date Page No. 19

SN
1 Sodium
b |Exheniacnt

Heat
auyduczide

the Aalt with tew


Cone-

tettbe
NooH solution
dest

in a
dachs
thceayalion

Calounler qau vdtd

amnohi smell
tybisl
elved.
NH reent..

neah the mouth oxned.


dest tube in aboye test

Q Necen't Resgent test

IPos thegad |NH confimed

Netle' sengentmed.
Jaken in ga deteelho
aa ju

(oten - NH
Anion - CHy C00
SoH CH CoONHa (Ammoniun acetate)
aseto
Page No.
20
Experiment No. 10 Date 132
cotion in given
alt.
Aini s detenine one. anion and one.

lestan Anion

SNesiNent Obteauoione

Estex Test.

Pleauant buily CH,CO0


Take. a omall. duantiky a the salt

Smel. ater! contsmed


in a test tube A'eone: H, So4
nd.

shoke buy,
heat. Now
the
add

eantent e
etylaliohal.
tube in

la beaken tes wate, Shrs

2Feunic chbride Test


Reddisa colouned CHsCo0 conHmed
Take. watex extract a the salt. Add

meutal Gesie chlarise solution..Ale. itale.

bortHons.

bant,add uater and bl.. Reddich blum t. conimed


ti To second

Test ton Cation


o

bseryoion

o
H, Soy test

one out ot soluon ,


add eu
Experiment No. Date Page No., 21

Potaium Todide Teat

lodide. solution.

Potosium Chtomate Test

T thid font of abvs solukton,ad Yelou Bht oi formed.Pl onimed.

kcoolutions

Caton

Anon CHac00

Lead. Aette
Experiment No. L Date 13&/24 Page No. 22

ts
Aim deteine one. anion and oe. cohon n

eat Anion.

BNa eximent Sbevotio Tatouente

1Diphenamine test
deeh tlue cdotugion is NDG confimed.
|Add a dnokt o dibhenulaumineA

Heot a sma.quanty 4 the salt

withooncertrated nl phuic aid |mikogen dioxido uteh fum contomed.

and. a few cofon chibs. eos colfhok sal" black.

3 Ring Test

douk. broun
o reslhy

feou lhatis fotmed. ot the


Atored souton. conglimed.

he. salt and Ehen þouk Cone

CaHew

btexyakone

1.D0 H, S04 test

ong While seomotes


hbt
aut
Experiment No, Date Page No.

.Potassiun Todide. Test

losecond batofsol", add. fes diops

of potaustum Ibdido solukon! Jamed.


QPotasium Chromate Teat

amd. romfimed.
solkon

Coton
Anion i NO,

[lead. witrote|

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