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    VishalB 21BCE1201 Exp5

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    vishal.bommisetty2021

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    VishalB 21BCE1201 Exp5

    Uploaded by

    vishal.bommisetty2021
    5 views3 pages

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    VishalB_21BCE1201_Exp5

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    5 views3 pages

    VishalB 21BCE1201 Exp5

    Uploaded by

    vishal.bommisetty2021

    Copyright:

    © All Rights Reserved
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    Download as pdf or txt
    of 3

    VISHAL kE No, 28cE 1201

    EwreRImuT5
    BoetMISETTY 19 1/2.011

    Kedutbion p-ito htnel top-AinePhanel


    AIM( Pveponation ducbien
    uduchen
    i p henel
    PP nibreplJ
    nibreplanol
    )
    CleLbig t il e raction bnd bniT nung
    7oduchic Monaltic al dota.
    Cionuicont e Hhuachan n phanma ceubal ndudriu,
    oinepkeno d t
    ybahesis o hacetone, delibrate and un devivatives.t
    alse duyd he pupar akion he cduelopen aA
    Kadlical
    Slack And atels, anioniolauts andl bil
    addib'ves,and
    en pheducts. The mehulatd dorivatives ke N-metyl- amainophend
    ano N-N- olinmathl - oniuephandl Aave comnmencia ppacahonu
    phan ma nclusty:-
    4-anmimepkonl a bidin -Bock d
    d
    hqanie chemistry rominetly, dt he dh moblin the
    ndlus tral Bynthesis Poracetanmd.
    PRINDCIPLE Te oduetion ua chons n
    the tganic
    0 ynlhesi ase
    nen ally uloreol T6 e Jumaval 0ygen b Ha
    00clation droesn otoms.n mes gugarul , Hhe a
    rous
    Onod
    Cotalyat availalla fo the uduchion reattion
    nHhis rechen,
    nHis reuchen, inrially, the shrong uducing
    desates dsgon LALH,
    agent LALH
    9a) up8n actien i h TiCL Tho
    hndbniolus lmad hom h uation kudbrog.pn ga wit C
    rduces ityotyo grou -niro plasb
    Praminefhend
    STEP T

    LiALH+Tid Lcl AIC, +2,+ T (


    STEP L

    STEP L
    LALH 4H,o LiO+ AL (o
    Tt >Tro Hd
    2no
    NHOH +AC NH,C +H,O
    REAGETS sbedlolendo

    hiun AluminumHyobnioleLiALH) ,Ttaviwn


    bra chleriole T ) , onhy dnes Tetrakgobretursn,
    EH Acetate Henant ond Ammonio eurien
    APPARAToSt
    3 Neck Rownd Bottom vFlasks, LC pLate ond

    TLC baieet

    oro hors
    REACT1ONN rRocEDURe

    Caleul orlcd
    Caleul oated mBunts tagenis m Atefhiomtne Juachon.
    8.No Molecule Meles oushb
    Com pouno Ceiaht
    weight molewlen wigkt
    NO
    1.31 13

    AHA o .5 38 OOI55

    3
    TA 3 18 19 O 02
    2.2mL)
    Lithium Alummum Hyebicle (o.5tq,
    petion - sise e a
    0-o1a H mol) added
    atirred
    Susgension ebtoineod y Mos addibon
    itanium detrathloride (2-2 m,o.o
    (6o mL) ot oc te he mol) Jo dy tetrahydre furan
    stired luy acbive ditnunm
    uagent. This Wachen mintusR
    S1eb emperectwu ond then 9uenchacl
    atreder 15in a
    at

    waten nd 50
    50 ml litlDe
    m 25. Onmmouo the mintwu
    Sttunon. Then
    Jientracted oi 2thy acetate C5x 50 mL) and kwnther the ,

    gonic doyer sill Je doried with ahyol6uw eoium


    Tronic elutien utate
    iltesred, ond all he velailes he
    ask meveo sta- evapevodon. inally, te cebioue u
    uxgthesigro o n ethansl
    9g vvCe p-annophansl as
    pu preoluct

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