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    Salt 6 Calcium Sulphate

    Uploaded by

    praneesh287

    Copyright:

    © All Rights Reserved
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    Salt 6 Calcium Sulphate

    Uploaded by

    praneesh287
    3 views2 pages

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    © © All Rights Reserved

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    3 views2 pages

    Salt 6 Calcium Sulphate

    Uploaded by

    praneesh287

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 2

    sYSTEMATIC ANALYSIS OFFSIMPL.

    E SALT-7

    EXPERIMENT
    CasO,
    OBSERVAIONS INFERENCE
    PRELIMINARY TEST:
    LCOLOUR. Absence of Cu
    the colour of the salt colourless
    Mn Co N
    .CIIODN OF WEAT:
    Abscnce of NO
    inch of salt is heated in a No charateristic change
    dy est tube (0.CuSO:
    FLAME TEST:
    in
    Apinch ol salt taken
    awatch glass a drop of
    concentrated HCl is added Presence of Ca'
    Brick red coloured flame
    and made into a paste The
    naste Is Introduccd into the
    non-luminous flame.
    4.ASH TEST:
    To a little bit of the salt
    solution in the test tube added Absence of Al.
    concentrated HNO, and No characteristic ash
    Zn'.Mg
    cobalt nitrate. A filter paper
    in dipped in the solution and
    ignited.
    IDENTIFICATION OF ACID RADICAL
    5.ACTION OF H,SO,: Absence of
    To a little of the salt in the test CO NO, CI
    tube added dilute H,SO No gas / vapours evolved
    CH,CO0
    To a little of the salt in the test
    tube added ConcH.SO,
    6. POTASSIUM
    PERMANGANATE TEST
    To a little of the salt in the KMnO, not decolourised Absence of Fe
    test tube added 2ml of dil C,0 Cl
    HSO,and then KMnO, soln
    dropwise
    7.COPPER TURNING TEST:
    To a little of the salt in a No Reddish brown gas Absence of NO
    dry test tube added few Cu
    tuming and concentrated
    H:SO..
    PREPARATION OF SODIUM CARBONATE EXTRACT: Apinch of saltis mixed
    with double the amount of Sodium carbonate and is boiled with distilled water .The sus
    pension obtaincd is filtered. the filtrate is Sodium carbonate extract.
    OBSERVAION INEERENE
    TENTEORE\PERIMENI
    SO ANDPO : Presence of SO 5
    BARIUMCH ORIDE EST:
    loa itle of
    Awhite precipitate
    insoluble in con lIC confirmed
    cxtrat added lBarnu
    chlonde soluton
    9 AMMONIUM IOLVBDATE
    TEST: No Canary yellow Absence of PO
    lo a littlc of the salt added precipitate is formed
    concentrated HNO, till the fumes
    CCasç to cvolhe and then added
    limonIum molybdate solution.
    (ONFIRMATOR TEST FOR ACID RADICAL.
    1. BARIUM CHLORIDE TEST: Awhite precipitate Presence of SO: is
    To a litle of extract added Barium insoluble in con. HCI confirmed
    chloride solution
    2. LEAD ACETATE TEST: A white precipitates Presence of SOis
    To a little of the extract added obtained confimed
    dil acetic acid and lead acetate
    solution
    IDENTIFICATION OF BASICRADICAL:
    To a little of the Salt solution added No characteristic Absence of Zero
    NaoH and warmed change group.
    GROUP ANALYSIS:
    Preparation of original solution : To a little of the given salt added water and dissolved
    and labeled as original solution (OS).
    EXPERIMENT OBSERVATION INFERENCE
    To alittle of the OS dil HCl added No characteristic precipitate is Absence of group 1
    obtained
    To a little of the OS added dil.HCl and No characteristic precipitate is Absence of group
    then passed H;S gas obtained
    Alittle of the OS solution added No characteristic precipitate is Absence of group
    NH.CI.NH.OH obtained Ill radical

    To alittle of the OS solution added Awhite precipitate is obtained Presence of


    NH.CI,NH.OH and (NH.),CO:. group Vradical
    (Ca BaSr
    CONFIRMATORY TEST FOR BASIC RADICAL
    Confirmatory test forCa Awhite precipitate is obtained Presence of Ca is
    To a little of the OS solution added confirmed
    (NH.):C:0:
    FLAME TEST: Brick red coloured tlame Presence ot Ca is
    Apinch of salt taken in a watch glass contimed
    a drop of concentrated HCT is added
    and made into a paste.The paste is
    introduced into the non-luminous flame.
    RESULT : The substance contains : Basic radical: CaAcidradical :SO,
    Therefore the substance is: CaSO,

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