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    Advanced Instrumentation Techniques Winter 2022

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    Vedantshaligram89
    The document discusses an exam for an advanced instrumentation techniques course. It contains three sections with objective, long, and short answer questions covering topics like NMR, mass spectrometry, thermal analysis techniques, chromatography, and spectroscopy. Students are asked to identify factors that affect chemical shifts, explain validation methods, and discuss calibration procedures and applications of various analytical techniques.

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    Advanced Instrumentation Techniques Winter 2022

    Uploaded by

    Vedantshaligram89
    22 views1 page
    The document discusses an exam for an advanced instrumentation techniques course. It contains three sections with objective, long, and short answer questions covering topics like NMR, mass spectrometry, thermal analysis techniques, chromatography, and spectroscopy. Students are asked to identify factors that affect chemical shifts, explain validation methods, and discuss calibration procedures and applications of various analytical techniques.

    Original Description:

    Dbatu AIT winter 2022 QP

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    The document discusses an exam for an advanced instrumentation techniques course. It contains three sections with objective, long, and short answer questions covering topics like NMR, mass spectrometry, thermal analysis techniques, chromatography, and spectroscopy. Students are asked to identify factors that affect chemical shifts, explain validation methods, and discuss calibration procedures and applications of various analytical techniques.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    22 views1 page

    Advanced Instrumentation Techniques Winter 2022

    Uploaded by

    Vedantshaligram89
    The document discusses an exam for an advanced instrumentation techniques course. It contains three sections with objective, long, and short answer questions covering topics like NMR, mass spectrometry, thermal analysis techniques, chromatography, and spectroscopy. Students are asked to identify factors that affect chemical shifts, explain validation methods, and discuss calibration procedures and applications of various analytical techniques.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 1

    DR.

    BABASAHEB AMBEDKAR TECHNOLOGICAL UNIVERSITY, LONERE


    End Semester Examination – Winter 2022
    Date: 22/02/2023
    Course : B. Pharmacy Sem: VIII
    Subject Name : Advanced Instrumentation Techniques Subject Code: BP811ET
    Max Marks : 75 Duration: 3 Hrs.
    Instructions:
    1. All questions are compulsory
    2. Draw diagrams / figures wherever necessary
    3. Figures to right indicate full marks
    Q. 1. Objective Type Questions (Answer all the questions) (10 x 2) = 20
    i) What is Chemical shift? Enlist the factors affecting Chemical shift.
    ii) Write down the principle of Mass spectroscopy. Enlist different ionizers used in MS.
    iii) Differentiate between TGA and DTA.
    iv) Explain Bragg’s law. Enlist the different X-ray Diffraction techniques.
    v) Define Distribution Coefficient and Distribution Ratio.
    vi) What is mean by Hyphenated Technique? Classify it.
    vii) Explain applications of RIA.
    viii) Differentiate between Calibration and Validation.
    ix) Enlist the ionization techniques used in LC-MS/MS.
    x) What do you mean by Spin- spin coupling? Write applications of NMR spectroscopy.

    Q. 2. Long Answers (Answer 2 out of 3) (2 x 10) = 20


    i) Explain in brief, “Analytical methods of validation as per ICH Guidelines”
    ii) Explain in detail Calibration of HPLC and electronic balance.
    iii) Enlist different methods of thermal analysis. Explain Thermogravimetric analysis in
    detail

    Q. 3. Short Answers (Answer 7 out of 9) (7 x 5) = 35


    i) Write a short note on H1 NMR.
    ii) Explain X-ray Diffraction techniques in brief.
    iii) Describe GC-MS MS with principle and applications.
    iv) Explain the calibration of UV spectrophotometer.
    v) Write a short note on Differential Scanning Calorimetry.
    vi) Describe the procedure and applications of RIA.
    vii) Explain fragmentation patterns in Mass Spectrometry.
    viii) What is mean by extraction technique. Explain solid phase extraction.
    ix) Write a short note on MALDI.

    ------END OF THE PAPER------

    CLICK HERE TO @DBATUPHARM


    TELEGRAM GROUP

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