PDF Iodine Value Aoac Official Method 99320 Compress

Download as pdf or txt
Download as pdf or txt
You are on page 1of 2

4>.>.>9 (i) Njncytaonc `ncnjoi.—Noournti tm ¾ 5.555> g.

NMNO Mllaoanc Kitbmd 11?.05 (l) Lactirs.—Nsbciss, omnrsi grndi (Wbntknj Jm. 94> as suat-
Amdaji \ncui ml Lnts njd Macs n`ci).
Wafs (Oyocmbixnji‟Noitao Noad _mcvijt) Kitbmd (g) Bmtnar mv ij.—On
mvij.—Onpn`c
pn`cii ml knaj
knajtnaj
tnajajg>55µO
ajg>55µO watb
watbaj
aj ¾>.9µO.
Larst Notamj >11?
Lajnc Notamj >11< O. Pingi
Pingijts
jts

AYUNO‟NMO_‟NMNO Kitbmd (n) Umtnssauk amdadi (HA) smcutamj.—>9%. Dassmcvi >9 g HA aj


>55 kC B0M.
(Nppcaon`ci tm ditirkajntamj ml amdaji vncui lmr lnts njd macs wbaob
(Nppcaon`ci (`) Wafs amdaji smcutamj.—(>) Dassmcvi >? g risu`cakid A aj > C
dm jmt omjtnaj omjfugntid
omjfugntid dmu`ci `mjds.) noitao noad, njd pnss aj draid (tbrmugb B 0_M4) Oc ujtac mragajnc
Jn0_0M? tatrntamj ml smcutamj as jmt quati dmu`cid. (Obnrnotirastao
Onutamj6 Wafs smcutamj
smcutamj onusis
onusis siviri `urjs8 vnpmrs
vnpmrs onj onusi omcmrr obnj
omcm obnjgi
gi nt ijd pmaj
pmajtt ajda
ajdaonti
ontiss prmp
prmpir
ir nkmu
nkmujt jt ml Oc. Omjv
Omjvijai
ijaijt
jt
cujg njd iyi dnkngi. Ysi ml luki bmmd as riomk- kitbmdas
kit bmdas tm ris
risirv
irvii smk
smkii ml mra
mraga
gajncA
jncA smc
smcut
utamj
amj,, nd
ndd
d sca
scagbtixois
gbtixoisss ml
kijdid. _ii Nppijdax @, Cn`mrntmry _nlity lmr prmoi- Oc tm `uch ml smcutamj, njd `rajg tm disarid tatir `y rinddatamjs ml ri-
duris mj snli bnjdcajg ml noads njd mrgnjao smcvijts sirvid pmrtamj.) Mr6 (0) Dassmcvi ><.9 g AOc aj > C noitao noad.
(oyocmbixnji). Ditirkaji A/Oc rntam ns lmccmws6
(>) Amdaji omjtijt.—Ua—Uapitpit 9 kC Wa Wafsfs smc
smcuta
utamj
mj aj
ajtm
tm 955 kC
_ii Tn`ci 11?.05N lmr tbi risu
risucts
cts ml tbi ajti
ajtircn`
rcn`mrnt
mrntmry
mry stud
study
y sup-
Ircijkiyir lcnsh omjtnajajg >95 kC snturntid Oc‟B0M njd smki
pmrtajg nooiptnjoi ml tbi kitbmd.
gcnss `inds. _bnhi, bint tm `macajg, njd `mac `rashcy >5 kaj. Ommc,
N. Urajoap
Urajoapci
ci ndd?5kCB0_M4 sm smcucuta
tamj(>
mj(> + 41
41)) nj
njdd >9kC >9 >9% % HAsmcu
HAsmcuta tamj
mj,, nj
njd
d
Lnt mr mac as kaxkaxidid wat
watb
b amd
amdaji
aji kmjmobcm
kmjmobcmradi
radi smcutamj
smcutamj tm tatrnti akkidanticy watb 5.>K Jn0_0M?.
bncmgijnti
bncmgij nti dmu`
dmu`ci
ci `mjd
`mjdss aj lnt mr mac.Ixoiss amda
amdaji
ji kmjm
kmjmobcm
obcmradi
radi as (0) Tmtnc bncmgij omjtijt.—Uap .—Uapit it 05 kC Waf Wafss smcu
smcutamj
tamj ajtm
riduoid tm lrii amdaji aj prisijoi ml pmtnssauk amdadi, njd lrii am- 955 kC Ircijkiyir lcnsh omjtnajajg >95 kC rioijtcy `macid njd
dajii as kin
daj kinsur
surid
id `y tat
tatrnt
rntamjwatb
amjwatb smd
smdauktbam
auktbamsuc
suclnt
lntii usa
usajg
jg stn
stnrob
rob ns ommcid B0M njd >9 kC >9% HA smcutamj. Tatrnti akkidanticy watb

ajdaontmr. 5.>K Jn0_0M?.


Amdaji vncui (A\), oncoucntid ns og amdaji n`smr`id pir g ml snk-
pci(% am
amdaj
dajii n`s
n`smr`
mr`id)
id),, asn kin
kinsur
surii mlujsnt
mlujsnturn
urntam
tamj
j mllnts njdmac
njdmacs.
s. 0R
A/Oc ;
@. Nppnr
Nppnrntus
ntus ?@ ∐ 0R
(n) Gcnss-stmpp irid amdaji lcnshs.—955 kC.
Gcnss-stmppirid
(`) Gcnss-stmpp
Gcnss-stmppirid vmcukitraoo lcnshs.—>5
irid vmcukitra .—>55555 kC, lmr prip
pripnraj
nrajgg
stnjdnrd smcutamj
smcutamjs.
s. wbiri R ; kC 5.> K Jn 0_0M? riquarid lmr A omjtijt njd @ ; kC ri-
(o) \mcuk itrao daspijsirs.—(>) 09 kC, lmr Wafs
\mcukitrao Wafs njnjd
d >9
>9%% pmtns-
pmtns- quari
quarid
d lmrtmtn
lmrtmtncc bnc
bncmgi
mgij
j om
omjti
jtijt.Al
jt.Al A/O
A/Occ rnt
rntamas
amas jm
jmtt >.>
>.>5
5 ¾ 5.
5.>,nddA
>,nddA mr
sauk amdadi (HA) smcutamjs. ( 0) 0 kC, lmr stnrob smcutamj. (?) 95 kC, Oc tm omrriot rntam.
lmr B0M. _tnjdnrdazid Wafs smcutamj kny `i m`tnajid lrmk omkkiroanc
(d) Pipin tir papit.—05kC, watblaccaj
Pipintir watblaccajg
g lcnsh
lcnsh,, lmr oyoc
oyocmbix
mbixnji.
nji. suppcairs (spioaly watbmut onr`mj titrnobcmradi).

Tn`ci 11?.05N Ajtircn`mrntmry study risucts lmr ditirkajntamj


ditirkajntamj ml amdaji vncui `y Wafs kitbmd usajg onr`mj titrnobcmradi smcvijt
mr oyocmbixnji‟noitao noad (> + >) smcvijt

Kinj \ncui` sr sP P_Dr, % P_DP, %


_nkpci OTOn OBR OTO OBR OTO OBR OTO OBR OTO OBR
OB
_ujlcmwir >??.< >?0.1
>? >. 4 >.7 ?. 4 0.? >. > >.? 0. < >.7
Pilajid pnck 9?.> 9?.5 5. > 5.0 5. ? 5.4 5. 0 5.? 5. 9 5.7
Orudi lasb >51.> >52.9 5. 7 5.9 >. 7 >.> 5. < 5.9 >. < >.5
Tujg ><4.9 ><?.> 0. 5 >.4 ?. > 0.9 >. 0 5.1 >. 1 > .9
>.
Tnccmw (`iil) 47.0 4<.1 5. 0 5.0 5. 9 5.4 5. 9 5.9 >. 5 5.2
Orudi pnck 90.9 90.< 5. ? 5.4 5. 4 5.9 5. 9 5.2 5. 2 >.5
Ysid lryajg ?7.7 ?7.7 5. > 5.0 5. 0 5.? 5. 4 5.9 5. 4 5.1
Unck hirjic >2.0 >2.? 5.5> 5.5> 5.5? 5.54 5. > 5.> 5. 0 5.0
Mcavi 20.? 20.0 5. 0 5.9 5. < 5.2 5. ? 5.< 5. 7 5.1
5.
o
B_@M -> >50.< >50.? 5. 9 5.2 >. 2 >.1 5. 9 5.2 >. 7 >.2
B_@M-0 74.7 74.2 5. 9 5.4 >. 5 5.< 5. < 5.9 >. ? 5 .2
5.
d
BLM 7?.5 70.2 5. 4 5.4 5. 7 5.< 5. < 5.< 5. 1 5.2
n Onr`mj titrnobcmradi.
`
Oyocmbixnji‟noitao noad (> + >).
o
Bydrmgijntid smy`inj mac.
d
Bydrmgijntid lasb mac.

© 0555 NMNO AJTIPJNTAMJNC


Tn`ci 11?.05
11?.05@
@ Tist snkpci
snkpci wiagbt
wiagbts
s njd omjtajui nddajg tbamsuclnti smcutamj scmwcy ujtac `cui omcmr fust
dasnppinrs.
\ncui Tist snkpci, g Noournoy, kg
? >5.92‟2.4< 5.9 05.?
05.?14
14 × wt H0 Or
Or0 M7
Jn0_0M? smcutamj kmcnraty, K ;
>5 ?.>7‟0.94 5.0 kC smdauk tbamsucln
tbamsuclnti
ti
05 >.91‟>.07 5.0
I. Ditir
Ditirkajnt
kajntamj
amj
45 5.71‟5.<? 5.0
Kictt tis
Kic tistt snk
snkpc
pci,
i, al jmtncri
jmtncrind
ndy
y ca
caqua
quad
d (dmjmt ixo
ixoiidsnkp
iidsnkpci
ci kic
kict-
t-
25 5.45‟5.?0 5.0
ajg pmajt `y :>5µO). Unss tist snkpci tbrmugb dmu`ci cnyir ml lactir
>05 5.0<‟5.0> 5.0 pnpir tm rikmvi njy smcad akpuratais njd trnois ml B 0M (lactrntamj
><5 5.05‟5.>< 5.0 kny `i pirlmrkid aj nar mvij, on >55µO, `ut sbmucd `i omkpcitid
055 5.><‟5.>? 5.0 watba
wa tbajj 9 kaj ¾ ?5 s). Tis
Tistt snk
snkpc
pcii ku
kustst `i n`s
n`smc
mcuti
uticy
cy dry
dry.. (Jmti6 Ncc
gcnsswnri kust `i n`smcuticy ocinj njd omkpciticy dry.)
Cit lactirid tist snkpci ommc tm <2‟7>µO. Akkidanticy wiagb
_tm
_tmri
ri aj nk`
nk`ir
ir `m
`mttc
ttcii sin
sincidwatbpnrn
cidwatbpnrnlla
llaj
j uj
ujtacrind
tacrindy
y lmrusi. Wa
Wafs
fs nkmujt ml tist snkpci ajdaontid aj Tn`ci 11?.05@ ajtm ocinj, dry
smcutamjs nri sijsatavi tm tikpirnturi, kmasturi, njd cagbt. _tmri aj 955 kC lcnsh, @(n).
dnrh nt 3?5µO. Uripnri nt cinst 0 `cnjh ditirkajntamjs tm ruj watb inob snkpci
(o) _mcu`ci stnrob smcutamj.—Kax pnsti ml > g stnrob watb skncc grmup.
nkmujt omcd B0M. Wbaci starrajg, ndd 055 kC `macajg B0M. Tist lmr Ndd >9 kC oyocmbixnji‟noitao noad smcvijt, O (b), tm inob tist
sijsatavaty6 pcnoi 9 kC stnrob smcutamj aj >55 kC B 0M njd ndd snkpci njd swarc tm ijsuri tbnt at as omkpciticy dassmcvid.
5.59 kC 5.>K amdaji smcutamj8 diip `cui omcmr prmduoid kust `i Daspijsi 09 kC Wafs smcutamj ajtm lcnsh omjtnajajg tist snkpci,
dasobnrgid `y 5.59 kC 5.>K smdauk tbamsuclnti smcutamj. ( Jmti6 stmppi
stm ppirr lcn
lcnsh,njdswarctm
sh,njdswarctm kaxkax.. Akk
Akkidaidanti
nticysit
cysit tak
takirlmr
irlmr >.
>.5 5 mr0.5 b,
>% stnrob smcutamj, omkkiroanccy nvnacn`ci, as suatn`ci.) dipij
dip ijdaj
dajgg mjamda
mjamdajivncu
jivncuii mlsnkpc
mlsnkpcii (A\3>95
(A\3>95,, >.5b8 A\ ≩>9 >95,0.5
5,0.5 b)
(d) Umtnssauk daobrmknti (H0Or0M7).—Lajicy grajd njd dry tm njd stmri lcnshs aj dnrh nt 09 µ ¾ 9 µO lmr durntamj ml rinotamj.
O`
omjstnjt wiagbt (on >>5µO) `ilmri usajg aj D. Ndd
Nd Pikmvi
d >9
>955 kCBlcnshs
M lrmk dnrh,nccy
njdgrnduncc
njdgrndu ndd
y 05rnti
kC
tatrnt
tat i HAbsmcutamj,
watb
wat 5.>K
5.> K stnjd
stn (nrd
jdnrd ), njd
Jn0_ kax.
(i) _mdauk tbamsuclnti (Jn0_0M?9B0M) smcutamj.—5.>K. _tnj- 0 0M?

dnrdazi ns aj D. smcutamj, D, watb omjstnjt njd vagmrmus sbnhajg mr kiobnjaonc star-


(l) Noads.—(>) Bydrmobcmrao noad (BOc).—Omjoijtrntid, sp gr rajg. Omjtajui tatrntajg ujtac yiccmw omcmr bns nckmst dasnppinrid.
>.>1.. (0) Noit
>.>1 Noitaoao noad (O0B4M0).—Gcnoanc. (? ) _uclurao noad Ndd >‟0kC stnro stnrob
b ajda
ajdaontm
ontmrr smcu
smcutamjtm
tamjtm lcnsh
lcnshss njd omjt
omjtaju
ajuii tatrn
tatrntajg
tajg
(B0_M4).—Omjoijtrntid. ujtac `cui omcmr bns fust dasnppinrid. (Jmti6 Al rinotamj as jmt tirka-
(g) Oyocmbixnji.—XJmti6 Irrntao risucts kny risuct al oyocmbix- jntid `y nddatamj ml HA njd B0M watbaj ? kaj pnst >.5 mr 0.5 b rino-
nji as mcd, a.i., omjtnajs mxadazn`ci knttir8 sii (b).[ tamj taki, snkpci kust `i dasonrdid. Tbi snkpci kust `i tatrntid
(b) Oyocmbixnj i‟noitao noad smcvijt.—Kax oyocmbixnji, (g),
Oyocmbixnji‟noitao watbaj
watb aj ?5 kajml rino
rinotamjtirkajn
tamjtirkajntamjtamj88 al jmt,tbi njnc
njncysasas
ysasas ajvn
ajvncad.
cad.))
njdnoitao
njdnoit ao noa
noad,
d, (l)(0), > + > (v/
(v/v).\iral
v).\iralyy n`
n`sij
sijoi
oi ml mx
mxada
adazn`
zn`ci
ci knt
knt-- L. Oncouc
Oncoucntamj
ntamj
tiraj smc
smcvi
vijt
jt `ysbnha
`ysbnhajgjg >5kC smc smcvi
vijt
jt wa
watb
tb > kC snt
snturn
urntidnqui
tidnquimumuss
H0Or0M7 smsmcu
cuta
tamjnjd>
mjnjd> kCB 0_M4, (l)(?). Jm gri griij
ij omc
omcmr
mr sbm
sbmucdnp-
ucdnp- ( @ ∐ _ ) × K × >0<1
.
Amdaji vncui (A\) ;
pinr. wt ml lnt mr mac

D. _tnjdnrdazntamj ml _mdauk Tbamsuclnti _mcutamj


Noournti
Noournticy
cy wiag
wiagb
b 5.><
5.><‟5.0
‟5.00
0 g drai
draid,
d, lajic
lajicy
y grmu
grmujd
jd H0Or0M7, wbiri @ ; tatrntamj ml `cnjh (kC)8 _ ; tatrntamj ml tist snkpci (kC)8
K ; kmcnraty ml Jn _ M smcutamj.
O (d),
ndd 9 tmjin
tmjinri
rist
kC BOc, stO5.55
5.
(555>g
l)(5>g ajtm
aj
>), njdtm05
955
955 kC
kC HAlc
lcns
nsh,
h, da
dass
ssmc
smcutamj, mcviaj
Oviaj 09kC
(`), njd B0M,
rmtnti tm
0 0 ?
Pilirijois6 Uuri & Nppc. Obik. <0 , 0??1(>11
0??1(>115).
5).
kax. Cit stnjd 9 kaj. Ndd >55 kC B 0M. Tatr Tatrnti
nti watb smdauk
F. NMNO Ajt. 77, <74(>114).
tbamsuclnti smcutamj, O (i), sbnhajg omjtajumuscy ujtac yiccmw omcmr
bns nckmst dasn
dasnppin
ppinrid.
rid. Ndd>‟0 kC stnr
stnrob
ob ajda
ajdaontm
ontmrr smcu
smcutamj
tamj,, O(o), Pivasid6 Knrob >117

© 0555 NMNO AJTIPJNTAMJNC

You might also like