DS2500 Liquid Analyzer

Manual
8.0929.8001EN / 2021-04-30
Metrohm AG
CH-9100 Herisau
Switzerland
Phone +41 71 353 85 85
Fax +41 71 353 89 01
[email protected]
www.metrohm.com

DS2500 Liquid Analyzer

Manual

8.0929.8001EN / 2021-04-30
Technical Communication
Metrohm AG
CH-9100 Herisau
[email protected]

This documentation is protected by copyright. All rights reserved.

This documentation has been prepared with great care. However, errors
can never be entirely ruled out. Please send comments regarding possible
errors to the address above.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

Table of contents
1 Introduction 1
1.1 Instrument description ........................................................ 1
1.2 Intended use ......................................................................... 2
1.3 About the documentation ................................................... 2
1.3.1 Symbols and conventions ........................................................ 2
1.4 Safety instructions ................................................................ 3
1.4.1 General notes on safety ........................................................... 3
1.4.2 Electrical safety ........................................................................ 4
1.4.3 Flammable solvents and chemicals ........................................... 5
1.4.4 Recycling and disposal ............................................................. 5

2 Overview of the instrument 6

2.1 Front ..................................................................................... 6
2.2 Rear ........................................................................................ 7
2.3 Sample holders ..................................................................... 8

3 Installation 9
3.1 Unpacking and inspecting the instrument ......................... 9
3.1.1 Packaging ................................................................................ 9
3.1.2 Checks .................................................................................... 9
3.2 Location ................................................................................. 9
3.3 Connecting the instrument to the power grid ................... 9
3.4 Connecting the data cable ................................................. 10
3.5 Switching on the instrument ............................................. 11
3.6 Initial start-up ..................................................................... 11
3.7 Temperature control ........................................................... 12
3.8 Setting up accessories ........................................................ 12
3.8.1 Calibrating the instrument ..................................................... 12
3.8.2 Analyzing liquid samples ........................................................ 14

4 Operation 19
5 Maintenance 20
5.1 Maintenance by Metrohm Service .................................... 20
5.2 Maintenance by the user ................................................... 20
5.2.1 Cleaning the instrument ........................................................ 21
5.2.2 Cleaning the sample holder ................................................... 22
5.2.3 Cleaning the sample compartment ........................................ 22

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 Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5.2.4 Replacing the lamp ................................................................ 23

5.2.5 Replacing the fan filter ........................................................... 32
5.2.6 Replacing a fuse .................................................................... 35

6 Technical specifications 38
6.1 Interfaces ............................................................................. 38
6.2 Power connection ............................................................... 38
6.3 Ambient conditions ............................................................ 38
6.4 Dimensions .......................................................................... 38
6.5 Housing ............................................................................... 39

7 Accessories 40
Index 41

IV ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

Table of figures
Figure 1 Front DS2500 Liquid Analyzer ............................................................ 6
Figure 2 Rear DS2500 Liquid Analyzer ............................................................. 7
Figure 3 DS2500 Liquid Analyzer sample holders ............................................. 8
Figure 4 Place the disposable vial in the sample compartment. ...................... 15
Figure 5 Disassembling the sample holder ..................................................... 22

￭￭￭￭￭￭￭￭ V
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

1 Introduction
This manual provides you with a comprehensive overview of the installa-
tion and maintenance of the DS2500 Liquid Analyzer. The DS2500 Liquid
Analyzer is operated with the control software. You can find information
on operating the instrument in the tutorial and in the manual for the con-
trol software (see 8.105.8032 Tutorial Vision Air Local and 8.105.8036
Tutorial Vision Air Network and Server).

NOTICE

You can request application descriptions in the form of

Application Notes and Application Bulletins from your
Metrohm representative or download them from
http://www.metrohm.com.

1.1 Instrument description

The DS2500 Liquid Analyzer is a compact measuring instrument for trans-
mission measurement in the near-infrared wavelength range. The poly-
chromatic light is dispersed by the monochromator built into the DS2500
Liquid Analyzer into monochromatic wavelengths before hitting the sam-
ple. This keeps heating of the sample to a minimum. The instrument oper-
ates in a wavelength range from 400 to 2,500 nm.
In order to ensure that each sample can be measured at the optimal tem-
perature, the DS2500 Liquid Analyzer heats the sample to the desired
temperature before the analysis. The DS2500 Liquid Analyzer can be
actively cooled so that there is no delay between measurements at various
temperatures.
The DS2500 Liquid Analyzer is designed for quality monitoring of the pro-
duction processes. Use the DS2500 Liquid Analyzer for the following pur-
poses:
￭ Quick and non-destructive incoming goods inspection of liquids
￭ Production process monitoring
￭ Pre-delivery inspection of the final product
Liquid samples can be measured using the DS2500 Liquid Analyzer.
The DS2500 Liquid Analyzer is a durable instrument that is resistant to
moisture, dust, vibrations and temperature fluctuations. As a result, the
DS2500 Liquid Analyzer can be used in a variety of production facilities.

￭￭￭￭￭￭￭￭ 1
 1.2 Intended use ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

The DS2500 Liquid Analyzer is operated with the control software via an
external computer.

1.2 Intended use

The DS2500 Liquid Analyzer is designed for use in production facilities.
The DS2500 Liquid Analyzer can be used for incoming goods inspection or
atline or offline for production process monitoring.
Usage requires the user to have basic knowledge and experience in han-
dling chemicals. Knowledge with respect to the application of the fire pre-
vention measures prescribed for laboratories is also required.
Adherence to this technical documentation and compliance with the
maintenance specifications make up an important part of intended use.
Any utilization in excess of or deviating from the intended use is regarded
as misuse.
Specifications regarding the operating values and limit values of individual
products are covered in the "Technical specifications" section (see chapter
6, page 38).
Exceeding and/or not observing the mentioned limit values during opera-
tion puts people and components at risk. The manufacturer assumes no
liability for damage due to non-observance of these limit values.
The EU declaration of conformity loses its validity as soon as modifications
are carried out on the products and/or the components.

1.3 About the documentation

CAUTION

Read through this documentation carefully before putting the instru-

ment into operation. The documentation contains information and
warnings which the user must follow in order to ensure safe operation
of the instrument.

1.3.1 Symbols and conventions

The following symbols and formatting may appear in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, the sec-
ond to the instrument part in the figure.

2 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

Instruction step
Carry out these steps in the sequence shown.
Method Dialog text, parameter in the software
File ▶ New Menu or menu item
[Next] Button or key
WARNING
This symbol draws attention to a possible life-threat-
ening hazard or risk of injury.
WARNING
This symbol draws attention to a possible hazard due
to electrical current.
WARNING
This symbol draws attention to a possible hazard due
to heat or hot instrument parts.
WARNING
This symbol draws attention to a possible biological
hazard.
CAUTION
This symbol draws attention to possible damage to
instruments or instrument parts.
NOTE
This symbol highlights additional information and
tips.

1.4 Safety instructions

1.4.1 General notes on safety

WARNING

Operate this instrument only according to the information contained in

this documentation.

This instrument left the factory in a flawless state in terms of technical

safety. To maintain this state and ensure non-hazardous operation of the
instrument, the following instructions must be observed carefully.

￭￭￭￭￭￭￭￭ 3
 1.4 Safety instructions ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

1.4.2 Electrical safety

The electrical safety when working with the instrument is ensured as part
of the international standard IEC 61010.

WARNING

Only personnel qualified by Metrohm are authorized to carry out service

work on electronic components.

WARNING

Never open the housing of the instrument. The instrument could be

damaged by this. There is also a risk of serious injury if live components
are touched.
There are no parts inside the housing which can be serviced or replaced
by the user.

Supply voltage

WARNING

An incorrect supply voltage can damage the instrument.

Only operate this instrument with a supply voltage specified for it (see
rear panel of the instrument).

Protection against electrostatic charges

WARNING

Electronic components are sensitive to electrostatic charges and can be

destroyed by discharges.
Do not fail to pull the power cord out of the power socket before you
set up or disconnect electrical plug connections at the rear of the
instrument.

4 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

1.4.3 Flammable solvents and chemicals

WARNING

All relevant safety measures are to be observed when working with

flammable solvents and chemicals.
￭ Set up the instrument in a well-ventilated location (e.g. fume cup-
board).
￭ Keep all sources of flame far from the workplace.
￭ Clean up spilled liquids and solids immediately.
￭ Follow the safety instructions of the chemical manufacturer.

1.4.4 Recycling and disposal

This product is covered by European Directive 2012/19/EU, WEEE – Waste
Electrical and Electronic Equipment.
The correct disposal of your old instrument will help to prevent negative
effects on the environment and public health.
More details about the disposal of your old instrument can be obtained
from your local authorities, from waste disposal companies or from your
local dealer.

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 2.1 Front ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2 Overview of the instrument

2.1 Front

Figure 1 Front DS2500 Liquid Analyzer

1 Lid 2 Sample compartment

3 LED display 4 Feet (shock-absorbing)

5 Lamp compartment 6 Cover plate

6 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2 Overview of the instrument

2.2 Rear

Figure 2 Rear DS2500 Liquid Analyzer

1 On/off switch 2 Fuse holder

For switching the instrument on and off

3 Power socket 4 Type plate

Sealed with protective cap

5 LAN connection socket 6 Fan

Sealed with protective cap With filter

￭￭￭￭￭￭￭￭ 7
 2.3 Sample holders ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2.3 Sample holders

Figure 3 DS2500 Liquid Analyzer sample holders

1 DS2500 holder for cuvettes 2 DS2500 holder for flow cells

3 DS2500 holder for disposable vials 4 DS2500 Liquid Wavelength Standard

8 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation

3 Installation

3.1 Unpacking and inspecting the instrument

3.1.1 Packaging
The instrument is supplied in protective packaging together with the sepa-
rately packed accessories. Keep this packaging, as only this ensures safe
transportation of the instrument.

3.1.2 Checks
Immediately after receipt, check whether the shipment has arrived com-
plete and without damage by comparing it with the delivery note.

3.2 Location
The instrument has been developed for operation indoors and may not be
used in explosive environments.
Place the instrument in a location of the laboratory which is suitable for
operation, free of vibrations, protected from corrosive atmosphere, and
contamination by chemicals.
The instrument should be protected against excessive temperature fluctua-
tions and direct sunlight.

3.3 Connecting the instrument to the power grid

WARNING

Electric shock from electrical potential

Risk of injury by touching live components or through moisture on live
parts.
￭ Never open the housing of the instrument while the power cord is
still connected.
￭ Protect live parts (e.g. power supply unit, power cord, connection
sockets) against moisture.
￭ Unplug the power plug immediately if you suspect that moisture has
gotten inside the instrument.
￭ Only personnel who have been issued Metrohm qualifications may
perform service and repair work on electrical and electronic parts.

￭￭￭￭￭￭￭￭ 9
 3.4 Connecting the data cable ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

Connecting the power cord

Accessories Power cord with the following specifications:

￭ Length: max. 2 m
￭ Number of cores: 3, with protective conductor
￭ Instrument plug: IEC 60320 type C13
￭ Conductor cross-section 3x min. 0.75 mm2 / 18 AWG
￭ Power plug:
– according to customer requirement (6.2122.XX0)
– min. 10 A

NOTICE

Do not use a not permitted power cord!

1 Plugging in the power cord

￭ Plug the power cord into the instrument's power socket.
￭ Connect the power cord to the power grid.

3.4 Connecting the data cable

In order to control the DS2500 Liquid Analyzer, connect it to a computer
either directly or via a local network (LAN).
For direct connection to the network card of a computer, use the supplied
data cable.
Additional steps might be required for connecting via your local network.
As network configurations vary considerably across different companies,
exact details are not provided in this manual. Have your network specialist
establish the connection between the instrument and the company net-
work.

Connecting the computer directly

Accessories ￭ DS2500 data cable

￭ Computer with installed control software

1 Remove the protective cap from the LAN connection socket (2-5).

2 Plug the cable into the LAN connection socket (2-5) and tighten it.

10 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation

3 Connect the other end of the data cable to the computer's network
cable connector.

3.5 Switching on the instrument

Switching on the instrument

1 Turn the on/off switch (2-1) to position I.

￭ The LED display on the front of the DS2500 Liquid Analyzer (1-3)
lights up.
￭ The instrument performs a self-test.
￭ The sample compartment lid opens.

2 Wait until the control software has recognized the instrument.

3.6 Initial start-up

The initial start-up of the DS2500 Liquid Analyzer is carried out by trained
and instructed specialists from Metrohm and/or its representative(s).

￭￭￭￭￭￭￭￭ 11
 3.7 Temperature control ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

3.7 Temperature control

The DS2500 Liquid Analyzer supports a temperature range between 25 °C
and 80 °C. The minimum temperature that can be set must be 10 °C
above the ambient temperature Tmin = Tambient + 10 °C
To achieve a temperature of 25 °C, the ambient temperature must be
15 °C. As the ambient temperature in most laboratories is approx. 25 °C,
Metrohm recommends to set the temperature to a minimum of 35 °C.

3.8 Setting up accessories

The following sample cups can be used with the DS2500 Liquid Analyzer:
Intended use Holder for sample cups Order number

Fast and convenient analysis DS2500 holder for 2 mm disposable vials 6.7492.000

DS2500 holder for 4 mm disposable vials 6.7492.010

DS2500 holder for 8 mm disposable vials 6.7492.020

DS2500 holder for 10 mm disposable vials 6.7492.030

High precision DS2500 holder for 1 mm cuvettes 6.7492.100

DS2500 holder for 2 mm cuvettes 6.7492.110

DS2500 holder for 5 mm cuvettes 6.7492.120

DS2500 holder for 10 mm cuvettes 6.7492.130

High sample throughput and automation DS2500 holder for flow cells 6.7493.000

Calibration DS2500 liquid wavelength calibration stan- 6.7494.000

dard

3.8.1 Calibrating the instrument

The DS2500 Liquid Analyzer is calibrated with an external wavelength
standard (see "Calibration with an external wavelength standard", page
13) and with an internal wavelength standard (see "Calibrating the
instrument with an internal wavelength standard", page 13).

WARNING

Hot surface
Danger of burning due to hot components. The sample holder can be
heated to a maximum of 80 °C. After operation, the sample compart-
ment, the sample holder and the sample vessel are very hot.
￭ Wear protective gloves when handling sample holders and samples.

12 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation

Calibration with an external wavelength standard

The external calibration is usually carried out by a regional Metrohm ser-
vice representative during the start-up of the instrument.
If necessary, the external standard can also be obtained separately (article
number 6.7494.000). The user can repeat the external calibration if
needed.

Calibrating the instrument with an external wavelength

calibration standard

Accessories ￭ DS2500 liquid wavelength calibration standard (6.7494.000)

1 Using the wavelength calibration standard

￭ Place the wavelength calibration standard in the sample compart-
ment.
￭ Optionally place the cover plate on the sample compartment. If
the sample holder is heated, the cover plate protects the user
from the heat that is generated.
￭ Tighten the screw.

2 Calibrating the instrument

Start the calibration in the control software (see 8.105.8032 Tutorial
Vision Air Local and 8.105.8036 Tutorial Vision Air Network and
Server).

Calibration with an internal wavelength standard

Carry out the internal calibration once a different type of sample vessel to
the one used in the previous measurement is inserted. The path length is
relevant. Carry out an internal calibration after a DS2500 holder for 2 mm
disposable vials was replaced with a DS2500 holder for 8 mm disposable
vials, for example.

Calibrating the instrument with an internal wavelength

standard

Accessories ￭ Sample holder

1 Inserting the sample vessel

￭ Define with which sample vessel the next measurement is to be
carried out.
￭ Insert the selected sample vessel.

￭￭￭￭￭￭￭￭ 13
 3.8 Setting up accessories ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

NOTICE

If an incorrect sample vessel was inserted for the calibration with

the internal wavelength standard, the error auto linearization
failed may be displayed during the routine analysis.

2 Calibrating the instrument

Start the calibration in the control software (see 8.105.8032 Tutorial
Vision Air Local and 8.105.8036 Tutorial Vision Air Network and
Server).

3 Repeating the calibration

Once a sample vessel with a different path length has been inserted,
repeat the internal calibration. To do this, start with Step 1 again.

For additional information on the calibration with the internal wavelength

standard, see 8.105.8032 Tutorial Vision Air Local or 8.105.8036 Tutorial
Vision Air Network and Server.

3.8.2 Analyzing liquid samples

WARNING

Hot surface
Danger of burning due to hot components. The sample holder can be
heated to a maximum of 80 °C. After operation, the sample compart-
ment, the sample holder and the sample cup are very hot.
￭ Wear protective gloves when handling sample holders and samples.

Fast and convenient analysis

Accessories ￭ Suitable holder for disposable vials (see chapter 3.8, page 12)
￭ Disposable vial
￭ Lint-free cloth
￭ Pipette

1 Preparing the vial

￭ Add the sample liquid to the disposable vial using a pipette.
￭ Wipe away sample residue and fingerprints from the outside of
the disposable vial using a lint-free cloth.

14 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation

2 Inserting the holder for disposable vials

￭ Place the holder for disposable vials in the sample compartment.

Figure 4 Place the disposable vial in the sample compartment.

￭ Tighten the screw.
￭ Insert the disposable vial with sample liquid into the holder.

3 Analyzing a sample
￭ Optionally place the cover plate on the sample compartment. If
the sample holder is heated, the cover plate protects the user
from the heat that is generated.
￭ If the Automatic start function is activated in Vision Air, close
the lid to start the measurement.
If the Automatic start function is not activated in Vision Air,
start the analysis using Vision Air.
The sample is measured during transmission.
Vision Air defines whether the DS2500 Liquid Analyzer performs a
reference scan after analyzing a sample. For this purpose, open the
Settings tab in the Methods area. Define settings for the reference
scan in the Analysis settings group.
If the function is activated, the DS2500 Liquid Analyzer then per-
forms a reference scan. For this purpose, the sample is automatically
moved out of the measuring beam. The DS2500 Liquid Analyzer
records an absorbance spectrum of air as a reference spectrum.

4 Removing the vial

Remove the disposable vial from the holder for disposable vials.

￭￭￭￭￭￭￭￭ 15
 3.8 Setting up accessories ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

The measurement is complete.

Analysis with high sample throughput and automation

Accessories ￭ DS2500 Holder for flow cells (6.7493.000)

￭ Flow cell
￭ 2 tubings, suitable for flow cell

1 Flow cell spring assembly 2 Flow cell positioning spring

3 Screw on sample holder 4 Flow cell assembly bridge

The screw on the sample holder is not part
of the flow cell spring assembly.

1 Loosening the flow cell spring assembly

￭ The spring assembly is mounted to the holder at the time the
instrument is delivered.
There is a screw at the end of each positioning spring. Loosen
both screws.
￭ Separate the spring assembly from the holder.

2 Inserting the DS2500 Holder for flow cells

￭ Place the holder in the sample compartment.
￭ Tighten the screw on the holder.

16 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation

3 Connecting the flow cell

￭ There is an inner thread at the inlet and the outlet of the flow cell.
On each inner thread, mount a tubing with a matching outer
thread.

4 Inserting the flow cell in the DS2500 Holder for flow cells
￭ The flow cell has a window. The holder has openings.
Insert the flow cell in the holder so that the window of the flow
cell is positioned at the openings of the holder.

5 Mounting the flow cell spring assembly

￭ The holder has 2 openings for the positioning springs of the
spring assembly. Place the spring assembly on the holder. The fol-
lowing is to be observed:
– The 2 tubings of the flow cell are in the center of the
bridge.
– The 2 positioning springs are in the openings of the holder.
￭ Fasten the screws on the positioning springs.

6 Connecting the flow cell

￭ Connect the inlet of the flow cell to a sample changer.
￭ Connect the outlet of the flow cell to the waste container.

￭￭￭￭￭￭￭￭ 17
 3.8 Setting up accessories ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

7 Analyzing samples
￭ Start the analysis with Vision Air. Leave the lid open.
The samples are measured in transmission mode.
￭ Vision Air defines whether the DS2500 Liquid Analyzer performs a
reference scan after analyzing a sample. For this purpose, open
the Settings tab in the Methods area. Define settings for the
reference scan in the Analysis settings group.
If the function is activated, the DS2500 Liquid Analyzer then per-
forms a reference scan. For this purpose, the sample is automati-
cally moved out of the measuring beam. The DS2500 Liquid Ana-
lyzer records an absorbance spectrum of air as a reference spec-
trum.
After the reference scan, the spring assembly pushes the flow cell
back into the starting position. The flow cell is again in the mea-
suring beam.
￭ To minimize cross contamination, rinse the flow cell and the cor-
responding tubings after each measurement. To this end, pump
suitable chemicals through the flow cell.

8 Removing the flow cell

￭ Once all samples are measured, remove the flow cell and the
holder. Proceed as follows:
– Separate the connection between flow cell and sample
changer as well as flow cell and waste container.
– Remove the spring assembly.
– Remove the flow cell from the holder.
– Loosen the screw on the holder and remove the holder
from the sample compartment.
The measurements are complete.

18 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Operation

4 Operation
The DS2500 Liquid Analyzer is operated with the control software.
You can find information on control software in the tutorial on control
software (see 8.105.8032 Tutorial Vision Air Local and 8.105.8036 Tuto-
rial Vision Air Network and Server).

￭￭￭￭￭￭￭￭ 19
 5.1 Maintenance by Metrohm Service ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5 Maintenance
The DS2500 Liquid Analyzer requires appropriate care. Excessive soiling of
the instrument leads to functional disruptions and shortens the service life
of the durable mechanical and electronic components.

5.1 Maintenance by Metrohm Service

Maintenance of the DS2500 Liquid Analyzer is best carried out as part of
an annual service appointment by Metrohm specialist personnel. If you
work with caustic and corrosive chemicals, a shorter maintenance interval
is required.
Metrohm Service offers every form of technical advice for maintenance
and servicing of all Metrohm instruments.

5.2 Maintenance by the user

Table 1 Maintenance tasks and intervals

Maintenance task Maintenance interval
Performance test in the non-regulated area monthly
(see 8.105.8032 Tutorial Vision Air Local and
8.105.8036 Tutorial Vision Air Network and Server)
Clean the instrument when necessary
(see chapter 5.2, page 20)
Clean the sample holder when necessary
(see chapter 5.2, page 20)
Clean the sample compartment when necessary
(see chapter 5.2, page 20)
Replace the lamp After a burning time of 3,500 hours
or
(see chapter 5.2, page 20)
if the Performance Test or the Instru-
ment diagnostic Test yields unsatis-
factory results
Check the fan filter and replace it if necessary monthly
(see chapter 5.2, page 20)

20 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

Maintenance task Maintenance interval

Replace the fuse if blown
(see chapter 5.2, page 20)

5.2.1 Cleaning the instrument

The instrument requires appropriate care. Excess soiling of the instrument
may result in functional disruptions and a reduction in the service life of
the durable mechanical and electronic components.
Clean the instrument using a lint-free cloth and ethanol.

NOTICE

Do not use aggressive solvents such as acetone. Aggressive solvents can

damage the surfaces of the instrument.

CAUTION

Spillage of chemicals or solvents

Damage to the instrument due to spillage of chemicals or solvents!
￭ Clean the instrument immediately if chemicals or solvents are spilled
on it.
￭ The plug connections (particularly the power plug) absolutely must
be protected against contamination.

CAUTION

Inward seepage of liquid

Instrument damage through inward seepage of liquid!
￭ The instrument has been designed so that liquid is largely prevented
from being able to get inside the instrument. However, unplug the
power plug immediately if you suspect that corrosive media have
gotten inside the instrument. This is the only way to prevent extreme
damage to the instrument electronics. Contact Metrohm Service
immediately.

WARNING

Only trained personnel may open the instrument's housing.

￭￭￭￭￭￭￭￭ 21
 5.2 Maintenance by the user ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5.2.2 Cleaning the sample holder

Clean the sample holder using a lint-free cloth and ethanol.

NOTICE

Do not use aggressive solvents such as acetone. Aggressive solvents can

damage the surfaces of the instrument.

In the event of heavy soiling, one part of the sample holder can be
cleaned in a dishwasher. The sample holder consists of two parts. The
front part contains no electrical components. The rear part contains elec-
trical components. To separate the two parts from each other, unscrew
the two screws on the front part of the sample holder. Clean the front
part of the sample holder in a dishwasher.

Figure 5 Disassembling the sample holder

5.2.3 Cleaning the sample compartment

Dirt, dust and sample deposits in the sample compartment can influence
the analytical results.
Clean the sample compartment using a lint-free cloth and ethanol.

NOTICE

Do not use aggressive solvents such as acetone. Aggressive solvents can

damage the surfaces of the instrument.

22 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

5.2.4 Replacing the lamp

Replace the lamp once it is blown or when its performance is insufficient.
Signs of insufficient lamp performance include:
￭ Noise impairs the measurements.
￭ The repeatability of the wavelengths deteriorates.
￭ The performance test is no longer completed successfully.

Removing the lamp

Accessories ￭ Screwdriver

WARNING

Electric shock from electrical potential

Risk of injury by touching live components or through moisture on live
parts.
￭ Never open the housing of the instrument while the power cord is
still connected.
￭ Protect live parts (e.g. power supply unit, power cord, connection
sockets) against moisture.
￭ Unplug the power plug immediately if you suspect that moisture has
gotten inside the instrument.
￭ Only personnel who have been issued Metrohm qualifications may
perform service and repair work on electrical and electronic parts.

WARNING

Hot surface
Danger of burning due to hot lamp. The lamp is extremely hot immedi-
ately after operation.
￭ Allow the lamp to cool down for approx. 10 to 15 minutes.
￭ Remove the lamp carefully.

NOTICE

Clean the instrument before replacing the lamp. This prevents dust from
damaging the lamp's reflector.

￭￭￭￭￭￭￭￭ 23
 5.2 Maintenance by the user ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

NOTICE

Spare part
A new spare lamp is available from your Metrohm representative under
the article number 6.7430.050.
￭ We recommend keeping spare lamps in stock.
￭ Only use original lamps in the instrument.

1 Switching off the instrument

￭ Turn the on/off switch (2-1) to the position O.

2 Disconnecting the instrument from the energy supply

￭ Disconnect the power cord.
￭ Wait 10 to 15 minutes until the lamp has cooled down.

3 Opening the lamp compartment

￭ Open the lid of the lamp compartment (1-5).
￭ Take the hex key out of the guide rail.
￭ Unscrew the four sealing plate screws using the hex key and put
them aside.
￭ Remove the sealing plate and put it aside.

24 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

4 Removing the lamp holder

￭ Push the 2 mm white lamp holder inwards.

￭ Rotate the white lamp holder 45° counterclockwise.

￭ Carefully pull the white lamp holder out straight.

￭￭￭￭￭￭￭￭ 25
 5.2 Maintenance by the user ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

￭ Place the lamp on the lid with the reflector facing down.

5 Disconnecting the cables

CAUTION

Functional disruption
Do not unscrew the screw terminals of the black cables.
Only unscrew the screw terminals of the white cables.

26 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

￭ Loosen the screw terminals of the white cables using a small

screwdriver.

￭ Carefully remove the cables from the terminals.

￭ Bend the cables upwards so that they stand vertically.

￭￭￭￭￭￭￭￭ 27
 5.2 Maintenance by the user ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

6 Removing the lamp from the holder

￭ Hold the lamp by the reflector.

￭ Lift the lamp holder off the lamp and the cables.

TIP: Bend the cables to mark the lamp as used.

Installing a new lamp

Accessories ￭ Spare lamp (6.7430.050)

￭ Screwdriver

28 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

CAUTION

Damage to the lamp

Fingerprints and greasy deposits damage the lamp.
Do not touch either the glass part of the lamp or the inside of the
reflector.

1 Keeping the new lamp ready

￭ Take the new lamp out of the packaging.
￭ Position the lamp cables upright so that the cables will fit through
the rectangular opening of the lamp holder.
￭ Place the lamp on the lamp compartment lid with the reflector
facing down.

2 Inserting the lamp into the lamp holder

￭ Guide the lamp cables through the rectangular opening of the
lamp holder.
￭ Attach the lamp holder to the cable side of the lamp. The spring
on the lamp holder keeps the lamp in the correct position.

￭￭￭￭￭￭￭￭ 29
 5.2 Maintenance by the user ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

3 Connecting the lamp cables

￭ Push the two white cables all the way into the corresponding
screw terminal by hand or using tweezers.

￭ Tighten the screw terminals using the small screwdriver.

30 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

4 Inserting the lamp holder

￭ Push the white lamp holder carefully all the way into the opening.

￭ Rotate the white lamp holder 45° clockwise.

￭￭￭￭￭￭￭￭ 31
 5.2 Maintenance by the user ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

￭ Let go of the white lamp holder.

5 Closing the lamp compartment

￭ Place the sealing plate onto the opening. Make sure that no
cables are being pinched.
￭ Insert the four screws and tighten them in crosswise sequence
using the hex key.
￭ Push the hex key into the guide rail on the lid.
￭ Close the lid.

6 Calibrating the instrument

Recalibrate the instrument every time a lamp is replaced.
￭ Switch on the instrument.
￭ Wait for at least 2 hours while the instrument warms up.
￭ Recalibrating the instrument (see 8.105.8032 Tutorial Vision Air
Local and 8.105.8036 Tutorial Vision Air Network and Server).

5.2.5 Replacing the fan filter

Clean the fan filter at least once a month. If the instrument is operated in
a dusty or otherwise dirty environment, check the fan filter weekly or
twice a week as necessary.
The fan is on the rear of the instrument. The filter cover is attached to the
fan filter by means of four plastic latches.

32 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

Replacing the fan filter

Accessories ￭ Fan filter, if replacement is required.

1 Switching off the instrument

￭ Turn the on/off switch (2-1) to the position O.

2 Removing the filter cover

Grab the filter cover with both hands and take it off starting from the
top and then proceeding to the sides.

3 Checking the state of the filter

Take out the filter and inspect it carefully.

￭￭￭￭￭￭￭￭ 33
 5.2 Maintenance by the user ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

￭ If you cannot see any small tears in the filter, clean the filter and
reinstall it.
￭ If the filter is damaged, install a new filter.

4 Cleaning the filter

￭ Blow out the dirty filter with a compressed air duster spray.
￭ Alternative: Rinse the dirty filter with clean water and allow to dry.

5 Mounting the filter

Place the new or cleaned filter symmetrically into the filter cover.

Do not crumple or fold the filter. The edges must form a good seal.

34 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

6 Mounting the filter cover

Mount the filter cover to the frame starting on the bottom and push
it in place until all latches snap in.

7 Switching on the instrument

Turn the on/off switch (2-1) to the position I.

5.2.6 Replacing a fuse

The fuse is located in the fuse holder (2-2) on the rear of the instrument,
directly underneath the on/off switch (2-1).

￭￭￭￭￭￭￭￭ 35
 5.2 Maintenance by the user ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

Replacing the fuse

Accessories ￭ Spare fuse type: 250 V, 5 A, slow-acting fuse, 20 mm

1 Switching off the instrument

￭ Turn the on/off switch (2-1) to the position O.

NOTICE

Unplug the power cord as well. This prevents the instrument from
being switched on accidentally while you insert the fuse.

2 Removing the faulty fuse

￭ Unscrew the fuse holder (2-2) by hand or, if necessary, unscrew
the holder using a size 5 flat-head screwdriver.
￭ Take the faulty fuse out of the holder.

3 Inserting the new fuse

￭ Insert a new fuse of the same type into the holder.

36 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Maintenance

￭ Place the fuse holder back into the opening on the rear of the
instrument and tighten by hand.

4 Switching on the instrument

￭ Plug the power cord back in.
￭ Turn the on/off switch (2-1) to the position I.

￭￭￭￭￭￭￭￭ 37
 6.1 Interfaces ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

6 Technical specifications

6.1 Interfaces
Ethernet connec- Ethernet connection for data transmission to a computer
tion port

6.2 Power connection

Nominal voltage 100–240 V (±10%, autosensing)
range
Frequency 50 and 60 Hz (autosensing)
Power consump- max. 125 W
tion
Protection 5 AT

6.3 Ambient conditions

Nominal function 5 - 40 °C
range At max. 60% humidity, non-condensing
Storage –20 - 70 °C
At max. 93% humidity, non-condensing

6.4 Dimensions
Measurements
Length 490 mm
Width 375 mm
Height 300 mm (closed)
534 mm (opened)

Weight 27 kg
Additional free at least 200 mm (on the sides and rear)
space

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￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Technical specifications

6.5 Housing
Material Steel sheet
Aluminum
ABS - Acrylonitrile butadiene styrene
IP degree of pro- 54
tection of the
sample compart-
ment

￭￭￭￭￭￭￭￭ 39
 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

7 Accessories
Up-to-date information on the scope of delivery and optional accessories
for your product can be found on the Internet. You can download this
information using the article number as follows:

Downloading the accessories list

1 Enter https://www.metrohm.com/ into your Internet browser.

2 Enter the article number (e.g. 2.929.0010) into the search field.
The search result is displayed.

3 Click on the product.

Detailed information regarding the product is shown on various tabs.

4 On the Included parts tab, click on Download the PDF.

The PDF file with the accessories data is created.

NOTICE

Once you have received your new product, we recommend download-

ing the accessories list from the Internet, printing it out and keeping it
together with the manual for reference purposes.

40 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Index

Index
A Front P
Accessories Overview of the instrument .. 6 Power connection ................ 9, 10
Setting up .......................... 12 fuse
Replacing a ......................... 35 R
C Rear
Cleaning the I Overview of the instrument .. 7
instrument .......................... 21 Initial start-up ........................... 11 Replacing a
sample compartment .......... 22 Installation ................................. 9 fuse .................................... 35
sample holder ..................... 22 instrument Replacing the
Connect Cleaning the ....................... 21 fan filter ............................. 32
Power grid ............................ 9 Instrument lamp ................................... 23
Connecting the Switch on ........................... 11
data cable .......................... 10 Instrument description ................ 1 S
Safety instructions ...................... 3
D L sample compartment
data cable lamp Cleaning the ....................... 22
Connecting the ................... 10 Replacing the ..................... 23 sample holder
data connection Cleaning the ....................... 22
Establishing the .................. 10 M Service ....................................... 4
Maintenance ............................ 20 Setting up
E Metrohm Service ...................... 20 Accessories ......................... 12
Electrostatic charge .................... 4 Specifications ........................... 38
Establishing the O Start-up .................................... 11
data connection ................. 10 Operation ................................. 19 Supply voltage ............................ 4
Overview of the instrument
F Front .................................... 6 T
fan filter Rear ..................................... 7 Temperature control ................. 12
Replacing the ..................... 32

￭￭￭￭￭￭￭￭ 41