NIRS XDS RapidContent Analyzer

Manual
8.921.8001EN / 2015-09-07
Metrohm AG
CH-9100 Herisau
Switzerland
Phone +41 71 353 85 85
Fax +41 71 353 89 01
[email protected]
www.metrohm.com

NIRS XDS RapidContent Analyzer

Manual

8.921.8001EN / 2015-09-07 fpe/ahag

Technische Dokumentation
Metrohm AG
CH-9100 Herisau
[email protected]

This documentation is protected by copyright. All rights reserved.

This document has been prepared with great care. However, errors can
never be entirely ruled out. Please send comments regarding possible
errors to the address above.
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

Table of contents
1 Introduction 1
1.1 Instrument description ......................................................... 1
1.2 Intended use ......................................................................... 2
1.3 About the documentation ................................................... 2
1.3.1 Symbols and conventions ........................................................ 2
1.4 Safety instructions ................................................................ 3
1.4.1 General notes on safety ........................................................... 3
1.4.2 Electrical safety ........................................................................ 3
1.4.3 Flammable solvents and chemicals ........................................... 4
1.4.4 Recycling and disposal ............................................................. 4

2 Overview of the instrument 5

2.1 Monochromator .................................................................... 5
2.1.1 Connectors/rear ....................................................................... 5
2.1.2 Status display .......................................................................... 6
2.1.3 Instrument connection ............................................................. 6

3 Installation 7
3.1 Unpacking and inspecting the instrument ......................... 7
3.1.1 Packaging ................................................................................ 7
3.1.2 Checks .................................................................................... 7
3.1.3 Scope of application ................................................................ 7
3.2 Setting up the instrument .................................................... 7
3.2.1 Lifting and transporting instruments ........................................ 7
3.2.2 Ambient conditions ................................................................. 8
3.2.3 General conditions .................................................................. 8
3.2.4 Vibrations and/or shocks .......................................................... 8
3.3 Connecting monochromator to measuring module .......... 9
3.4 Connecting the power supply cable ................................. 10
3.5 Connecting the network cable .......................................... 11
3.6 Switching on the instrument ............................................. 11
3.7 Initial start-up ..................................................................... 12
3.8 Setting up accessories ........................................................ 12

4 Operation 13
5 Operation and maintenance 14
5.1 General notes ...................................................................... 14
5.1.1 Care ...................................................................................... 14

￭￭￭￭￭￭￭￭ III
 Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5.1.2 Maintenance by Metrohm Service .......................................... 14

5.2 Maintenance ....................................................................... 14
5.2.1 Overview ............................................................................... 15
5.2.2 Replacing the fan filter ........................................................... 15
5.2.3 Replacing the lamp ................................................................ 18
5.2.4 Replacing the fuse ................................................................. 26
5.2.5 Cleaning the sampling window .............................................. 28
5.3 Quality management and qualification with Metrohm . . 30

6 Appendix 31
6.1 Accessories for sample compartment ............................... 32
6.1.1 Sample cell ............................................................................ 32
6.1.2 Iris ......................................................................................... 33
6.2 Calibration standards ......................................................... 36

7 Technical specifications 37
7.1 LAN interface ...................................................................... 37
7.2 Power connection ............................................................... 37
7.3 Ambient conditions ............................................................ 37
7.4 Operation ............................................................................ 38
7.5 Safety specifications ........................................................... 39
7.6 Electromagnetic compatibility (EMC) ................................ 39
7.7 Reference conditions .......................................................... 39
7.8 Dimensions/material ........................................................... 40

8 Accessories 41
Glossary 42
Index 44

IV ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures

Table of figures
Figure 1 Front - measuring instrument ............................................................ 5
Figure 2 Rear - monochromator ...................................................................... 5
Figure 3 Status display .................................................................................... 6
Figure 4 Instrument connection ...................................................................... 6
Figure 5 On/off switch .................................................................................. 11
Figure 6 Mini sample cup with disposable back ............................................. 35
Figure 7 Vials ................................................................................................ 35
Figure 8 Transflection vessel with gold or stainless steel diffuse reflector ....... 35

￭￭￭￭￭￭￭￭ V
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1 Introduction
This manual gives you a comprehensive overview of the installation and
maintenance of the NIRS XDS RapidContent Analyzer. The NIRS XDS Rap-
idContent Analyzer is operated with the control software. You can find
information on operating the instrument in the tutorial and in the manual
for the control software.

NOTE

You can request application descriptions in the form of

Application Notes and Application Bulletins from your
Metrohm representative or download them from
http://www.metrohm.com.

1.1 Instrument description

The NIRS XDS RapidContent Analyzer is a measuring instrument for reflec-
tion measurement in the visible to near-infrared wavelength range.
The complete NIRS XDS RapidContent Analyzer measuring instrument
consists of two modules, monochromator and measuring module.
The monochromator operates in the range from 400 to 2,500 nm.
The measuring module to the NIRS XDS RapidContent Analyzer is
equipped with the corresponding accessories for specific samples and can
be replaced with other measuring modules during ongoing operation
(hot-swappable).
The NIRS XDS RapidContent Analyzer is designed for quality monitoring in
production processes and can be applied for the following purposes:
￭ Quick and non-destructive incoming goods inspection of raw materials
￭ Production process monitoring
￭ Final inspection of finished products
The NIRS XDS RapidContent Analyzer can be used to measure the follow-
ing sample types:
￭ Powders
￭ Coarse solids/granulates
￭ Solids/coatings/paper
￭ Tablets/capsules
￭ Turbid liquids
￭ Pastes/creams

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 1.2 Intended use ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

￭ Viscous liquids/gels
￭ Clear liquids
The NIRS XDS RapidContent Analyzer is operated with the control soft-
ware via an external computer.

1.2 Intended use

The NIRS XDS RapidContent Analyzer is designed for use in production
facilities. It can be used for incoming goods inspection or for production
process monitoring.
This instrument is suitable for measuring chemicals and flammable sam-
ples. Usage of the NIRS XDS RapidContent Analyzer therefore requires the
user to have basic knowledge and experience in handling toxic and caustic
substances. Knowledge with respect to the application of the fire preven-
tion measures prescribed for laboratories is also mandatory.

1.3 About the documentation

CAUTION

Please read through this documentation carefully before putting the

instrument into operation. The documentation contains information
and warnings which the user must follow in order to ensure safe opera-
tion of the instrument.

1.3.1 Symbols and conventions

The following symbols and formatting may appear in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, the sec-
ond to the instrument part in the figure.
Instruction step
Carry out these steps in the sequence shown.
Method Dialog text, parameter in the software
File ▶ New Menu or menu item
[Next] Button or key
WARNING
This symbol draws attention to a possible life-threat-
ening hazard or risk of injury.

2 ￭￭￭￭￭￭￭￭
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WARNING
This symbol draws attention to a possible hazard due
to electrical current.
WARNING
This symbol draws attention to a possible hazard due
to heat or hot instrument parts.
WARNING
This symbol draws attention to a possible biological
hazard.
CAUTION
This symbol draws attention to possible damage to
instruments or instrument parts.
NOTE
This symbol highlights additional information and
tips.

1.4 Safety instructions

1.4.1 General notes on safety

WARNING

This instrument may only be operated in accordance with the specifica-

tions in this documentation.

This instrument has left the factory in a flawless state in terms of technical
safety. To maintain this state and ensure non-hazardous operation of the
instrument, the following instructions must be observed carefully.

1.4.2 Electrical safety

The electrical safety when working with the instrument is ensured as part
of the international standard IEC 61010.

WARNING

Only personnel qualified by Metrohm are authorized to carry out service

work on electronic components.

￭￭￭￭￭￭￭￭ 3
 1.4 Safety instructions ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

WARNING

Never open the housing of the instrument. The instrument could be

damaged by this. There is also a risk of serious injury if live components
are touched.
There are no parts inside the housing which can be serviced or replaced
by the user.

Supply voltage

WARNING

An incorrect mains voltage can damage the instrument.

Only operate this instrument with a mains voltage specified for it (see
rear panel of the instrument).

1.4.3 Flammable solvents and chemicals

WARNING

All relevant safety measures are to be observed when working with

flammable solvents and chemicals.
￭ Set up the instrument in a well-ventilated location (e.g. fume cup-
board).
￭ Keep all sources of flame far from the workplace.
￭ Clean up spilled liquids and solids immediately.
￭ Follow the safety instructions of the chemical manufacturer.

1.4.4 Recycling and disposal

This product is covered by European Directive 2002/96/EC, WEEE – Waste
from Electrical and Electronic Equipment.
The correct disposal of your old equipment will help to prevent negative
effects on the environment and public health.
More details about the disposal of your old equipment can be obtained
from your local authorities, from waste disposal companies or from your
local dealer.

4 ￭￭￭￭￭￭￭￭
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2 Overview of the instrument

Figure 1 Front - measuring instrument

1 Status display 2 Monochromator

3 Measuring module

2.1 Monochromator
2.1.1 Connectors/rear

Figure 2 Rear - monochromator

1 On/off switch 2 Fuse holder

￭￭￭￭￭￭￭￭ 5
 2.1 Monochromator ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

3 Power socket 4 Covering

5 Fan 6 Network connection socket

2.1.2 Status display

Figure 3 Status display

1 Instrument on 2 Measurement ongoing

3 Connected to network 4 Lamp on

5 Monochromator connected to measur-

ing module

2.1.3 Instrument connection

The two modules are connected via mechanical, optical and electrical
interfaces, combining monochromator and measuring module to one
measuring instrument.

Figure 4 Instrument connection

1 Locking lever 2 Optical interface

3 Mechanical interface 4 Electrical interface

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￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation

3 Installation

3.1 Unpacking and inspecting the instrument

3.1.1 Packaging
The instrument is supplied in highly protective special packaging together
with the separately packed accessories. Keep this packaging, as only this
ensures safe transportation of the instrument.

3.1.2 Checks
Immediately after receipt, check whether the shipment has arrived com-
plete and without damage by comparing it with the delivery note.

3.1.3 Scope of application

The NIRS XDS RapidContent Analyzer is designed for offline use in the lab-
oratory or for monitoring production processes.

3.2 Setting up the instrument

Like most high-precision instruments, the NIRS XDS RapidContent Ana-
lyzer is sensitive to ambient conditions, which may negatively influence its
performance and shorten its service life. The following guidelines have to
be observed when the instrument is set up and put into operation:

3.2.1 Lifting and transporting instruments

WARNING

Heavy modular instruments

Incorrect handling when lifting and transporting can lead to injuries and
damages.
￭ Instrument modules must be disconnected for moving and lifting
(see Chapter 3.3, page 9).
￭ Only lift or move heavy instruments with caution and/or the appro-
priate auxiliary tools.
￭ Only transport heavy instruments on a trolley.
￭ Put instruments down carefully to avoid damage to the optical-
mechanical elements.

￭￭￭￭￭￭￭￭ 7
 3.2 Setting up the instrument ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

NOTE

Dimensions and weights

The dimensions and weights are listed in the technical specifications
(see Chapter 7.8, page 40).

3.2.2 Ambient conditions

The ambient conditions are decisive for a proper functioning and to
ensure accurate measured values. These conditions are listed in the techni-
cal specifications (see Chapter 7.3, page 37).
High humidity and climatic fluctuations caused by unstable ambient condi-
tions hamper the instrument's stability in respect to calibration and mea-
suring accuracy.

NOTE

Problems during calibration/measurement

If the expected values are not obtained during calibration and the test
runs, then you should check the ambient conditions.
Draft (air conditioning, open windows, etc.) and exposure to direct sun-
light should be prevented.
Make sure to allow enough free space (on the sides and the back at
least 75 mm) around the instrument to prevent heat accumulation.

3.2.3 General conditions

Dust and dirt may compromise the instrument's cooling and should there-
fore be prevented as far as possible.
The maintenance procedures for the fan filter are described as follows (see
Chapter 5.2.2, page 15).

3.2.4 Vibrations and/or shocks

Vibrations and shocks interfere with the sensitive optical and mechanical
components and can compromise calibration and measuring accuracy.
Do not set up other instruments that cause vibrations and shocks (mills,
mixers, stirrers, etc.) on the same workplace as the NIRS XDS RapidCon-
tent Analyzer.
Set the instrument up on a stable workplace that does not pass on vibra-
tions (e.g. typing on keyboard).

8 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation

3.3 Connecting monochromator to measuring module

CAUTION

Mechanical damage
Rough and careless handling may damage the connection elements.
￭ Set the instrument up on a level workplace.
￭ Align the instrument parts correctly before pushing them together.
￭ Do not use excessive force.

Connecting monochromator to measuring module

1 Positioning the monochromator

￭ Position the monochromator on the laboratory table in the shown
position.

2 Positioning measuring module and pushing together

￭ Align the measuring module with the monochromator and push
together.

￭￭￭￭￭￭￭￭ 9
 3.4 Connecting the power supply cable ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

3 Locking monochromator and measuring module

￭ Push the locking lever down to connect the two instrument parts.

3.4 Connecting the power supply cable

The NIRS XDS RapidContent Analyzer instrument contains a permanently
installed power supply unit and can be directly connected to the power
supply with a power supply cable.
The power supply unit automatically supports operating voltages between
100 and 240 VAC at 50 / 60 Hz. The maximum power consumption is 750
watt.

10 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation

3.5 Connecting the network cable

In order to control the NIRS XDS RapidContent Analyzer, it is connected to
a computer either directly or via a local network (LAN). Use the supplied
crossover network cable for connecting the instrument directly to a com-
puter's network card.
For a connection via your local network, you need a network cable.
As network configurations vary considerably across different companies, a
full discussion is not possible in this manual. We recommend that you
have your network specialist establish the connection between the instru-
ment and the company network.

NOTE

Direct connection to computer

When directly connecting the measuring instrument to a computer, no
other network card for connection to a local network may be installed
at the same time.
This leads to communication errors and disruptions.
￭ In network operation, connect the measuring instrument via the net-
work as well.

3.6 Switching on the instrument

Use the switch at the rear to switch on the instrument.

Figure 5 On/off switch

￭￭￭￭￭￭￭￭ 11
 3.7 Initial start-up ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

3.7 Initial start-up

The initial start-up of the instrument is always carried out with the control
software.
You can find detailed information on the procedure in the tutorial for the
control software.

3.8 Setting up accessories

Metrohm offers a wide range of accessories for the NIRS XDS RapidCon-
tent Analyzer instrument.
A detailed description of how to use the accessories can be found in the
appendix (see Chapter 6, page 31).

12 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Operation

4 Operation
Apart from the main switch for switching on and off, the NIRS XDS Rapid-
Content Analyzer instrument does not have any other controls.
The complete instrument configuration, calibration and measurement is
set up and operated via the control software.

￭￭￭￭￭￭￭￭ 13
 5.1 General notes ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5 Operation and maintenance

5.1 General notes

5.1.1 Care
The NIRS XDS RapidContent Analyzer requires appropriate care. Excess
contamination of the instrument may result in functional disruptions and a
reduction in the service life of the otherwise sturdy mechanics and elec-
tronics.
Spilled chemicals and solvents should be removed immediately. In particu-
lar, the plug connections on the rear of the instrument should be protec-
ted from contamination.

CAUTION

Although this is largely prevented by design measures, Metrohm Service

should immediately be notified if aggressive substances have found
their way into the instrument.

5.1.2 Maintenance by Metrohm Service

Maintenance of the NIRS XDS RapidContent Analyzer instrument is best
carried out as part of annual service, which is performed by specialist per-
sonnel from Metrohm. A shorter maintenance interval may be necessary if
you frequently work with caustic and corrosive chemicals.
Metrohm Service offers every form of technical advice for maintenance
and service of all Metrohm instruments.

5.2 Maintenance
The instrument maintenance for the NIRS XDS RapidContent Analyzer is
designed to be easy to carry out.
The optical housing of the monochromator is sealed to prevent contami-
nation of critical parts and minimize maintenance.

14 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation and maintenance

NOTE

Do not attempt to open the optical housing of the monochromator.

There are no parts inside the housing which can be serviced by the
user.
Damages resulting from opening the instrument are not covered by the
warranty.

5.2.1 Overview

NOTE

Maintenance log
The control software features a maintenance log in the diagnosis data-
base to keep track of maintenance activities. It can be used to record
information on tests and maintenance work and to store comments.

NOTE

Instrument environment
Check regularly that no other instruments producing vibrations or other
immissions that could be transmitted to the NIRS XDS RapidContent
Analyzer are in proximity. Such immissions can cause spectral interfer-
ences which compromise the calibration and the measuring accuracy.

5.2.2 Replacing the fan filter

The fan filter should be checked at least once a month. If the instrument is
operated in a dusty or otherwise dirty environment, then a check is
required once or even twice a week.

Replacing the fan filter

The fan is located on the rear of the instrument. The filter cover is
attached to the fan filter by means of four plastic latches.

1 Disconnecting the instrument from the power supply

￭ Turn the on/off switch to the position O.
￭ Pull out the power supply cable.
￭ Remove the network cable (optional).

￭￭￭￭￭￭￭￭ 15
 5.2 Maintenance ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2 Removing the filter cover

￭ Grab the filter cover with both hands and gently take it off start-
ing on top.

3 Cleaning/replacing the filter

￭ Remove the filter from the cover and examine it.
￭ If the filter shows no damage, then it can be cleaned and used
again.
￭ If the filter is damaged, then a spare filter of the same type has to
be used.

16 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation and maintenance

￭ Place the cleaned or new filter symmetrically into the filter cover.
Make sure the filter material is correctly positioned and is not
wrinkled or folded. The edges should form a good seal.

4 Mounting the filter cover

￭ Mount the filter cover to the frame starting on the top and push it
in place until all latches snap in.

￭￭￭￭￭￭￭￭ 17
 5.2 Maintenance ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5 Connecting the instrument

￭ Plug in the network cable.
￭ Plug in the power supply cable.
￭ Switch on the instrument.

5.2.3 Replacing the lamp

Replacing the lamp

The lamp must be replaced if it is defective or when its performance is

insufficient. Signs of an insufficient lamp performance include:
￭ Measurements are impaired by noise.
￭ The repeatability of the wavelengths is deteriorating.
￭ The performance test is no longer completed successfully.

18 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation and maintenance

WARNING

Electric shock
There is a danger of life-threatening electric shock if an instrument con-
nected to the power supply is opened.
￭ Remove the power supply cable before starting with the according
maintenance procedure.

WARNING

Hot surface
Immediately after use, the lamp is extremely hot and can cause burns.
￭ Allow the lamp to cool down for approx. 10 to 15 minutes.
￭ Remove the lamp with appropriate care.

NOTE

Spare part
A new spare lamp is available from your Metrohm distributor under the
article number 6.7430.000.
￭ It is advisable to keep spare lamps in stock.
￭ Only original lamps must be used in the instrument.

1 Disconnecting the instrument from the power supply

￭ Turn the on/off switch to the position O.
￭ Pull out the power supply cable.
￭ Remove the network cable (optional).
￭ Wait 10 to 15 minutes until the lamp has cooled down.

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 5.2 Maintenance ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2 Removing the lamp covering

￭ Loosen the six knurled screws until they are free.
￭ If the screws are too tight, loosen them with a screwdriver.
￭ Carefully remove the back panel and put it aside.

NOTE

The built-in lamp is the only part subject to maintenance work.

All other construction elements are maintenance-free and must
not be opened or removed.

This overview shows the area inside the rear covering.

The lamp box is located in the lower left corner.

20 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation and maintenance

3 Loosening the lamp cables

The cable clips for connecting the lamp are in the upper right corner
of the lamp box.
The lamp itself is secured with a quick-opening clamping fixture. On
the lamp is a black arrow, which has to be aligned with the milled
groove at the top of the mounting area.
Loosen the screw terminals using a screwdriver and pull out the
spade terminals.
Do not remove the terminal screws.

4 Removing the lamp holder

￭ Push the lamp holder to the inside and then rotate it clockwise (to
the right) until it is completely unlocked.
￭ Remove the lamp holder with the lamp from the lamp box.

￭￭￭￭￭￭￭￭ 21
 5.2 Maintenance ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5 Replacing the lamp

CAUTION

Damage to the lamp

Fingerprints and greasy deposits may damage the lamp.
Do not touch the glass part of the lamp or the inner side of the
reflector.

￭ Remove the lamp from the lamp holder and replace it with a new
lamp.

NOTE

Disposal
Follow the country-specific regulations and guidelines to dispose
of the old lamp.

22 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation and maintenance

6 Inserting the lamp holder

￭ Place the lamp into the opening and align the black arrow with
the milled groove (on top).
￭ Position the lamp holder over the lamp and the locking bolts.
￭ Carefully push the lamp holder down, rotate anti-clockwise (to
the left) and lock.

The following image shows the lamp in the correct position with the
black arrow facing the top groove.

￭￭￭￭￭￭￭￭ 23
 5.2 Maintenance ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

7 Connecting the lamp cables

￭ Place the two spade terminals into their according screw terminal
and tighten with a screwdriver.

NOTE

Polarity
The polarity is irrelevant.

8 Attaching the lamp covering

￭ Position the covering with the screws over the thread bore holes.
￭ Fasten the screws by hand.

24 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation and maintenance

9 Connecting the instrument

￭ Plug in the network cable.
￭ Plug in the power supply cable.
￭ Switch on the instrument.

10 Connecting the instrument to the control software

￭ Start the control software and connect to the instrument.
￭ Connect the instrument according to the specific procedure (see
tutorial) to the control software.
￭ The lamp symbol of the status display on the monochromator
lights up.
￭ The instrument warms up and a message is shown in the control
software until the instrument is stable enough for further use.

￭￭￭￭￭￭￭￭ 25
 5.2 Maintenance ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

NOTE

Stabilizing time
The instrument features a monitoring function for stabilizing which
can be deactivated in the control software. If the monitoring is
deactivated, the instrument takes about 20 to 30 minutes for cor-
rect stabilizing.

11 Calibrate the instrument

The instrument has to be recalibrated every time a lamp is replaced.
￭ Calibrate the instrument according to the specific procedure (see
tutorial for the control software).
The instrument is ready for operation again once the calibration and
the according tests have been carried out successfully.

5.2.4 Replacing the fuse

Replacing the fuse

1 Disconnecting the instrument from the power supply

￭ Turn the on/off switch to the position O.
￭ Pull out the power supply cable.
￭ Remove the network cable (optional).

2 Removing the fuse holder

￭ Pull out the fuse holder with a screwdriver.

26 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation and maintenance

3 Replacing the fuse

￭ Remove the old fuses from the fuse holder and replace with new
fuses (see Chapter 7.2, page 37).
￭ Insert the fuse holder with the new fuses into the opening until it
latches.

4 Connecting the instrument

￭ Plug in the network cable.
￭ Plug in the power supply cable.
￭ Switch on the instrument.

￭￭￭￭￭￭￭￭ 27
 5.2 Maintenance ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5.2.5 Cleaning the sampling window

Cleaning the sampling window

The sampling window should be checked and cleaned at regular intervals.

Dirt, dust and sample residue on the sampling window can impair the
analytical results.
Cleaning can be performed any time, even when the instrument is in use
and, if necessary, between samples.

CAUTION

Surface damage
Do not use strong solvents such as acetone that can damage the instru-
ment surface permanently.
If needed, use a cloth moistened with isopropanol (do not soak).

1 Wiping the sampling window

￭ Remove dirt and sample residue from the sampling window using
a clean microfiber cloth suitable for optics.

28 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation and maintenance

2 Wiping away dry residue

￭ After the cleaned surface has dried, the remaining dust or lint can
be carefully wiped away with a brush (from the accessory kit).
￭ Repeat this process until the sampling window is free from con-
tamination.

￭￭￭￭￭￭￭￭ 29
 5.3 Quality management and qualification with Metrohm ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

5.3 Quality management and qualification with

Metrohm
Quality management
Metrohm offers you comprehensive support in implementing quality man-
agement measures for instruments and software.

Qualification
Please contact your local Metrohm representative for support in qualifica-
tion of instruments and software. The Installation Qualification (IQ)
and Operational Qualification (OQ) are offered by Metrohm represen-
tatives as a service. They are carried out by trained employees using stan-
dardized qualification documents and in accordance with the currently
applicable requirements of the regulated industry.

Maintenance
The electronic and mechanical functional groups of Metrohm instruments
can and should be checked by specialist personnel from Metrohm as part
of a regular preventive maintenance schedule. Please ask your local
Metrohm representative regarding the precise terms and conditions
involved in concluding a corresponding maintenance agreement.
For detailed information on this topic, please visit www.metrohm.com.

30 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Appendix

6 Appendix
CAUTION

Sample preparation
Spilled sample material can enter the instrument and cause damages.
￭ Prepare samples outside of the instrument.
￭ Use appropriate sample cups.
￭ After filling, the sample cup must be clean on the outside.

NOTE

Cleanliness of sample cups

Only clean and flawless sample cups ensure correct measurements.
Use only clean sample cups and replace them if there is any doubt.

NOTE

Cleaning validation
Pharmaceutical applications require validation of the cleaning process
to ensure cleanliness requirements regarding sample handling are met.

NOTE

Control software
The operation of the control software with the required settings and
operating steps is described in the tutorial.

￭￭￭￭￭￭￭￭ 31
 6.1 Accessories for sample compartment ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

6.1 Accessories for sample compartment

6.1.1 Sample cell
The sample cell has a glass bottom and is used to measure sample materi-
als with irregular structures (e.g. granulates, fibers, mill material etc.) or for
bigger flat samples (e.g. films, textiles etc.). The sample material is scan-
ned in the longitudinal direction of the sample cell over several positions
in order to obtain a representative spectrum.

NOTE

Restriction
The NIRS XDS RapidContent Solids Analyzer instrument does not
have a tray slide drive.

Setting up the sample cell

The sample cell is set up in the instrument as follows:

1 Inserting tray slide

￭ Position the tray slide on the rear centering pins in the instrument
and secure it with the knurled screw.

2 Inserting the sample cell

￭ Latch the loaded sample cell onto the tray slide.

32 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Appendix

3 Defining measuring positions

￭ Enter the required settings for the type and number of measure-
ments into the control software.
￭ Carry out the measurements.

6.1.2 Iris
The iris is a universal device for positioning sample cups in an instrument.

Setting up the iris

The iris is set up in the instrument as follows:

1 Defining measuring settings

￭ Enter the required settings for the type of measurements into the
control software.

2 Inserting the iris

￭ Insert the iris onto the front centering pins in the instrument.

￭￭￭￭￭￭￭￭ 33
 6.1 Accessories for sample compartment ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

3 Positioning the sample cup

￭ Place the sample cup into the iris opening.
￭ Close the iris using the handle until the sample cup is centered.
￭ Open the iris again for the measurement.

The following sample cups can be used by way of example:

34 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Appendix

Figure 6 Mini sample cup with disposable back

Figure 7 Vials

Figure 8 Transflection vessel with gold or stainless steel diffuse

reflector

￭￭￭￭￭￭￭￭ 35
 6.2 Calibration standards ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

6.2 Calibration standards

NOTE

Choosing the calibration standard

The necessary calibration standards for the calibration of the measuring
instrument are listed in the tutorial for the control software under the
respective measuring modules.

36 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 7 Technical specifications

7 Technical specifications

7.1 LAN interface

RJ-45 Ethernet connection socket for the data transfer to the PC with the
control software via direct connection or via the network.

7.2 Power connection

Nominal voltage 100 - 120 V and 220 - 240 V (±10%, autosensing)
range
Frequency 50 and 60 Hz (autosensing)
Power consump- 750 VAmax
tion
Fuse Diameter 5 mm, length 20 mm
5.0 ATH (slow-acting)
2 pieces per instrument

7.3 Ambient conditions

Temperature
range
Operation 5 - 35 °C
Storage –20 - 70 °C
Transport –20 - 70 °C

Humidity < 93% relative humidity, no condensation

￭￭￭￭￭￭￭￭ 37
 7.4 Operation ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

7.4 Operation
Measuring mode Reflection
Wavelength range 400 - 2,500 nm
Detectors Silicon (400 - 1,100 nm),
Lead sulfide (1,100 - 2,500 nm)
Optical bandwidth 8.75 nm (±0.10 nm)
Spectral data 0.5 nm
interval
Number of data 4,200
points per spec-
trum
Scan rate 2 scans/second
Wavelength accu- < 0.05 nm (NIST SRM 1920)
racy
Wavelength preci-
sion
Based on one < 0.005 nm
instrument
Based on an < 0.020 nm
instrument
group

Photometric noise
400 - 700 nm < 50 µAU
700 - 2,200 nm N/A
700 - 2,500 nm < 20 µAU
850 - 1,100 nm N/A
1,100 - 1,600 N/A
nm

38 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 7 Technical specifications

7.5 Safety specifications

This instrument fulfills the following electrical safety requirements:
CE marking in accordance with the EU directives:
￭ 2006/95/EC (Low Voltage Directive, LVD)
￭ 2004/108/EC (EMC Directive, EMC)

Design and testing According to EN/IEC/UL 61010-1, CSA-C22.2 No. 61010-1, protection
class I, EN/IEC 60529, degree of protection IP52.
Safety instructions This document contains safety instructions which have to be followed
by the user in order to ensure safe operation of the instrument.

7.6 Electromagnetic compatibility (EMC)

Emission Standards fulfilled:
￭ EN/IEC 61326-1
￭ EN/IEC 61000-6-1
￭ EN/IEC 61000-6-3

Immunity Standards fulfilled:

￭ EN/IEC 61326-1
￭ EN/IEC 61000-6-1
￭ EN/IEC 61000-6-3

7.7 Reference conditions

Ambient tempera- +25 °C (±3 °C)
ture
Relative humidity ≤ 60 %
Instrument status > 30 minutes in operation
Validity of the After adjustment
data

￭￭￭￭￭￭￭￭ 39
 7.8 Dimensions/material ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

7.8 Dimensions/material
Monochromator
Dimensions
Width 380 mm
Height 348 mm
Depth 335 mm

Weight 21.0 kg
Material
Housing Steel sheet

NIRS XDS RapidContent Analyzer module

Dimensions
Width 380 mm
Height 351 mm
Depth 275 mm

Weight 15.5 kg
Material
Housing Steel sheet

40 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 8 Accessories

8 Accessories
Up-to-date information on the scope of delivery and optional accessories
for your instrument can be found on the Internet. You can download this
information using the article number as follows:

Downloading the accessories list

1 Type http://partslists.metrohm.com into your Internet browser.

The Partslists webpage will be displayed.

2 Select the desired output language.

3 Enter the article number (e.g. 2.884.0010) and click on the Gener-
ate PDF command.
The PDF file with the accessories data will be created in the language
selected.

NOTE

When you receive your new instrument, we recommend downloading

the accessories list from the Internet, printing it out and keeping it
together with the manual for reference purposes.

￭￭￭￭￭￭￭￭ 41
 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

Glossary
AU
Absorbance Units; unit of the (actually dimensionless) absorbance.

Data interval
Distance of nearby data points on the wavelength axis; depends on the
angle between nearby grid positions. Not to be confused with the optical
bandwidth; the spectral data interval does not show the optical resolution
of the spectrometer.

Optical bandwidth
The optical bandwidth is the spectral broadening of an ideal monochro-
matic light source with a spectrometer. It is determined by the spectral
dispersion of the monochromator, among other things.

Optical pathlength
Distance a light beam covers in a sample from entry point to exit point. In
transmission measurements of clear samples, the optical pathlength is the
same as the thickness of the sample, in reflection measurements it
depends on different factors (particle size, packing density, and others).

Photometric noise
Statistical fluctuations of the measured absorbance.

Reflection measurement
Reflection measurements are performed on diffuse scattering or opaque
materials. Hereby the light that is remitted out of the sample by the scat-
tering angle is detected.

Transflection measurement
Transflection measurements enable the measurement of absorption spec-
tra of transparent samples in reflection geometry. Hereby the light going
through the sample is reflected with a mirror in the direction of the
incoming light beam and collected, for example with a fiber.

Transmission measurement
Transmission measurements are performed on transparent samples.
Hereby the light that directly goes through the sample (along the optical
axis) is detected.

Wavelength accuracy
Absolute deviation of measured and actual wavelength.

42 ￭￭￭￭￭￭￭￭
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Glossary

Wavelength precision
Variance of the measured wavelength at repeated measurements with a
single instrument or a group of instruments.

￭￭￭￭￭￭￭￭ 43
 Index ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

Index
A Maintenance agreement .......... 30 Q
Accessories Metrohm Service ...................... 14 Quality management ................ 30
Set up ................................ 12
O S
I Operational qualification .......... 30 Safety instructions ...................... 3
Installation qualification ............ 30 Sample compartment ............... 32
Instrument P Sample cup
Switch on ........................... 11 Power supply ............................ 10 Sample cell ......................... 32
Power supply unit ............... 10 Service ....................................... 3
M Power supply unit ..................... 10 Start-up .................................... 12
Mains voltage ............................. 4

44 ￭￭￭￭￭￭￭￭