Chemistry Practical

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BEBE#

I n d e X
S. Name of the Experiment Page Date of Date of
No. No. Experiment Submission
o1Cstimah'on o Soclitum 01-02
Liunbonale dod Soclium
bi tanbonale presenl ina
mintune
02SAimadion ol nalie 03-04
attd by HEratine i
b

with kMa04
CAmahion o fet in 05-6
Mohy Salk Using Polauitumn
peamanejanatpoAastsium
cluchyomute.
D4stimahon oLul) -09
lon lodomemially Uins
Ala, S03
05Sepcnahion Ominttue l042
by thiomakoejraphy
D6. Uelechon mAra 13-4
elemen! CAL,L d) hjn
OY9anC (ompouncll
ovneavoeoeneooee
pt. No. 01 Page No. 01

AIM OF THE EXPERIMENT


o estimaBe eamoun ok tanbonale and
n d biCanbo0ake
in a nixdeure.

Pocedune
Pant Shandandisaion o ularic aud CHa So.)
Gdrengdb ol lgSO4=Sq
SAsenadb o o Nag COg S=L.0lN

5 m 0.b1 N 22.4X

5Xol 112 N.

pan
DipeAeoul 25mol. qiven mindtune Soluhoon n Conia!
a

Hn. Ad 1-2chop' henopthaine inclcator. the Solution


bume Pin {oloun. mle _u-th sAancland aud Aaken in
unetk Ihe end poinB is ocen to bi disappeanante of
ilbe V,.
Pink toloun.ake 3 fon(ocden1 Teackhe.ll 2dvop
PinK
:rale the above mintune solusion Lwit
me-ty O1eoee aquny SAancland s o 4aken in a
bune The encd poin is Jounal lo be 1* pink oloun
eke 2 (oncundaal aalinas. e l il Le V_
,laudakion-1 (Slandanelisabion ot Hhsos)
N obs | No,t0,LBR (inml) FeRin) FBR-LBR
CDenonce)KeMank
25 22.5 22.5 oua
22.5 4.9
suneesnt
23.4
3
25 2.4 224 Carnor dant

h A5 22-4 41. 224


abulatiop-2
No obs. radion ,oith -Phenplhaln Ttatiowh Meth orang
ABR FBR D:/enenteiBR FBR DHenence
4.1 4. 145 10.4
11.5 24 0.4
29 31 4.1 43.5 U4

Calulaion
Amoun o Nall 2,
Ameunt o NaHCog 3
1 0 - 2=23 Ce
Man Ala;C0a SX2X53
112 x 2 x93 =4¢(5
oAlaH
Mao CDq S212 x21 X4
25401
ResL
Amoun oo AlaH C0 is 21 2n2l wmountol Na,lDa s
6.2 .May Ala H0 s 251-DI aolNlallg le
415
.No. 02 P'age N. 0

AIM OF THE EXPERIMENT


Ghmakíon o 0Malit liel ung KMnO4 Soluhon.

PROCC DURE
ake 25L o oxalic lid in 250 te m easunin lak
Make up ae Nolume adhh leskilleduaten lo Prepaue
homGeneous Soluthon.
Pipploul
P iPp 2te blhi plkilles Coluhion n a oniCal
lasx
5om AN H2S04 and tarm upto 60c 100'c
sale wih KMA04 Solukion aken in a bunellr b
ho The end pin ound o be fade Pin white
pndox 20 Seconel.

QBSERVATIDN
The maun o OMalc aied eken inu ppele 25ml
Volume o KMnO4 Coleio.n laken i n bunee V

AtBLATnON.
TeR in.) FBRCincc) DiWenexe
O 23.6 23
23.G 416
3 237 23.7
Expt. No P'age N 04

ÇALCULATlON
GtsengthD KMnO, VS,VS
a5 x 1.01 N)-23. xS2
S2 25 x1.ol 0659 kMO4
23.7

23.1Cc S 62XIO1 221-o.150


Do00

a Co clllide malr aue


elilluded solutioa ondtih 0g
o d Soluion tondaun 0:15 Onclit aud
2

1000Ccelilule dColdion condaun l5x 10o0 Onalc


2 aiel
Date

Expt. No. 03 Page No. 0 5

AIM OFTHE EXPERIMENIT


sAimalion o Ee* in Mo Salk uxho Polassiun poruman
Canate ttomt. _and po-aiuo elichromate..

Theony
Pipile ouk
Pipee ectN/b) Mohy' Scalk inlo a A5oc
Conitallask clilike ilap to - e te:mank _wk eliski lles
Wakenby shakin ta prepan e eu homo sienecus
Solukion.

PROCEDURE
Pipele bul 250 D this plellukel talution inloa
Lonital lask Add9soc CI/ID) Ha So4 aliel anel 4tde
EwHkMad4 Coluctonakeo ia a bunete he end
Poin Cund tobe pink.tolatn Teuk e 3 Contorcland
eadinS
CALCOLATION
25 t o ltte Solutioo -V2 (C o S KMn

lo0oc o\ CAL) KMnO4=1OO0C Ca)(NH4), f e (C04Ja


G9.(4 m o Fet*
Au o [NAo) KuMa04 t CNA) CAIHL) 2 fe Co)
55 1 qm ote

Teacher's Signatura
feSCA)
Expt. No. Pa N 06

5S4Xlov, Xb= cm De
800
Jonic equadion2
-e-
MH14H,0 +5 et1

ObSeRVATIDN

SLoo TBR FBR Dienence


13 13
13 25.
12. 12S

Conclumoo
O000
5 _ o Soluth'on fonein00 Fetfett
Solution Cantain 07 q fe
25

1b00 C04 Solution ton-taio 0 XO:01 m


q1 i
PL INO.
Page o. 06

PROCE DURE
1Pani'
Pipe_out 25C oAD Moh1's l jnto 260c
MEOnn akMaKe up olume toi clitille.l oaten
and haketell to ppepane homoqeneaus olution. prpele
ow ASm ofhis alllute.l solcioo indo a tontéal lak,
ae ADm) aCn) So Cnto olsops o Phelanlhran ilk|
CuLi-nitalov The encd point found tobé viole
e k e Bcon fofelon ea.lin e lel it Le Y

LOLSERYANON
na TARtmd PRR(m) Dilenente

CALLLAON
290calluse soluhoo=lo x ST o SaKL1, Og

6fe t
lto / o Moh's Salt
T0000

l000

Ss.4Xlo kly.S *V3 fet


000
Teacher's Signature_
26 CeSol Conelo.2q o
ACc Sol? Coneu ) .2 lar o fet
Sol?
Con-aln toad Fe"-aesq/u

2dpund
Clanclani Scution_ol kv0 nn Mokr's Sct
Npee_Out afcc CA) Moh SulinBo 2so_te measunino
Hask Dilluke upla mank wt 14,0 ancd 4i drcte w
Mohy Sel Aaken n a unele oih Af X2 2 Oa
telline 0 olrop Dfhtnylanlhyaoili add.the
end btbint
int ound to_blue Take 2 Lontaidant
eacline
CALLULAIONL
S=V, S

25 X o
1:3a

Resull
Te
he amoua o fe ous ton in 6e whole_ol qiveo
Soluh'on is 1
Expt. No. O Page No. 07

AIM OF THE EXPERIMENT


bshimaion o (oggen uine Soliam Thiosulphate

Ppee Oul CusD4 Solukion Asanslon he whol e


om he mankel belle into a la» Rihse 4he bunete
h t ewth5 o io m clidilleel H0 and chetke senfen
tnothe laskMaue he volume oith _rlstilled H>0 on
Chake_well_lo toPreprepan p ahomeqenous Soluhèn.
Ppette_@AOuA 85 ohi' ude tolutbn in a (onilal
lak aclel Ala H[o, SolutoD elop wis e until a in
Penmanenl blue PpL ijus ormed elissole oe pP
in_minimum ampLen o clilule CHa(0o|H tll a Uean So
Sul"
_amee ielelR0 kJ Splution hake well end add
50m dssille-l Hg0.
PROCEDVRE
alt the whole hbenabtelL with la, SPa ak
ina bunele 4ilIa e l l o toloun ahia o icdevelopeel
Acld mi slanth u cnindicatoy Deep blur pr is
ot me Coninu e the ieldiHon of Na S0g blue
loloune
hange -Bo lehi blu e, alow acdel LOCC1oy
Loce Joy.
AIH SCN on KSCALL aqaio ue Coloun clevelops dil blue
slrap_w)
bate
ibatea quickly
olotunlyappéan ak
a ossible
Eang
xeaclng
CcnCordan!_
Page No. OX
Expt. No.

on quaion
Cut e

Cut x
a Cut+A1 2Cut+L,
2 Cp 2 SOg
21
as04 S0321
CuSO4 t2 Kj- t u l tk, SO4

aAla S,0+T la, S+AAaII


C CULALON
25Lilutel Solukion =2410 o .0IN/1o lo, S, O
20 _cl:/utel Kolakon=24qe of ol N/to la, 203

63.5 9 0l tut*

AlagS0, 244Lo N/1o Culo


63 x249 X\.ol-ut Sgm o tu
0000
Expt. No. Page No. 0

ODSERVATION
Na. of TBR FBR Drthenente
ohs
1 31.2 12
2 3 1
3 311 3

CONNCLISiON
25C Omiinal Solukion. tonaini Sqm0 tuf
Lttlution tontaios em o utt
lo00Ce Solutio Conlen 2 y1000 qm 0 lu
25
Expt. No. 05 10

AM OF THE EXPERIMENT
o Sepcncale mikune o woSugans b Papen
Chrsomatoeraph
Appanalan eaurel
fillen papen Oaden Satcenatel phero/ I ummona
n-bukanalacelic atid walen Sprau agy enl Ammonum
Silven nitate Alkaline _penmanganale , Re orcinol 1eagend

Leary
The tenm ChaomaBecsaphy Come Tom the Aan lien
|tmewhen he Lechnieae wa uieed h e Sepanat
toloune plaal Memenls-chromto enaphy isa techomjae
Jer Sepanadion o Aosely xelatel graps el lomocuncl
h e sepcenation /aoughL ahu hy ellehent'al
miayanion alona e Poxou melittn nd the miqrahdo
b Cawed y h e desd a1 soluen.

PRO CEDURE
Plare Sullicien Solyenl nto 4he bolam o\ he an
Coven the led and alew -he tanx 4o be akunate!
OHh the Solven
aNkeaheel al whal ma) homaBogs aphy fapen
Caboul xlo Cm)and plaLe il ona preLe o leun apen
on_a henth
Daw aaine lnt wih a pmuil olons he
Dxad wialL
the papenand abous 1.4 Cm tom ae louien e.lqe.
iv Akoa
Akog4 Line_plareen tatulity Spates Small trcle

wha_penul
Expt. No. .
Page N

v)Label he pen at the top wth -he name o


each ot the suan nd label 4h e lask
Vi)Vse ine apillany on toth piek do Plae
-the
cdeep o he Solutiony do 4e sucans lutoiey autoue,
maltose,Lacbie anol -the 'mihtane
VAAltenSpothnea l r +he papen uh hof air clyen
a pne_min,yepeai thi f e Lajan.
Vh)Place the Spotle pepon in hehrameuto-qnapht lank
Aacd make the _elevelopmen b ine he astenclin e
techniaue:
i ) clele the lant with Aiallow he solvent4o low
heuboul O-4 min.
Remove -the papenand immeliately maunkthe poution
he Solven on1oi-th aPenul
Ccle he pohkión oeach Spo wih Peny
xi Caloulate 4eR[- valutor Cach p01 nc! ako
o e Cpob/ mlmttune Con-leuneal.
OLSERVATONZ
Sno. Component Dikanre raveldes al Mean D/
lpoinh tom) Cem)
Solvent 2,6 6.49 6.1
Glucose G2 6 02 0
Haltose 4 0 1.4 2
Expt. No. Page No. 12

CONOLUS1ON

R Nalue_o gutae 0 L19


R alue_ol Maltose 2
06 P'age N). 3
NE. NO.

AIM OFTHE EXPERIMEANIT


Detechio 0 entra elemeals CAL,S, t ) in Orqanic
Lompoluncds.

Ned lar Mimge wia


he entruck isboileed wth SeSOA ndauelifiecl
unsakenade.l SO4The appeanaote o l Poaiium blue
inicacbesHae prestnleofnitroseo
The Jallouwine seadion oCtun
Cfe CCNI)
f e t +0
i)Ce CCAD1 43
The awelhelps in e Owlackion a exxou ion o
enit ibn he Jotmabon OenmLexou Cyanicle
incdttakehe preente_o itroejen

et_io Sulphun
TheeMtrat realeel i t h ColitnnoprusSidt..
The
lhe app.eanance o iolek tolouninclCafes he
phesente o Sulphun.
The lollo@inet- Keachon

i CEe to), NOT- tfe (CN);NoS

dahalaaen
entac s acteliie i HN0n ond Gnd e
The
reade wh AenNo whie precupidede toluble_in
ÎNLGOH noutalehe Piescote of , a yelluiv.
Teacher's Signature
xpt. No.
Page No. 14

Pseciptete
the Spcurnnqly-
PmesenLe D
foluble in M,614 inclicates
ncl nncl a elloulprecipcke inia luble
in ALHAO4 inclicate 4he
1eendeoll
AqAld3 +Nax SAeqX HAla AlO,

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