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    Identification of Dyestuff (Acid)

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    Md. Sazzadul Islam
    This document describes a procedure for identifying an unknown acid dye sample. It outlines two procedures: 1) boiling the sample with soap and ammonium hydroxide, which would destroy the color of acid, direct or basic dyes; and 2) boiling with soap and acid, which would cause the color to bleed onto a white sample, confirming an acid dye. The document provides background on dye types and the objective to identify unknown dyes. It describes the required chemicals, preparation of solutions, working procedures for the two tests, results showing the sample was an acid dye, and conclusions.

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    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd

    Identification of Dyestuff (Acid)

    Uploaded by

    Md. Sazzadul Islam
    62 views3 pages
    This document describes a procedure for identifying an unknown acid dye sample. It outlines two procedures: 1) boiling the sample with soap and ammonium hydroxide, which would destroy the color of acid, direct or basic dyes; and 2) boiling with soap and acid, which would cause the color to bleed onto a white sample, confirming an acid dye. The document provides background on dye types and the objective to identify unknown dyes. It describes the required chemicals, preparation of solutions, working procedures for the two tests, results showing the sample was an acid dye, and conclusions.

    Original Title

    3. Identification of Dyestuff( Acid )

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    This document describes a procedure for identifying an unknown acid dye sample. It outlines two procedures: 1) boiling the sample with soap and ammonium hydroxide, which would destroy the color of acid, direct or basic dyes; and 2) boiling with soap and acid, which would cause the color to bleed onto a white sample, confirming an acid dye. The document provides background on dye types and the objective to identify unknown dyes. It describes the required chemicals, preparation of solutions, working procedures for the two tests, results showing the sample was an acid dye, and conclusions.

    Copyright:

    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd
    Download as doc, pdf, or txt
    62 views3 pages

    Identification of Dyestuff (Acid)

    Uploaded by

    Md. Sazzadul Islam
    This document describes a procedure for identifying an unknown acid dye sample. It outlines two procedures: 1) boiling the sample with soap and ammonium hydroxide, which would destroy the color of acid, direct or basic dyes; and 2) boiling with soap and acid, which would cause the color to bleed onto a white sample, confirming an acid dye. The document provides background on dye types and the objective to identify unknown dyes. It describes the required chemicals, preparation of solutions, working procedures for the two tests, results showing the sample was an acid dye, and conclusions.

    Copyright:

    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd
    Download as doc, pdf, or txt
    of 3

    Identification of dyestuff from unknown dyed sample

    ( Acid dye )
    Experiment No: 03

    Experiment Name : Identification of dyestuff from unknown dyed sample ( Acid dye ).

    Introduction:

    Dyeing is a distribution process, which is happened in the dye bath between dyes solution &
    textile materials.

    There are many types of dyes. Such:


     Direct dyes
     Acid dyes
     Basic dyes
     Vat dyes
     Sulpher dyes
     Azonic dyes
     Reactive dyes
     Disperse dyes etc.

    Sometimes it is needed to know the name of the dyes on unknown dyed sample for different
    purpose like costing.

    Theory:

    To identifying of any dyestuff from unknown dyed sample, there are two procedure are
    follow. Such:

    Procedure 1:

    The sample is boiled with 5% soap solution & 10% NH4OH solution for 5 minutes.

    Observation Possibility Remarks


    1. Color destroyed Direct, acid, basic dye
    2. No change Vat, sulphr, napthol, reactive, Not found
    aniline

    Procedure 2:

    Sample is boiled with 5% soap solution & is acidified with few drops of acidic
    acid & boiled with a pieces of white wool or silk fiber.

    Observation Possibility Remarks


    Color bleeds & the
    white wool or silk is Acid dye Confirmed
    dyed

    Objective:
    13

    Prepared By: Md. Kamruzzaman Kazal ; ID: 2010000400068 ;


    Batch: 13th WPT
    Identification of dyestuff from unknown dyed sample
    ( Acid dye )
     To know the name of the dyes on unknown dyed sample
     To know the procedure of identifying the dyes on dyed sample
     To know the types of dyes on fabric etc.

    Required Chemicals & Apparatus:

     Bicker
     Pipet
     Burner
     Conical flux
     Raw water
     Soap
     Soda
     Salt
     Ammonium hydroxide
     Dyed fabric
     White cotton fabric
     Stop watch etc.

    Working Procedure:

    Preparation of 5% soap solution:

     Taken 5 gm soap on 100 ml water in a bicker to make 100 ml 5% soap


    solution.

    Preparation of 10% Ammonium hydroxide solution:

     Taken 10 gm ammonia on 100 ml water in a bicker to make 100 ml 10%


    ammonium hydroxide solution.

    Procedure 1:

     Taken 20 ml soap & ammonium hydroxide solution in a bath


     Boiling the solution with unknown dyed sample about 5 minute
     During boiling the sample dyed color destroyed.

    Procedure 2:

     Taken 20 ml soap solution in a bath & added few drop of acidic acid
     Boiling the solution with unknown dyed sample & white wool about 5
    minute
     During boiling the sample dyed color destroyed & re-dyeing is done on
    white wool sample in the presence of acidic acid.

    Sample Attachment:
    13

    Prepared By: Md. Kamruzzaman Kazal ; ID: 2010000400068 ;


    Batch: 13th WPT
    Identification of dyestuff from unknown dyed sample
    ( Acid dye )

    Unknown dyed sample Color destroyed sample Re-dyeing sample

    Result:

    So the sample is dyed with acid dyes.

    Precaution:

     Before each procedure , new sample must be taken


     Observation must be perfect
     Preparation of solution must be perfect
     Weighting of chemical must be careful
     Concentration of solution must be perfect
     During re-dyeing, salt must be used to ensure the direct dye etc.

    Conclusion:

    From this experiment, we know about the identification process of unknown dyed sample
    which used in wet processing. I know this experiment is very helpful for our job sector &
    increase our knowledge about this. Special thanks to our teacher & his assistant for helping us
    to know it properly.

    Thanks
    13

    Prepared By: Md. Kamruzzaman Kazal ; ID: 2010000400068 ;


    Batch: 13th WPT

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