Acidic Acid
Acidic Acid
Acidic Acid
On
Online Summer Internship Programme
(OSIP-2020)
Submitted in Partial Fulfilment of the Requirements for the mandatory Industrial Internship training
programme
Submitted by:
CHEMICAL ENGINEERING
This is to certify that Mr. Dodiya Manharsinh Ranamalbhai from Maharaja sayajirao University
organization. The matter embodied in this report is a genuine to the best of our knowledge and
belief and has not been submitted before, neither to this Institute nor to any other organization
for the fulfilment of the requirement of any course of study. During his internship tenure in
IIChE, we found him as a hardworking, sincere, and diligent person and his/her behaviour and
The internship opportunity I had with IICHE OSIP-2020 was a great chance for learning and
professional development. Therefore, I consider myself as a very lucky individual as I was
provided with an opportunity to be a part of it. I am also grateful for having a chance to meet
so many wonderful people and professionals who led me though this internship period.
Bearing in mind previous I am using this opportunity to express my deepest gratitude and
special thanks to Shri S D Karve, Mr.Rajagopal RJ and Mr.Hayavadana who in spite of being
I express my deepest thanks to Mr.Dhawal Saxena, IICHE course co-ordinator for taking part
in useful decision & giving necessary advices and guidance and arranged all facilities to make
life easier. I choose this moment to acknowledge his contribution gratefully.
It is my radiant sentiment to place on record my best regards, deepest sense of gratitude to Prof.
V.V. Basava Rao, President of IICHE and Dr. Avijit Ghosh, Convenor-OSIP 2020 for
providing such an impeccable programme and helping students in all ways possible.
Preface
Course Outcome
● Provides basic idea of different real life industrial processes, problems, trouble
shooting, decision making and preventive maintenance techniques and professional
culture of industry, work ethics and attitudes in industry. The different live situation,
trouble shooting and modern technological application.
● Provides course materials to the students for reference (in PDF format). The study
materials have been shared with the students through IIChE for its record.
● Improves to deal with the assignments which has been given for the solution /
conceptual ideas based on discussion during the tutorial classs.
● Helps to understand the importance of the application of modern tools for the industrial
automation / up-gradation / scale-up.
● Develops conceptual theory n the regular class room discussion and its application in
real-life industrial problem resolution.
● Gives primary idea to analyse Case studies based on real life application.
Content
Six Sigma is a highly disciplined process that focuses on delivering near-perfect products
and services consistently. Its strength is that it is a continuous improvement process with
an unwavering focus on change empowerment, seamless training of resources and
continuous top management support. These three are known as the Pillars of Six Sigma. If
Six Sigma is implemented methodically, it will give sustained results for any process.
Now the question arises as to what is a process. This will be explained in the next screen. Process
of Six Sigma
Six Sigma follows a process called DMAIC (Pronounced as D-MAC). DMAIC stands for
Define, Measure, Analyze, Improve, and Control. Click each tab to know more. In the
Define phase, we define the problem statement and plan the improvement initiative.
Consider a typical problem in an Organization. A particular organization’s customers are
not satisfied with the current support process of the organization. You can define the
problem as the support process of the organization is at 20% satisfaction. In Six Sigma,
the projects are always defined objectively. In addition to defining the problem, the Six
Sigma project team is also formed in this phase. The Measure phase collects the data from
the process and determines the current quality and operational performance levels. Also,
the measurement criteria such as how to measure, when to measure, and who will
measure are established. In the Analyze phase, the business process and the data
generated from the measurement phase are studied to understand the root causes of the
problem. In the Improvement phase, possible improvement actions are identified and
prioritized. These are then tested and the improvement action plan is finalized. In the last
phase, which is the Control phase, the Six Sigma team goes for a full-scale
implementation of the improvement action plan and sets up controls to monitor the
system in order to sustain the gains.
The list of DMAIC tools is discussed in this screen. There are specific tools used in each
phase of the Define, Measure, Analyze, Improve, and Control process. Later in this
course, important tools of each phase will be discussed. Click each phase to view the list
of tools. The define phase uses tools such as Supply, Input, Process, Output, Customer or
SIPOC (Pronounce as: sye-poc) Diagram, Voice of Customer or VOC (Pronounce as: vo-
c), Critical to Quality or CTQ Trees, Quality Function Deployment or QFD, Failure Mode
and Effects Analysis or FMEA, Cause and Effect or CE Matrix, and Project
Charter. The measure phase uses tools such as GAGE R and R Variables, Run Charts or
Control Charts, Cp, Cpk, Sigma level (Z Level) and Defects per Million Opportunity or
DPMO, and Anderson Darling Test. The tools used in the analyze phase are SimpleLinear
Regression or SLR, Pareto Charts, Fishbone Diagram, FMEA, and Multi-Vari Charts or
the tools that can be used are Brainstorming, Piloting and FMEA, and Design of Experiments
or DOE (Pronounce as: d-o-e) (If needed). The control phase uses tools such as Control
Charts, Control Plan, and Measurement System Analysis or MSA Re-analysis. Note that
some of these tools can be used interchangeably between the phases
The generally accepted methodology for managing Six Sigma projects includes the following
phases:
Define: The objectives and scope of the project are defined. Relevant information about the process
and customer are collected.
Measure: Data on the current situation and process metrics are collected.
● Reduce of high rejection rate of the painted damper outer tube of shock absorber.
Aviation
Analyze: Collected data are analyzed to find the root cause(s) of the problem.
Control: The implemented solution(s) are evaluated and the mechanisms are implemented to hold
the gains, which may include standardization.
Applications in fertilizer industry – Not many people are aware that the one of the most
potent Six Sigma techniques named as Design of Experiments (covered in detail in our
Black Belt training program) was first used in agriculture.
In the 1920s, Fisher created the statistical approach to Design of Experiments (DOE), and
the data analysis tool – Analysis of Variance (ANOVA), while working at Great Britain’s
Rothamsted Agricultural Experimental Station.
Design of Experiments was first used in a major way outside agriculture in the late 1940s and
early 1950s. Today the statistical approach to design of experiments is used in many areas
like manufacturing and R&D, sales and marketing, and service.
Last few decades have witnessed a phenomenal increase in the fertilizer consumption in
many countries. As a result farmers and governments have stepped up efforts to expand
farm production to feed the growing populations and increase agricultural exports. The
major aim of these countries is to expand the agricultural output at a rapid pace as well as
to improve the overall quality of the produce. Six Sigma has a number of applications in
Fertilizers Industry which is an industry growing at a rapid pace across the world. IMC
Global, one of the Leading Fertilizer companies across the world has adopted Six Sigma
and is using it extensively to deliver high quality of products & services to its customers.
Six Sigma is used across the organization to improve and streamline procedures with an
objective to yield high quality produce. The company believes in “feed the land that feeds
the world”.
Six Sigma tools like ANOVA and DoE have huge applicability in Fertilizer Industry.
Using these tools, the impact of type and quantity of fertilizer variants on Crop Yield can
be studied. In India it will be critical to increase the produce/unit of land since the demand
for food is going up considerably. Moreover, the quality of produce is also increasingly
becoming a central theme with more and more people getting health conscious. This is the
right time to utilize the benefits of Six Sigma in the Fertilizer Industry
3. Case study
Phase
Define
SIPOC
Customers and CTQs established
Problem Statement, Business Case, Goals &
Scope
Team
Measur Key output measures Y identified
e Data Collection Plan
Do MSA (Gage R&R – Only for Black Belt)
Process Variation displayed (Span)
Baseline sigma performance calculated
Purification Column
Packing
DMAIC Project Charter
●
●
●
●
High Level Improvement Timeline
Measure
Data Collection Plan Worksheet Key Output Measure Y
Production
Amount of
of Acetic
Acetic Acid By Excel Sheets, Team
Acid in Continuous 50 Samples Nil
Produced Per By Log Sheets. Members
Tonnes Per
Day
Day
Measure
Output Sigma
Understanding the Capability of the process
DPMO
You may need to do more than one sheet (or consolidate in a table) to show other Baseline calc’s or summary sigma.
Explain any sampling as appropriate. Hint: Update your problem and goal statements. Did they change based on your findings?
Measurement Data Display
Natural Government
Calamities Norms,
Environment
Conditions.
Narrow to Root Causes, Use Pareto Analysis
Vital Few Causes
2 1
9
Improve
Describe Solution(s) Selected
Six sigma is likely to remain as one of the key initiatives to improve the management
process than just being remembered as one of the fads. The primary focus should be on
improving overall management performance, not just pinpointing and counting defects.
Researchers and practitioners are trying to integrate six sigma with other existing
innovative management practices that have been around to make six sigma method even
more attractive to different organizations that might have not started or fully implemented
the six sigma method. Integrating and comparing principles and characteristics of six
sigma with Total Quality Management, Human Resource Functions, Lean Production,
ISO 9000, ISO 9001, the capability maturity model are all part of the quality
community’s effort to maximize the positive effect of the six sigma method.
In 2002, Bechtel Corporation, one of the largest engineering and construction companies
in the world, reported savings of $200 million with an investment of $30 million in its six
sigma program to identify and prevent rework and defects in everything from design to
construction to on time delivery of employee payroll. For example, six sigma was
implemented to streamline the process of neutralizing chemical agents, and in a national
telecommunications project to help optimize the management of cost and schedule. The
objectives of implementing six sigma in R&D organizations are to reduce cost, increase
speed to market, and improve R&D processes. To measure the effectiveness of six sigma,
organizations need to focus on data driven reviews, improved project success rate, and
integration of R&D into regular work processes. One survey noted that as of 2003 only
37% of the respondents had formally implemented six sigma principles in their R&D
organization reported that the development and manufacturing of the new prototype at W
R Grace (Refining Industry) was cut to 8-9 months from 11-12 months by implementing
the DFSS process. Figure 4 shows the conceptual benefits and improvement of
implementing six sigma in R&D projects.
HEALTHCARE SECTOR :
Six sigma principles and the healthcare sector are very well matched because of the
healthcare nature of zero tolerance for mistakes and potential for reducing medical errors.
Some of the successfully implemented six sigma projects include improving timely and
accurate claims reimbursement, streamlining the process of healthcare delivery, and
reducing the inventory of surgical equipment and related costs. The radiology film library
at the University of Texas MD Anderson Cancer Centre also adopted six sigma and
improved service activities greatly .Also in the same institution’s outpatient CT exam lab,
patient preparation times were reduced from 45 min to less than 5 min in many cases and
there was a 45% increase in examinations with no additional machines or shifts.
MANUFACTURING SECTOR:
Motorola was the first organization to use the term six sigma in the 1980s as part of its
quality performance measurement and improvement program. Six sigma has since been
successfully applied in other manufacturing organizations such as General Electric,
Boeing, DuPont, Toshiba, Seagate, Allied Signal, Kodak, Honeywell, Texas Instruments,
Sony, etc. The reported benefits and savings are composed and presented from
investigating various literatures in six sigma.
In recent years, finance and credit department are pressured to reduce cash collection
cycle time and variation in collection performance to remain competitive. Typical six
sigma projects in financial institutions include improving accuracy of allocation of cash to
reduce bank charges, automatic payments, improving accuracy of reporting, reducing
documentary credits defects, reducing check collection defects, and reducing variation in
collector performance. Bank of America (BOA) is one of the pioneers in adopting and
implementing six sigma concepts to stream-line operations, attract and retain customers,
and create competitiveness over credit unions. It has hundreds of six sigma projects in
areas of cross-selling, deposits, and problem resolution. BOA reported a 10.4% increase
in customer satisfaction and 24% decrease in customer problems after implementing six
sigma. American Express applied six sigma principles to improve external vendor
processes, and eliminate non-received renewal credit cards. The result showed an
improved sigma level of 0.3 in each case. Other financial institutions including, GE
Capital Corp, JP Morgan Chase, and SunTrust Banks are using six sigma to focus on and
improve customer requirements and satisfaction.
CONCLUSION:
Here through the implementation of six sigma tool in the project increased the Acetic Acid
Production from 100 tons to 125 tons per day. This gives the annual profit of 31 crore. This
lean six sigma reduces the waste and variation. The wastes are generally Factory inventory,
over production, over processing, Defects and Scrap, Transporting, Waiting, Movements etc.
These wastes are eliminated through lean implementation and the variations are reduced by
six sigma. Hence this lean six sigma tools helped us in making the process effective &
efficient and in turn increases the profit.
4. Summary
Six Sigma is a production philosophy that uses data, processes, and tools to nearly eliminate
defects and bring performance close to perfection. There are two different business strategies
basically Push and Pull. Push strategy is to push a product at a customer, while a pull strategy
pulls a customer towards a product.
Six Sigma is moreover a statistical approach where we take feedback from customers and
convert it to some measurable quantity.
We were then introduced to different tools to describe the data graphically which include:
Six sigma is a road to achieve Zero defects, Quality Control and Total Quality Management.
Selection of Six Sigma Projects usually employs three different approaches namely Critical to
Quality (CTQ), Critical to Cost (CTC) and Critical to Satisfaction (CTS).
• In define phase, we clearly state the target business Problem and the scope of the
intended improvements. We also define the goal of our project here and map out what
success looks like.
• One primarily used tool for Define phase is SIPOC (Supplier-Input-Process-Output-
Customer).
• In Measure Phase, we put the data received from customers in the matrix form.
• Tools used in Measure Phase includes Process Flowchart, Data Collection, Voice of the
Customer Gathering etc.
• In Six Sigma process, main focus is given to the VOICE OF CUSTOMER (VOC).
Kano Model is used to describe VOC.
• Tree Plot is used to describe the customer’s needs into three categories Primary,
Secondary and Tertiary. The goal is to determine customer requirements based on Voice
of Customer Input.
• Later on, we discussed various voices that exist in any organisation namely VOB
(Voice of Business), VOC (Voice of Customer), VOE (Voice of Employee), VOP
(Voice of Process).
• In Analyse Phase, a root cause analysis is performed to determine the underlying
reasons for the business problems mentioned in the Define Phase.
• Different tools used in Analyse Phase includes Histogram, Pareto Chart, Scatter Plot
etc.
• The final step in the DMAIC cycle is the Control Phase. It basically emphasizes that
successful improvements being employed in the process doesn’t degrade over time. At
• After identifying the root cause for the Problem going to the implementation Phase
getting the solutions and Implementing & Monitoring in the Control Phase.
5. My observation / Opinion
Sigma is the symbol of standard deviation, a measurement of deviation of a sample from
the population average. Each sigma you depart from the average, the event, in this case
failure, becomes more an more improbable. At 6 sigma, the probability is about
3.5/million. But this is just the statistical side of Six Sigma. The bulk of the work in a Six
Sigma project would be in defining failures, measuring deviations, and other activities
which ultimately lead to product quality. In fact, Six Sigma is used as a term for a
management style, with the ultimate goal of high levels of customer satisfaction."
It was a productive and helpful online internship experience for me where i have got to
know many skills in 6 sigma
Today, as a result of Six Sigma or similar approaches, many organizations are operating at
very high levels of efficiency. But as leaders now shift their focus to the acceleration of
growth, they are discovering that the very culture of little to no variance that allowed them
Eliminating variation in a large organization can be a laudable goal, leading to profit and
efficiency. Yet variation is also not an obstacle to steadfastly avoid; it is a key to unlocking
your breakthrough future. Success requires embracing the alternative paths that markets
randomly present to us in order to find your organization– s own unique place to grow and
thrive.
Winning the quarter often requires the elimination of variance, but winning the long game
will require embracing it
According to me Future of Lean Six Sigma is bright if you use it judiciously. For example
over reliance of any system will result in few disadvantages. Lean Six Sigma may result in
operational efficiency of the business and it should be limited to that level. Coming to
business growth and innovation, LSS mind set may backfire.
Assignment No: 1
Topic of Assignment:
1) Project Charter:
It is an important tool used in defines stage. It consists of project name, problem statement,
Business case, scope, goal, timeline, team members, CTQ’s etc.
Example:
• Problem statement: Plant produces only 90 of yield of acetic acid and 10% of byproducts
of no value wasting the costlier raw material.
(problem statement the objective should be clear, concise and in measurable terms).
• Scope: To find out the route cause for the low yield.
• Business Case: Reducing the waste product efficient use of raw material.
s supplier, i input
feed, p process,
o output,
c customer.
Output: we will be entering what are the products that are produced.
Example:
Also called cause and effect diagram or fish bone diagram an important tool used in
Analyze Stage it tells what are the reasons that causes effect.
FISHBONE DIAGRAM
Machine
Person Method
Poor training
Defective equipments Side reaction
Lack information
Measurement
environment
Material
It’s a brain storming tool 6 persons assemble together where three ideas are written by each for 5
minutes after 5 minutes paper moves to the next person.
With the use of brainstorming we discussed on the data collected and came with a idea of
intermitten removal of product to avoid by product formation.
5) CTQ’s
CTQ trees helps us to translate broad customer needs into specific, actionable, measurable
performance requirements. We can use this requirements to deliver high quality products and
services.
SUBMITTED BY:
Email ID:[email protected]
Mobile Number:7490084384
LECTURE NUMBERE: 1
INTRODUCTION:
A process is a series of steps designed to produce a product and/or service as required by the
customer
1) Unit operation
2) Unit process
DMAIC
CONCLUSION:
In this lecture we learned about basic methodology and origins of six sigma and it’s
importance in industry .How it is useful for quality development and solved some examples Boxplates
with given data.
NEXT LECTURE:
SUBMITTED BY:
Email ID:[email protected]
Mobile Number:9327433171
LECTURE NUMBERE:02
Topic of the lecture: Tools for six sigma yellow belt part-1
One of the example of how to do this is by using The power/interest grid and grouped into
four catogories
CTQ: In six sigma CTQ is an acronym that stands for Critical- to- Quality, CTQs are the
internal critical quality parameters that relate to the wants and needs of the customer.
Examine
Understand
Ideate
Experiment
Distill
Strengths
Weaknesses
Opportunity
Threats
CONCLUSION:
NEXT LECTURE:
SUBMITTED BY:
Email ID:[email protected]
Mobile Number:7490084384
LECTURE NUMBERE:3
Six sigma help us to how can we look to the issues or a problem and solving those
problems using certain techniques
competition
The managerial aspects of six sigma and technical aspects of six sigma
CONCLUSION:
In this lecture we learned about The managerial aspects of six sigma and technical
aspects of six sigma and also the benefits of six sigma
LEAN 6 SIGMA YELLOW BELT TRAINING REPORT
SUBMITTED BY :
Email ID : [email protected]
LECTURE NUMBER : 4
• INTRODUCTION : The Yellow Belt Training generally covers the basic tools used in
Six Sigma. Some basic tools discussed during the Yellow Belt training are the SIPOC
diagram, Pareto chart, Various types of process Mapping, Histogram and other basic
• The first topic which was discussed about “Cause and Effect Diagram” .
➢ The second step is Classify the major causes under various headings.
➢ Third step is Draw a cause and effect diagram with the problem at the point of
chosen.
• Then he discussed some of the examples of the Cause and effect diagram.
• Next topic which was discussed about “ Regression Equations” and solved some
numerical problems.
• Next he discussed about Team Dynamics . There are five typical stages in the team
building process.
1. Forming .
2. Storming .
3. Norming .
4. Performing .
5. Adjourning .
CONCLUSION : After the lecture we got the basic information about some Tools used in
Define phase and how it is used in the industry. We also got to know about different tools like
SIPOC, Cause and Effect diagram etc . The fourth lecture was very informative and we have
NEXT LECTURE :
In the next lecture we will be discussing about “ Tools For Six Sigma”
LEAN 6 SIGMA YELLOW BELT TRAINING REPORT
SUBMITTED BY :
Email ID : [email protected]
LECTURE NUMBER : 5
• INTRODUCTION : The Yellow Belt Training generally covers the basic tools used in
Six Sigma. There are mainly 5 stages in six sigma . In this lecture mainly Define phase
has discussed.
• Next he discussed how “Dabbawallas” served food 2 lakh people everyday without any
error.
CONCLUSION : After the lecture we got the basic information about some Tools used in
Define phase and how it is used in the industry. We also got to know about different tools like
SIPOC, Process Mapping , Pareto analysis etc . The fifth lecture was very informative and we
NEXT LECTURE :
SUBMITTED BY:
Email ID:[email protected]
Mobile Number:7490084384
LECTURE NUMBERE:6
measure phase, gist of six sigma, why process maping, types of flow
diagram, process map analysis, CTQS and CTPS, planning for data collection, what is data?,
variable data, craete new project qqq
INTRODUCTION
(x1,x2,x3). (x4,x5,x6)
a good data collection will have,what,which,where,and who about the data to be collected
>Brief introduction on six sigma geen belt project, productivity improvement in PET bottle
production line
CONCLUSION:
In this lecture we learned about gist of six sigma, process maping, brief about process map,
flow diagram, CTQS and CTPS and data collection
NEXT LECTURE :
SIPOC and project charter measure phase- data collection and case study by s.d.karve
TOOLS FOR SIX SIGMA YELLOW BELT TRAINING REPORT
SUBMITTED BY:
Mobile Number:7490084384
LECTURE NUMBERE:7
Topic of the lecture: Sipoc and project charter-measure phase-data collection and case
studies by shri S. D karvw
ANOVA-analysis of variance
INTRODUCTION
>>ANOVA is powerful stastical analysis tool that can be used to compare means of three or
more populations
>>while this is called analysis of variance it actually compare means
>>Definition :value
+ Noun:a fair return or equivalent of goods, services or money for something exchanged
>>Principles
CONCLUSION:
In this lecture we learned about The hypothesis, various test on same , Anova is best
and value definitions and many more parameters.
NEXT LECTURE:
SUBMITTED BY:
Mobile Number:7490084384
LECTURE NUMBERE: 8
1-Descriptive Statistics :
2-Inferential Statistics:
Concept of probability
Concept of variation
CONCLUSION:
NEXT LECTURE:
SUBMITTED BY :
Email ID : [email protected]
Lecture By : Rajagopal RJ
• INTRODUCTION : Six sigma is a process that uses data and tools to remove defects
and bring the performance close to perfection . Six Sigma introduced by “Sir Bill
approach where we take feedback from customers and convert it to some measurable
quantity.
• Next he explained with the help of a example that the root causes of problem are real
or not.
• After this he explained what is Null hypothesis(Ho) and Alternate Hypothesis (Ha).
• Next he explained the importance of P value. He said in Hypothesis testing we rejected
T – test done when the sample size is less than 40 and Z- test done when the sample
• Then he explained ANOVA testing with the help of example of a paint manufacturing
process.
Conclusion : From this lecture I have learned lots of new thing like Hypothesis, ANOVA
testing, Null Hypothesis etc. It will help me lot in future to make a Six Sigma project.
NEXT LECTURE :
SUBMITTED BY :
Email ID :[email protected]
LECTURE NUMBER : 10
• INTRODUCTION : Six sigma is a process that uses data and tools to remove defects
and bring the performance close to perfection . Six Sigma introduced by “Sir Bill
approach where we take feedback from customers and convert it to some measurable
quantity.
• First topic which was discussed about steps involved in Design of Experiment like
2. Brain Storming .
6. Draw conclusion.
• After this he discussed the Main effect plots and explained what should the optimum
setting.
• Next he explained the types of variation like Special cause and Common cause.
• If it depends on the volume two types of chart are there. For low production I-MR chart
• If it depends on the Lot Size there are 4 types of chart u-chart , p- chart ,c -chart, np-
chart.
• After this he explained Control Chart zone like Upper control and Lower Control Chart.
CONCLUSION : After the lecture we got the basic information of what is Design of
experiment and what is control Chart in Six Sigma and how it is used in the industry. In this
lecture he explained the case studies which will help us lot in future The last lecture was very
informative and we have learned lot of new things.