IS4031(Part1):1996

Indian Standard
METHOD OF PHYSICAL TESTS FOR
HYDRAULIC CEMENT
PART 1 DETERMINATION OF FINENESS BY DRY SIEVING

(Second Revision )

KS 91.100.10

.-

8BIS 1996

BUREAU OF INDIAN STANDARDS

MANAKBHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002

Mgy 1996 Price Group 2

‘
Cement and Concrete Sectional Committee, CED 2

FOREWORD
This Indian Standard (Second Revision) was adopted by the Bureau of Indian Standards, after the draft
finalized by Cement and Concrete Sectional Committee had been approved by Civil Engineering Division
Council.
Standard methods of testing cement are essential adjunct to the cement specifications. This standard in
different parts lays down the procedure for the tests to evaluate physical properties of different types.
of hydraulic cements. The procedure for conducting chemical tests of hydraulic cement is covered in
IS 4032 : 1985 ‘Methods of chemical analysis of hydraulic cement ( first revision )‘. Originally all the
tests to evaluate the physical properties of hydraulic cement were covered in one standard but for facilitating
the use of this standard and future revisions, the revised standard was brought out in different parts, each
part covering different tests. This part covers determination of fineness of cement by dry sieving.
The second revision of this standard has been prepared with a view to align this test method with European
S!andard EN 196 (Part 6) Method of testing cements: Determination of fineness.
The composition of the Committee responsible for the formulation of this standard is given at Annex A.
For the purpose of deciding whether a particular requirement of this standard is complied, the final value,
observed or calculated, expressing the result of a test or analysis, shall be rounded off in accordance with
IS 2 : 1960 ‘Rules for rounding off numerical values ( revised )‘. The number of significant places
retained in the rounded off value should be the same as that of the specified value in this standard.
 IS 4031 (Part 1) : 1996

Indian Standard
METHOD OF PHYSICAL TESTS F<OR
HYDRAULIC CEMENT
PART 1 DETERMINATION OF FINENESS BY DRY SIEVING

( Second Revision )

1 SCOPE cylindrical frame of 150 mm to 200 mm nominal

diameter and 40 mm to 100 mm depth, fitted with 90
1.1 This standard (Part 1) covers the procedure for pm mesh sieve cloth of woven stainless steel, or other
determining the fineness of cement by dry sieving as abrasion-resisting and non-corrodible metal wire.
represented by the mass of residue left on a standard
90 w IS Sieve. The sieve cloth shall comply with the requirements
of IS 460 ( Part 1) : 1985 and IS 460 ( Part 3 ) : 1985
2 REFERENCES and shall be free of visible irregularities in mesh size
2.1 The following Indian Standards are necessary when inspected optically by the methods of IS 460
adjuncts to this standard: ( Part 3 ) : 1985. A tray fitting beneath the sieve frame
and a lid fitting above it shall be provided to avoid
IS No. Title loss of material during sieving.
460 Specification for test sieves: 4.2.2 Balance
( Part 1 ) : 1985 Wire cloth test sieves (third Capable of weighing up to 10 g to the nearest 10 mg.
revision)
4.2.3 Brush
( Part 3 ) : 1985 Methods of examination of
apertures of test sieves (third A nylone or pure bristle brush, preferably with 25 to
revision) 40 mm bristle, for cleaning the sieve.

3535 : 1986 Methods of sampling hydraulic 4.3 Material for Checking the Sieve
cements (f?rst revision) A Standard reference material of known sieve residue
5165 : 1969 Interchangeable conical ground shall be used for checking the sieve.
- glass joints The material shall be stored in sealed, airtight
3 SAMPLING AND SELECTION OF TEST containers to avoid changes in its characteristics due
SPECIMENS to absorption or deposition from the atmosphere. The
containers shall be marked with the sieve residue of
3.1 The samples of the cement shall be taken according the reference material.
to the requirements of IS 3535:1986 (see 2.1) and
the relevant standard specification for the type of 4.4 Procedure
cement being tested. The representative sample of 4.4.1 Determination of the Cement Residue
the cement selected as above shall be thoroughly mixed
before testing. Agitate the sample of cement to be tested by shaking
for 2 min in a stoppered jar to disperse agglomerates.
4 SIEVING METHOD Wait 2 min. Stir the resulting powder gently using a
4.1 Principle clean dry rod in order to distribute the fines throughout
the cement.
The fineness of cement is measured by sieving it on
standard sieve. The proportion of cement of which Fit the tray under the sieve, weigh approximately 10 g
the grain sizes are larger than the specified mesh size of cement to the nearest 0.01 g and place it on the
is thus determined. sieve, being careful to avoid loss. Disperse any
agglomerates. Fit the lid over the sieve. Agitate the
A reference sample having a known proportion of sieve by swirling, planetary and linear movement until
material coarser than the specified mesh size is used no more fine material passes through it. Remove and
for checking the specified sieve. weigh the residue. Express its mass as a percentage,
R,, of the quantity first placed in the sieve to the nearest
4.2 Apparatus 0.1 percent. Gently brush all the fine material off the
base of the sieve into the tray.
4.2.1 Test Sieve
It comprises a firm, durable, non-corrodible, Repeat the whole procedure using a fresh 10 g sample
i
1
 IS 4031 (Part 1) : 1996
to obtain 5. Then calculate the residue of the cement repeat determination of residue to yield two values p,
R as the mean of R, and R, as a percentage, expressed and P, expressed to the nearest 0.1 percent.
to the nearest 0.1 percent.
The two values of P, and P, for a satisfactory sieve
When the results differ by more than 1 percent should differ by not more than 0.3 percent. Their mean
absolute, carry out a third sieving and calculate the P characterizes the state of the sieve.
mean of the three values.
Given the known residue on the 90 m mesh of the
The sieving process is carried out manually by a skilled reference material, R, calculate R/P as the sieve
and experienced operator. factor, F, expressed to the nearest 0.0 1. The residue,
R, determined as in 4.4.1 shall be corrected by
NOTE - Alternatively a sieving machine may be multiplying by F, which may have a value of 1.00 +
used provided that it can be shown to give the same 0.20
results as the manual operation.
Check the sieve after every 100 sievings.
4.4.2 Checking the Sieve
NOTE - Any other checking procedure, such as the optical
methods described in IS 460 ( Part 3 ) : 1985 may be used. All
Agitate the sample of cemem LObe tested by shaking sieves will wear slowly and consequently their sieve factor, F,
for 2 min in a stoppered jar to disperse agglomerates. will slowly change.
Wait 2 min. Stir the resulting powder gently using a
clean dry rod in order to distribute the fines throughout 5 EXPRESSION OF RESULTS
the cement.
eport the value of R, to the nearest 0. Ipercent, as
Fit the tray under the sieve. Weigh approximately 10 t e residue on the 90 pm sieve for the cement tested.
%
g of the reference material to the nearest 0.01 g and
place it in the sieve, being careful to avoid loss. Carry The standard deviation of the repeatability is about 0.2
out the sieving procedure as in 4.4.1 including the percent and of the reproducibility is about 0.3 percent.

ANNEX A
( Foreword )
COMMITTEE COMPOSITION
Cement and Concrete Sectional Committee, CED 2
Chairman Represenfing

DR H.C. VISVESVARVA In personal capacity ( University of Roorkee# Roorkee 247 667 )

Members

SHRI H. BHATTACHARYA Orissa Cement Limited, New Delhi

SHRI G. R. BHARTIKAR B.G. Shirke & Co, Pune
DR A. K. CHAITERJEE The Associated Cement Companies Ltd, Bombay
SHRI S. H. SUBRAMANIAN ( Alternaie )
CHIEF ENGINEER(DESIGN ) Central Public Works Department, New Delhi
SUPERI~JTENDMGENGINEER,( S&S ) ( Alternate )
CHIEFENGINEER,NAVAGAM DALU( Sardar Sarovar Narmada Nigam Ltd, Gandhinagar
SUPER~NTENDMG ENGINEER,QCC (Alternate )
CHIEFENGINEER, RESEARCH-CUM-DIRECTOR Irrigation and Power Research Institute, Amritsar
RESEARCHOFFICER, CONCRETETECHNOLOGY
( Alternate )
DIRECTOR A.P. Engineering Research Laboratories, Hyderabad
JOINTDIRECTOR( AItemate )
DIRECTOR(CMDD) ( N&W ) Central Water Commission, New Delhi
DEPUTYDIRECTOR( CMDD ) ( NW&S )
( Alternate )
SHRI K. H. GANGWAL Hyderabad Industries Ltd, Hyderabad
SHRI V. P~ABHI ( Alternate )
SHRI V. K. GHANEKAR Structural Engineering Research Centre (CSIR), Ghaziabad

( Continued on page 3 )

2
 IS 4031 (Part 1) : 1996

( Continued from page 2 )

Members Repnzsenting

SHRI s. &PlNATH The India Cements Ltd, Madras

SHRI R. TAMILAKARAN
( Alternate )
SHRI S. K. GUHA THAKURTA Gannon Dunkerley & Co Ltd, Bombay
SHR~ S. P. SANKARANARAYANAN
( Alternate )
SHRIN. S. BHAL Central Building Research Institute ( CSIR ), Roorkee
DR IRSHADMASOOD( Alternate )
DR IRSHAD MASOOD Cement Corporation of India, New Delhi
SHRIN. C. J~JN(Alternate)
JOINTDrsscro~ STANDARDS ( B&S )( CB-I ) Research, Designs & Standards Organization ( Ministry of Railway ).
Lucknow
JOINT,,DIRECTORSTANDARDS( B&S )( CB-II )
( Alternate )
SHRI N. G. JOSHI Indian Hume Pipes Co Ltd, Bombay
SHRI P. D. KELKAR ( Alternate )
SHR, D. K. KANUNGO National Test House, Calcutta
SHRI B. R. MEENA ( Alternate )
SHRI P. KRISHNAMURTHY Larsen and Toubro Limited, Bombay
SHRI S. CHAKRAVARTHY ( Alternate )
DR A. G. MADHAVARAO Structural Engineering Research Centre ( CSIR ), Madras
SHRI K. MANI (Alternate )
SHRI G. K. MAJIJMDAR Hospital Services Consultancy Corporation (India) Ltd, New Delhi
SHRI J. SARIJP( Alternate )
SHRIPUFULLA KUMAR Ministry of Transport, Department of Surface Transport Roads Wing,
SHRI P. P NAIR ( Alternate ) New Delhi
MEMBER SECRETARY Central Board of Irrigation and Power, New Delhi
DIRECTOR
( CIVIL ) ( Alternate )
SHRI S. K. NATHANI, SO I Engineer-in-Chiefs Branch, Army Headquarters, New Delhi
DR A. S. GOEL, EE (Alternate )
SHRIy. R. PHULL Central Road Research Institute ( CSIR ), New Delhi
SHRIS. S. SEEHRA( Alternate )
ShRl Y.R. PHULL Indian Roads Congress, New Delhi
SHRIA.K. SHARMA( Alternate )
DR C. RAJKUMAR National Council for Cement and Building Materials, New Delhi
DR S. C. AHLWALIA ( Alternate )
SHRIG. hMDAS Directorate General of Supplies and Disposals, New Delhi
SHRIR. C. &ARM (Alternate )
SHRIS. A. REDDI Gammon India Ltd, Bombay
REPRESENTATIVE Builder’s Association of India, Bombay
SHRI J. S. SANGANEW Geological Survey of India, Calcutta
SHRIL. N. AGARWAL( Alternate )
SHRIS. B. SURl Central Soil and Materials, Research Station, New Delhi
SHRI N. CHANDRASEKARAN( Alternate )
SUPERINTENDING
ENGINEER
( DESIGN) Public Works Department, Government of Tamil Nadu, Madras
EXECUTIVEENGINEER
(S. M. R. DMSION )
(Alternate)
SHRIA. K. CHADHA Hindustan Prefab Ltd, New Delhi
SHRI J. R. SIL (Alternate )
DR H. C. VISVESVARAYA The Institution of Engineers ( India ), Calcutta
SHRI D. C. CHATURVEDI ( Alternate )
SHRIVINODKUMAR Director General, BIS ( Ex-officio Member )
Director ( Civ Engg )

MemberSecretary
SHRLJ.K. PRASAD
Joint Director (Civil Engg), BIS

( Continued on page 4 )

3
 IS 4031 (Part 1) : 1996

( Continued from page 3 )

Composition of Cement, Pozzolana and Cement Additives Subcommittee, CED 2 : 1

Convener Representing

DR H. C. VISVESVARAYA In personal capacity ( University ofRoorkee, Roorkee 247 667 )

Members

SHRI. B. R. MEENA National Test House, Calcutta

SHFL B. K. &NDAL ( AJtemate )
SHRI N. G. BASAK Directorate General of Technical Development, New Delhi
SHIU T. MADNESHEAR (Alternate )
SHRI SOMN~H BANERIEE Cement Manufacturer’s Association,Bombay
CHIEF ENGINEER( RESEARCH-CUM-DIRECTOR) Irrigation Department,Government of Punjab
RESEARCHOFFICER (CONCRETETECHNOLOGY)
(Alternate)
DIRECTOR Gujarat Engineering Research Institute, Baroda
SHRI J. K. PANEL( Alternate )
DIRECTOR Maharashtra Engineering Research Institute, Nasik
RESEARCHOFFICER ( Alternate )
DIRECTOR(CLMDD II) Central Water Commission, New Delhi
,DEPUT~ DIRECTOR( CLMDD II ) ( Alternate )
SHRI R. K. G.XITANI Shree Digvijay Cement Co Ltd, Bombay
DR R. K. &ID ( AJtemate )
DR A. K. CH~UTERJEE The Associated Cement Company Ltd, Bombay
SHRI C. H. PAGE ( AJtemate )
DEPUTYDIRECTOR( B&F ) Research, Designs and Standards Organization, Lucknow
ASSISTANTDESIGN ENGINEER( Alternate )
SHR~V K. MEHTA The Hindustan Construction Co Ltd, Bombay
SHRI U. B. DANGI ( Alternate )
SHRI G. K. MAJUMDAR Hospital Services Consultancy Corporation (India) Ltd, New Delhi
DR IRSHAD MASSED Central Building Research Institute (CSIR), Roorkee
SHRI S. K. GARG ( Alternate )
SHRI R. KUNJITHAP~~ Vishnu Cement Ltd, Hyderabad
EXEC~I-I~E ENGINEER Central Warehousing Corporation, New Delhi
SHRI K. NARANAPPA Central Electricity Authority, New Delhi
SHR~ D. P. KEWALRAGMANI(Alternate )
DR S. C. AHLUWALIA National Council for Cement and Building Materials, New Delhi
SHRI K. H. BABU ( AJtemate )
SHRI M. K. MUKHERJEE Road Wing, Department of Surface Transport, New Delhi
SHRI N. K. S~HA ( AJtemate )
SHRI J .D. DESAI Gujarat Ambuja Cement, Ahmedabad
SHIU B. K. JAG- ( AJtemate )
SHRI y. R. PHULL Central Road Research Institute, New Delhi
SHRI S. S. SEEHRA( Alternate )
DR K. C. NARANG Dalmia Cement (Bharat) Ltd, New Delhi
SHRIC. S. SHARMA(Alternate )
SHlu PuRAM MAL Engineer-in-Chiefs Branch, Army Headquarters, New Delhi
SHRI K. M. NAMB~AR( AJtemate )
SHRI S. A. REDDI Gammon India Ltd, Bombay
PROJECT DIRECTOR Cement Corporation of India Ltd, New Delhi
SHRI M. P. SINGH Federation of Mini Cement Plants, New Delhi
SUPERRJTENDMG ENGINEER( D ) Public Works Department, Government of Tamil Nadu
SENIORDEPIJIY CHIEF ENGINEER( GENERAL )
(Alternate )
SHRl S. B. SURI Central Soil L Materials Research Station, New Delhi
SHRI N. CHANDRASEKARAN ( AJtemate )
SHRI L. SWA~XIP Orissa Cement Ltd. New Delhi
SHRI H. BHATTACHARYE ( Alternate )
SHRI D. P. CHAKRAWAKtl Bhilai Steel Plant. Bhilai
SHRI RAJAN C. M~~~HAw( AJtemate )

4
Bureau of Indian Standards

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development of the activities of standardization, marking and quality certification of goods and attending to
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Review of Indian Standards

Amendmehts are issued to standards as the need arises on the basis of comments. Standards are also reviewed
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should ascertain that they are in possession of the latest amendments or edition.

This Indian Standard has been developed from Dot No. CED 2 ( 5168 ).

Amendments Issued Since Publication

Amend No. Date of Issue Text Affected

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