TECHNICAL SPECIFICATION SHEET-H For North OBM

中国石油川庆钻探工程有限公司
CNPC Chuanqing Drilling Engineering Company Ltd. (CCDC)

No. 6, Meng Zhui Wan St. Chengdu, P R China, Tel: 0086-28-83330871, 0086-28-83336605
SECTION 8 TECHNICAL
SPECIFICATION SHEET-H
for
OGDCL North Region
39- 43. OIL BASE MUD PACKAGE
DETAILS OF PACKAGE
The package will consist of the following chemicals/additives.
39. Primary emulsifier for oil base mud
40. Secondary emulsifier for oil base mud
41. Viscosifier / Oil base mud gel
42. Fluid Loss Control Agent / high temperature stabilizer for oil base mud
43. Wetting agent for oil base mud
The OBM package provided by CCDC which consists of 7 chemicals.
(1) Primary emulsifier TYODF-301

(2)Secondary emulsifier TYODF-401 same function with Wetting agent
(3)Viscosifier / Oil base mud gel TYODF-601
Tender Enquiry No. PROC-SERVICES/CB/WS-4223/2019- Hiring of Mud Engineering Services (North) 1

CNPC Chuanqing Drilling Engineering Company Ltd. (CCDC) Pakistan Branch
House No.56, St. No.1, F6/3, Islamabad, Pakistan. Tel: 0092-51-111-822-922 Fax: 0092-51-2826826 mail: [email protected]
(4)Fluid Loss Control Agent TYODF-101

(5)Wetting agent for oil base mud TYODF-501
(6) Lime/CaO
(7) Calcium Chloride/ CaCl2
39- 43. OIL BASE MUD PACKAGE
39.Primary emulsifier for oil base mud

TYODF-301
SR. PHYSICAL EXACT VALUE OF THE
Specification
NO. PROPERTIES OFFERED PRODUCT
1 Appearance Thick liquid to cream
2 Apparent Viscosity, cP 10~30

Precipitated water at
3 0 Maximum
25℃*8 hrs, ml
Precipitated oil at
4 2 Maximum
25℃*8 hrs, ml
Break Down Voltage
5 400 Minimum
(volts）
40.Secondary emulsifier for oil base mud

TYODF-401
Specification
3 0 Maximum
25℃*8 hrs, ml
Precipitated oil at 25℃*8
4 10 Maximum
hrs, ml
Break Down Voltage
5 400 Minimum
(volts）
41.Viscosifier / Oil base mud gel

TYODF-601
Specification
1 Appearance Free flowing powder
2 Loss on Drying (% by 10 Maximum

weight)
Retention on 100 US
3 10 Maximum
Mesh Sieve,%
4 Colloid fraction,% 80 Minimum
42. Fluid Loss Control Agent / high temperature stabilizer for oil base mud
TYODF-101
Specification
Black to black gray ,free flowing
1 Appearance
powder
Retention on 30 US
2 10 Maximum
Mesh Sieve,%
Loss on Drying (% by
3 10 Maximum
weight)
4 API fluid loss, ml 2.5 Maximum
HTHP fluid loss
5 12 Maximum
(150℃,3.5MPa), ml
43.Wetting agent for oil base mud
TYODF-501
Specification
3 0 Maximum
25℃*8 hrs, ml
Precipitated oil at
4 10 Maximum
25℃*8 hrs, ml
OBM PERFORMANCE TEST
PERFORMANCE TEST
The supplier will mention the exact quantities of the above said chemicals / additives of the package,
Barite and HSD oil along with detail mixing procedure to formulate 1 liter of oil base mud ( oil water
ratio 90:10, containing 28 grams of 94 % pure anhydrous calcium chloride CaCl 2 ) in 100 ml
distilled water ( having the following properties at 49(+) 3°C.
1. Specific Gravity = 2.0
2. Yield Point = 30 lbs/100 sq.ft (Maximum)
3. HT-HP Fluid Loss at 175° C and 500 Psi differential pressure=10 ml (Max)
4. Break Down Voltage = 1200 volts (Minimum)
The oil base mud having above mentioned properties, when hot rolled in a roller oven for 16 hrs at

175°C, cooled to 49 (+) 3° C and stirred for 20 minutes in Hamilton Beach Mixer at high speed,
should have not more than 10 % variation in the values of above mentioned properties.
The OBM Formula:

900ml HSD oil+0.5%Primary Emulsifier TY ODF-301+1.8% Secondary Emulsifier TY ODF 401+2.0%
Wetting Agent TY ODF501+3.0% Viscosifier TY ODF-601+100ml (CaCl2 brine)+3.0%Lime
+8.0%Fluid Loss Control Agent TYODF-101+Barite (O/W=90:10, Specific Gravity=2.0 SG).
Remark: The concentration of each chemical is based on 1000ml base fluid, and calculated on (M/V)%.
Details Mixing Procedure of pilot sample：
1. Calcium chloride brine mixing steps:
(1) Measure the 100ml distilled water , pour into a beaker,stir it on the Hamilton Beach Mixer at
speed of 200 rpm;
(2) Add 28g calcium chloride into the beaker slowly, continue to stir after all the calcium chloride
dissolved.
2.OBM mixing steps:
(1)According to the Formulation of oil-based drilling fluid, a certain amount of Primary Emulsifier
TYODF301(5.0g), Secondary Emulsifier TYODF 401(18.0g) and Wetting Agent TYODF 501
(20.0g)directly weighed in the mud mixing cup. Then, Measuring 0# Diesel with Volume of 900 mL into
mud mixing cup.
(2) Then, the emulsifier, wetting agent and 0# diesel oil in the mixing mud cup were stirred by a high-
speed mixer with a stirring speed of 12 000 rpm for 10 minutes, so that the emulsifier and diesel oil were
fully and uniformly mixed.

(3)Weigh a certain amount of Viscosifier TYODF-601(30.0g) with a balance . In the state of high
stirring(12 000 rpm), the Viscosifier TYODF-601 was added into the mud mixing cup and stirred for 20
minutes.
(4)Calcium chloride aqueous solution was prepared by adding 28g calcium chloride into 100 mL
distilled water . In the state of high stirring(12 000 rpm), 35 mL above-mentioned Calcium
chlorideaqueous solution was added into the mud mixing cup and stirred for 10 minutes.
(5)Weigh Lime (30.0g)with a balance . In the state of high stirring(12 000 rpm), the calcium oxide was
added into the mud mixing cup and stirred for 10 minutes.
(6)Remove the high stirring cup, scrape the material attached to the wall of the cup into the high stirring
cup with a glass rod, and then place the high stirring cup on the high stirring machine.
(7)Weigh a certain amount of Fluid Loss Control Agent TYODF-101(80.0g) with a balance . In the state
of high stirring(12 000 rpm), the Fluid Loss Control Agent TYODF-101was added into the mud mixing
OBM PERFORMANCE TEST
EXACT VALUE OF THE
OFFERED PRODUCT
PHYSICAL REQUIRED
SR.NO. BEFORE AFTER HOT
PROPERTIES SPECIFICATIONS
HOT ROLLING AT
ROLLING 175°C
1 Specific Gravity (S.G) 2.0
2 Yield Point (lbs/100 sq.ft) 30 Maximum
3 HT-HP Fluid Loss (ml) 10 Maximum
4 Break Down Voltage (volts） 1200 Minimum


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中国石油川庆钻探工程有限公司

CNPC Chuanqing Drilling Engineering Company Ltd. (CCDC)

39- 43. OIL BASE MUD PACKAGE

The OBM package provided by CCDC which consists of 7 chemicals.

(1) Primary emulsifier TYODF-301

Tender Enquiry No. PROC-SERVICES/CB/WS-4223/2019- Hiring of Mud Engineering Services (North) 1

(4)Fluid Loss Control Agent TYODF-101

39- 43. OIL BASE MUD PACKAGE

39.Primary emulsifier for oil base mud

1 Appearance Thick liquid to cream

2 Apparent Viscosity, cP 10~30

40.Secondary emulsifier for oil base mud

41.Viscosifier / Oil base mud gel

Tender Enquiry No. PROC-SERVICES/CB/WS-4223/2019- Hiring of Mud Engineering Services (North) 2

OBM PERFORMANCE TEST

Tender Enquiry No. PROC-SERVICES/CB/WS-4223/2019- Hiring of Mud Engineering Services (North) 3

The OBM Formula:

Tender Enquiry No. PROC-SERVICES/CB/WS-4223/2019- Hiring of Mud Engineering Services (North) 4

Tender Enquiry No. PROC-SERVICES/CB/WS-4223/2019- Hiring of Mud Engineering Services (North) 5

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