Magnetic Particle Testing: Standard Practice For

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Designation: E1444/E1444M − 16´1

Standard Practice for


Magnetic Particle Testing1
This standard is issued under the fixed designation E1444/E1444M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.

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This standard has been approved for use by agencies of the U.S. Department of Defense.

ε1 NOTE—Summary of Changes updated editorially in July 2016.

1. Scope* priate safety and health practices and determine the applica-
1.1 This practice establishes minimum requirements for bility of regulatory limitations prior to use.
magnetic particle testing used for the detection of surface or
slightly subsurface discontinuities in ferromagnetic material. 2. Referenced Documents
Guide E709 can be used in conjunction with this practice as a 2.1 The following documents form a part of this standard
tutorial. practice to the extent specified herein.
NOTE 1—This Practice replaces MIL-STD-1949. 2.2 ASTM Standards:2
1.2 The magnetic particle testing method is used to detect A275/A275M Practice for Magnetic Particle Examination of
cracks, laps, seams, inclusions, and other discontinuities on or Steel Forgings
near the surface of ferromagnetic materials. Magnetic particle A456/A456M Specification for Magnetic Particle Examina-
testing may be applied to raw material, billets, finished and tion of Large Crankshaft Forgings
semi-finished materials, welds, and in-service parts. Magnetic E543 Specification for Agencies Performing Nondestructive
particle testing is not applicable to non-ferromagnetic metals Testing
and alloys such as austenitic stainless steels. See Appendix X1 E709 Guide for Magnetic Particle Testing
for additional information. E1316 Terminology for Nondestructive Examinations
E2297 Guide for Use of UV-A and Visible Light Sources and
1.3 All areas of this Practice may be open to agreement Meters used in the Liquid Penetrant and Magnetic Particle
between the Cognizant Engineering Organization and the Methods
supplier, or specific direction from the Cognizant Engineering E3022 Practice for Measurement of Emission Characteris-
Organization. tics and Requirements for LED UV-A Lamps Used in
1.4 This standard is a combined standard, an ASTM stan- Fluorescent Penetrant and Magnetic Particle Testing
dard in which rationalized SI units and inch-pound units are 2.3 ASNT Documents:3
included in the same standard, with each system of units to be SNT-TC-1A Recommended Practice No. “Personnel Quali-
regarded separately as standard. fication and Certification in Nondestructive Testing
1.4.1 Units—The values stated in either SI units or inch- ANSI/ASNT CP-189 Standard for Qualification and Certifi-
pound units are to be regarded separately as standard. The cation of NDT Personnel
values stated in each system may not be exact equivalents;
2.4 Society of Automotive Engineers (SAE)-AMS
therefore, each system shall be used independently of the other.
Documents:4,5
Combining values from the two systems may result in non-
AMS 2641 Magnetic Particle Inspection Vehicle
conformance with the standard.
1.5 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
responsibility of the user of this standard to establish appro- contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3
Available from American Society for Nondestructive Testing (ASNT), P.O. Box
1
This practice is under the jurisdiction of ASTM Committee E07 on Nonde- 28518, 1711 Arlingate Ln., Columbus, OH 43228-0518, http://www.asnt.org.
4
structive Testing and is the direct responsibility of Subcommittee E07.03 on Liquid Copies of standards, specifications, drawings, and publications required by
Penetrant and Magnetic Particle Methods. manufacturers in connection with specification acquisition should be obtained from
Current edition approved June 1, 2016. Published June 2016. Originally the contracting activity or as directed by the contracting officer.
5
approved in 1991. Last previous edition approved in 2012 as E1444 - 12. DOI: Available from SAE International (SAE), 400 Commonwealth Dr., Warrendale,
10.1520/E1444_E1444M-16ϵ1. PA 15096-0001, http://www.sae.org.

*A Summary of Changes section appears at the end of this standard


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AMS 3040 Magnetic Particles, Nonfluorescent, Dry 2.11 DoD Contracts—Unless otherwise specified, the edi-
Method tions of the documents that are DoD adopted are those listed in
AMS 3041 Magnetic Particles, Nonfluorescent, Wet the issue of the DoDISS (Department of Defense Index of
Method, Oil Vehicle, Ready-To-Use Specifications and Standards) cited in the solicitation.
AMS 3042 Magnetic Particles, Nonfluorescent, Wet
Method, Dry Powder 2.12 Order of Precedence—In the event of conflict between
AMS 3043 Magnetic Particles, Nonfluorescent, Wet the text of this practice and the referenced documents cited
Method, Oil Vehicle, Aerosol Packaged herein, the text of this practice takes precedence.
AMS 3044 Magnetic Particles, Fluorescent, Wet Method,
Dry Powder
AMS 3045 Magnetic Particles, Fluorescent, Wet Method, 3. Terminology
Oil Vehicle, Ready-To-Use 3.1 Definitions—The definitions relating to magnetic par-
AMS 3046 Magnetic Particles, Fluorescent, Wet Method, ticle testing, which appear in Terminology E1316, shall apply
Oil Vehicle, Aerosol Packaged5 to the terms used in this practice.
AMS 5062 Steel, Low Carbon Bars, Forgings, Tubing,
Sheet, Strip, and Plate 0.25 Carbon, Maximum 4. Significance and Use
AMS 5355 Investment Castings 4.1 Description of Process—Magnetic particle testing con-
AMS I-83387 Inspection Process, Magnetic Rubber sists of magnetizing the area to be examined, applying suitably
AMS 2175 Castings, Classification and Inspection of prepared magnetic particles while the area is magnetized, and
AS 4792 Water Conditioning Agents for Aqueous Magnetic subsequently interpreting and evaluating any resulting particle
Particle Inspection accumulations. Maximum detectability occurs when the dis-
AS 5282 Tool Steel Ring Standard for Magnetic Particle continuity is positioned on the surface and perpendicular to the
Inspection magnetic flux.
AS 5371 Reference Standards Notched Shims for Magnetic
4.2 This practice establishes the basic parameters for con-
Particle Inspection
trolling the application of the magnetic particle testing method.
2.5 Federal Standards:4,6 This practice is written so that it can be specified on the
FED-STD-313 Material Safety Data Sheets, Preparation and engineering drawing, specification, or contract. It is not a
the Submission of detailed how-to procedure to be used by the examination
FED-STD-595 Colors personnel and, therefore, must be supplemented by a detailed
2.6 Military Standards:4,6 written procedure that conforms to the requirements of this
MIL-STD 45562A Calibration Systems Requirements practice.
A-A-59230 Fluid, Magnetic Particle Inspection, Suspension
5. General Practice
2.7 OSHA Document:7
5.1 Personnel Qualification—Personnel performing exami-
29 CFR 1910.1200 Hazard Communication
nations in accordance with this practice shall be qualified and
2.8 ANSI Document:4,8 certified in accordance with ASNT Recommended Practice No.
ANSI/NCSL Z 540-1 General Requirement for Calibration SNT-TC-1A, ANSI/ASNT Standard CP-189, NAS 410, or as
Laboratories and Measuring Test Equipment specified in the contract or purchase order.
2.9 ISO Document: 5.2 Agency Qualification—If specified in the contractual
ISO 10012-1 Measurement Management Systems— agreement, NDT agencies shall be qualified and evaluated as
Requirements for Measurement Processes and Measuring described in E543. The applicable edition of E543 shall be
Equipment9 specified in the contractual agreement.
2.10 AIA Document: 5.3 Written Procedure—Magnetic particle testing shall be
NAS 410 NAS Certification and Qualification of Nonde- performed in accordance with a written procedure applicable to
structive Test Personnel10 the part or group of parts under examination. The procedure
shall be in accordance with the requirements of this Practice.
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The process, when conducted in accordance with the written


6
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
procedure, shall be capable of detecting discontinuities speci-
Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:// fied in the acceptance criteria. The written procedure may be
dodssp.daps.dla.mil. general if it clearly applies to all of the specified parts being
7
Available from U.S. Government Printing Office Superintendent of Documents, examined and meets the requirements of this practice. All
732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http://
www.access.gpo.gov. written procedures, including technique sheets for specific
8
Available from National Conference of Standards Laboratories, 1800 30th St. parts, shall be approved by an individual qualified and certified
Suite 305b, Boulder, CO. 80301.
9
at Level III for magnetic particle testing in accordance with the
Available from International Organization for Standardization (ISO), 1, ch. de
requirements of 5.1. Procedures shall be submitted to the
la Voie-Creuse, CP 56, CH-1211 Geneva 20, Switzerland, http://www.iso.org.
10
Available from Aerospace Industries Association of America, Inc. (AIA), 1000 Cognizant Engineering Organization for review, or approval,
Wilson Blvd., Suite 1700, Arlington, VA 22209-3928, http://www.aia-aerospace.org. or both, when requested.

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5.3.1 Elements of the Written Procedure—The written pro- discontinuities. Such operations include, but are not limited to,
cedure shall include at least the following elements, either forging, heat treating, electroplating, forming, welding,
directly or by reference to the applicable documents: grinding, straightening, machining, and proof loading.
5.3.1.1 Procedure identification number and the date it was 5.4.1 Perform magnetic particle examination prior to shot
written; peening (to provide a beneficial compressive layer) and prior to
5.3.1.2 Identification of the part(s) to which the procedure applying protective finishes such as priming, painting, plating
applies; this shall include the material, or alloy, or both; (see 5.4.3 through 5.4.3.5) or other coatings.
5.3.1.3 For new components, sequence of magnetic particle 5.4.2 In-process examinations may not be substituted for
testing as related to manufacturing process operation (for final examination.
example, post plating, after heat treat, etc.);
5.3.1.4 Identification of test parts used for system perfor- 5.4.3 Plating and Coatings—Examine parts which will
mance verification (see 7.1.1 and 7.1.2); receive either a plating or coating as follows:
5.3.1.5 Process controls (see Table 1); 5.4.3.1 Examination is required prior to all non-
5.3.1.6 Areas of the part to be examined; electroplated coatings.
5.3.1.7 Part preparation required before examination; 5.4.3.2 Electroplated surfaces with a final plating thickness
5.3.1.8 Directions for positioning the item with respect to of 0.0008 in. [0.02 mm] or less shall be examined either before
the magnetizing equipment; or after electroplating, or grinding, or both, of electroplated
5.3.1.9 The type of magnetizing current and the equipment surfaces.
to be used; 5.4.3.3 Electroplated surfaces with a final plating thickness
5.3.1.10 Method of establishing the magnetization (head, of between 0.0008 in. [0.02 mm] and 0.0050 in. [0.13 mm]
coil, prods, yoke, cable wrap, etc.); shall be examined both before and after electroplating, or
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5.3.1.11 Directions of magnetization to be used, the order in grinding, or both, of electroplated surfaces.
which they are applied, and any demagnetization procedures to (1) Electroplated surfaces with a final plating thickness of
be used between shots; 0.0050 in. [0.13 mm] or greater shall be examined before
5.3.1.12 The current level, or the number of ampere turns, to electroplating, or grinding, or both, of electroplated surfaces.
be used and the duration of its application; (2) Magnetic particle examination after electroplating is
5.3.1.13 Type of magnetic particle material (dry or wet, not required for steels with a tensile strength less than or equal
visible or fluorescent, etc.) to be used and the method and to 160 ksi.
equipment to be used for its application and, for the case of wet
5.4.3.4 Use caution when examining parts with an electro-
particles, the particle concentration limits;
plated nickel coating as indications may form from the
5.3.1.14 Type of records and method of marking parts after
resulting leakage fields within the nickel plating itself.
examination;
5.3.1.15 Acceptance requirements, to be used for evaluating 5.4.3.5 For in-service examination, plating or coatings do
indications and disposition of parts after evaluation; and not require removal prior to examination unless they are
5.3.1.16 Post-examination demagnetization and cleaning re- damaged, or they interfere with the examination process.
quirements. 5.5 Materials:
5.4 Examination Sequence—Perform magnetic particle ex- 5.5.1 Dry Particle Requirements—Dry particles shall meet
amination after all operations which might cause or reveal the requirements of AMS 3040.

TABLE 1 Required Verification Intervals


Item Maximum Time Paragraph
Between VerificationA
Lighting:B
Visible light intensity Weekly 7.3.1.1
Ambient light intensity Weekly 7.3.1.2
Black light intensity Daily 7.3.2, 7.4.5
Battery powered black Before and after each use 7.4.5.2
light intensity check
Black light integrity Weekly 7.3.2
System Performance:B Daily 7.1, 7.1.1, 7.1.2
Wet particle concentration 8 hours, or every shift change 7.2.1.1
Wet particle contamination:B 1 week 7.2.1.2
Water break test Daily 7.2.2
Equipment calibration check:B
Ammeter accuracy 6 months 7.4.1
Timer control 6 months 7.4.2
Quick break 6 months 7.4.3
Yoke dead weight check 6 months 7.4.4
Black and white light meters 6 months 7.4.7
Gaussmeter or Field Indicator accuracy 6 months 7.4.6
A
When the test system is in operation.
B
The maximum time between verifications may be reduced or extended when substantiated by actual technical/reliability data.

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5.5.2 Wet Particle Requirements—Wet particles shall meet 6.1.1 Pre-examination Demagnetization—The part shall be
the requirements of AMS 3041, 3042, 3043, 3044, 3045, or demagnetized before testing if prior operations have produced
3046, as applicable. a residual magnetic field that may interfere with the examina-
5.5.3 Suspension Vehicles—The suspension vehicle for the tion.
wet method shall be a light petroleum distillate conforming to 6.1.2 Surface Cleanliness and Finish—The surface of the
AMS 2641 (Type I) or A-A-59230, or a suitably conditioned part to be examined shall be essentially smooth, clean, dry, and
water that conforms to the requirements of 5.5.4. When free of oil, scale, machining marks, or other contaminants or
approved by the contracting agency, AMS 2641 (Type II) may conditions that might interfere with the efficiency of the
be used. When specified, the oil suspension vehicle shall meet examination.
the salient characteristics specified in A-A-59230. 6.1.3 Plugging and Masking—Plugging and masking is
required when specified by the Cognizant Engineering Orga-
5.5.4 Conditioned Water Vehicle—When water is used as a
nization.
suspension vehicle for magnetic particles, the conditioning
6.1.4 All areas on the part where electrical contact is made
agents used shall comply with AS 4792. Proper wetting shall
shall be sufficiently clean to prevent electrical arcing.
be determined by a water break test (see 7.2.2). Smoother
6.1.5 Aircraft-Quality Steel Cleanliness—The examination
surfaces generally require a greater percent of wetting agent
of aircraft-quality steel for cleanliness using magnetic particle
than rough surfaces. Foaming of the bath must be minimized to
testing shall be as appropriate to the type of steel being
the point that it does not interfere with the examination inspected. However, testing of parts fabricated from this
process. material shall be in accordance with the requirements of this
5.5.4.1 Water Vehicle Conditioning Agents—Any agents practice.
added to the water vehicle for any purpose shall conform to the
6.2 Magnetization Methods:
requirements of the particle manufacturer.
6.2.1 Types of Magnetizing Current—The types of currents
5.5.5 Particle Concentration—The concentration of par- used for magnetic particle testing are full-wave rectified
ticles in the suspension bath shall be as specified in the written current (1 or 3 phase), half-wave rectified current, and alter-
procedure. Particle concentrations outside of the range of 0.1 to nating current. The equipment used shall fulfill the magnetiz-
0.4 mL in a 100-mL bath sample for fluorescent particles and ing and demagnetizing requirements adequately, as outlined
1.2 to 2.4 mL in a 100 mL sample for nonfluorescent particles herein, without damage to the part under examination, and they
shall not be used. Fluorescent particles and nonfluorescent shall include the necessary features required for safe operation.
particles shall not be used together. 6.2.2 Permanent Magnets—Permanent magnets are not to
5.6 Safety—The safe handling of magnetic particles (wet or be used for magnetic particle testing unless specifically autho-
dry), oil vehicles, water baths, and water conditioner concen- rized by the Cognizant Engineering Organization. When per-
trates are governed by the suppliers’ Material Safety Data manent magnets are used, adequate magnetic field strength
Sheets (MSDS). Material Safety Data Sheets, conforming to 29 shall be established in accordance with 7.4.4.
CFR 1910.1200, or equivalent, must be provided by the 6.2.3 Yokes—When using yokes (electromagnetic probes)
supplier to any user and shall be prepared in accordance with for magnetic particle testing, they shall meet the requirements
FEDSTD-313. of 7.4.4.
6.2.4 Magnetizing Current Application—Alternating current
5.6.1 Flammability—Flash point of oil vehicles shall be in
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is to be only used for the detection of discontinuities open to


accordance with AMS 2641, Type I carriers. The suppliers’
the surface. Full-wave direct current has the deepest possible
MSDS shall certify the flash point.
penetration and must be used for examination of sub-surface
5.6.2 Personnel Hazards—Precautions against inhalation, discontinuities when using the wet magnetic particle method.
skin contact, and eye exposure are detailed in the suppliers’ Half-wave direct current can also be used for examination of
MSDS. These precautions shall be observed. sub-surface discontinuities and due to the pulsating nature of
5.6.3 Electrical Hazards—Magnetizing equipment shall be the waveform; it has the advantage of increased particle
maintained properly to prevent personnel hazards from elec- mobility.
trical short circuits. Care must be taken to reduce arcing and 6.2.5 Magnetic Field Directions—Discontinuities are diffi-
the possible ignition of oil baths. cult to detect by the magnetic particle method when they make
5.6.4 Black Light—Replace cracked or broken ultraviolet an angle less than 45° to the direction of magnetization. To
filters immediately. Broken filters can allow harmful shortwave ensure the detection of discontinuities in any direction, each
ultraviolet energy to be emitted and must be replaced imme- part must be magnetized in a minimum of two directions at
diately. Spectacles designed to absorb ultraviolet wavelength approximately right angles to each other. Depending on part
radiation are suggested for close, high-intensity black light geometry, this may consist of circular magnetization in two or
examination. LED UV-A lamps used for evaluation purposes more directions, multiple circular and longitudinal
shall comply with Practice E3022. magnetization, or of longitudinal magnetization in two or more
directions. The pie gauge as illustrated in Fig. X5.1, the flexible
laminated strips as described in Annex A3, or a properly
6. Specific Practice
prepared master part using notched shims may only be used as
6.1 Preparation of Parts for Testing: a tool to demonstrate the direction of the external magnetic

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field. The pie gauge or flexible laminated strips shall not be masking of relevant indications by nonrelevant accumulations
used to determine adequate field strength. Exceptions necessi- of magnetic particles. Adequate magnetic field strength may be
tated by part geometry, size, or other factors require specific determined by one or a combination of the following methods:
approval of the Cognizant Engineering Organization. 6.3.1.1 In unidirectional, or multidirectional magnetizing
6.2.6 Multidirectional Magnetization—Multidirectional applications, by examining parts having known or artificial
magnetization may be used to fulfill the requirement for discontinuities of the type, size, and location specified in the
magnetization in two or more directions if it is demonstrated acceptance requirements or by using the notched shims as
that it is effective in all areas, which require examination as defined in Annex A1;
practical. Test parts in accordance with 6.3.1.1 or shims 6.3.1.2 In unidirectional magnetizing applications only, by
manufactured to the requirements of AS 5371, or as otherwise using a Hall Effect probe gaussmeter capable of measuring the
approved by the Cognizant Engineering Organization, shall be peak values of the tangential field as described in Annex A5.
used to verify field direction, strength, and balance in multidi- Tangential-field strengths shall have a minimum value of 30
rectional magnetization. Balancing of the combined magnetic Gauss (30 × 10-4 Tesla [T]) when measured at the part surface
field is critical and an adequate balance must be visually using a Hall Effect probe gaussmeter as described in Annex
demonstrated to be effective in all areas, which require A5. The maximum Gauss value derived is limited by the
examination. The particle application must be timed so that the restrictions of 6.3.1.
magnetization levels reach full value in all directions while the 6.3.1.3 Using the current levels specified by the formulas
particles are mobile on the surface under examination. The given in Appendix X3 and Appendix X4. These current levels
residual method shall only be used with the approval of the and formulas provide only a rough guide and shall only be used
Cognizant Engineering Organization. in conjunction with either 6.3.1.1, or 6.3.1.2, or Cognizant
6.2.7 Direct Magnetization—Direct magnetization is ac- Engineering Organization approval, or a combination thereof.
complished by passing current directly through the part under In some cases the formulas in Appendix X3 and Appendix X4
examination. Electrical contact is made to the part using head may lead to over magnetization of the work piece and care
and tail stock, prods, clamps, magnetic leeches, or by other should be exercised when using them.
means. Caution shall be taken to ensure that the electrical 6.3.2 Longitudinal Magnetization Using Coils—
current is not flowing while contacts are being applied or Longitudinal magnetization is often accomplished by passing
removed and that excessive heating does not occur in any area current through a coil encircling the part, or section of the part,
of the part. Unless otherwise specified by the Cognizant to be examined (that is, by using a coil shot). This produces a
Engineering Organization, prods shall not be used for the magnetic field parallel to the axis of the coil. The actual
examination of aerospace components (flight hardware) or on effective distance must be demonstrated based on the particular
finished surfaces. part to be examined. For parts longer than these effective
6.2.8 Indirect Magnetization—Indirect part magnetization distances, the entire length shall be examined by repositioning
uses pre-formed coils, cable wraps, yokes, field (flux) flow the part within the coil, allowing for approximately 10 %
fixtures, or a central conductor to induce a magnetic field in a effective magnetic field overlap. See 6.3.1 for field strength
part when no direct electrical contact is made. methods that can be used in coil magnetization.
6.2.9 Induced Current Magnetization—Induced current 6.4 Particle Application:
magnetization (toroidal or circumferential field) is accom-
6.4.1 Dry Magnetic Particle Application, Continuous
plished by inductively coupling a part to an electrical coil in
Method—When using dry particles, the flow of magnetizing
order to create a suitable current flow within the part as
current shall be initiated prior to application of the magnetic
illustrated in Fig. X5.2. This method is often advantageous on
particles to the surface under examination and terminated after
ring-shaped parts with a central aperture and with an L/D ratio
powder application has been completed and any excess blown
less than three, especially where the elimination of arcing or
off. Precautions shall be taken to prevent any damage to the
burning is of vital importance.
part due to overheating.
6.2.10 Parallel Current Induced Magnetization—This
6.4.1.1 Apply dry powder so that a light, uniform, dust-like
method of magnetization may occur when a ferromagnetic part
coating settles on the surface of the part under examination
is placed alongside and parallel to a current-carrying conduc-
while the part is being magnetized. Specially designed powder
tor. A magnetic field will be induced in the part that is more
blowers or shakers using compressed air or hand power shall
transverse than circular. This type of magnetization shall not be
be used. The applicators shall introduce the particles into the
used for magnetic particle testing unless approved by the
air in a manner such that they reach the part surface in a
Cognizant Engineering Organization.
uniform cloud with a minimum of force.
6.2.11 Magnetization of Aerospace Lifting Hardware—The
6.4.1.2 After the powder is applied, and before the magne-
use of permanent magnets, electromagnetic yokes, coil wraps
tizing force is removed, excess powder shall be removed, by
or prods on aerospace lifting hardware must be approved by the
means of a dry air current with sufficient force to remove the
Cognizant Engineering Organization.
excess particles if it interferes with interpretation and
6.3 Magnetic Field Strength: evaluation, but not strong enough to disturb particles held by a
6.3.1 Magnetic Field Strength—The applied magnetic field leakage field that is indicative of discontinuities. In order to
shall have sufficient strength to produce satisfactory recognize the broad, fuzzy, lightly held powder patterns formed
indications, but it must not be so strong that it causes the by near-surface discontinuities, the formation of indications
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must be observed carefully during both powder application and the part under examination during the period of its cure. Before
removal of the excess powder. The dry particle method shall curing takes place, and while the magnetic particles are still
not be used to examine aerospace components (flight hard- mobile, the part shall be magnetized to the specified level. This
ware). Dry magnetic particles shall not be reused. requires prolonged or repeated periods of magnetization. This
6.4.2 Wet Magnetic Particle Application, Continuous method is for special applications, such as bolt holes which
Method—Fluorescent or nonfluorescent particles suspended in cannot be examined readily by the wet or dry method, and shall
a liquid vehicle at the required concentration shall be applied be used only when specifically approved by the Cognizant
by gently spraying or flowing the suspension over the area to Engineering Organization. AMS-I-83387 establishes the ex-
be examined. amination process for magnetic rubber.
6.4.2.1 Proper sequencing and timing of part magnetization 6.4.6 Particle Selection for Aerospace Lifting Hardware—
and application of particle suspension are required to obtain the The use of dry powder or non-fluorescent wet particles on
proper formation and retention of indications. This requires aerospace lifting hardware must be approved by the Cognizant
that the stream of suspension be diverted from the part Engineering Organization.
simultaneously with, or slightly before, energizing the mag- 6.5 Evaluation—Following magnetization and particle
netic circuit. application, the parts shall be examined for indications. All

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6.4.2.2 The magnetizing current shall be applied for a indications will be identified as relevant or nonrelevant. Rel-
duration of at least 0.5 second for each application, with a evant indications will be compared to the proper accept/reject
minimum of two shots being used. The second shot shall criteria and the parts accepted or rejected accordingly.
follow the first while the particles are still mobile on the 6.5.1 Eye Glasses—When using fluorescent materials, per-
surface of the part. sonnel shall not wear eye glasses that are photochromic or that
6.4.2.3 Under special circumstances, such as the use of have permanently darkened lenses. This is not intended to
automated equipment or for critical parts, the 0.5–second prohibit the use of eyeglasses with lenses treated to absorb
duration and the two-shot requirement may be waived provided ultraviolet light.
it is demonstrated that the procedure can detect known discon- 6.5.2 Dark Adaptation—Personnel must wait at least one
tinuities in reference parts. minute after entering a darkened area for their eyes to adjust to
6.4.2.4 Care shall be exercised to prevent any damage to the the low-level lighting before performing fluorescent magnetic
part due to overheating or other causes. Weakly held indica- particle testing.
tions on highly finished parts are readily washed away, and 6.5.3 Acceptance Requirements—The acceptance require-
care must be exercised to prevent high-velocity flow over ments applicable to the part or group of parts shall be
critical surfaces. incorporated as part of the written procedure either specifically
6.4.2.5 Particle application by continuous immersion shall or by reference to other applicable documents containing the
be used only when specifically approved by the Cognizant necessary information. When parts are zoned, the acceptance
Engineering Organization or when it has been documented that criteria for each zone shall be specified. Methods for establish-
it can detect discontinuities or artificial discontinuities in parts ing acceptance requirements for large crankshaft forgings are
under examination. covered in Specification A456/A456M. Methods for establish-
6.4.3 Residual Magnetization Method—In the residual mag- ing requirements for steel forgings are covered in Practice
netization method, the magnetic particles are applied to the part A275/A275M. Methods for classifying metal castings are
under examination after the magnetizing force has been dis- given in AMS 2175 and AMS 5355.
continued. The residual method is not as sensitive as the 6.6 Recording of Indications—When required by the written
continuous method. It can be useful on materials with high procedure, the location of all rejectable indications shall be
retentivity. It is also useful for the examination of parts or areas marked on the part, and permanent records of the location,
of parts, which because of geometric constraints, cannot be direction, and frequency of indications may be made by one or
examined with the continuous method. The residual method more of the following methods:
shall be used only when specifically approved by the Cognizant 6.6.1 Written Description—By recording the location,
Engineering Organization or when it has been documented that length, direction, and number of indications in sketch or tabular
it can detect discontinuities or artificial discontinuities in parts form.
under examination. The test parts shall have the same material 6.6.2 Transparent Tape—For dry particle indications, by
and processing steps, and similar geometry, to the actual parts applying transparent adhesive-backed tape to which the indi-
being examined. cations will adhere and placing it on an approved form along
6.4.4 Magnetic Slurry/Paint Application—Magnetic paints with information giving its location on the part.
or slurries are applied to the part with a brush, squeeze bottle, 6.6.3 Strippable Film—By covering the indication with a
or aerosol can before or during the magnetization operation. spray-on strippable film that fixes the indications in place and
This method is for special applications, such as overhead or placing the resultant reproduction on an approved form along
underwater examination. This method may be used only when with information giving its location on the part.
specifically approved by the Cognizant Engineering Organiza- 6.6.4 Photography—By photographing or video recording
tion. the indications themselves, the tape, or the strippable film
6.4.5 Magnetic Polymer Application—Polymerizable mate- reproduction and placing the photograph in a tabular form
rial containing magnetic particles shall be held in contact with along with information giving its location on the part.

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6.7 Post Examination Demagnetization and Cleaning—All 6.9.1.1 When subsequent processing would remove the
parts shall be demagnetized and cleaned after final examina- identification, the applicable marking shall be affixed to the
tion. Apply corrosion protection as required. record accompanying the finished parts or assembly.
6.7.1 Demagnetization: 6.9.1.2 Bolts and nuts and other fastener products may be
6.7.1.1 When using AC demagnetization, the part shall be identified as having met the requirements of magnetic particle
subjected to a field with a peak value greater than, and in nearly testing by marking each package conspicuously.
the same direction as, the field used during examination. This 6.9.2 Impression Stamping, Ink Stamping, Laser Marking,
AC field is then decreased gradually to zero. When using an Dyeing, Vibro Engraving or Etching—Impression stamping,
AC demagnetizing coil, the part is passed through the coil ink stamping, laser marking, dyeing, vibro engraving or
while the current is flowing. For effective demagnetization, etching may be used when permitted or required by the
parts having complex configurations may require rotating or applicable written procedure, detail specification or drawing, or
tumbling while passing through the field of the coil prior to the when the nature of the part is such as to provide for impression
current being shut off. Repeat this process as necessary. stamping of part numbers or other examination personnel
6.7.1.2 When using DC demagnetization, the initial field markings. Impression stamping shall be located only in the
shall be higher than, and in nearly the same direction as, the area provided adjacent to the part number or examination
field reached during examination. The field shall then be personnel’s stamp.
reversed, decreased in magnitude, and the process repeated 6.9.3 Other Identification—Other means of identification,
(cycled) until an acceptably low value of residual field is such as tagging, may be used for parts that have a configuration
--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---

reached. or function precluding the use of stamping, vibro engraving, or


6.7.1.3 Whenever possible, parts that have been magnetized etching, as in the case of completely ground or polished balls,
circularly shall be magnetized in the longitudinal direction rollers, pins, or bushings.
before being demagnetized. After demagnetization, a calibrated 6.10 Identifying Symbols and Color Markings:
field indicator shall not detect magnetic flux fields with an 6.10.1 One-Hundred Percent Examination—When items are
absolute value above 3 G (3 × 10-4 T) anywhere on the part. examined and accepted by 100 % examination, each item shall
6.7.2 Post-examination Cleaning—Cleaning shall be done be marked as follows:
with a suitable solvent, air blower, or by other means. 6.10.1.1 Dyeing—When dyeing is applicable, a dye of
6.7.2.1 Parts shall be examined to ensure that the cleaning acceptable adherence which is predominantly blue (in accor-
procedure has removed magnetic particle residues from holes, dance with FED-STD-595) shall be employed. However, if a
crevices, passage ways, etc. Such residue could have an color conflict is incurred with any other method, magnetic
adverse effect on the intended use of the part. particle examination may be indicated by two adjacent blue
6.7.2.2 Care shall be taken to remove all plugs, masking, or dots or other suitable means.
other processing aids that may affect the intended use of the 6.10.1.2 Stamping, Laser Marking, Vibro Engraving, or
part. Etching—When impression stamping or ink stamping, laser
6.7.2.3 Parts shall be protected from corrosion or damage as marking, vibro engraving, or etching is used to mark 100 %
required. examined parts, the letter “M” with a circle around it shall be
6.8 Record of Examination—Results of all final magnetic employed.
particle examinations shall be recorded. All recorded results 6.10.2 Marking Accepted Lots—When items are accepted
shall be identified, filed, and made available to the cognizant by means of a sampling procedure, each item of an accepted lot
engineering organization upon request. Records shall provide shall be marked as follows:
for traceability to the specific part or lot inspected. As a 6.10.2.1 Dyeing—When dyeing is applicable, a dye of
minimum, the records shall include: identification of the acceptable adherence that is predominantly orange (in accor-
procedure used, disposition of the examination; identification dance with FED-STD-595) shall be employed.
of the inspector’s examination stamp, electronic ID or signa- 6.10.2.2 Stamping, Laser Marking Vibro Engraving, or
ture; and the date of examination. Records shall be kept for a Etching—When impression stamping, vibro engraving or etch-
minimum of three years or as otherwise specified in the ing is used to mark lot examined parts, the letter “M”, without
purchase order or contract. a circle around it shall be employed.
6.9 Marking of Accepted Parts—Unless otherwise specified
by the Cognizant Engineering Organization, parts that have 7. Quality Control
been accepted using magnetic particle testing shall be marked 7.1 System Performance Verification—The overall perfor-
in accordance with the applicable drawing, purchase order, mance of the magnetic particle testing system, including the
contract, or as specified herein prior to leaving the testing equipment, materials, and the lighting environment being used,
facility. shall be verified initially and at regular intervals thereafter. The
6.9.1 Marking shall be applied in such a manner and required verification intervals are stated in Table 1. Records of
location as to be harmless to the part. The identification shall the verification results shall be maintained and retained for the
not be obliterated or smeared by subsequent handling and, time period specified in the contract. Establish a system in
when practicable, placed in a location that will be visible after accordance with ANSI Z540-1 or ISO 10012-1 for calibration
assembly. and certification of all current and voltage measuring devices,

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ammeter shunts, timers, lightmeters, gaussmeters, and field exceeds 30 % of the volume of magnetic particles the bath
indicators used in verification. must be adjusted or replaced.
7.1.1 Use of Test Parts with Discontinuities—A reliable 7.2.2 Water Break Test—In this test of water-based vehicles,
method for system performance verification is the use of a clean part with a surface finish the same as the parts to be
representative reference parts containing discontinuities of the examined or an actual production part is flooded with the
type, location, and size specified in the acceptance require- conditioned water, and the appearance of the surface is noted
ments and examined in accordance with a written procedure. If after flooding is stopped. Sufficient wetting agent is present if

--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---
correct magnetic particle indications can be produced and a continuous even film forms over the entire part. If the film of
identified in these representative parts, the overall system suspension breaks, exposing bare surface, insufficient wetting
performance is verified. Parts used for verification will be agent is present or the part has not been cleaned adequately.
demagnetized, cleaned thoroughly following the examination, For adequacy, this visual observation shall be performed
and checked under black or visible light, as appropriate to the individually under both white light and black light conditions
examination process, to ensure that residual indications do not as applicable.
remain. 7.2.3 Determination of Particle Sensitivity—Appendix X2
describes several devices that can demonstrate the sensitivity
7.1.2 Fabricated Test Parts with Artificial Discontinuities—
of either wet-method or dry-method particles. These devices
When actual production parts with known discontinuities of the
contain permanent magnetization in some form and are inde-
type, location, and size needed for verification are not available
pendent of the magnetizing system. They should not be
or are impractical, fabricated test or production parts with
magnetized or demagnetized before or after use. Such devices
artificial discontinuities or a ring specimen similar to the ring
can be useful whenever performance of the particles are subject
in Annex A4 may be used. Artificial discontinuities may be
to question or need to be verified.
fabricated to meet a particular need or may be commercially
available magnetic field indicators or shims as shown in Annex 7.3 Lighting:
A2. All applicable conditions for the use of such reference 7.3.1 Visible Light—Conduct visible light intensity mea-
parts, as described in 7.1.1, shall apply. surements upon initial light installation, or when changes occur
that would cause the light intensity to change and at the
7.2 Suspension Vehicle Tests (Not required for aerosol can intervals specified in Table 1.
suspensions): 7.3.1.1 Visible light shall be used when examining with
7.2.1 Concentration/Contamination Tests—Particle concen- nonfluorescent magnetic particles and for interpretation of
tration and contamination shall be determined upon start up, at indications found with fluorescent magnetic particles. A mini-
regular intervals thereafter, and whenever the bath is changed mum light intensity of 100 fc [1076 lx] shall be available at the
or adjusted. The required testing intervals are stated in Table 1. surface of the part undergoing examination or evaluation.
7.2.1.1 Determination of Wet Particle Concentration— 7.3.1.2 Ambient Visible Light—Fluorescent magnetic par-
Agitate the particle suspension a minimum of 30 min to ensure ticle examinations shall be performed in a darkened area with
uniform distribution of particles throughout the bath. Place a a maximum ambient visible light level of 2 fc [22 lx] measured
100-mL sample of the agitated suspension in a pear-shaped at the part surface.
centrifuge tube with a graduated stem in 0.05-mL increments 7.3.2 Black Lights—Black lights used for evaluation pur-
for fluorescent baths and 0.1 mL for non-fluorescent baths. poses shall meet the requirements of 7.4.5. The minimum
(Centrifuge tubes shall be as specified in Guide E709). De- acceptable intensity is 1000 µW/cm2 at the surface being
magnetize the sample and allow the tube to stand undisturbed examined. Black lights shall be checked daily for cleanliness
for a settling time of at least 60 min if using petroleum distillate and integrity and shall be cleaned, repaired or replaced as
or at least 30 min for conditioned water suspension. Read the appropriate. These daily checks of cleanliness/integrity need
volume of settled particles. If the concentration is out of the not be recorded. LED UV-A lamps used for evaluation pur-
tolerance stated in the written procedure add particles or poses shall comply with Practice E3022.
suspension vehicle, as required, and re-determine the particle 7.3.3 Restricted Area Examination—Where lamps are
concentration. If the settled particles appear to be loose physically too large to directly illuminate the examination
agglomerates rather than a solid layer, repeat the process with surface, special lighting, such as UV pencil lights, or UV light
a second sample. If the second sample also appears guides, or borescopes shall be used. The image viewed must
agglomerated, replace the entire bath suspension. Thirty- have sufficient resolution to effectively evaluate the required
minute settling times (for oil suspensions), or other accelerated discontinuities. Light intensity shall be measured at the ex-
tests, may be used if they have been verified to give results pected working distance and shall meet the requirements of
equivalent to the procedure described in this clause. 7.3.2 as appropriate.
7.2.1.2 Determination of Wet Particle Contamination— 7.4 Equipment Calibration—Magnetic particle testing
Perform the tests specified in 7.2.1.1. Examine the graduated equipment shall be checked for performance and accuracy at
portion of the tube, under both black light (for fluorescent baths the time of purchase and at intervals thereafter as indicated in
only) and visible light (for both fluorescent and nonfluorescent Table 1; whenever malfunction is suspected, when specified by
baths), for striations or bands, different in color or appearance. the Cognizant Engineering Organization, or whenever electri-
Bands or striations may indicate contamination. If the total cal maintenance that might affect equipment accuracy is
volume of the contaminants, including bands or striations, performed.

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7.4.1 Ammeter Accuracy—To check the equipment its delegate. Minimum acceptable intensity is 1000 µW/cm2 at
ammeter, a suitable calibrated shunt test kit shall be connected 15 in. [38.1 cm] from the front of the filter to the face of the
in series with the output circuit. Comparative readings shall be sensor. All black light filters shall be replaced or otherwise
taken at three output levels encompassing the usable range of corrected as appropriate.
the equipment. The equipment meter reading shall not deviate
NOTE 2—Some UV-A sources other than mercury vapor, for example,
by more than 610 % or 50 amperes, whichever is greater, from micro-discharge, LED, etc., have been shown to have emission charac-
the current value shown by the calibrated ammeter. (When teristics such as excessive visible light, and UV intensity that may result
measuring half-wave rectified current, the current values in fluorescent fade, veiling glare, etc., all of which can significantly
shown by the calibrated FW-Rectified ammeter readings shall degrade examination reliability.
be doubled.) The frequency of the ammeter check is specified 7.4.5.1 Black lights that use a UV-A LED source shall
in Table 1. Machine output repeatability shall not vary more comply with the requirements of Practice E3022.
than 610 % or 50 amperes, whichever is greater, at any 7.4.5.2 Battery-powered black lights used to inspect parts
setpoint and the machine under test shall be marked with the shall have their intensity measured prior to use and after each
value representing the lowest repeatable current level. use.
7.4.2 Timer Control Check—On equipment using a timer to 7.4.6 Gaussmeters—All field indicators shall be calibrated
control the current duration, the timer should be calibrated to and reading taken at a minimum of three points in each
within 60.1 s using a suitable electronic timer. dynamic range and each polarity, in addition to zero.
7.4.3 Magnetic Field Quick Break Check—On equipment 7.4.7 Black Light Meters—All meters shall be calibrated in
that uses a quick break feature, proper functioning of this accordance with manufacturers recommended procedures and
circuit shall be verified. The check may be performed using a shall be traceable to the National Institute of Standards and
suitable oscilloscope or other applicable method as specified by Technology (NIST) or other recognized national standards,
the equipment manufacturer. where applicable.
7.4.4 Dead Weight Check—Yokes and permanent magnets 7.4.8 White Light Meters—All meters shall be calibrated in
(when allowed) shall be dead weight checked at intervals as accordance with manufacturers recommended procedures and
stated in Table 1. Alternating current and permanent magnet shall be traceable to the National Institute of Standards and
yokes shall have a lifting force of at least 10 lb [4.5 kg], with Technology (NIST) or other recognized national standards,
a 2- to 6-in. [50- to 150-mm] spacing between legs. Direct where applicable.
current yokes shall have a lifting force of at least 30 lb [13.5
kg], with a 2- to 4-in. [50- to 100-mm] spacing between legs, NOTE 3—More information on UV-A visible lights and meters can be
or 50 lb [22.5 kg], with a 4- to 6-in. [100- to 150-mm] spacing. found in Guide E2297.
7.4.5 Black Lights—Black lights, which are portable, hand-
held, permanently mounted or fixed, and used to examine parts, 8. Keywords
shall be checked for output at the frequency specified in Table 8.1 dye; fluorescent; FP; FPI; magnetic particle; MPI; MT;
1 and after bulb replacement. A longer period may be used if a nondestructive evaluation; nondestructive examination; nonde-
plan justifying this extension is prepared by the NDT facility or structive testing; NDT
--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---

ANNEXES

(Mandatory Information)

A1. INSTRUCTIONS FOR THE USE OF AS 5371 STANDARD NOTCHED SHIMS

A1.1 Application of Shims—The Reference Standard NOTE A1.1—Polar solvents such as water, will break down the
Notched Shims of AS 5371, as shown in Annex A2, require cynoacrolate based (super glue) adhesives commonly used to apply these
specific handling, attachment, and care for accurate indication shims.
of magnetic field strength and direction. To select amperage A1.4 The shim shall be placed in intimate contact with the
settings for multi-directional magnetization, the use of part with the flaw side next to the material to be examined.
AS 5371 shims or parts described in 6.3.1.1 is mandatory.
A1.5 The shim shall be securely fastened to the part by
A1.2 Shims 0.002 in. [0.05 mm] thick shall be used on using an adhesive or tape (such as Scotch Brand 191, 471, or
curved or complex surfaces.
600 series) that prevents the magnetic particle suspension from
A1.3 Shims are manufactured of low carbon steel and must entering between the shim and part. Whatever means is used to
be protected from corrosion when not in use. They may be secure the shim to the part shall not interfere with the visibility
submerged in a solvent such as MEK or naphtha for storage. of the indications.
Before attaching the shim to the part, both the shim and part
shall be clean and dry.

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A1.6 Tape may be used to secure the shim and shall have A1.9.3.1 Field strength for the first direction shall be deter-
the following properties: (1) Good adhesion to steel, (2 ) mined by slowly increasing the amperage until a satisfactory
Impervious to the suspension used, and (3) the tape shall be indication is observed on each shim.
non-fluorescent under blacklight (for fluorescent suspensions). A1.9.3.2 Record the amperage setting and indication re-
sults.
A1.7 If the tape becomes loose, allowing the suspension to A1.9.3.3 Demagnetize the part and carefully clean the shims
seep under the shim, the tape and shim shall be carefully prior to determining the amperage in the next direction.
removed, the shim and the part shall be cleaned and the shim A1.9.3.4 Field strength for the second direction shall be
shall be reattached. determined by incrementally increasing the amperage until a
satisfactory indication is observed on each shim.
A1.8 Re-use of the shims is acceptable, provided they are
A1.9.3.5 Record the amperage setting and indication re-
not distorted when removed and intimate contact is achieved
sults.
when replaced.
A1.9.4 Place the selector switch in the multi-directional
A1.9 Determining Field Strength and Direction—Use of the mode and magnetize the part at the previously recorded
circle or cross configuration shims will indicate fields in any settings. If the entire circle on the shims is observed, the fields
direction. are in balance. If any portion of the circle has a weak
indication, adjust the amperage accordingly and repeat the field
A1.9.1 In developing a magnetic particle procedure, first
verification process until the magnetic fields are balanced.
determine the locations the shims should be placed to ensure
adequate coverage to monitor the field strength and direction, A1.9.5 Use care when applying the suspension to the shims.
and then attach the shims. Proper shim indications may not form unless the suspension is
applied in a gentle manner.
A1.9.2 Using the continuous method, begin by starting with
the amperage selection at a minimum level and increasing the A1.10 The shims are made of a low retentivity and high
amperage slowly until the shim indications are readily ob- permeability material that cannot be used for indicating re-
--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---

served. When magnetized, one leg of the X will be indicated sidual fields when developing magnetic particle testing proce-
perpendicular to the field direction and the circle shim will dures.
show quadrants that are approximately perpendicular to the
A1.11 In unidirectional applications, the actual field
direction of the applied field.
strength measurements can be obtained by placing a Hall Effect
A1.9.3 In multi-directional magnetization, longitudinal and probe adjacent to the shim or at a nearby location where probe
circular fields shall be determined separately as follows: placement can easily be replicated.

A2. REFERENCE STANDARD NOTCHED SHIMS FOR MAGNETIC PARTICLE TESTING IN ACCORDANCE WITH AS 5371

A2.1 The following standard flawed shims are typically square of Fig. A2.3. The shims of Fig. A2.3 are cut, by the user,
used to establish proper field direction and ensure adequate into four 0.395 in. [10 mm] square shims for use in restricted
field strength during technique development in magnetic par- areas.
ticle testing. The shims shown in Fig. A2.1 may be used to
ensure the establishment of fields in the unidirectional magne- A2.1.3 Shims shall be low carbon steel, AMS 5062 or
tization method and to ensure the establishment and field equivalent.
balance in the multidirectional magnetization method. A2.1.4 Shims shall be used as specified in AS 5371. Shims
A2.1.1 Except for shims illustrated in Fig. A2.3, the shims are placed in the area(s) of interest with the notches toward the
are available in two thicknesses, 0.002 in. [0.05 mm] and 0.004 surface of the part being examined. Use enough shims by
in. [0.10 mm]. Thinner shims are used when the thicker shims placing the shims in multiple areas to ensure proper field
cannot conform to the part surface in the area of interest. directions and strengths are obtained.
A2.1.2 The shims are available in two sizes, 0.75 in. [19
mm] square for Figs. A2.1 and A2.2 and 0.79 in. [20 mm]

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--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---
FIG. A2.1 Shims for Magnetic Particle Testing

FIG. A2.3 Shims for Magnetic Particle Testing

FIG. A2.2 Shims for Magnetic Particle Testing

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A3. FLEXIBLE LAMINATED STRIPS FOR MAGNETIC PARTICLE TESTING

A3.1 Flexible laminated strips are typically used to ensure


proper field direction during magnetic particle testing. The
longitudinal axis of the strip should be placed perpendicular to
the direction of the magnetic field of interest in order to
generate the strongest particle indications on the strip.
A3.1.1 The strips are available in two types, General Use
and Aerospace Use. Both types of strip contain a steel layer
FIG. A3.2 A cross-sectional view illustrates the magnetic leakage
sandwiched between two brass plates that are 0.0020 in. flux generated by the slots in the central steel layer of a flexible
[0.0508 mm] thick. The bottom brass layer acts as a lift-off of laminated strip exposed to a magnetic field perpendicular to the
0.0020 in. [0.0508 mm] from the examination surface. The strip axis.
brass is non-magnetic and functions only to provide lift-off and
to protect the steel layer. The entire strip may have a polymeric
coating for further protection. 600 series) that prevents the magnetic particle suspension from
A3.1.2 The longitudinal dimension of the strips is 1.95 in. entering between the strip and part.
[50 mm] and the width of the strip is 0.47 in. [12 mm]. A3.2.3.2 Tape may be used to secure the strip and shall have
the following properties: (1) good adhesion to steel, (2)
A3.1.3 Both types of strips contain three longitudinal slots impervious to the suspension used, and (3) the tape shall be
in the center steel layer. non-fluorescent (for fluorescent suspensions).
A3.1.3.1 The widths of the slots in the General strip are A3.2.3.3 If the tape becomes loose, allowing the suspension
0.0075 in. [0.1905 mm], 0.009 in. [0.2286 mm], and 0.010 in. to seep under the strip, the tape and strip shall be carefully
[0.254 mm]. removed, the strip and the part shall be cleaned and the strip
A3.1.3.2 The widths of the slots in the Aerospace strip are shall be reattached.
0.003 in. [0.0762 mm], 0.004 in. [0.1016 mm] and 0.005 in. A3.2.3.4 Any tape or adhesive used to secure the strip to the
[0.127 mm].
--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---

part shall neither cover nor interfere with the visibility of the
A3.1.4 The center steel layer of the strips is made of a high indications.
“µ” magnetic material. A3.2.4 Re-use of the strips is acceptable, provided they are
A3.1.5 Strips shall be placed in the area(s) of interest part or not distorted when removed and intimate contact is achieved
surface being examined. Use enough strips, or place the strips when replaced.
in multiple areas to ensure that proper field directions are A3.2.5 Use care when applying the suspension to the strips.
obtained. Proper strip indications may not form unless the suspension is
A3.2 Instructions for the Use of Flexible Laminated Strips applied in a gentle manner.

A3.2.1 Application of Strips A3.2.6 The active center layer of the strips are made of a
Flexible laminated strips, as shown in Annex A3, require low retentivity and high permeability material. Use of the strips
specific handling, attachment, and care for accurate indication in verifying the presence of residual magnetic fields can only
of magnetic field direction. be made with approval of the Cognizant Engineering Organi-
zation.
A3.2.2 Strips are manufactured of high permeability carbon
steel and must be protected from corrosion when not in use. A3.2.7 Determining Field Direction
They should be stored in a dry location. Before placing the Strips provide the strongest particle indications on the three
strip onto the part, both the strip and part shall be clean and dry. lines when positioned such that the longitudinal axis of the
strip is perpendicular to the applied magnetic field. A strip
A3.2.3 The strip shall be placed in intimate contact with whose longitudinal axis is parallel to the applied field will not
material to be examined. The strip may be held in place provide any particle indications. Refer to Fig. A3.3 and Fig.
manually or with the use of an adhesive or tape. A3.4.
A3.2.3.1 If the strip is to be fastened to the part by using an A3.2.7.1 To use the strips to determine field direction, first
adhesive or tape select one (such as Scotch Brand 191, 471, or determine the location(s) for the strip(s) to be placed.
A3.2.7.2 Position a strip onto the surface so that it is
perpendicular to the direction of the applied magnetic field.
(1) A second strip may be placed perpendicular to the first.
A3.2.7.3 Using the continuous method, begin by starting the
amperage selection at a minimum level and increasing the
amperage slowly until the indications of the lines in one or both
FIG. A3.1 The longitudinal lines represent the location of the
strip(s) are readily observed.
slots cut into the center steel layer of either the General or Aero- A3.2.7.4 If both strips show particle indications, the applied
space flexible laminated strips. field is at an angle of between 30° to 60° to them. If no

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FIG. A3.4 Weak particle indications can mean that the longitudi-
FIG. A3.3 Particle indications are strongest when applied mag- nal axis of the strip is at an angle (θ) from the applied magnetic
netic field (H) is of sufficient strength and perpendicular to the field (H), or that the applied field is not strong enough to gener-
longitudinal axis of the strip. No indications will form when the ate indications.
longitudinal axis is parallel to the applied field or the strength of
H is insufficient. A3.2.7.5 Actual field strength measurements (in the air at
the point of measurement) can be obtained by placing a Hall
indications are visible in either strip when the field is applied, Effect probe adjacent to the strip or at a nearby location where
the field is not strong enough to generate indications. probe placement can easily be replicated.

A4. AS 5282 TOOL STEEL RING SPECIMEN FOR SYSTEM PERFORMANCE TEST

A4.1 A ring specimen similar to Fig. A4.1 may be used to TABLE A4.2 Amperage and Hole Indication Requirements for
perform the system performance verification of subsection 7.1. Ketos 01 Tool Steel Ring Specimen
Amperage
Minimum Number
A4.2 Wet Particle Test. (Conducted in accordance with a Type of Suspension FW or HW
of Holes Indicated
Rectified
written procedure.)
Fluorescent Oxide 1400 3
A4.2.1 Demagnetize the ring. (Wet) 2500 5
3400 6
A4.2.2 Place a non-ferromagnetic conductor with a diam- Visible Oxides 1400 3
eter between 1 and 1.25 in. [25.4 and 31.75 mm] through the (Wet) 2500 5
center of the ring. 3400 6
Dry Powder 1400 4
A4.2.2.1 Center the ring on the conductor. 2500 6
A4.2.3 Magnetize the ring circularly by passing the required 3400 7

current through the conductor. Use the current levels of Table


A4.1 or Table A4.2, as applicable to the ring being used.
TABLE A4.1 Amperage and Hole Indication Requirements for A4.2.4 Apply the suspension to the ring using the continu-
AS 5282 Rings ous method.
Amperage A4.2.5 Examine the ring within 1 min after current appli-
Minimum Number
Type of Suspension FW or HW
Rectified
of Holes Indicated cation.
Fluorescent Oxide 500 3 A4.2.5.1 Nonfluorescent baths shall be examined under
(Wet) 1000 5 visible light of not less than 100 fc [1076 lx].
1500 6 A4.2.5.2 Fluorescent baths shall be examined under black
2500 7
3500 9 light of not less than 1000 µW/cm2 and an ambient white light
Visible Oxides 500 3 level not greater than 2 fc [22 lx].
(Wet) 1000 4
1500 5
A4.2.5.3 The number of hole indications visible shall meet
2500 6 or exceed those specified in Table A4.1 or Table A4.2, as
3500 8 applicable to the ring being used.
Dry Powder 500 4
1000 6
A4.2.5.4 Current levels used and number of holes observed
1500 7 may be limited by equipment current capacity, or the intended
2500 8 working range based upon the type of parts being examined.
3500 9
A4.2.6 Demagnetize the ring.
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Hole 1 2 3 4 5 6
Diameter 0.07 0.07 0.07 0.07 0.07 0.07
Note 1 [1.78 [1.78 [1.78 [1.78 [1.78 [1.78
mm] mm] mm] mm] mm] mm]
“D” 0.07 0.14 0.21 0.28 0.35 0.42
Note 2 [1.78 [3.56 [5.33 [7.11 [8.89 [10.67
mm] mm] mm] mm] mm] mm]
Hole 7 8 9 10 11 12
Diameter 0.07 0.07 0.07 0.07 0.07 0.07
Note 1 [1.78 [1.78 [1.78 [1.78 [1.78 [1.78
mm] mm] mm] mm] mm] mm]
“D” 0.49 0.56 0.63 0.70 0.77 0.84
Note 2 [12.45 [14.22 [16.00 [17.78 [19.56 [21.34
mm] mm] mm] mm] mm] mm]

NOTE 1—All hole diameters are 60.005 in. [60.13 mm]. Rings with holes 10 through 12 are optional.
NOTE 2—Tolerance on the D distance is 60.005 in. [60.13 mm].
NOTE 3—All other dimensions are 60.03 in. [60.76 mm].
FIG. A4.1 AISI KETOS Tool Steel Ring

A4.3 Dry Particle Test. (Conducted in accordance with a A4.3.4 Apply the particles to the ring using a squeeze bulb
written procedure.) or other suitable applicator while the current is flowing.
A4.3.1 Place a non-ferromagnetic conductor with a diam- A4.3.5 Examine the ring within 1 min after current appli-
eter between 1 and 1.25 in. [25.4 and 31.75 mm] through the cation under a minimum of 100 fc [1076 lx] of visible light.
center of the ring. A4.3.5.1 The number of hole indications visible shall meet
A4.3.2 Center the ring on the conductor. or exceed those specified in Table A4.1, Table A4.2, or the
written procedure, or both.
A4.3.3 Magnetize the ring circularly by passing the required
A4.3.5.2 Current levels used and number of holes observed
current through the conductor. Use the applicable current levels
may be limited by equipment current capacity.
of Table A4.1 or Table A4.2, as applicable to the ring being
used. A4.3.6 Demagnetize the ring.

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A5. MEASUREMENT OF TANGENTIAL FIELD STRENGTH

A5.1 Care must be exercised when measuring the tangential to read the peak value during the shot. The gaussmeter should
applied field strengths as specified in 6.3.2. The active area of have a frequency response of *300 Hz or higher. The direction
the Hall Effect probe should be no larger than 0.2 in. [5.1 mm] and magnitude of the tangential field on the part surface can be
by 0.2 in. [5.1 mm] and should have a maximum center determined by two measurements made at right angles to each
location 5 mm from the part surface. The plane of the probe other at the same spot. The gaussmeter probe leads should be
must be perpendicular to the surface of the part at the location shielded or twisted to prevent reading errors due to voltage
of measurement to within 5 degrees. This is difficult to induced during the large field changes encountered during
accomplish by hand orientation, therefore the probe should be magnetic particle testing.
held in a jig or fixture of some type. If the current is being NOTE A5.1—Lack of effective bandwidth could have a significant effect
applied in shots, or if alternating current or half-wave rectified on the resultant value when measuring fields generated by pulse-width
alternating current is being used, the gaussmeter should be set modulated MPI equipment.

APPENDIXES

(Nonmandatory Information)

X1. SUITABILITY OF MATERIALS FOR MAGNETIC PARTICLE TESTING

X1.1 Some materials are far more suitable for magnetic tized but should not be examined with the residual method.
particle testing than others. In some cases, liquid penetrant
testing may be a more reliable testing method. X1.5 Fig. X1.1 is a tabulation of stainless and corrosion
resistant steels and their suitability for examination with the
X1.2 Some of the precipitation hardening (PH) steels are magnetic particle testing method.
austenitic in the annealed or low heat treat ranges. Austenitic X1.6 Aluminum and aluminum based alloys, copper and
materials cannot be examined by the magnetic particle testing copper based alloys, and nickel based alloys cannot be exam-
method. ined by the magnetic particle testing method.
X1.3 Care must be taken with low permeability steels, such X1.7 All low-alloy carbon steels, 1000 series (1020, 1050,
as the PH steels, to use a high enough amperage to provide 1117, 1340 etc.), 4000 series (4130, 4330 4340M, and so
proper field strength. forth), 5000, 6000, 8000, 9000 series, HY 80, HY 100,
9Ni-4Co, and Maraging steels are ferro-magnetic and can be
X1.4 Steels with very high permeability are easily magne- examined with the magnetic particle testing method.

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FIG. X1.1 Tabulation of Stainless and Corrosion Resistant Steels

X2. PARTICLE PERFORMANCE EVALUATION DEVICES

X2.1 Scope X2.2 Procedures Considerations


X2.1.1 This appendix illustrates several types of devices X2.2.1 Preparation—The surface of the device must be
that can be used to evaluate or compare the performance of clean dry and free of any particles from previous test, fluid or
both wet and dry magnetic particle testing materials. Particle other contaminants or conditions that might interfere with the
performance evaluation devices may be used to: check for efficiency of the evaluation prior to the application of the
material degradation; compare difference materials; check the testing material.
visibility of any material(s) under varying illumination condi- X2.2.2 Device Verification—Device should be checked with
tions; and other types of comparisons. a new material or known material prior to use, to verify the
NOTE X2.1—The devices discussed in this section shall not be device has not been magnetically altered. If the test indicates
re-magnetized in any manner or demagnetized in any manner. They
contain some form of permanent magnetization. With suitable care the the magnetic properties of the device have been altered, it
magnetization within each device should not be subject to change over should be replaced. Contact the device manufacture with
time. regard to any magnetization or performance issues.
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X2.2.3 Equipment and Procedures—The equipment X2.2.6 Particle indications may be recorded in accordance
requirements, test condition and testing procedures for particle with 6.6.
evaluation should be established and documented to the extent
X2.2.7 Evaluation of materials not meeting company stan-
required in order to provide a standardized evaluation. The
requirements may cover such things as black light distance and dard shall not be used for examination.
illumination requirements, visible light requirements, particle
applicator and application procedure, the use of contrast X2.3 Handling—After the visual examination has been
backgrounds, removal of excess particles and method of made, the surface of the device should be cleaned of remaining
documenting results. fluid and particles in a manner non-detrimental to the device.
When not in use the device should be stored sway from
NOTE X2.2—Non-fluorescent particles results are particularly impacted excessive heat and strong magnetic fields. Contact the device
by background color. A thin coating simulating test condition background
color may be considered in order to provide an additional aid in evaluating manufacture with regard to any magnetization or performance
particle performance under actual test conditions. issues.
X2.2.4 Prior to examination verify that required test proce-
dures have been met. X2.4 Devices

X2.2.5 Particle Application—Wet Method and Dry Method X2.4.1 Encoded Magnetic Media—The magnetic encoding
materials should be consistent with the method of application process can generate magnetic gradients in a highly controlled
that will be used for examination. manner. These gradients, when encode into a media (that is, a
X2.2.5.1 Wet Method Materials—Fluorescent or non- magnetic strip card) can be used as an indicator of magnetic
fluorescent particles suspended in a liquid vehicle at the particle performance. Fig. X2.1 illustrates how particles can be
required concentration shall be applied as they would be used attracted to the encoded strip on the magnetic strip card.
for examination by gently spraying or flowing the suspension X2.4.2 Permanently magnetized devices—Cracks in perma-
over the area to be examined or by immersion of the device in nently magnetized disks provide the flux leakage required for
the suspension. Excess bath shall be allowed to flow away from magnetic particle indications. Observation of the intensity and
the device. The device shall be observed under appropriate brightness of indication allow a comparison or evaluation of
illumination for the formation of particle indications. Obser- particle performance. Fig. X2.2 illustrates cracks that have
vations shall be noted as to the quality of particle indications been formed in a small disk.
and the clarity thereof.
X2.2.5.2 Dry Method Materials—Apply dry powder so that X2.4.3 Devices containing permanent magnets—The seam
a light, uniform, dust-like coating settles on the surface of the between two magnetically coupled blocks provide the flux
device. The applicators shall introduce the particles into the air leakage required for magnetic particle indications. The flux
in a manner such that they reach the part surface in a uniform density decrease as the distance from the magnet increases and
cloud with a minimum of force. Excess particles shall be the resulting magnetic particle indication reduces. Fig. X2.3
removed by a gentle air current. The device shall be observed illustrates how a permanent magnet can be located to result in
under appropriate illumination for the formation of particle a particle indication along the seam between two precision
indications. Observation shall be noted as to the quality of formed steel blocks. The seam can be incremented so that the
particle indications and the clarity thereof. particle performance can be graded.

FIG. X2.1 Particle indications appear where magnetic gradients have been encoded in the magnetic strip of the card. In this case the
gradients decrease in value from “0” (strongest) to “X” (weakest). Particle performance can be graded on the basis of the weakest
indication.

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FIG. X2.2 Typical dimensions (millimetres) of a disk containing surface cracks that has been permanently magnetized. In this case (1)
indicates larger cracks formed by grinding and (2) indicates finer cracks caused by stress (induced by quenching)
--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---

FIG. X2.3 One type of device containing a permanent magnet held next to two precision formed steel blocks with a brass cover. The
seam between the steel blocks acts as a discontinuity; particles form an indication on the seam that is strongest close to the magnet
and weakens with distance away from the magnet.

X3. FORMULAS FOR DETERMINING PROPER CURRENT VALUES FOR CIRCULAR MAGNETISM

X3.1 Magnetization Current Levels—The current values X3.3 Direct Circular Magnetization—When magnetizing
given in X3.2 and X3.3 are average current values and are by passing current directly through the part the nominal current
applied directly to full-wave direct current. For other types of shall be 300 to 800 A/in. of part diameter [12 to 32 A/mm]. The
current, the operator’s manual, the equipment manufacturer, or diameter of the part shall be taken as the greatest distance
the Cognizant Engineering Organization should be consulted. between any two points on the outside circumference of the
part. Currents will normally be 500 A/in. [20 A/mm] or lower,
X3.2 Prod Current Levels—When using prods on material with the higher currents up to 800 A/in. [32 A/mm] being used
⁄ in. [19 mm] in thickness or less, 90 to 115 A/in. of prod
34 to examine for inclusions or to examine low-permeability
spacing [3.5 to 4.5 A/mm] shall be used. For material greater alloys such as precipitation-hardened steels. Amperages of less
than 3⁄4 in. [19 mm] in thickness, 100 to 125 A/in. of prod than 300 A/in. [12 A/mm] may be used when part configuration
spacing [4.0 to 5.0 A/mm] shall be used. Prod spacing shall not dictates and approval is obtained from the Level III and the
be less than 2 in. [50 mm] or greater than 8 in. [200 mm]. The Cognizant Engineering Organization.
effective width of the magnetizing field when using prods is
one fourth of the prod spacing on each side of a line through X3.4 Central Conductor Circular Magnetization—Circular
the prod centers. magnetization may be provided by passing current through a

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conductor that is positioned inside the part. If only the inside of the part, the current levels as given in X3.3 shall apply, except
the part is to be examined, the diameter shall be the greatest that the total diameter shall be the sum of the diameter of the
distance between two points, 180 degrees apart on the inside central conductor plus twice the wall thickness of the part. The
circumference. Otherwise, the diameter is determined as in distance along the part circumference (interior) that may be
X3.3. effectively examined shall be taken as approximately four
X3.4.1 Centrally Located Conductor—When the axis of the times the diameter of the central conductor up to 360 degrees
central conductor is located near the central axis of the part, the provided the presence of suitable fields is verified. The entire
same current levels as given in X3.3 shall apply. circumference shall be examined by rotating the part on the
X3.4.2 Offset Central Conductor—When the conductor that conductor, allowing for approximately a 10 % magnetic field
is positioned inside the part, is placed against the inside wall of overlap. See Fig. X3.1 for an illustration.
--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---

FIG. X3.1 The Effective Region of Examination When Using an Offset Central Conductor is Equal to Four Times the Diameter of the
Conductor as Indicated

X4. FORMULAS FOR DETERMINING PROPER CURRENT VALUES FOR COILS

X4.1 Longitudinal Magnetization Using Coils— than 2, pole pieces (pieces of ferromagnetic material with the
Longitudinal magnetization is often accomplished by passing same diameter as the part being examined) may be placed on
current through a coil encircling the part, or section of the part, one or each end to effectively increase the L/D to 2 or greater.
to be examined (that is, by using a coil shot). This produces a If the part has hollow portions, D may be replaced with Deff as
magnetic field parallel to the axis of the coil. The effective field outlined in X4.3.4. If the part has a length longer than the
extends a distance on either side of the coil center approxi- effective length of the coil (as described in 6.3.1.1) the length
mately equal to the radius of the coil. The actual effective of the part when calculating the L/D ratio shall be the actual
distance must be demonstrated based on the particular part to length of the section of the part to be examined.
be examined. For parts longer than these effective distances,
the entire length shall be examined by repositioning the part X4.3.1 Longitudinal Magnetization with Low Fill Factor
within the coil, allowing for approximately 10 % effective Coils—When the cross-sectional area of the coil is ten or more
magnetic field overlap. times the cross-sectional area of part being examined, the
following formulae apply:
X4.2 The following formulas have been used for many X4.3.1.1 For parts positioned to the side of the coil:
years to develop techniques for examining parts using longi-
tudinal fields produced by coils and cable wraps. Recent K
NI 5
L/D
~ 610 % ! (X4.1)
studies have indicated that the fields produced by these
formulas may be excessive for some parts. They may be used where:
as a guide to establish preliminary magnetizing current values
N = the number of turns in the coil,
and shall be verified by one of the magnetic field strength I = the current in amperes applied to the coil,
monitoring methods referenced in 6.3.1. K = 45 000 permeability constant,
X4.3 Coil and Cable Wrap—The following formulas hold L = length of the part, and
D = the diameter of the part in the same units as the length.
only if the L/D is greater than 2 and less than 15. If L/D is less

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X4.3.1.2 For parts positioned in the center of the coil: (NI)l = value of NI calculated for low-fill factor coils using
KR X4.3.1.1 or X4.3.1.2,
~ 6L/D ! 2 5 ~
NI 5 610 % ! (X4.2) (NI)h = value of NI calculated for high-fill factor coils using
X4.3.2, and
where: τ = the ratio of the cross-sectional area of the coil to the
N = the number of turns in the coil, cross-sectional area of the part. For example, if the
I = the current in amperes applied to the coil, coil is 10 in. in diameter and the part is 5 in. in
R = radius of the coil, mm (or in.), diameter, then:
K = 1690 if R is in mm (43 000 if R is in inches),
L = length of the part, and ~ π·5 2 !
τ5 54 (X4.5)
D = the diameter of the part in the same units as the length. ~ π·2.52 !
X4.3.4 Calculating the L/D Ratio for a Hollow or Partially
X4.3.2 Longitudinal Magnetization with Cable Wrap or
Hollow Part—When calculating for a hollow or partially
High Fill Factor Coils—When the cross-sectional area of the
hollow part, D may be replaced with an effective diameter Deff
coil is less than twice the cross-sectional area (including
the following formulae:
hollow portions) of the part under examination, the following
formula applies: D eff 5 2 @ ~ A t 2 A h ! /π # 1/2 (X4.6)
K or
@ ~ L/D ! 12 # ~
NI 5 610 % ! (X4.3)

where:
N = the number of turns in the coil,
D eff 5 Œ
2 ~ A t 2 A h!
π
I = the current in amperes applied to the coil, where:
K = 35 000 A turns,
At = the total cross-sectional area of the part, and
L = the length of the part, and
Ah = the total cross-sectional area of the hollow sections of
D = the diameter of the part in the same units as the length.
the part.
X4.3.3 Longitudinal Magnetization for Intermediate Fill For hollow cylindrical parts this is equal to the following:
Factor Coils—When the cross-sectional area of the coil is
D eff 5 @ ~ OD! 2 2 ~ ID! 2 # 1/2 (X4.7)
between 2 and 10 times the cross-sectional area of the part
being examined, the following formula applies: or

NI 5 ~ NI! h F 10 2 τ
8 G
1 ~ NI! l F G
τ22
8
(X4.4)
D eff 5 =~ OD! 2 2 ~ ID! 2

where: where:
N = the number of turns in the coil, OD = the outside diameter of the cylinder, and
I = the current in amperes applied to the coil, ID = the inside diameter of the cylinder.

X5. PIE FIELD INDICATOR AND TORROID FIELD FIXTURE

X5.1 See Fig. X5.1 and Fig. X5.2.

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FIG. X5.1 Pie-field Indicator for Use in Magnetic Particle Testing


--```,,`,```,,,,,`,,,`,,``,,````-`-`,,`,,`,`,,`---

NOTE 1—Only a changing magnetic field will generate a resulting eddy current in the ring-shaped part, such as when the magnetic field in the
magnetizing coil suddenly collapses, or when using a moving waveform such as AC; no eddy current is produce in the part by a non-moving waveform.
The resultant toroidal shaped magnetic field may be used to detect circumferential discontinuities in the part.
FIG. X5.2 Example of Induced Current Magnetization

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SUMMARY OF CHANGES

Committee E07 has identified the location of selected changes to this standard since the last issue (E1444 - 12)
that may impact the use of this standard. (June 1, 2016)

(1) Added E3022 to the list of Referenced Documents.


(2) Revised subsections 5.6.4, 7.3.2, and 7.4.5.1 to incorporate
E3022.

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