ELECTROLYTICAL SAMPLE PREPARATION

ELOPREP
102
metkon.com
ELECTROLYTIC
POLISHING & ETCHING
 ELOPREP
102
ELOPREP 102 is an automatic and programmable electrolytic
polishing and etching equipment for the preparation of
metallographic specimens.

• Fully automatic electrolytic polisher / etcher

• Programmable with HMI touch screen controls
• Automatic determination of polishing and etching voltage
• Fast & effective polishing results
• Highest safety standards
• External Etching Unit
• Ability to operate two Polishing & Etching unit from the same control unit
• Suitable for both normal and low temperature electrolytic polishing

POLISHING & ETCHING

Fully automatic electrolytic polishing and etching equipment with
independent control unit.Shorter preparing time is needed for
electrolytic polishing and etching process compared to traditional
mechanical preparation.

The ELOPREP 102 has advanced techniques and software with

programmable colored HMI touch screen controls, increasing the
productivity, sample consistency and operator comfort. All
parameters; temperature, time, current, pump speed, etc. can be
monitored during the process. The speed of the amount to be
pumped is also variable.

A library of 99 different polishing programs with related specimen

name or number can be saved with all parameters which can be
recalled at any time.

ELOPREP 102 has two separate units, the control unit and the
polishing unit.Separate polishing and etching unit can be placed away
from the control unit and can be installed under a fume extraction
system. The electrolyte cartridge is easily exchangeable and inserted
into the polishing and etching unit.

Additional polishing and etching unit can be connected the same

control unit. Thus, two polishing & etching unit can be operated
individually. This is very useful feature especially for specimens
which require different electrolytes for polishing and etching.
Polishing & Etching Unit Exchangeable Electrolyte Cartridge
With the scanning function of ELOPREP, correct voltage of polishing
as well as etching can be defined automatically.
ELOPREP 102 is suitable for both normal and low temperature
The sample is placed on the polishing and etching table where electrolytic polishing. The water connection and circulation system is
optional masks are available as 0,5 cm² – 5 cm². The cooling tube is specially designed for both purpose. The polishing & etching unit can
fixed to the lid and directly lowered into the container. ELOPREP 102 be connected to either city water for normal polishing or external
has the highest safety standards. The cooling water is automatically cooling unit for low temperature polishing at subzero temperatures.
switched on as soon as the set temperature is reached.The cooling No separate or additional equipment is necessary for this purpose.
water consumption is minimized where the cooling water is activated
with a solenoid valve.
 If ELOPREP 102 is not connected to water source or the temperature
increases above pre-defined temperature limit, an audible warning
signal notifies the operator and the process will automatically shut
down.

ELOPREP 102 has 3 different operation modes; Polishing or Etching,

Automatic Etching after Polishing and External Etching.

Optional External etching is available incase different electrolytes

have to be used for polishing and etching. ELOPREP will automatically
start as soon as the specimen contacts to the electrolyte in the
external etching unit. The process automatically shuts down when
the set etching time is reached.

Etial 160 Aluminum WC-Co Sinter Metal

Magnification: 100 x Magnification 800x (DIC)

All preparation parameters can be stored in memory under a specific

program number. Each program can be saved for a material specific
name such as “Cast Iron, Bronze, Al-Si Alloy, etc.” The parameters
which can be saved are; Polishing voltage, time and Flow rate,
Etching Voltage and time. These parameters are entered and stored in
memory and displayed on the coloured LCD screen as preset values.
All the operator needs to do is to call up a specific program and press
the “Start” key. It is possible to transfer parameters from an USB
memory stick (export or import programs).

Programmable HMI Touch Screen Controls

Dual Polishing & Etching External Etching Unit

 SPECIFICATION

46 01 ELOPREP
ORDER NO 46 02 Electrolytic Polishing&Etching System
Automatic and programmable electrolytic polishing and etching of
metallographic specimens, with Siemens PLC control unit,
MODEL NO ELOPREP 102 user friendly coloured 7'' LCD touch screen controls,
short polishing times and maximum reproducibility,
seperate polishing unit equipped with drain pipe and integrated
Temperature limiter, C 30 - 50 cooling system, optional external etching unit, 0-100 V output
voltage for polishing, 0-25 V for etching and 0-15 V for external
etching. Variable polishing time and current, with current
Pump Magnetic Stirrer
limitation,
built in safety features with continuous control of electrolyte,
Electrolytic Container Volume, mL 1000 ml scanning function for easy determination of parameters,
variable speed controlled pump with magnetic stirrer for
electrolyte flow.
External Etching Volume, mL 1200 ml Ready for operation. Included: Stainless steel cathode(1pc.)
230 V, 1-phase, 50 Hz.

Cooling System Integrated Optional Accessories for ELOPREP

46 09 Additional Polishing & Etching Unit
(Suitable for both normal and low temperature electrolytic
Low Temperature Polishing Yes
polishing) (Dual Polishing & Etching units operatable by the same
control unit) (To be ordered simultaneously together with the
Mask Dimensions, cm2 0 - 0,5 - 1 - 2 - 5 ELOPREP 102 order)
46 10 External Etching unit
46 11 Electrolyte container with lid
Scanning Function Automatic 46 12 1 set of 5 masks 0.5 cm2
46 13 1 set of 5 masks 1 cm2
46 14 1 set of 5 masks 2 cm2
Control Panel 7" HMI Touch Screen
46 15 1 set of 5 masks 5 cm2
46 16 1 set of 5 masks without aperture
Program Memory 99
46 17 1 set of masks (0.5, 1, 2, 5 cm2 and 1 without aperture.)

YM 6904-00 Stainless Steel cathode

Output Voltage / Current YM 6937-00 Cupper cathode
YM 6936-00 Titanium cathode

Polishing 0-120 V

Etching 0-35 V

External Etching 0-15 V

1x 110/120 V
Power Supply 1 x 230 V

Dimensions, WxDxH, mm

Control Unit 404 x 370 x 305

Polishing Unit 210 x 370 x 305

Weight, kgs

Control Unit 20

Polishing Unit 5

* Other voltages and frequencies available upon request. Please state when
ordering. All specifications are subject to change without notice.
ELECTROLYTIC SAMPLE PREPARATION
Electrolytic polishing is the best way to polish very soft materials
which are prone to smearing and deformation. It can be easily applied
to objects of complex shape.

Materials that work well for electropolishing or etching include soft

austenitic stainless steels, aluminum and aluminum alloys, copper
and copper alloys, among others.

Shorter preparing time is needed for electrolytic polishing and

etching process compared to traditional mechanical preparation.
The primary requirement for electropolishing is that the specimen be
conductive.

Electropolishing is also commonly applied to the preparation of thin metal samples for transmission electron microscopy because
electropolishing does not cause mechanical deformation of surface layers usually observed when mechanical polishing is used.

METKON offers ELOPREP Electrolytic Polishing & Etching Unit for fully automatic electrolytic sample preparation. Electrolytic sample
preparation process consist of several steps. See step by step electrolytic sample preparation as follow:

STEP 1: Preparing Electrolyte

Each specimen may require different types of electrolytes. Proper
electrolyte should be selected for specimen. Please see instruction
manual of ELOPREP to see common electrolytes.

Fill electrolyte container of ELOPREP with correct electrolyte and

place it on polishing unit. If you have different specimens which
required different electrolytes, you can use additional electrolyte
containers. Thus, you do not have to change electrolyte for different
types of specimen, you only need to change electrolyte container.

STEP 3: Adjusting Flowrate

Flowrate of electrolyte should be adjusted before operation. In other
words, electrolyte should be reached upper level of the mask without
any turbulance. Otherwise, polishing operation cannot be done
properly.

To adjust flowrate, press Pump button without placing sample. If the

flow rate is not enough, increase the set value until the flow is
sufficient.

STEP 4: Preparing Specimen

Surface of specimen should not be rough for electrolyic preparation.
Specimen should be grinded with 600 grit SiC grinding paper before
STEP 2: Choosing Masks electrolytic preparation.

Acid resistant masks are used for determining polishing area of

specimen. There are specific aperture on the masks. Electrolyte will
contact the specimen surface from this aperture thus only this area
will be polished. Masks are available with 0,5-1-2 and 5 cm2 aperture
size. Mask should be placed on cathode and specimen should be
placed on the mask.
STEP 5: Determining Correct Voltage
Voltage is one of the most important parameter for electrolytic
polishing. ELOPREP has scanning function for easy and exact
determination of the parameters. With the scanning function of
ELOPREP, correct voltage of polishing can be defined automatically. If
you do not have the knowledge for the polishing voltage to be set for
your sample, you can use the scanning function to determine exact
voltage. You do not have to make time consuming trials and error
testing for the correct voltage.

*Place specimen on the mask. Be sure that the aperture is covered

and closed completely.
*Place the anode arm on the top of the sample to ensure good
contact.
*Enter Scan menu, set scanning voltage and flowrate parameters and (Microstructure of Al-Cu-Steel)
press Start. For only etching:
*After a while, ideal polishing voltage for your specimen will be seen Set only polishing time and polishing voltage. Do not set etching
on the screen. time and etching voltage, these should be zero “0”. Press start and
operation will be completed automatically. The specimen must be
washed after etching operation is completed. Microstructure of
etched surface can be seen as below:

(Microstructure of Al-Cu-Steel)

For automatic etching after polishing:

Set polishing voltage, polishing time, etching voltage and etching
time. Do not set etching time and etching voltage. Press start.
Etching will be done automatically after polishing operation is
completed. The specimen must be washed after etching operation
is completed.

For external etching:

If polishing and etching electrolytes different than each other, in this
case external etching unit can be used.

*Fill external etching unit with electrolyte.

STEP 6: Electrolytic Polishing & Etching *Connect cables of external etching unit to control unit.
*Enter External Etching menu. Set etching voltage and time.
ELOPREP has 4 different operation modes; only polishing, only *Hold the sample with scissors.
etching, automatic etching after polishing and external etching. *Plunge the sample into the external etching unit. As soon as the
sample contacts with the electrolyte the process will start
*Place specimen on the mask. Be sure that the aperture is covered automatically.
and closed completely. *As soon as the set etching time is reached an audible signal notifies
*Place the anode arm on the top of the sample to ensure good the operator that the process is completed. Wash your specimen
contact. after etching is completed.
*Enter Polishing&Etching menu. Set parameters: Voltage, flowrate,
mask type and time.

For only polishing:

Set only polishing time and polishing voltage. Do not set etching time
and etching voltage, these should be zero “0”. Press start and
operation will be completed automatically. The specimen must be
washed after polishing operation is completed.
Polished surface and microstructure can be seen as below:
METKON Demirtas Dumlupinar Organize Sanayi Bolgesi Tel : +90 224 261 18 40 [email protected]
Instruments Inc. Ali Osman Sonmez Cd. No: 14 Bursa-TURKEY Fax : +90 224 261 18 44 metkon.com