The document provides a 9-step process for etching low alloy steels that includes: 1) grinding and cleaning the surface, 2) using a nital etch solution for 15-60 seconds, 3) rinsing in water, 4) dipping in hydrochloric acid for 30-60 seconds to remove oxides, 5) rinsing again, 6) neutralizing for 15 seconds at 16-82°C, 7) rinsing with water and alcohol, 8) inspecting, and 9) applying oil to prevent corrosion.
The document provides a 9-step process for etching low alloy steels that includes: 1) grinding and cleaning the surface, 2) using a nital etch solution for 15-60 seconds, 3) rinsing in water, 4) dipping in hydrochloric acid for 30-60 seconds to remove oxides, 5) rinsing again, 6) neutralizing for 15 seconds at 16-82°C, 7) rinsing with water and alcohol, 8) inspecting, and 9) applying oil to prevent corrosion.
The document provides a 9-step process for etching low alloy steels that includes: 1) grinding and cleaning the surface, 2) using a nital etch solution for 15-60 seconds, 3) rinsing in water, 4) dipping in hydrochloric acid for 30-60 seconds to remove oxides, 5) rinsing again, 6) neutralizing for 15 seconds at 16-82°C, 7) rinsing with water and alcohol, 8) inspecting, and 9) applying oil to prevent corrosion.
The document provides a 9-step process for etching low alloy steels that includes: 1) grinding and cleaning the surface, 2) using a nital etch solution for 15-60 seconds, 3) rinsing in water, 4) dipping in hydrochloric acid for 30-60 seconds to remove oxides, 5) rinsing again, 6) neutralizing for 15 seconds at 16-82°C, 7) rinsing with water and alcohol, 8) inspecting, and 9) applying oil to prevent corrosion.
Before etching, wet grind/polish the surface with 400 grit sand papers to remove any rust, surface
oxides, etc. The surface needs to be cleaned and dried.
The procedure may be used to etch low alloy steels
PROCESS SOLUTION TIME TEMPERATURE REMARKS
1. Nital etch Nital solution 15 – 60 seconds Ambient Agitate parts when immersed. Exact time may vary to produce desired black oxide film. 2. Rinse Circulating Rinse only Ambient To remove acid. water Total immersion required. 3. Hydrochloric Hydrochloric 30 – 60 seconds Ambient Agitate parts acid dip Acid solution when immersed to remove black oxide film and provide uniform brownish grey surface. 4. Rinse Running water Rinse only Ambient Agitate parts when immersed. 5. Neutralize Acid Neutralizer 15 seconds 16 – 82 °C Agitate parts minimum (60 – 180 °F) when immersed. 6. Rinse Circulating Rinse only Ambient To remove water caustic. 7. Rinse Alcohol Rinse only Ambient To remove water. 8. Inspect and evaluate per appropriate criteria.