M010027 Serinus 30 CO User Manual 2.2 PDF
M010027 Serinus 30 CO User Manual 2.2 PDF
M010027 Serinus 30 CO User Manual 2.2 PDF
Carbon Monoxide
Analyser
User Manual
Version: 2.2
www.ecotech.com
Ser in u s 3 0 Us er M an u a l 2. 2
Page 2
Table of Contents
1. Introduction .................................................................................................................................... 17
1.1 Description .......................................................................................................................................................... 17
1.2 Specifications ...................................................................................................................................................... 17
1.2.1 Measurement ...................................................................................................................................... 17
1.2.2 Precision/Accuracy .............................................................................................................................. 17
1.2.3 Calibration ........................................................................................................................................... 18
1.2.4 Power ................................................................................................................................................ 18
1.2.5 Operating Conditions ........................................................................................................................... 18
1.2.6 Communications .................................................................................................................................. 18
1.2.7 Physical Dimensions............................................................................................................................. 19
1.2.8 Certifications ........................................................................................................................................ 19
1.3 Nomenclature ..................................................................................................................................................... 20
1.4 Background/Theory ............................................................................................................................................. 21
1.4.1 Measurement Theory .......................................................................................................................... 21
1.4.2 Kalman Filter Theory ............................................................................................................................ 22
1.5 Instrument Description ....................................................................................................................................... 23
1.5.1 Calibration Valve Manifold .................................................................................................................. 23
1.5.2 Particulate Filter .................................................................................................................................. 23
1.5.3 CO-CO2 Converter ................................................................................................................................ 23
1.5.4 Optical Cell ........................................................................................................................................... 23
1.5.5 Pressure Sensor/PCB ........................................................................................................................... 24
1.5.6 Main Controller PCB ............................................................................................................................ 24
1.5.7 Power Supply ....................................................................................................................................... 25
1.5.8 On/Off Switch ...................................................................................................................................... 25
1.5.9 Communications .................................................................................................................................. 25
2. Installation ...................................................................................................................................... 27
2.1 Initial Check ......................................................................................................................................................... 27
2.2 Mounting/Installing ............................................................................................................................................. 28
2.3 Instrument Set-up ............................................................................................................................................... 29
2.3.1 Pneumatic Connections ....................................................................................................................... 29
2.3.2 Power Connections .............................................................................................................................. 30
2.3.3 Communications Connections ............................................................................................................. 30
2.3.4 Analyser Set-up .................................................................................................................................... 31
2.4 U.S. EPA Reference Set-up .................................................................................................................................. 32
Introduction Page 3
Ser in u s 3 0 Us er M an u a l 2. 2
3. Operation ....................................................................................................................................... 35
3.1 Warm-up............................................................................................................................................................. 35
3.2 Measurement ..................................................................................................................................................... 35
3.3 General Operational Information ....................................................................................................................... 36
3.4 Main Display ....................................................................................................................................................... 37
3.5 Menus & Screens ................................................................................................................................................ 38
3.5.1 Quick Menu ......................................................................................................................................... 38
3.5.2 Main Menu .......................................................................................................................................... 40
3.5.3 Analyser State ..................................................................................................................................... 41
3.5.4 Status ................................................................................................................................................ 41
3.5.5 Temperatures ...................................................................................................................................... 42
3.5.6 Pressures and Flow ............................................................................................................................. 42
3.5.7 Voltages............................................................................................................................................... 43
3.5.8 General Settings .................................................................................................................................. 43
3.5.9 Measurement Settings ........................................................................................................................ 44
3.5.10 Calibration Menu ................................................................................................................................ 45
3.5.11 Manual Mode ...................................................................................................................................... 46
3.5.12 Timed Mode ........................................................................................................................................ 46
3.5.13 Flow Calibration .................................................................................................................................. 47
3.5.14 Service ................................................................................................................................................ 47
3.5.15 Diagnostics .......................................................................................................................................... 48
3.5.16 Digital Pots .......................................................................................................................................... 49
3.5.17 Valve Menu ......................................................................................................................................... 50
3.5.18 Tests ................................................................................................................................................ 50
3.5.19 Calculation Factors .............................................................................................................................. 51
3.5.20 Communications Menu ....................................................................................................................... 51
3.5.21 Data Logging Menu ............................................................................................................................. 51
3.5.22 Serial Communications ........................................................................................................................ 52
3.5.23 Analog Input Menu ............................................................................................................................. 53
3.5.24 Analog Output Menu........................................................................................................................... 53
3.5.25 Digital Inputs Menu ............................................................................................................................. 54
3.5.26 Digital Outputs Menu .......................................................................................................................... 54
3.5.27 Network Adaptor Menu ...................................................................................................................... 55
3.5.28 Bluetooth Menu .................................................................................................................................. 56
4. Communications ............................................................................................................................ 59
4.1 RS232 Communication........................................................................................................................................ 59
4.2 USB Communication ........................................................................................................................................... 59
4.3 TCP/IP Network Communication (optional) ....................................................................................................... 60
4.4 Digital/Analog Communication ........................................................................................................................... 60
4.4.1 Analog Outputs ................................................................................................................................... 60
4.4.2 Analog Output Calibration Procedure ................................................................................................. 61
4.4.3 Analog Inputs ...................................................................................................................................... 61
4.4.4 Digital Status Inputs ............................................................................................................................ 61
4.4.5 Digital Status Outputs ......................................................................................................................... 61
4.5 Using Airodis Software to Download Data from a Serinus Gas Analyser ............................................................ 63
4.5.1 Installation .......................................................................................................................................... 63
4.5.2 Connecting the Serinus to your PC ...................................................................................................... 63
Page 4
4.5.3 Installing Airodis .................................................................................................................................. 66
4.5.4 Configuring Airodis .............................................................................................................................. 67
4.6 Serinus Remote App/Bluetooth .......................................................................................................................... 73
4.6.1 Installation ........................................................................................................................................... 73
4.6.2 Connecting to the Analyser ................................................................................................................. 74
4.6.3 Control Serinus Analyser ...................................................................................................................... 75
4.6.4 Real-time Plot ...................................................................................................................................... 76
4.6.5 Download............................................................................................................................................. 78
4.6.6 Get Parameters .................................................................................................................................... 79
4.6.7 Preferences .......................................................................................................................................... 79
5. Calibration ...................................................................................................................................... 83
5.1 Zero Calibration ................................................................................................................................................... 83
5.2 Span Calibration .................................................................................................................................................. 84
5.3 Multipoint Precision Check ................................................................................................................................. 85
5.4 Precision Check ................................................................................................................................................... 86
5.5 Pressure Calibration ............................................................................................................................................ 87
5.5.1 Pressure Calibration (with internal pump option only) ....................................................................... 89
5.5.2 Flow Calibration (with internal pump option only) .............................................................................. 91
5.6 High Pressure Zero/Span Valve ........................................................................................................................... 93
5.6.1 Single Pressurised Calibration Option .................................................................................................. 93
5.6.2 Dual Pressurised Calibration Option .................................................................................................... 94
6. Service ............................................................................................................................................ 97
6.1 Pneumatic Diagram ............................................................................................................................................. 97
6.2 Maintenance Tools .............................................................................................................................................. 97
6.3 Maintenance Schedule ........................................................................................................................................ 98
6.4 Maintenance Procedures .................................................................................................................................... 98
6.4.1 Particulate Filter Replacement ............................................................................................................ 98
6.4.2 Clean Fan Filter .................................................................................................................................... 99
6.4.3 DFU Replacement ................................................................................................................................ 99
6.4.4 Leak Check ......................................................................................................................................... 100
6.4.5 CO-CO2 Converter Check ................................................................................................................... 101
6.4.6 Sintered Filter/Orifice Replacement .................................................................................................. 102
6.4.7 Trim pot Tuning Procedure ................................................................................................................ 103
6.4.8 Clean Pneumatics .............................................................................................................................. 103
6.4.9 Pressure Sensor Check ....................................................................................................................... 103
6.4.10 Battery Replacement ......................................................................................................................... 104
6.5 Parts List ............................................................................................................................................................ 106
6.6 Bootloader ........................................................................................................................................................ 108
6.6.1 Display Help Screen ........................................................................................................................... 108
6.6.2 Communications Port Test ................................................................................................................ 108
6.6.3 Updating Firmware ............................................................................................................................ 108
6.6.4 Erase All Settings................................................................................................................................ 109
6.6.5 Start Analyser .................................................................................................................................... 109
Introduction Page 5
Ser in u s 3 0 Us er M an u a l 2. 2
List of Figures
Figure 1 Measurement cell theory ..................................................................................................... 21
Figure 2 Correlation wheel ................................................................................................................. 22
Figure 3 Major components ............................................................................................................... 23
Figure 4 - Opening the instrument ........................................................................................................ 27
Figure 5 Instrument back panel .......................................................................................................... 29
Figure 6 Travel screw locations .......................................................................................................... 31
Figure 7 Switching the battery on/off ................................................................................................ 34
Figure 8 Serinus front panel ............................................................................................................... 36
Figure 9 Main screen .......................................................................................................................... 37
Figure 10 Main menu.......................................................................................................................... 40
Figure 11 Communication ports ......................................................................................................... 59
Figure 12 Serinus 25-pin microprocessor board (with default jumpers highlighted) ........................ 62
Figure 13 External 25pin I/O individual pin descriptions ................................................................... 62
Figure 14 Configure Serinus logging interval ...................................................................................... 63
Figure 15 Installing driver software .................................................................................................... 63
Figure 16 Installing driver software .................................................................................................... 64
Figure 17 Installing driver software .................................................................................................... 64
Figure 18 Installing driver ................................................................................................................... 65
Figure 19 Successful driver installation .............................................................................................. 65
Figure 20 Serial communications menu ............................................................................................. 66
Figure 21 Network adaptor menu ...................................................................................................... 66
Figure 22 Airodis workspace manager ............................................................................................... 67
Figure 23 Adding a new station .......................................................................................................... 68
Figure 24 New station connection...................................................................................................... 68
Page 6
Figure 25 Station configuration ........................................................................................................... 69
Figure 26 Error status notification ...................................................................................................... 70
Figure 27 Downloading data ............................................................................................................... 70
Figure 28 Download data status.......................................................................................................... 71
Figure 29 Data visibility ....................................................................................................................... 72
Figure 30 Exporting data ..................................................................................................................... 72
Figure 31 Data download complete .................................................................................................... 73
Figure 32 Downloading the app from Google Play store .................................................................... 74
Figure 33 Bluetooth pairing request ................................................................................................... 74
Figure 34 Entering numbers into the Serinus Application .................................................................. 75
Figure 35 Switching analysers in Serinus Application ......................................................................... 76
Figure 36 Real-time plot ...................................................................................................................... 77
Figure 37 Plot of downloaded data ..................................................................................................... 79
Figure 38 Directory settings ................................................................................................................ 80
Figure 39 Logs format.......................................................................................................................... 80
Figure 40 Colour theme settings ......................................................................................................... 81
Figure 41 Excel graph of multipoint calibration .................................................................................. 86
Figure 42 Pressure calibration ............................................................................................................. 87
Figure 43 Vacuum set pt...................................................................................................................... 87
Figure 44 Edit vacuum set pt. .............................................................................................................. 88
Figure 45 Ambient set pt. .................................................................................................................... 88
Figure 46 Setting the ambient set point.............................................................................................. 89
Figure 47 Exit calibration menu........................................................................................................... 89
Figure 48 Pressure calibration menu .................................................................................................. 89
Figure 49 Valves automatically set ...................................................................................................... 90
Figure 50 Vacuum set pt...................................................................................................................... 90
Figure 51 Connect a pressure meter ................................................................................................... 90
Figure 52 Adjust ambient set pt. ......................................................................................................... 91
Figure 53 Exit pressure calibration menu............................................................................................ 91
Figure 54 Manual flow calibration ...................................................................................................... 92
Figure 55 Single high pressure calibration option ............................................................................... 94
Figure 56 Dual high pressure calibration option ................................................................................. 95
Figure 57 Serinus 30 pneumatic diagram ........................................................................................... 97
Figure 58 Removing plunger ............................................................................................................... 99
Figure 59 Removing fan filter .............................................................................................................. 99
Figure 60 DFU filter ........................................................................................................................... 100
Figure 61 Pressure gauge on exhaust................................................................................................ 100
Figure 62 Kynar fitting containing orifice and sintered filter ............................................................ 102
Figure 63 Test point location ............................................................................................................. 104
Figure 64 Typical test point reading of cell pressure sensor ............................................................. 104
Figure 65 Flow fault diagnostic procedure ........................................................................................ 114
Figure 66 Noisy zero or unstable span diagnostic procedure ........................................................... 115
Figure 67 Cell temperature failure diagnostic procedure ................................................................. 116
Figure 68 Mirror temperature failure diagnostic procedure ............................................................ 117
Introduction Page 7
Ser in u s 3 0 Us er M an u a l 2. 2
List of Tables
Table 1 Manual revision history ......................................................................................................... 15
Table 2 Digital pots ............................................................................................................................. 49
Table 3 Analog outputs ....................................................................................................................... 60
Table 4 Setting up a new station via Airodis ...................................................................................... 68
Table 5 Maintenance schedule ........................................................................................................... 98
Table 6 Spare parts list ..................................................................................................................... 106
Table 7 Serinus 30 Maintenance Kit ................................................................................................. 107
Table 8 Other Consumables Not included in Maintenance Kit...................................................... 107
Table 9 Troubleshoot list .................................................................................................................. 111
Table 10 Internal pump additional components .............................................................................. 123
Table 11 Internal pump removed components ................................................................................ 124
Table 12 Advanced protocol parameter list ..................................................................................... 125
Table 13 Bavarian data ..................................................................................................................... 137
Table 14 Block check operation ........................................................................................................ 138
Table 15 Bavarian Protocol Commands............................................................................................ 138
Table 16 Bit map ............................................................................................................................... 140
Table 17 Bit map (positive logic)....................................................................................................... 140
List of Equations
Equation 1 Instrument accuracy......................................................................................................... 85
Page 8
Manufacturers Statement
Thank you for selecting the Ecotech Serinus 30 Carbon Monoxide Analyser.
The Serinus series is the next generation of Ecotech designed and manufactured gas analysers. The
Serinus 30 will perform carbon monoxide measurements over a range of 0-200ppm with a lower
detectable limit of 40 ppb.
This User Manual provides a complete product description including operating instructions,
calibration, and maintenance requirements for the Serinus 30.
Reference should also be made to the relevant local standards which should be used in conjunction
with this manual.
If, after reading this manual you have any questions or you are still unsure or unclear on any part of
the Serinus 30 then please do not hesitate to contact Ecotech or your local Ecotech distributor.
Please help the environment and recycle the pages of this manual when you have finished
using it.
Notice
The information contained in this manual is subject to change without notice. Ecotech reserves the
right to make changes to equipment construction, design, specifications and/or procedures without
notice.
Copyright 2013. All rights reserved. Reproduction of this manual, in any form, is prohibited
without the written consent of Ecotech Pty Ltd.
CAUTION
Hazardous voltages exist within the analyser. The analyser lid should be closed
when the analyser is left unattended or turned on. Ensure the power cable, plugs
and sockets are maintained in a safe working condition.
Introduction Page 9
Ser in u s 3 0 Us er M an u a l 2. 2
Safety Requirements
To reduce the risk of personal injury caused by electrical shock, follow all safety notices and warnings
in this documentation.
If the equipment is used for purposes not specified by Ecotech, the protection provided by this
equipment may be impaired.
Replacement of any part should only be carried out by qualified personnel, using only parts specified
by Ecotech as these parts meet stringent Ecotech quality assurance standards. Always disconnect the
power source before removing or replacing any components.
Warranty
This product has been manufactured in an ISO 9001/ISO 14001 facility with care and attention to
quality.
The product is subject to a 24-month warranty on parts and labour from date of shipment. The
warranty period commences when the product is shipped from the factory. Lamps, fuses, filters,
batteries and other consumable items are not covered by this warranty.
Each analyser is subjected to a vigorous testing procedure prior to despatch and will be accompanied
with a parameter list and a multipoint calibration check thereby enabling the analyser to be installed
and ready for use without any further testing.
Page 10
Service & Repairs
Our qualified and experienced technicians are available to provide fast and friendly service between
the hours of 8:30am 5:00pm AEST Monday to Friday. You are welcome to speak to a service
technician regarding any questions you have about your analyser.
Service Guidelines
In the first instance, please call or email us if you are experiencing any problems or issues with your
analyser.
If you are within Australia or New Zealand please contact our service response centre via email on
[email protected] or call +61 (0)3 9730 7800
If outside of Australia and New Zealand please email our international support department at
[email protected] or call +61 3 9730 7800
If we cannot resolve the problem through technical support, please email the following information:
When you email us we will assign a Return Material Authorisation (RMA) number to your shipment
and initiate the necessary paperwork to process your equipment within 48 hours.
Please include this RMA number when you return equipment, preferably both inside and outside the
shipping packaging. This will ensure you receive prompt service.
Introduction Page 11
Ser in u s 3 0 Us er M an u a l 2. 2
Council Directive of 15 December 2004 on the approximation of the laws of Member States
relating to electromagnetic compatibility (2004/108/EC)
EN 61326-1:2006 Electrical equipment for measurement, control and laboratory use EMC
requirements Part 1: General requirements.
Council Directive of 12 December 2006 on the harmonisation of the laws of member states relating
to electrical equipment designed for use within certain voltage limits (2006/95/EC)
EN 61010-1:2001 Safety requirements for electrical equipment, for measurement control and
laboratory use Part 1: General requirements.
Page 12
Claims for Damaged Shipments and Shipping Discrepancies
Damaged Shipments
Inspect all instruments thoroughly on receipt. Check materials in the container/s against the
enclosed packing list. If the contents are damaged and/or the instrument fails to operate properly,
notify the carrier and Ecotech immediately.
You may want to keep a copy of these documents for your records.
Please refer to the instrument name, model number, serial number, sales order number and your
purchase order number on all claims.
Shipping Discrepancies
Check all packages against the packing list immediately on receipt. If a shortage or other discrepancy
is found, notify the carrier and Ecotech immediately. We will not be responsible for shortages against
the packing list unless they are reported promptly (within 7 days).
Contact Details
Head Office
1492 Ferntree Gully Road, Knoxfield VIC Australia 3180
Phone: +61 (0)3 9730 7800 Fax: +61 (0)3 9730 7899
Email: [email protected]
Service: [email protected]
International Support: [email protected]
www.ecotech.com
Introduction Page 13
Ser in u s 3 0 Us er M an u a l 2. 2
Page 14
Manual Revision History
Manual PN: M010027
Current revision: 2.2
Date released: 10 December 2013
Description: User Manual for the Serinus 30 Carbon Monoxide Analyser
This manual is the full user manual for the Serinus 30 Carbon Monoxide Analyser. This manual
contains all relevant information on theory, specifications, installation, operation, maintenance and
calibration. Any information that cannot be found within this manual can be obtained by contacting
Ecotech.
Introduction Page 15
Ser in u s 3 0 Us er M an u a l 2. 2
Page 16
1. Introduction
1.1 Description
The Ecotech Serinus 30 Carbon Monoxide Analyser is used to measure CO in ambient air, in the range
of 0-200ppm. The Serinus 30 measures CO using the following components:
Microprocessor control
Proven Gas Filter Correlation (GFC)
Combined with Non-Dispersive Infrared Spectrophotometry (NDIR) technology
A microprocessor programmed with Serinus firmware monitors the detector response and many
other parameters. The CO concentrations are automatically corrected for gas temperature and
pressure changes and when using gravimetric units (e.g. g/m) is referenced to 0C, 20C or 25C at
1 atmosphere. This allows the Serinus 30 to provide readings in the relevant units for your
requirements.
The U.S. EPA has designated the Serinus 30 Carbon Monoxide Analyser as a Reference Method and
SIRA has designated it as an EN approved instrument
1.2 Specifications
1.2.1 Measurement
Range
0-200 ppm auto ranging.
USEPA designated range: Any full scale range between 0-50 ppm.
Lower detectable limit: 0.04 ppm (40 ppb), with Kalman filter active.
1.2.2 Precision/Accuracy
Precision
20 ppb or 0.1% of reading, whichever is greater.
Linearity
Better than 1% of full scale (0-50 ppm); 2% of full scale (0-200 ppm), from best straight-line fit.
Noise at Zero
0.02 ppm.
Response Time
60 seconds to 95%.
Introduction Page 17
Ser in u s 3 0 Us er M an u a l 2. 2
1.2.3 Calibration
Zero Drift
Temperature dependant: 0.01 ppm per C.
Span Drift
Temperature dependant: 0.05% per C.
1.2.4 Power
Operating Voltage
99 to 132 VAC (57-63 Hz) or via switch 198 to 264 VAC (47-53 Hz).
Power Consumption
265 VA maximum (typical at start-up).
Fuse Rating
20x5 mm, T 250 V, 5 A (slow blow).
1.2.6 Communications
USB port connection on rear panel
Page 18
Bluetooth (digital communication via Android App)
TCP/IP Ethernet network connection (optional)
RS232 port #1: Normal digital communication
RS232 port #2: Multi-drop port used for multiple analyser connections on a single
RS232 cable
USB memory stick (front panel) for data logging, event logging and parameter/configuration
storage
Protocols
Modbus RTU/TCP, Bavarian, EC9800, Advanced.
1.2.8 Certifications
U.S. EPA approved (RFCA-0509-174)
EN approval (Sira MC 100166/02)
Non Dispersive I.R. Spectrometry method EN1426
Determination of carbon monoxide AS 3580.7.1.2011 Australian/New Zealand standards
Introduction Page 19
Ser in u s 3 0 Us er M an u a l 2. 2
1.3 Nomenclature
Zero: Zero calibration uses zero air (CO scrubbed ambient air) to calibrate/check
the lower range of the instrument.
Background: Is the reading of the sample without carbon monoxide present in the
measurement cell
Zero Drift: The change in instrument response to zero air over a period of continuous
unadjusted operation.
Automatic Zero: The automatic zero performs a zero check at a specified time through a 24
hour cycle which adjusts the lower limit of the analysers.
Zero Air: Is purified air in which the concentration of CO is <50 ppb with water vapour
of less than 10% RH. The internal CO-CO2 catalytic converter uses platinum
impregnated alumina beads heated to 90 C as a conversion agent to achieve
this under ambient conditions.
External Span Source: Span gas that is delivered via an external accredited cylinder (e.g.
NATA/NIST).
Sample Air: Sample air is defined as the sample before it has entered the reaction cell, as
distinguished from the exhaust air.
Exhaust Air: Exhaust air is the sample air after it has passed through the
reaction/measurement/detection cell and is moving towards being expelled
from the analyser.
ID and OD: These are measurements of tubing. ID is the internal diameter of tubing, OD
is the outer diameter.
Multi-drop: A configuration of multiple analysers connected via the same RS232 cable.
Photomultiplier Tube: A highly sensitive device which can detect extremely low levels of light
(photons) and multiply the electrical signal to a point where it can be
accurately measured. These are often called PMTs for short.
Bootloader: A program that checks whether the current firmware is valid, then executes
the instrument start-up. The Bootloader can be entered by pressing the +
key on the front keypad during the first second after power on, and
following the prompts. The Bootloader then enables various low level
recovery tools, including updating the main firmware from a USB key.
Page 20
1.4 Background/Theory
Carbon monoxide poisoning is the most common type of fatal poisoning in many industrialised
countries1. Carbon monoxide is a colourless, odourless and tasteless gas caused by the incomplete
combustion of hydrocarbon fuels.
Carbon monoxide is a toxic gas to the human body, when inhaled it binds to haemoglobin,
myoglobin, and mitochondrial cytochrome oxidase reducing oxygen storage, transport and
respiration in these organelles.
This can affect humans by causing low level symptoms such as headaches, nausea and dizziness
leading up to vomiting and loss of mental/muscular control at high exposure and death in extreme
cases.
CO absorbs infrared radiation (IR) at a wavelength near 4.7 microns. IR radiation (at 4.7 microns) is
passed through a 5 metre folded path length through sample air. The strength of the signal received
is proportional to the amount of CO in the sample as shown in the Beer Lambert Law. A band pass
filter is fitted to the signal detector to ensure only light near 4.7 microns wavelength is detected.
A gas filter correlation wheel is combined with this system. This wheel contains 3 parts to increase
measurement accuracy; CO, N2 and the mask.
1
Toxicology. 2002 Nov 15;180(2):139-50
Introduction Page 21
Ser in u s 3 0 Us er M an u a l 2. 2
The CO window contains a saturation (40%) of CO which acts as a reference beam absorbing a
known amount of light.
The N2 window, containing 100% N2, does not absorb IR at 4.7 microns at all and is used during
normal CO measurement.
The mask totally blocks the light source and is used to determine background signals and the
strength of other signals relative to each other and the background.
The Kalman filter enhances measurements by modifying the filter time base variable, depending on
the change rate of the measured value. If the signal is changing rapidly, the instrument is allowed to
respond quickly. When the signal is steady, a long integration time is used to reduce noise. The
system continuously analyses the signal and uses the appropriate filtering time.
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1.5 Instrument Description
Introduction Page 23
Ser in u s 3 0 Us er M an u a l 2. 2
IR Source
The IR source emits broadband infrared radiation that irradiates the filter in the correlation wheel.
The N2 chamber allows all the IR radiation to pass through which allows the radiation to be
absorbed by CO in the measurement cell and readings to be recorded.
The CO filled chamber absorbs wavelengths sensitive to CO. The sample gas (containing CO) in
the measurement cell does not receive CO specific IR radiation and the only detected signals
registered by the IR detector are from background sources and interference.
The mask blocks all IR light entering the cell. This allows the intensity of the other two signals to
be corrected for the detector response to no IR.
Opto-detector
The correlation wheel has four tabs that act as an opto electronic switch ensuring that the main PCB
can determine accurate timing of the wheel and which segment is currently exposed to the IR
radiation.
Measurement Cell
The measurement cell contains 5 mirrors that form a five meter path length through the cell. The
sample gas fills this chamber and the IR light travels through the sample.
Narrow-Bandpass Filter
The narrow bandpass filter allows only the CO sensitive portion of the IR radiation to pass through to
the IR detector (4.7 microns) reducing noise and interference.
IR Detector
The IR detector is a cooled lead selenide (PbSe) photoconductive IR detector. It creates an electrical
signal when wavelengths centred at 4.7 microns reach it.
Page 24
CAUTION
Never place objects on top of the main controller PCB as it may result in
damage.
It has a selectable input voltage of 115 or 230 VAC, 50/60 Hz and an output voltage of 12 VDC power
for distribution within the analyser.
CAUTION
Input voltage can be manually changed by sliding the red switch left (230) for 220-
240 V or right (110) for the 100-120 V. Ensure the switch is set to the correct
voltage (from supply) before switching on.
1.5.9 Communications
Communication between the analyser and either a data logger, laptop or network can be performed
with the following communication connections located on the back panel (refer to Figure 5).
RS232 #1
This port is designed to be used for simple RS232 communication.
RS232 #2
This port is designed to be used for simple RS232 communication, or in multi-drop configuration.
USB
This port can be used for instrument communication and is also good for quickly downloading data,
onsite diagnostics, maintenance and firmware upgrades.
TCP/IP (optional)
This port is best used for remote access and real-time access to instruments when a network is
available to connect with.
Analog Outputs
The analyser is equipped with three analog outputs. Menu selectable as either voltage output 0-5
VDC, or current output 0-20, 2-20, 4-20 mA.
Introduction Page 25
Ser in u s 3 0 Us er M an u a l 2. 2
Analog Inputs
The analyser is also equipped with three analog voltage inputs (0-5 VDC CAT 1) with resolution of 15
bits plus polarity.
CAUTION
Exceeding these voltages can permanently damage the instrument and void the
warranty.
CAUTION
Exceeding these voltages can permanently damage the instrument and void the
warranty.
CAUTION
Exceeding 12 VDC or drawing greater than 400 mA on a single output or a total
greater than 2 A across the 8 outputs can permanently damage the instrument
and void the warranty.
Bluetooth
This allows for remote access of the analyser to any Android device with the Serinus Remote
Application installed on it. Uses Bluetooth to control the analyser, view parameters, download data
and construct real-time graphs.
Page 26
2. Installation
2.1 Initial Check
Packaging
The Serinus 30 is transported in packaging which is specifically designed to minimise the effects of
shock and vibration during transportation. Ecotech recommends that the packaging be kept if there
is a likelihood that the instrument is going to be relocated.
Note: The red plastic caps that seal the pneumatic connections during transport must be removed
prior to operation.
Installation Page 27
Ser in u s 3 0 Us er M an u a l 2. 2
Items Received
With the delivery of the Serinus 30, you should have received the following:
UK PN: C040010
*Power cord received depends on the power supply of the country (120 V or 240 V).
Note: Please check that all these items have been delivered undamaged. If any item appears
damaged, please contact your supplier before turning the instrument on.
2.2 Mounting/Installing
When installing the instrument the following points must be taken into account:
The analyser should be placed in an environment with minimal dust, moisture and variation in
temperature (20-30 C for U.S. EPA designated range).
For best results the analyser should be located in a temperature and humidity controlled
environment (air conditioned shelter). An enclosure temperature of 25-27 C is optimum.
Whether in a rack or placed on a bench, the instrument should not have anything placed on top
of it or touching the case.
Instruments should be sited with easy access to the front panel (instrument screen/USB flash)
and to the back panel (communication ports/pneumatic connections).
It is recommended that the sample line be as short as possible and/or a heated manifold be used
for sampling (minimising moisture condensation in the sample).
Do not pressurise the sample line under any circumstances. Sample should be drawn through the
instrument under atmospheric pressure. This should be achieved by either using the internal
pump option (if installed) or an external vacuum pump connected to the exhaust port of the
analyser.
When supplying span gas, ensure the flow is approximately 1.5 lpm and excess is sufficiently
vented.
Undo the travel screws from the cell as shown in the drawing supplied (refer to Section 2.3.4).
Note: The power on/off switch is accessible from the rear of the instrument only. Site the
analyser so that the on/off power switch is accessible.
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2.3 Instrument Set-up
After installing the instrument the following procedures should be followed to ready the analyser for
monitoring:
Must be made of Teflon FEP material, Kynar, stainless steel, glass or any other suitably inert
material
Sample line should be no more than 2 meters in length with inch ID, inch OD
Sample inlet pressure should not exceed 5 kPa above ambient pressure
Tubing must be cut squarely and any burrs removed
Remove the inlet port nut, then insert the tubing through the back of the nut with the tube
extending 1 inch through the front
Place the tubing into the port until it hits the tube stop located inside the fitting
Place the nut back onto the fitting and tighten clockwise until finger tight
Nuts should be re-tightened when instrument reaches operating temperature
Sample Port
The Sample Port must be connected to an ambient source of sample air. When using a sample
manifold the Serinus requires at least 1.5 slpm delivered to sample manifold (1 slpm for
measurement plus approximately 50% overflow).
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Ser in u s 3 0 Us er M an u a l 2. 2
Calibration Port
The Calibration Port should be connected to the span/zero source. It is recommended that a dilution
gas calibrator be used with carbon monoxide to deliver precise concentrations of CO.
Note: All connections to this port should not exceed ambient pressure. A vent is required for excess
span gas.
Exhaust Port
The Exhaust Port is where the measured sample is exhausted from the analyser. The exhaust tubing
should be fitted to a vacuum pump (minimum: 1.5 SLPM at 50 kPa) if the internal pump option is not
installed in your analyser.
CAUTION
Carbon monoxide (CO) is a toxic gas. It is recommended that exhaust air is expelled
into an unoccupied area, as it contains trace levels of carbon monoxide.
Furthermore, the exhaust must be a suitable distance from the sample inlet to
avoid influencing the ambient measurements.
The Background Port is used to supply air to the CO to CO2 converter (i.e. CO scrubber) within the
instrument. This is used for backgrounds and internal zero calibration.
When connecting the power source the following must be adhered to:
Verify that the red switch (above power switch) is switched to the correct setting (230 V or 110 V)
A three pin power plug (with ground) MUST be used with an earthed power socket
(3 pin)
Connect the power plug into the mains power point and turn the power switch on.
RS232 #1
Connect this port to a data logger (such as WinAQMS) with an RS232 cable.
RS232 #2
Connect the RS232 cable from the instrument to a computer, data logger or in a multi-drop
formation.
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Note: When using multi-drop ensure each analyser is given a unique instrument ID.
USB
Connect a USB cable to a computer and run either the Serinus downloader program or the Ecotech
WinAQMS data logger.
TCP/IP (optional)
Plug in a network cable (this cable should be attached to a network), then use the supplied Airodis
software to access the instrument and download data. The Airodis software is supplied on the green
USB resources key provided with the instrument.
Analog/Digital
This port is used to send and receive analog and digital signals. It is normally used to connect with a
gas calibrator or to activate alarm signals.
Each instrument contains 8 digital inputs, 8 digital outputs, 3 analog inputs and 3 analog outputs.
Bluetooth
Connection is enabled using Ecotechs Serinus Remote Android Application.
Use the Serinus Remote Android Application to access instrument and download data. It is available
for download directly from the Google Play Store. Search for Ecotech Serinus Remote.
3. Check that the battery is turned on at the main controller PCB (refer to Figure 7).
4. Turn on the instrument and allow the warm-up procedure to complete (refer to Section 3.1).
5. Check/set time and date (refer to Section 3.5.8).
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Ser in u s 3 0 Us er M an u a l 2. 2
The Serinus 30 is designated as reference method RFCA0509174 by the U.S. EPA (40 CFR Part 53).
The Serinus 30 must be used under the following conditions to satisfy this approval:
Range
0-50 ppm
Ambient Temperature
20-30 C
Line Voltage
105-125 VAC, 60 Hz
Pump
Ecotech optional internal or external pump
Filter
5 micron PTFE filter must be installed in front of the sample inlet (zero and span gas must pass
through this filter).
If the units in the measurement menu are changed from volumetric to gravimetric (or gravimetric
to volumetric) the analyser must be re-calibrated
The analyser must be operated and maintained in accordance with this user manual
The following menu selections must be used:
Measurement Settings
Background interval: Enabled
Calibration Menu
Span comp: Disabled
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Diagnostics Menu
Press/Temp/Flow comp: On
The Serinus 30 analyser is designated U.S. EPA reference method with or without the following
options/items:
Internal pump
Rack mount assembly
Internal zero/span assembly (IZS)
Optional Ethernet Port
The Serinus 40 has been certified to MCERTS performance standards for Continuous Ambient Air
Quality Monitoring Systems. The certificate number is Sira MC 100167/02. The Serinus 40 must be
used under the following conditions to meet EN requirements:
Range
0-50 ppb
Ambient Temperature
0-30 C
The analyser must be operated and maintained in accordance with this user manual.
Measurement Settings
Background interval: Enabled
Calibration Menu
Span comp: Disabled
ServiceDiagnostics Menu
Press/Temp/Flow comp: On
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Ser in u s 3 0 Us er M an u a l 2. 2
2.6 Transporting/Storage
Transporting the Serinus should be done with great care. It is recommended that the packaging the
Serinus was delivered in should be used when transporting or storing the instrument.
When transporting or storing the instrument the following points should be followed:
Note: After transport or storage the instrument must be set up and calibrated
(refer to Section 2.3.4).
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3. Operation
3.1 Warm-up
Once the instrument is turned on it will adjust itself to prepare for monitoring. No measurements are
taken during the warm-up.
Converter is Cold
The analyser progressively increases the temperature of the converter until it reaches the desired
temperature of 90C. When heating from cold, the converter will take approximately 20-30 minutes
to reach desired temperature.
After this warm-up has completed the instrument will immediately begin taking measurements.
3.2 Measurement
The Serinus 30 primarily operates in one continuous cycle, the sample cycle. A background is
performed after warm-up, once a day (at 23:50) or when the chassis temperature changes by 4. It is
used to measure background absorption in the cell and is subtracted from sample measurements.
Sample Cycle
Sample fill: Measurement cell fills with sample air
Sample measure: Measurement of sample air
Background Cycle
Background fill: Measurement cell fills with background air
Background measure: Measurement of background air
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The Serinus is operated with the use of 4 sets of buttons: (1) selection buttons (2) scrolling buttons
(3) keypad and (4) instrument status light buttons.
On the main screen these buttons are used for adjusting the screen contrast. Press and hold the up
button to increase contrast; press and hold the down button to decrease contrast.
Keypad (3)
The keypad contains numbers 0-9, decimal point/minus key ( ) and a space/plus key ( ). The
number keys are used to input numbers; in those cases where letters can be entered, the number
keys act like a telephone keypad.
The ( ) and key () key functions depend on context. When editing a floating point number, the
key () inserts a negative sign if the editing cursor is at the start of the number and negative signs are
allowed. Otherwise it moves the decimal place to the current cursor location. The ( ) key inserts
a positive sign if the cursor is at the start of the number. Otherwise it enters a space.
For non-floating point numbers, these keys usually increment or decrement the current value by 1.
When editing the month field of a date, the ( ) and the ( ) key change the month.
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Instrument Status Light Buttons (4)
Located in the top left corner, these lights indicate the status of the instrument as a whole.
A flashing red light indicates that the instrument has a major failure and is not functioning.
An orange light indicates there is a minor problem with the instrument, but the instrument may
still take measurements reliably.
A green light indicates that the instrument is working and there are no problems.
In the case of a yellow or red light enter the Main Menu Analyser State Status Menu to find
which components are failing (refer to Section 3.5.4).
The green status button will cancel any open edit box or menu and return to the main display.
If no instrument status lights are on and the keypad is backlit, then this indicates that the instrument
is running the bootloader.
The main display is composed of seven parts: the readings (1), the error/status line (2), the
instrument activity line (3), selection buttons (4), the time/date (5), the concentration units (6) and
USB status (7).
Readings (1)
Displays the concentration being measured in real time. The display can be configured to show just
the instantaneous data or the instantaneous and average data (refer to Section 3.5.8).
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Ser in u s 3 0 Us er M an u a l 2. 2
Note: To safely remove the USB memory stick, navigate to the Quick Menu and use the Safely
Remove USB Stick function (refer to Section 3.5.1)
The menu system is divided into two sections, the Quick Menu and the Main Menu. The Quick Menu
contains all information and operations necessary during scheduled maintenance visits. The Main
Menu contains all fields that are accessible to users; they provide information on component
failures, measurement parameters as well as editable fields and test procedures.
In general, editable parameters are displayed in bold font. Non-editable information is displayed in a
thin font. Some parameters may become editable based on the state of the machine (for example,
the manual Cal. Mode and Port can only be changed when the instrument is out of warm-up).
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Span Calibrate
This field is used to perform a span calibration and should be only used when a known concentration
of span gas is running through the measurement cell and the reading is stable.
After activating the span calibrate field, a window will open with editable numbers. Change the
numbers to match the concentration of the span gas that the instrument is sampling and select
Accept. The instrument span calibration has now been performed.
Event Log
This field enters a screen with a log of all the events that the instrument has performed. These
events include calibrations, errors, backgrounds and warnings. This log is stored on the removable
USB flash memory.
Instrument
This field allows the instrument to be set to either Online (normal instrument operation) or In
Maintenance. This field is used to change the instrument to In Maintenance when service work is
being performed.
Gain
This is a multiplication factor which is used to adjust the concentration measurement to the
appropriate level (set by performing a Span Calibrate). This should be recorded after each calibration
in the station log book.
Service Due
A field that notifies the user when the next instrument service is due. This value is editable in the
Next Service Due field of the Service Menu (refer to Section 3.5.14). This field is only displayed in the
2 weeks prior to the date displayed in this field, or after the date has occurred.
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3.5.3 Analyser State
This displays the status of various parameters that affect instrument measurements.
3.5.4 Status
The Status Menu presents a list of the current Pass/Fail statuses of the main components. During
warm-up, the status of some parameters will be a dashed line.
Service Due This field is visible with the next service due date if the service is
due within the next two weeks.
Cell Temp. Pass if the cell temperature is within 10% of the heater set point
(refer to Section 3.5.8).
Mirror Temp. Pass if the mirror temperature is within 10% of the heater set
point (refer to Section 3.5.8).
Converter Temp. The converter temperature should be 90C 10% to pass.
Sample Flow Indicates whether the instrument has acceptable sample flow
(based on the difference between cell and ambient pressures).
Flow Block Temp. Pass if the flow block temperature is within 10% of the heater set
point (to keep a constant accurate flow). This field is only present
when the internal pump option is installed.
A/D Input A reference voltage is monitored by the analog to digital converter
IC; this field will display a pass if the voltage has acceptable limits.
Chassis Temperature Displays whether the chassis temperature is within the acceptable
limits (0-50 C).
Ref Voltage Checks that the reference voltage is within acceptable limits 3.6 V
to 4.4 V.
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3.5.5 Temperatures
Temp. Units Editable field to allow the user to change the current temperature
units of the analyser (Celsius, Fahrenheit, or Kelvin).
Set Point (cell) Editable field that sets the target temperature that some heated
components are regulated to including the cell.
Cell Displays current temperature of the reaction cell.
Converter Temperature of the catalytic converter that converts CO to CO2 at
a temperature of 90 C.
Flow block If an internal pump is installed, if this field displays the current
temperature of the flow block.
Chassis Displays the temperature of air inside the chassis, measured on
the main controller board.
Mirror Temperature of the end-cap mirror plate on the reaction cell.
Press. Units Select the units that the pressure will be displayed in (torr, PSI,
mBar, ATM, kPa).
Ambient Current ambient pressure.
Sample Flow Indicates the gas flow through the Sample Port of the instrument
(should be around 1.0).
Note: The sample flow will read 0.00 if there is a sample flow error.
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3.5.7 Voltages
Conc Volt (raw) Voltage from the sensor proportional to the detected signal from
the reaction cell. This voltage represents the actual measurement
of gas.
Ref. Voltage The reference voltage is a measure of the IR source intensity.
Cooler Voltage Voltage of the peltier cooler within the IR detector (~1.17 V). This
voltage should be stable.
Analog Supply +12 V (primary) power supply.
Digital Supply +5 V microprocessor power supply.
-10V Supply -10 V reading from the main controller board.
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3.5.10 Calibration Menu
Calibrating the instrument should be done with care. Refer to Section 5 before using these menus.
Calibration Type Depending on the selection in this field, a number of extra menu
items will be displayed. These are separately documented in
Sections 0 and 3.5.12.
Select the Calibration Type field and select either Timed or
Manual. Timed calibration is an automatic calibration controlled
by the:
Interval between cycles
Length of each calibration cycle
When the calibration will begin
Whether the calibration will perform automatic compensation
Note: Timed calibration with span compensation enabled does not
fulfil U.S. EPA approval.
Manual calibration will perform a manual calibration depending on
the calibration mode selected below.
Zero Source Select whether the instrument will sample from the external
Calibration Port or from the internal zero source when zero gas is
requested.
Span Calibrate This field is used to correct the span calibration setting and should
be used only when a known concentration of span gas is running
through the measurement cell. When the readings are stable,
activate the Span Calibrate field, a window will open with editable
numbers, change the numbers to the concentration that the
instrument is receiving and select accept. The instrument span
calibration has now been set.
Zero Calibrate This field is used to correct the zero calibration setting on the CO
channel. This option should be used only when zero gas is running
through the measurement cell. When this is stable activate the
Zero Calibrate field, a window will open with editable numbers.
Leave the numbers at 0000.000 and select Accept.
Pressure Calibration This menu allows the user to calibrate the pressure sensors as
explained in section 5.5.
Flow Calibration This menu only appears if the optional internal pump is installed,
allowing the instrument flow sensors to be calibrated.
Calibration Pressure This field displays the measured manifold pressure during the last
calibration.
Calibration Temperature Cell temperature when the last span calibration was performed.
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3.5.13 Flow Calibration
When the internal pump is installed in the analyser this menu is added, unique only to instruments
with an internal pump.
Cal. Point When Manual Flow Control is set to Enabled, then this is the
flow at which the flow calibration was last performed. When
set to Disabled, editing this field sets the current flow
calibrated point to the value entered (must be calibrated at
Flow Set Point for accurate flow control). Refer to Section 5.5.2
for details on the flow calibration procedure.
Zero Flow When there is no flow through instrument (Sample Flow = 0)
select this field to calibrate the zero flow point.
Valves Menu Opens the Valves Menu where individual valves can be opened
and closed (refer to Section 3.5.17 for the Valves Menu).
3.5.14 Service
Diagnostics Refer to Section 3.5.15
Calculation Factors Refer to Section 3.5.19
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Instrument This field allows the instrument to be set to either Online (Normal
instrument operation) or In Maintenance (data is not valid, as
service work etc is being performed).
Next Service Due User editable field to set the date when the next instrument
service is required. Section 6.3 has a recommended maintenance
schedule that may be used as a basis for the interval entered
above. This value is also displayed as a non-editable field in the
Quick Menu section.
Safely Remove USB Stick This feature must be activated to safely remove the USB stick (also
found in the Quick Menu).
System Restart Activating this will reboot the microprocessor.
3.5.15 Diagnostics
Digital Pots Refer to Section 3.5.16
Valves Menu Refer to Section 3.5.17
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3.5.16 Digital Pots
Pots are electronically controlled digital potentiometers used for adjustments to operations of the
analyser. This menu should be accessed only during diagnostics.
Unless the control loop is turned off (refer to Section 3.5.15), changes to the pots may be modified
by the microprocessor. This is intentional; some diagnostics are best done with instrument feedback,
and some are best done with the instrument inactive.
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Valve Sequencing When Enabled the instruments valves will open and close under
microprocessor control. When Disabled the valves will change only
in response to manual controls.
Manually changing a valve while sequencing is enabled does not
prevent the microprocessor from changing it again.
Valve sequencing will remain off unless the instrument has
returned to main screen for longer than 2 minutes.
Sample/Cal Shows the action of the valve that determines whether sample gas
or calibration gas/internal zero air is being sampled (Open =
Span/Zero, Closed = Sample gas).
Internal Zero/Cal Shows the action of the valve that determines whether the sample
calibration gas is taken from the Calibration Port or the internal
zero (Closed = Internal Zero, Open = Calibration Port).
Pressurised Span (optional) Shows the action of the valve that determines whether the
instrument calibration gas is taken from the optional pressurised
Span Port (refer to Section 5.6).
Pressurised Zero (optional) Shows the action of the valve that determines whether the
instrument calibration gas is taken from the optional pressurised
Zero Port (refer to Section 5.6).
3.5.18 Tests
Screen Test Performs a screen test by drawing lines and images on the screen
so that the operator can determine if there are any faults in the
screen. Press a keypad key to step through the test.
The up and down arrow keys will adjust the contrast.
Digital Inputs Displays the status of the 0-7 digital input pins. Value will be a 0 or
a 1.
Digital Outputs This menu item allows the user to view the pins that digital
outputs are located on. The output can be switched on and off to
test the connection.
Note: Entering either the Digital Inputs or Digital Outputs Menu
will temporarily disable all digital and analog input/outputs. This
will affect logging via these outputs. Exiting the menu restores
automatic control.
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3.5.19 Calculation Factors
The calculation factors provide the values used to calculate different aspects of measurement and
calibration.
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Ser in u s 3 0 Us er M an u a l 2. 2
Note: The key will delete the currently highlighted parameter; the + key will insert a new
parameter at that location, moving the others down. The list of parameters must be contiguous.
Thus, when you delete a logging parameter, any parameters below it will be moved up.
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3.5.23 Analog Input Menu
The Serinus supports 3 analog inputs from the 25 pin I/O connector. Each input is a 0 to 5 volt CAT 1
input that can be scaled and then logged to the internal memory, or accessed remotely as
parameters 199-201.
CAUTION
Exceeding these voltages can permanently damage the instrument and void the
warranty.
Input 1/2/3 Multiplier The input voltage will be multiplied by this number. E.g. if a
sensor has a 0-5 V output for a temperature of -40 C to 60 C,
then the multiplier would be (60-(-40))/5 = 20.
Input 1/2/3 Offset This value will be added to the above calculation. Continuing
the example in the multiplier description, the offset should be
set to -40, so that a voltage of 0 V will be recorded as -40 C.
Input 1/2/3 Reading The current reading from the input voltage after the multiplier
and offset have been applied. This is the value that would
currently be logged, or reported as parameter 199-201 via
USB or serial requests.
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0.5 V Calibration Enables the user to calibrate the analog output at a low point.
Increase/decrease the value until the connected equipment
reads 0.5 V.
Current Range Enables the user to set desired current ranges. Choices are 0-
20 mA, 2-20 mA or 4-20 mA.
20mA Calibration Enables the user to calibrate the current output at a full scale
point of 20mA. Increase/decrease the value until the
connected equipment reads 20 mA.
4mA Calibration Enables the user to calibrate the current output at a low point.
Increase/decrease the value until the connected equipment
reads 4 mA.
Disabled
No action taken
Do Span
Perform a span check
Do Zero
Perform a zero check
The input is triggered with an active low. The actual digital input pin-outs are listed in the menu.
Example
Here is an example for a typical configuration between an analyser and either a data logger or
calibrator (master device):
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There are 8 different pins available, which will be set high during an associated event:
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Ser in u s 3 0 Us er M an u a l 2. 2
Protocol (Network) Sets the protocol used for the Network Port (EC9800,
Bavarian, Advanced, or Modbus). This must be set to
Advanced for Ecotech supplied software.
Start-up Mode The following modes are available:
Normal: In this mode nothing is done with the Network Port
during boot-up. It is assumed to be configured correctly or
unused.
Read IP: This mode interrogates the Network Port for its IP
address. The menu will display the network address after
boot-up.
Set IP: You may enter an IP address, Netmask, and Gateway
address (following the usual rules for formatting these
addresses). Please note that at this time the Serinus does not
validate the correctness of these entries.
When you cycle power, the Serinus will first instruct the
Network Port on its new address. It will then switch to Read IP
mode and read back the address it just set so that you may
verify it in the menu.
Set DHCP: This sets the Network Port into DHCP mode,
allowing the network to assign the Serinus an IP address.
IP Address This is the current IP address of the analyser e.g. 192.168.1.2
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ID This is the Bluetooth ID of the analyser. In edit mode the
number keys act like a telephone keypad. Every time a
number key is pressed, it cycles through its choices. The
up/down arrow keys scroll through all the numbers and the
entire alphabet.
1 = 1 or space
2 = 2, A, B, C, a, b, c
3 = 3, D, E, F, d, e, f
4 = 4, G, H, I, g, h, i
5 = 5, J, K, L, j, k, l
6 = 6, M, N, O, m, n, o
7 = 7, P, Q, R, S, p, q, r, s
8 = 8, T, U, V, t, u, v
9 = 9, W, X, Y, Z, w, x, y, z
0 = 0 or space
The default setting is the Serinus ID/Serial Number. Note: The
word Serinus is always the first part of the name and cannot
be edited.
PIN This is a passcode/pin required for the Serinus Remote
Application to connect to the analyser. The default pin is 1234.
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4. Communications
The Serinus has a number of different interfaces for communication with other equipment (RS232,
USB, 25 pin digital/analog input/output, TCP/IP network (optional) and Bluetooth). A demonstration
version of Ecotechs Airodis software is included with the instrument, enabling basic data
downloads and remote operation from a PC running MS Windows (7 or 8). The full version of Airodis
is available separately, and includes automated collection, data validation and complex reporting by
multiple users. Refer to the Airodis Manual for details on setting up and communicating with the
Serinus.
RS232 communication is a very reliable way to access data from the instrument, and is
recommended for use in connection to a data logger for 24/7 communication. Both RS232 ports are
configured as DCE, and can be connected to DTE (Data Terminal Equipment such as a data logger or
computer). Port #2 also supports a multi-drop arrangement (a configuration of multiple analysers
connected via the same RS232 cable where the transmit signal is only asserted by the instrument
that is spoken to). Verify that the Multi-drop ID is set to either 0 (for direct connection) or a unique
value which is different to the other analysers in the chain for a multi-drop configuration (refer to
Section 1.5.9).
This is ideal for irregular connection to a laptop running Ecotechs Airodis software to download
logged data and remotely control the instrument. Due to the nature of USB, this is a less reliable
permanent connection as external electrical noise can cause USB disconnection errors on a data
logger.
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Ser in u s 3 0 Us er M an u a l 2. 2
This port is best used for remote and real-time access to instruments when network connectivity is
available.
The 25 Pin analog/digital port on the rear of the analyser sends and receives analog/digital signals to
other devices. These signals are commonly used to activate gas calibrators or for warning alarms.
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4.4.2 Analog Output Calibration Procedure
Voltage Calibration
1. Navigate to the CommunicationsAnalogue Output Menu.
2. Ensure that Output Type is set to Voltage.
3. Connect a volt meter (using an appropriate adaptor or probes on the volt meter) to the ground
(pin 24) and the relevant output pin (pin 10).
4. Adjust the 0.5V Calibration value until the volt meter reads 0.500 +/ .002.
5. Adjust the 5.0V Calibration value until the volt meter reads 5.00 +/ .002.
Current Calibration
1. Navigate to the CommunicationsAnalogue Output Menu.
2. Ensure that Output Type is set to Current.
3. Connect a current meter (using an appropriate adaptor or probes on the current meter) to the
ground (pin 24) and the relevant output pin (pin 10).
4. Adjust the 4mA Calibration value until the volt meter reads 4mA +/ .01.
5. Adjust the 20mA Calibration value until the volt meter reads 4mA +/ .01.
In the default jumper locations (Figure 12) these two outputs will function normally as open collector
outputs. If moved to the position closer to the 25 pin connector then DO 0 will supply +12 V and DO
1 will supply +5 V. These supplies are limited to about 100 mA.
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Ser in u s 3 0 Us er M an u a l 2. 2
CAUTION
The analog and digital inputs and outputs are rated to CAT I.
Exceeding 12 VDC or drawing greater than 400 mA on a single output or a total
greater than 2 A across the 8 outputs can permanently damage the instrument
and void the warranty.
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4.5 Using Airodis Software to Download Data from a Serinus Gas Analyser
4.5.1 Installation
Power on the Serinus and connect it to your PC with a USB cable. You should receive a prompt if the
driver needs to be installed. If not, open Device Manager (Under System in Control Panel), find the
device and select Update Driver Software.
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When prompted where to search for the driver, select Browse my computer.
The Serinus USB driver is located on the green Ecotech Resources USB stick under \Drivers\Ecotech
Analyser. Select this directory and click Next.
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If you receive a confirmation prompt to install the driver, select Install.
If everything went smoothly, Windows will inform you that the driver was successfully installed.
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Ser in u s 3 0 Us er M an u a l 2. 2
1. Determine which RS232 Port you are physically connecting with. You can use either; however,
multidrop is only supported on RS232 #2.
2. Set the appropriate baud rate (in most situations, fastest is best).
3. Ensure that the protocol is set to Advanced.
4. If you are running Airodis in a multidrop configuration (multiple instruments on a single COM
port), ensure that the multidrop ID is unique for each instrument on the chain.
http://www.airodis.com.au/
Page 66
The installer is straightforward ensure you install the correct version for your operating system. If
you are running 64-bit windows, install the 64-bit (x64) version. Otherwise, install the 32-bit (x32)
version.
2. Start the Client, Server and Download Server by single-clicking the toggle button for each. The
client may prompt to register with Ecotech or install an update. Follow the prompts if it does.
3. Once the Client application has loaded, click HomeAdd StationNew Physical Station.
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Ser in u s 3 0 Us er M an u a l 2. 2
4. Select the new station and move to the Station tab on the ribbon. Enter the details to
connect to the Serinus.
Property Description
Station Name The name of the station. If you have other loggers, the name is used to distinguish them.
Logger Set this to Ecotech Serinus when downloading from any Serinus series instrument. This
will communicate with the Serinus on the Advanced protocol. If using a network or serial
connection, ensure that the Advanced protocol has also been selected on the Serinus
itself (Refer to Appendix A).
Time Zone Set this to the time zone that the Serinus is configured to log in.
DST Enable this option if you plan on changing the clock on the Serinus with daylight savings.
Leave this disabled if the clock does not shift during DST. Note: the Serinus will need to be
adjusted manually for DST it will not happen automatically.
Database Name This is the name to be used for the table in the SQL database containing this stations data.
It must be unique for each station.
Device ID Enter the multidrop ID of the Serinus (Refer to Section 4.1). If you are not using multidrop,
this can be set to 0 or left blank.
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Property Description
Link Type Select the type of connection used to connect to the Serinus. Additional properties will
appear to connect to the Serinus. Make these align with the configured communications
settings on the Serinus.
Log Interval This needs to be the same as the Data Log Interval setting on the Serinus.
The available fields for communications parameters will change when you change the link type. You
will need to set the communication parameters that have been defined on the Serinus.
5. Once the station has been created, save the station by clicking the Save shortcut icon or
FileSave.
6. Click Acquire Configuration. This will probe the Serinus for a channel list. After a few seconds,
the channel list should be visible in the Channels tab.
Note: If there was an error connecting to the Serinus, a red dot will appear next to its name in the
station list. Hovering over the red dot will present you with an error message.
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7. Select the Data Manager tab, click download. The Download Data window will appear. Select
the appropriate time period that you wish to download and click Download.
The status of the download will appear in the bottom-left corner of the window. You can also
monitor the status of the download from the Home tab.
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Figure 28 Download data status
8. Data will become available in the data manager as it is downloaded. You can load data for a date
range by entering the start and end dates and clicking Display. The selected data will then be
loaded into the data manager.
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9. Data can be exported by clicking the export function. This will allow you to save your data in CSV
format, which can then be loaded into another program such as Microsoft Excel. It is also
possible to copy/paste (ctrl+C / ctrl+V) data directly from the Airodis data manager.
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10. Thats it! The data has been downloaded from the instrument and exported to a standard CSV
file.
Ecotechs Serinus Remote Application allows for any Android device (Tablet or Smartphone) to
connect to an analyser.
Completely control the analyser using a remote screen displayed on the device
Download logged data and take snapshots of all the instrument parameters
Construct graphs from logged data or real time measurements
4.6.1 Installation
The Serinus Remote Application can be found in the Google Play Store by searching for Ecotech or
Serinus. Once found, choose to Install the application and then Open to start the application.
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Note: A menu containing additional features and functions can be accessed by entering the
Options menu (or similar) on your device. The location and format of this menu may vary.
To connect to an analyser:
4. Touch the Scan Serinus Analysers button at the bottom of the screen.
5. Select the Analyser ID from either the Paired Devices or the Other Available Devices
(see ID in the Bluetooth Menu).
6. Input the PIN (if prompted to do so) then press OK (see PIN in the Bluetooth Menu).
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A screen shot of the analysers current screen should appear on your Smartphone or Tablet. To
disconnect press the Back key/button on the device.
Note: Once the analyser has been paired with the device it will appear under Paired Devices
and the PIN will not need to be entered again.
Main Screen
Touching the upper half of the screen increases the contrast and touching the lower half of the
screen decreases contrast on the real instrument.
Menus
Touching the upper or lower half of the screen allows the user to scroll up and down respectively.
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Back Button
This button will return to the selection screen, allowing you to connect to a different analyser.
Options Menu
The Options Menu is accessed by the grey button in the top right corner of the screen or pressing
the Menu Button, depending on your Android device.
Once the plot is zoomed or scrolled, it enters into Observer Mode, meaning that auto-scaling is
suspended. Press at the top of the screen (where it says Observer Mode) to return to Normal Mode.
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Figure 36 Real-time plot
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Options Menu
The Options Menu is accessed by the grey button in the top right corner of the screen or pressing
the menu button, depending on your Android device.
Start Restarts graphing if it has been stopped and returns the graph to Normal Mode.
Stop Stops collecting data. In this mode you can scroll the display without going into Observer
Mode, because the system has no data collection to suspend. It is necessary to Stop
data collection to set the interval.
Clear Clears the window and restarts the graphing.
Save Saves an image of the graph and accompanying data in the location specified in
preferences (refer to Section 4.6.7). The user will also be asked whether they want to
send the file and data via email. When saving the data, you can choose to Save All Data
or Customise the length of the data by entering a time between 5 minutes and 6 hours.
Only the data from the start of collection to that limit will be saved (although the plot
will still appear exactly as it does on the screen).
Set Interval While data collection is stopped, the user can specify the time intervals between
collections.
4.6.5 Download
Downloads logged data from the USB stick inside the analyser. All data logged by the analyser to the
USB stick over the period of time specified will be collected. Due to the slow connection speed of
Bluetooth, this should only be used for relatively short sections of data. Downloading 1 days worth
of 1 minute data is likely to take a couple of minutes.
Options Menu
Save Generates a filename based on the start and end date/time specified, saves the
downloaded data in the location specified in preferences, and then asks to send the saved
comma separated text file (.csv) as an attachment to an email. Note that this file format
does not include the parameter headings, just the values.
Send E-Mail Sends an email with the parameter data in the body of the email, formatted as displayed
(this includes the parameter name and the values).
Plot Graphs the data that has been downloaded. The user is prompted to select which
parameters to plot based on the parameters that were being logged. Refer to Figure 37
for an example.
Preferences Refer to Section 4.6.7
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Figure 37 Plot of downloaded data
Options Menu
Get Parameters Refreshes the parameter list display.
Save Generates a filename from the current date and time, saves the parameter data in the
location specified in preferences, and then asks to send the saved text file as an
attachment to an email.
Send E-Mail Sends an email with the parameter data in the body of the email, formatted as displayed.
Preferences Refer to Section 4.6.7
4.6.7 Preferences
The Preferences Menu allows the operator to adjust the directory settings, logged data format and
the colour scheme settings. It can be accessed through the Options Menu in most windows.
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Directory Settings
The operator can specify/select where to save the parameter lists, logged data and real-time plots.
Logs Format
When downloading logged data, the parameters can be displayed on one line or each parameter on
a separate line.
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Colour Theme Settings
Allows the operator to choose a colour scheme for the remote screen (Matrix, Classic, Emacs
or Custom).
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5. Calibration
These procedures describe how to calibrate the Span and Zero point for the analyser.
The following sections assume the instrument is in the Calibration Menu (refer to Section 3.5.10).
Zero calibrations are used to set the zero point of the analyser.
Note: This calibration is unnecessary and Ecotech recommends that the zero calibration only be used
when specifically required as it tends to mask issues that should be addressed during
maintenance/service.
A zero calibration can be performed through either the Calibration Port, Background Air Port or the
Sample Port. Follow the instructions below:
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Span calibrations calibrate the instrument to the upper limits of normal monitoring. Ecotech
recommends that 80% of the required measurement range should be sufficient for calibrations in
ambient monitoring situations (~ 40 ppm). A span calibration can be performed through either the
Calibration Port or Sample Port. Follow the relevant instructions below:
Calibration Port
1. Ensure a suitable span gas source is connected to the Calibration Port on the back panel of the
analyser (refer to Section 2.3.1).
2. Set the span source to a known concentration (80% of the required measurement range
recommended).
3. Enter the Main Menu Calibration Menu.
4. Set Cal. Mode to Span.
5. Let the instrument stabilise (15 minutes).
6. Enter the Quick Menu and select Span Calibrate.
(Also accessible through: Main MenuCalibration MenuSpan Calibrate).
7. A box will appear with editable numbers. Enter the concentration being delivered to the
instrument.
8. The instrument will perform a span calibration.
9. Enter Main Menu Calibration Menu and set Cal. Mode back to Measure
10. The instrument will return to normal activities.
Sample Port
1. Ensure suitable span gas source is connected to the Sample Port on the back panel of analyser
(refer to Section 2.3.1).
2. Set the span source to a known concentration (80% of the required measurement range
recommended).
3. Let the instrument stabilise (15 minutes).
4. Enter the Quick Menu and select Span Calibrate.
(Also accessible through: Main MenuCalibration MenuSpan Calibrate).
5. A box will appear with editable numbers. Enter the concentration being delivered to the
instrument.
6. Instrument will perform a span calibration, when finished the instrument will return to normal
activities.
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5.3 Multipoint Precision Check
The multipoint check involves supplying the instrument with span gas at multiple known
concentrations and recording the output of the instrument. Multipoint calibrations are used to
determine the linearity of the concentration readings over the range of the multipoint calibration.
The instrument gain should not be adjusted to each individual point.
1. Ensure a suitable span source is connected to the instrument from a gas calibrator (Ecotech
recommends the GasCal-1100) through the Calibration Port.
2. Record the analysers instrument gain before performing a calibration (refer to Section 3.5.10).
3. Perform a precision check using zero air as described in Section 5.4.
4. Perform a span calibration as described in Section 5.25.2.
5. Set up a program for measuring the span concentration through 5 steps down from 80% of
required measurement range.
6. Example for measurement range of 50ppm:
a. Set the 1st concentration on the gas calibrator to 40 ppm, allow the instrument to sample for
15 minutes, record the measurement.
b. Set the 2nd concentration on the gas calibrator to 30 ppm, allow the instrument to sample
for 15 minutes, record the measurement.
c. Set the 3rd point at a concentration of 0 ppm (zero air); allow the instrument to sample for
15 minutes and record the measurement.
d. Set the 4th concentration on the gas calibrator to 10 ppm, allow the instrument to sample for
15 minutes, record the measurement.
e. Set the 5th concentration on the gas calibrator to 20 ppm, allow the instrument to sample for
15 minutes, record the measurement.
7. The linearity and correlation can be calculated for each point manually or all points calculated
within an excel spread sheet. Both options are detailed below.
Manual Calculations
Record the concentration measurement at each point and determine the percentage difference
between instrument response and the supplied concentration using the following equation:
If the difference between values is less than 1% of full scale then the instrument is within
specifications. If not, a leak check and/or service are required (refer to Section 6).
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Microsoft Excel
Alternatively all the data can be placed in an excel spread sheet in columns next to the supplied
concentration.
1. Create an X Y scatter plot of expected calibration against instrument response. Right click on
either point and select Add Trend line. Tick the Display Equation on Chart and Display R-squared
Value on Chart.
2. The linear regression equation y = mx + b will be displayed.
A precision check is a Level 2 calibration. This means that the instrument has a known concentration
of span gas (or zero air) run through it and an observation of the instruments concentration is made
with no adjustment. A precision check can be performed either manually or automatically. If an
instrument fails a precision check (based on your local applicable standards), perform a span
calibration (refer to Section 5.2) or zero calibration (refer to Section 5.1) where appropriate.
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5.5 Pressure Calibration
The pressure calibration involves a two point calibration, one point under vacuum and the other
point at ambient pressure. To perform a pressure calibration the following steps must be completed.
Note: The vacuum calibration must be performed first when performing a full pressure calibration.
4. Connect vacuum source to Exhaust Port of analyser, switch vacuum source on.
5. Enter Calibration Menu Pressure Calibration and select Vacuum Set pt.
6. Ensure that the pressure reading on the external meter is stable. Now edit the Vacuum Set pt.
value to equal the pressure measured by the external meter.
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9. Disconnect the vacuum line from Exhaust Port and remove the external meter.
10. Reconnect the original tube to the top of measuring cell.
Full pressure calibrations are generally recommended, however it is possible to adjust only the
ambient point in cases where only a minor ambient pressure adjustment is required.
1. Ensure that any vacuum source connected to the Exhaust Port of the analyser has been switched
off and disconnected. Also disconnect any tubing connected to the Sample Port.
2. Obtain the current ambient pressure with a pressure meter.
3. Enter the Main Menu Calibration Menu Pressure CalibrationAmbient Set pt. (If
continuing from the vacuum pressure calibration this step is not necessary).
4. Edit the Ambient Set pt. value using the keypad to input the current ambient pressure (ensure
you are using the same pressure units that are shown on screen).
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Figure 46 Setting the ambient set point
1. Disconnect any external tubing connected to the rear of the analyser. Also ensure the analyser
has been powered up for at least two hours prior to this calibration.
2. Go to Main Menu Calibration Pressure Calibration.
3. Once the Pressure Calibration Menu is open, the valves will be set automatically to enable this
pressure calibration procedure.
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5. Connect a pressure meter (barometer) to top fitting of the optical bench (detector end). Ensure
you set or convert the pressure units as per the units set on the analyser.
6. The internal pump should automatically start running at full speed. Wait until the pressure
stabilises (about 5 minutes). Edit Vacuum Set Pt. by entering the pressure shown on the external
meter. Select Accept.
7. The pump should now stop automatically. Remove the external pressure sensor and wait a few
minutes. Adjust the ambient set point to the current ambient pressure and select Accept.
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Figure 52 Adjust ambient set pt.
8. Reconnect the original tube to the cell assembly. Also reconnect the ports on the rear of the
analyser (Sample, Calibration and Exhaust).
9. Exit the Pressure Calibration Menu and return to the Flow Calibration Menu.
10. Set the internal pump to Off.
11. Remove barometer from Sample Port.
12. Return to the Calibration Menu.
Instrument will prompt user Do you want to resume the flow control select NO.
13. Under the Pressure Calibration Menu select Ambient.
14. Allow 3 to 5 minutes for the pressure reading to stabilise to ambient (both barometer and
analyser).
15. Press EDIT and enter the measured reading from the barometer and press Accept.
16. Go to the Pressure & Flow Menu (Main Menu Analyser State) and compare the Ambient and
Cell pressures to each other. If they are within 5 TORR of each other pressure calibration was
fine, if they are > 5 TORR repeat pressure calibration procedure.
17. When completed return to the Flow Control field and set to Enabled.
18. Go to the Valve Menu and set Valve Sequencing to ON.
19. The procedure is now completed.
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Note: Make sure that the Flow Set point and the Cal. Point are both preset
to 1.00.
Note: Set fine pot to 253, then adjust coarse to be as close as possible to desired reading, then use
fine pot to make it exact.
14. Enter the reading from the flow meter into the Cal. Point field.
15. Set the Flow Control field to Enabled.
16. Go to the Valve Menu and set Valve Sequencing to ON.
17. (Main Menu Service Menu Diagnostics Valve Menu)
18. Leave for up to 5 minutes to return to normal operation. If instrument doesnt return to normal
there may be a blockage (Refer to Section 7.1).
19. Remove external meter and reconnect external tubbing to the rear of analyser.
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5.6 High Pressure Zero/Span Valve
If the analyser was ordered with this option, the internal pressurised calibration valves will already
be installed within the analyser as either a zero or span calibration source, thus no other internal
connections need to be made.
Note: This is NOT intended as a source for calibrating the instrument. This should only be used as an
operational check of the instruments zero point and single upscale point (recommended as 80% of
full scale).
1. Ensure the gas cylinder is fitted with an appropriate gas regulator with a shut off valve.
2. Connect a line of stainless steel tubing between the gas cylinder and the analysers Auxiliary Port
inlet.
3. Open the cylinder main valve and adjust the regulator to 15 psig or 1 bar.
4. Open the regulators shutoff valve and test for leakage.
5. Temporarily place a flow meter on the Calibration Port inlet (used as a span/zero gas vent during
this check).
6. Enter the Calibration Menu (Main Menu Calibration Menu).
7. Change Set Cal Port to External.
8. Select either Span or Zero under the Cal Mode option depending on which calibration check is
being performed. This will initiate the pressurised calibration.
9. Open the shutoff valve on the cylinder, and adjust the regulator pressure until the flow on the
vent line (Calibration Port) is between 0.5 and 1 lpm.
Note: Do not exceed a pressure of 2 bar, this can damage the analyser and cause gas leakage.
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1. Ensure the gas cylinder is fitted with an appropriate gas regulator with shut off valve.
2. Connect a line of stainless steel tubing between the appropriate gas cylinder and the analysers
Inlet Port.
3. Open the Main Valve and adjust the regulator to 15 psig or 1 bar.
4. Open the regulator shutoff valve and test for leaks.
5. Temporarily place a flow meter on the Auxiliary Out Port (used as a span/zero gas vent during
this check).
6. Change Set Cal Port to External (Main Menu Calibration Menu) then select zero under the Cal
Mode option this will initiate the pressurised zero calibration.
7. Open the shutoff valve on the zero-air cylinder; adjust the regulator pressure until the flow on
the vent line (Auxiliary Out Port) is between 0.5 and 1 lpm.
8. Change Set Cal Port to External (Main Menu Calibration Menu) then select span under the
Cal Mode option this will initiate the pressurised span calibration.
9. Open the shutoff valve on the span-gas cylinder; adjust the regulator pressure until the flow on
the vent line (Auxiliary Out Port) is between 0.5 and 1 lpm.
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Note: Do not exceed a pressure of 2 bar, this can damage the analyser and cause gas
leakage.
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6. Service
6.1 Pneumatic Diagram
To perform general maintenance on the Serinus 30 the user may require the following equipment:
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* Suggested intervals for maintenance procedure are a guide only and may vary with sampling
intensity and/or environmental conditions.
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Figure 58 Removing plunger
5. Remove the old filter, wipe down the plunger with a damp cloth and insert new filter.
6. Replace the plunger, screw the cap on and reconnect the pump.
7. Close the instrument and perform a leak check (refer to Section 6.4.4).
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2. Connect a pump to the shut off valve ensuring the shut off valve is in the open position, turn on
the pump.
3. Block the analysers Sample Calibration and BGnd Air Ports with a Swagelok blocker nut.
4. Switch on the analyser; navigate from the Main Menu Service Menu Diagnostics Valve
menu. Switch off the valve sequencing and close all valves.
5. Close the shut off valve and record the vacuum. Wait for 3 minutes and then observe the gauge
on the leak check jig. It should not drop more than 5 kpa. If it has then a leak is present within the
sample cycle of the instrument.
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6. Enter Main Menu Service Menu Diagnostics Valve menu. Then set Sample/Cal Open.
7. Turn on the pump, switch the shut off valve to the Open position and allow the pump to
evacuate the pneumatics.
Switch the shut off valve to the Closed position and turn off pump. Record the vacuum indicated
on the leak checking device. Wait 3 minutes then observe the gauge on the leak check device. It
should not drop more than 5 kpa. If it does then a leak is present within the zero cycle of the
instrument.
8. Enter Main Menu Service Menu Diagnostics Valve Menu. Then set Sample/Cal Open
and Internal Zero/Cal Open.
9. Turn on the pump, switch the shut off valve to the Open position and allow the pump to
evacuate the pneumatics.
10. Switch the shut off valve to the Closed position and turn off pump. Record the vacuum indicated
on the leak checking device. Wait 3 minutes then observe the gauge on the leak check device it
should not drop more than 5 kpa. If it has then a leak is present within the span calibration cycle
of the instrument.
11. If the instrument did not leak then skip to step number 15.
12. Inspect the instruments plumbing looking for obvious damage. Check the condition of fittings,
sample filter housing, O rings both in the filter assembly and in the cell assembly.
13. When the location of the leak has been determined, repair and then rerun the leak check
procedure.
14. Inspect the tubing again ensuring the tubing is cleanly connected to the fittings and that the
internal Teflon lining has not been kinked or crumpled.
15. Remove the leak check jig and Swagelok blocking nuts.
16. Re-enable valve sequencing from the Valve Menu.
1. Enter Main Menu Calibration Menu and change the Cal. Mode field to Zero and the Cal. Port
to Internal.
2. Allow the analyser to sample zero air from the zero air scrubber for approximately 5 minutes.
3. Record the front panel CO reading as the initial value.
Note: This value should be 0.00 0.1 ppm. If it is not, a background should be initiated by initiating
the background field within the Calibration menu. The background will take approximately 5 minutes
to complete.
4. Connect 40 ppm of span gas to the Background Air Port ensuring the inlet pressure is maintained
at ambient pressure.
5. Enter Main Menu Calibration Menu and change Cal. Mode field to Zero and the Cal. Port to
Internal.
6. Allow the analyser to sample the span gas for 10 minutes.
7. Record the indicated CO reading as the Challenge value.
8. Compare the CO initial value and the challenge value. They should agree within 2 ppm. If the
initial value is less positive than the challenge value, the CO-CO2 converter should be replaced.
9. Disconnect the span gas and set the Cal. Port to your normal setting. Verify that the analyser is
in the measure mode.
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6.4.7 Trim pot Tuning Procedure
The following must be performed to ensure the Serinus 30 receives an optimal signal after the cell
has been aligned. If this procedure is not performed, then the Serinus 30 is likely to produce
unstable results. If the Input pot reads less than 180 (refer to Section 3.5.16), this is an indication
that this procedure needs to be performed.
1. Ensure the laser and detector has been aligned to provide an optimum shaped response.
2. Disable the control loop.
3. Adjust the input pot to 190 in the diagnostic menu.
4. Adjust the trim pot on the detector board (on the side of the reaction cell) such that the
reference voltage reads 4.00 V 0.03 V.
5. Re-enable the control loop, reset the instrument.
6. Ensure that the Input pot reads 19010 after the analyser is out of start-up. If not, perform this
procedure again.
7. Perform a leak check (refer to Section 6.4.4).
Note: If the tubing shows signs of significant contamination, then it should be replaced with new
tubing. Do not clean the converter or the mirrors found within the cell.
During normal operation ensure that the pressure and flow menu indicate the following parameters.
Ambient should display the current ambient pressure at site. Cell should indicate current cell
pressure depending on the pump condition and location. The cell pressure is normally about 20 torr
below ambient.
To navigate to the pressure and flow menu: Enter Main Menu Analyser State Pressures and
Flow.
1. A simple way of checking the pressure sensors response is to disconnect the exhaust and sample
tubing from the back of the analyser. After 2-5 minutes observe the pressure readings: ambient
and cell. Ensure that they are reading the same 3 torr ( 0.4 kPa).
2. If the readings are outside this level then perform a pressure calibration (refer to Section 5.5).
3. If the calibration fails then the instrument may have a hardware fault. The cell pressure PCA has
test points. To determine if the pressure sensor is faulty simply measure the voltage on the test
points shown in the photos. The voltage measured across the test point is proportional to the
pressure measured by the sensor so if the sensor is exposed to ambient pressure at sea level
then the voltage will be around 4 volts but if the sensor is under vacuum then the voltage will be
low (e.g. 0.5 volts). If the test point measures zero of negative voltage then the assembly is most
likely faulty and will need to be replaced.
1. Turn off the instrument, open the lid and remove the 2 screws holding down the main controller
PCB.
2. Lift the PCB up to its open position. The battery (BT1) is located toward the front of the PCB.
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3. Using a small flat screwdriver, lift the metallic clip holding the battery whilst sliding the old
battery out.
4. Now place the new battery in with the positive (+) side facing up.
5. Close the main PCB and return the screws. Close the lid again.
6. Turn on the instrument and set the clock time and date in the General Settings Menu (refer to
Section 3.5.8).
Below is a list of the replaceable parts of the Serinus 30. Some of these parts will not need replacing
and other consumables will need constant replacing. See below for information on yearly
consumable kits available from Ecotech.
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Table 7 Serinus 30 Maintenance Kit
6.6 Bootloader
The Serinus Bootloader is the initial set of operations that the instruments microprocessor performs
when first powered up (similar to the BIOS found in a personal computer). This occurs every time the
instrument is powered up or during instrument resets. Once the instrument boots up it will
automatically load the instruments firmware. A service technician may need to enter the Bootloader
to perform advanced microprocessor functions as described below.
To do this, power up the instrument and immediately press the plus key multiple times until the
following screen appears.
If the analyser displays the normal start up screen then the power will need to be toggled and
another attempt will need to be made to enter the Bootloader screen. Once successful, press 1 to
enter the Bootloader Menu.
This command forces the following communication ports to output a string of characters: Serial Port
RS232 #1, USB rear, and Ethernet Port. The default baud rate is 38400 for the RS232 Serial Port. To
initiate the test press the number 2 key from the Bootloader screen.
http://www.ecotech.com/downloads/firmware
To update the firmware from a USB memory stick, use this procedure.
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4. Select option 3, (Upgrade from USB memory stick) press 3 on keypad.
5. Wait till upgrade has completed.
6. Press 9 to start the analyser with new firmware.
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7. Troubleshooting
Before troubleshooting any specific issues, Ecotech recommends ensuring the analyser has
successfully completed its start-up routine, and then resolving all issues listed in the instrument
status menu (refer to Section 3.3).
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Error Message/Problem Cause Solution
No response to span gas Leaks/blockages Leak or blockages in tubes or valves. Perform leak
check and flow check and repair any
leaks/blockages.
Faulty calibration source Ensure calibration gas is plumbed correctly, is not
contaminated, has no leaks and is a NATA/NIST
reference gas.
Hardware fault Faulty measurement cell.
Correlation wheel leaking Replace correlation wheel.
Zero drift No flow Check sample flow.
Faulty zero air Ensure zero air source is not overly polluted.
Leak Perform leak test.
CO-CO2 converter faulty Replace CO-CO2 converter.
A/D conversion error Temperature/pressure Replace main PCB.
error
Negative zero Indicates that the internal Check the internal zero air supply is equipped with a
zero air is less efficient functioning CO removing device.
than the external zero
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7.2 Noisy/Unstable Readings
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7.4 Mirror Temperature Failure
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8. Optional Extras
8.1 Dual Sample Filter PN E020100
The dual filter is designed with two sample filters plumbed in parallel with a split line. This formation
allows sample flow not to be affected, yet reduces the loading on each filter, and therefore the
frequency with which they will need to be changed.
The dual filter option is shown in the pneumatic diagram (dashed line) and requires no operational
changes to the instrument.
The rack mount kit is necessary for installing the Serinus into a 19 rack (the Serinus is 4RU in height).
Included Items
1 Rack Slide Set H010112
4 Rack Mount Adaptors H010133
2 Rack Mount Ears H010134
4 Spacers HAR-8700
8 M6 x 20 Button Head Screws
16 M6 Washers
8 M6 Nyloc Nuts
14 M4 x 10 Button Head Screws
8 M4 Washers
8 M4 Nyloc Nuts
4 M4 x 10 Phillips Pan Head Screws
8 M6 Cage Nuts
3. Attach the inner slide rails to each side of the analyser using M4 x 10 button screws - three each
side. Make sure you use the vertical slotted holes and push the slide firmly downwards so that
the screws sit at the top of the slot. This ensures that any protrusions under the base of the
analyser do not hit any blanking panels which may be fitted (refer to Figure 71).
4. Attach the rack mount adaptors to the ends of the outer slide rails using M4 x 10 button screws,
washers and locknuts. Do not fully tighten at this stage as minor adjustments may be required to
suit the length of the rack (refer to Figure 72).
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Figure 72 Attach rack mount adaptors to outer slides
5. Install the two assembled outer slide rails onto the left and right side of the rack securely with
M6 bolts, washer and locknuts (refer to Figure 74).
6. Use a spacer (or cage nut) to space the rear claw from the side of the rack and a washer and
locknut to secure it (refer to Figure 75).
7. Install rack mount ears on the front of the instrument using two M4 x 10 screws on each side
(refer to Figure 76).
8. Now carefully insert the instrument into the rack by fitting the instrument slides into the
mounted rails. Ensuring that the rack slide locks engage on each side (you will hear a click from
both sides).
Note: Ensure both sides of the inner slide are attached to the outer slides before pushing into the
rack fully.
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9. Push the analyser fully in. At this point, make sure that the analyser slides reach and locate in to
the plastic catches at the rear end of the outer slides. Adjust the outer slides as required until this
is achieved. Remove analyser and now tighten the M4 screws and nuts that secure the front and
rear claws on both sides of the rack.
To Remove the Instrument
1. To remove the instrument first pull instrument forward of rack giving access to the slides.
2. Find the rack slide lock labelled Push and push it in whilst sliding the instrument out of the rack,
complete this for both sides while carefully removing instrument.
The internal pump requires a separate flow calibration procedure. The flow calibration detailed in
section 5.5.1 must be performed after any exchanges/changes to fittings or filters.
Note: This is NOT intended as a source for calibrating the instrument. This should only be used as an
operational check of the instruments zero point and single upscale point (recommended as 80% of
full scale).
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Appendix A. Advanced Protocol Parameter List
Note: Parameters are for all Serinus series analysers and may not be applicable to an individual
analyser.
# Description Notes
0 Sample / Cal Valve 0=Sample, 1=Cal/Zero
1 Cal / Zero Valve 0=Zero, 1=Cal
2 Internal Span Valve 0=Closed, 1=Open
3 Spare Valve 1 0=Closed, 1=Open
4 Spare Valve 2 0=Closed, 1=Open
5 Spare Valve 3 0=Closed, 1=Open
6 Spare Valve 4 0=Closed, 1=Open
7 NOX Measure Valve 0=NO, 1=NOX
8 NOX Bypass Valve 0=NO, 1=NOX
9 NOX Background Valve 0=Closed, 1=Open
10 Valve Sequencing 0=Off, 1=On
11 LCD Contrast Pot 0=Lightest, 255=Darkest
12 SO2 Reference Zero Gain Pot S50 reference zero pot
13 CO Measure Gain Pot S30 measure gain adjust
14 CO Reference Gain Pot
15 CO Test Measure Pot See 149. Exists
16 PMT High Voltage Pot High voltage controller pot for PMT S50 & S40
17 SO2 Lamp Adj Pot S50 lamp adjust pot
18 O3 Lamp Adj Pot S10 lamp adjust pot
19 O3 Zero Measure Pot: Coarse S10 signal zero (coarse)
20 O3 Zero Measure Pot: Fine S10 signal zero (fine)
21 PMT Fan Pot PMT fan speed controller pot
22 Rear Fan Pot Chassis fan speed control pot
23 Pump Speed Motor Driver Pot: Fine Internal pump speed fine pot
24 Pump Speed Motor Driver Pot: Coarse Internal pump speed coarse pot
25 Analogue Input 0 SO2 reference signal
26 Analogue Input 1 CO reference signal
27 Analogue Input 2 O3 reference signal
28 Analogue Input 3 SO2 & O3 lamp current
# Description Notes
29 Analogue Input 4 Flow block pressure
30 Analogue Input 5 Cell pressure
31 Analogue Input 6 Ambient pressure
32 Analogue Input 7 Raw ADC calibration input
33 Analogue Input 8 MFC1 not used
34 Analogue Input 9 Concentration data
35 Analogue Input 10 MFC2 not used
36 Analogue Input 11 MFC3 not used
37 Analogue Input 12 External analog input 0
38 Analogue Input 13 External analog input 1
39 Analogue Input 14 External analog input 1
40 Analogue Input 15 MFC0 not used
41 CO Measure Pot : Coarse S30 measure zero coarse adjustment pot
42 CO Measure Pot: Fine S30 measure zero fine adjustment pot
43 SO2 Measure Signal Gain Pot SO2 measure signal gain pot
44 SO2 Reference Gain Pot SO2 reference signal gain pot
45 SO2 Signal Zero SO2 measure zero pot
46 O3 Signal Gain Pot O3 input signal gain pot
47 Test Pot Test pot for all the analysers
48 NOX signal gain pot PMT signal input gain control for NOX
49 PGA Gain 1, 2, 4, 8, 16, 32, 64, 128
50 Primary Gas Concentration Current value on front screen
51 Secondary Gas Concentration Current value on front screen (if applicable e.g. NOx)
52 Calculated Gas Concentration Gas 3 (e.g. NO2)
53 Primary Gas Average Average of the readings(for Gas1) of the last n minutes
where n is the averaging period
54 Secondary Gas Average
55 Calculated Gas Average
56 Instrument Gain
57 Main Gas ID
58 Aux Gas ID
59 Decimal Places 2-5
60 Noise
61 Gas 1 Offset
62 Gas 3 Offset
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# Description Notes
63 Flow Temperature
64 Lamp Current
65 Digital Supply Voltage Digital supply voltage (should always read close to 5
volts)
66 Concentration Voltage
67 PMT High Voltage High voltage reading for PMT
68 Ozonator Status 0=Off, 1=On
69 Control Loop
70 Diagnostic Mode
71 Gas Flow
72 Gas Pressure
73 Ambient Pressure
74 12V Supply Voltage The 12 volt power supply voltage
75 Cell Temperature
76 Converter Temperature
77 Chassis Temperature
78 Manifold Temperature
79 Cooler Temperature
80 Mirror Temperature
81 Lamp Temperature
82 O) Lamp Temperature
83 Instrument Status
84 Reference Voltage
85 Calibration State 0 = MEASURE
1 = CYCLE
2 = ZERO
3 = SPAN
86 Primary Raw Concentration (Before NOx background and gain)
87 Secondary Raw Concentration (Before NOx background and gain)
88 NOx Background Concentration (Before gain)
89 Calibration Pressure
90 Converter Efficiency
91 Multidrop Baud Rate
92 Analog Range Gas 1
93 Analog Range Gas 2
94 Analog Range Gas 3
# Description Notes
95 Output Type Gas 1 1=Voltage
0=Current
96 Output Type Gas 2 1=Voltage
0=Current
97 Output Type Gas 3 1=Voltage
0=Current
98 Voltage Offset /Current Range Gas1 0=0% or 0-20mA
1=5% or 2-20mA
2=10% or 4-20mA
99 Voltage Offset /Current Range Gas2 0=0% or 0-20mA
1=5% or 2-20mA
2=10% or 4-20mA
100 Voltage Offset /Current Range Gas3 0=0% or 0-20mA
1=5% or 2-20mA
2=10% or 4-20mA
101 Full Scale Gas 1 5.0 Volt calibration value for analog output 1
102 Full Scale Gas 2 5.0 Volt calibration value for analog output 2
103 Full Scale Gas 3 5.0 Volt calibration value for Analog output 3
104 Zero Adjust Gas 1 0.5 Volt calibration value for analog output 1
105 Zero Adjust Gas 2 0.5 Volt calibration value for analog output 2
106 Zero Adjust Gas 3 0.5 Volt calibration value for analog output 3
107 Negative 10V Supply
108 N/A Unsupported
109 N/A Unsupported
110 Instrument State
111 CO Linearisation Factor A
112 CO Linearisation Factor B
113 CO Linearisation Factor C
114 CO Linearisation Factor D
115 CO Linearisation Factor E
116 Instrument Units 0= PPM
1=PPB
2=PPT
3=mG/M
4=G/M
5=nG/M
117 Background Measure Time In seconds
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# Description Notes
118 Sample Fill Time In seconds
119 Sample Measure Time In seconds
120 Aux Measure Time In seconds
121 Aux Sample Fill Time In seconds
122 Background Fill Time In seconds
123 Zero Fill Time In seconds
124 Zero Measure Time In seconds
125 Span Fill Time In seconds
126 Span Measure Time In seconds
127 Span Purge Time In seconds
128 Background Pause Time In seconds
129 Background Interleave Factor In seconds
130 Calibration Pressure 2
131 Aux Instrument Gain
132 Background Voltage
133 Aux Background Voltage
134 O3 Generator Output PPM
135 O3 Generator On/Off
136 Calibration Point 1 PPM
137 Calibration Point 2 PPM
138 Calibration Point 3 PPM
139 Calibration Point 4 PPM
140 Calibration Point 5 PPM
141 Desired Pump Flow SLPM
142 Actual Pump Flow SLPM
143 Set Lamp Current %
144 Lamp Current mA
145 Cycle Time Minutes
146 CO Cooler Pot CO cooler voltage adjustment pot
147 CO Source Pot CO source voltage adjustment pot
148 CO Measure Test Pot 0 CO measure test pot
149 CO Reference Test Pot 1 CO reference test pot
150 O3 Ref Average S10 background average
151 PTF Gain 0 Pressure temperature flow compensation factor for first
gas
# Description Notes
152 PTF Gain 1 Pressure temperature flow compensation factor for
second gas in dual gas analysers
153 Inst. Cell Pressure Instantaneous cell pressure
154 Manifold Pressure Valve manifold pressure
155 Cell Gas 1 Pressure Cell pressure for gas 1
156 Cell Gas 2 Pressure Cell pressure for gas 2
157 Cell Bgnd Pressure Cell pressure when in background
158 Reserved
159 Reserved
160 Reserved
o
161 Temperature Units 0 = " C"
o
1 = " F"
o
2 = " K"
162 Pressure Units 0 = "torr"
1 = "psi"
2 = "mbar"
3 = "atm"
4 = "kPa"
163 Averaging Period 0 = " 1 min"
1 = " 3 mins"
2 = " 5 mins"
3 = "10 mins"
4 = "15 mins"
5 = "30 mins"
6 = "1 hr"
7 = "4 hrs"
8 = "8 hrs"
9 = "12 hrs"
10 = "24 hrs"
164 Filter Type No filter = 0,
Kalman filter = 1
10 sec filter = 2
30 sec filter = 3
60 sec filter = 4
90 sec filter = 5
300 sec filter = 6
Adaptive filter =7
165 NO2 Filter 0 = Disabled, 1 = Enabled
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# Description Notes
166 Background Interval 0 = "24 hrs"
1 = "12 hrs"
2 = "8 hrs"
3 = "6 hrs"
4 = "4 hrs"
5 = "2 hrs"
6 = "Disable"
167 Service Baud 0 = "1200 bps"
1 = "2400 bps"
2 = "4800 bps "
3 = "9600 bps"
4 = "14400 bps"
5 = "19200 bps"
6 = "38400 bps"
168 Multidrop Baud 0 = "1200 bps"
1 = "2400 bps"
2 = "4800 bps
3 = "9600 bps"
4 = "14400 bps"
5 = "19200 bps"
6 = "38400 bps"
169 Service Port (COM 1) Protocol 0 = "EC9800"
1 = "Bavarian"
2 = "Advanced"
170 Multidrop Port (COM 2) Protocol 0 = "EC9800"
1 = "Bavarian"
2 = "Advanced"
171 Gas1 Over Range The upper concentration range when over-ranging is
enabled for analog output 1
172 Gas2 Over Range The upper concentration range when over-ranging is
enabled for analog output 2
173 Gas3 Over Range The upper concentration range when over-ranging is
enabled for analog output 3
174 Gas1 Over Ranging 0 = over ranging disabled
1 = over ranging enabled (gas1)
175 Gas2 Over Ranging 0 = over ranging disabled
1 = over ranging enabled (gas2)
176 Gas3 Over Ranging 0 = over ranging disabled
1 = over ranging enabled (gas3)
177 Heater Set Point Cell heater set point
# Description Notes
178 PMT HV Ctrl Pot PMT high voltage controller pot
179 PMT Test Led Pot PMT test LED intensity controller pot
180 Last Power Failure Time Time stamp of the Last power fail (4 byte time stamp)
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# Description Notes
205 Traffic Light 0=illegal value
1=Green
2=Amber
3=Flashing Red
206 Network Protocol
207 Gas 4 Offset
208 IZS Pot
209 IZS Pot Setting
210 IZS Lamp Current
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Appendix B. EC9800 Protocol
The following commands are supported.
DCONC
Function: Sends the current instantaneous concentration data to the serial port.
Format: DCONC,{<DEVICE I.D.>}{TERMINATOR}
Device response: {GAS}<SPACE>{STATUS WORD}<CR><LF>
All numbers are in floating point format. The STATUS WORD indicates the instrument status in hex
using the following format:
DSPAN
Function: Commands the unit under test to enter the span mode and stay there.
Format: DSPAN,{<DEVICE I.D.>}{TERMINATOR}
Device response: <ACK> if the unit under test is able to perform the command, <NAK> if
not.
DZERO
Function: Commands the unit under test to enter the zero mode and stay there.
Format: DZERO,{<DEVICE I.D.>}{TERMINATOR}
Device response: <ACK> if the unit under test is able to perform the command, <NAK> if
not.
ABORT
Function: Commands the addressed device to abort the current mode and return
to the measure mode.
Format: ABORT,{<DEVICE I.D.>}{TERMINATOR}
Device response: <ACK> if the unit under test is able to perform the command, <NAK> if
not.
RESET
Function: Reboots the instrument (software reset).
Format: RESET, {<DEVICE I.D.>}{TERMINATOR}
Device response: <ACK>
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Appendix C. Bavarian Protocol
All Bavarian Network commands follow the command format as specified in this section.
Where:
Examples
The following is an example of a valid Bavarian data request for an instrument that has an ID of 97:
<STX>DA097<EXT>3A
The binary value 0011 1010 corresponds to the hex value 3A. This value in ASCII forms the last two
characters of the data request message. Please note that the I.D. of 97 is sent as the sequence 097.
All I.D. strings must have 3 digits and the user should always pad with ASCII zero characters.
This is an example of a valid command to put the unit in the manual span mode if the instrument has
an ID of 843:
<STX>ST843 K<ETX>52
The block check operation is best shown with the following table:
The binary block check value is 0101 0010 which is the hex value 52 as shown at the end of the
command string.
Supported Commands
The command set supported by the Bavarian protocol is:
Command Effect
DA<id> Returns gas concentration
DA Returns gas concentration w/o ID
ST<id> M Enter Measure mode
ST<id> N Enter Zero mode
ST<id> K Enter Span mode
ST<id> S Force a background check
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DA
Return the current instantaneous concentration.
Format:
<STX>{DA}{<kkk>}<ETX>< bcc1><bcc2>
Or:
<STX>{DA}<ETX>< bcc1><bcc2>
Where:
<STX>{MD}{01}<SP><kkk><SP><+nnnn+ee><SP><ss><SP><ff><{000}><SP>{00000000}
<SP><ETC>< bcc1><bcc2>
<STX>{MD}{02}<SP><kkk><SP><+nnnn+ee><SP><ss><SP><ff><SP>{00000000}
<SP><mmm><SP><+pppp+ee><SP><ss><SP><ff><SP>{00000000}
<SP><ETC><bcc1><bcc2>
Where:
kkk = Devices multi-drop ID. If the DA command is issued without an ID, then the response omits this
field. Exception: the S40 family always includes both ID fields, even when a DA command without an
ID is issued.
+nnnn+ee = Main instantaneous gas concentration (for S40 family, this is NO)
ss = status byte with the following bit map:
ff = failure byte for both channels with the following bit map (positive logic):
mmm = NO instrument ID
+pppp+ee = NOx gas concentration (unless the NO2 option was selected in the Serial
Communications Menu, in which case it is NO2)
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ST
Set the instrument mode.
Format:
<STX>{ST}{< kkk>}<SP>{command}<ETC><bcc1><bcc2>
Where:
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Appendix D. Modbus Protocol
The Serinus supports a limited Modbus implementation.
The only function codes supported are 3 (Read holding register) and 16 (Write multiple registers).
Read requests specify which Advanced Protocol IEEE value they want to read as the starting
reference. Refer the appendix on the Advanced Protocol to see what values are available and what
index to specify for them. The Modbus index is calculated from the Advanced Protocol index via the
following formula:
Note: You must read an even number of registers because the return data is always 4 bytes
(a float).
The Serinus expects 8 data bits, 1 stop bit, and no parity. The baud rate is specified by the Serial
Communications Menu.
The value will be returned as a big-endian 32-bit IEEE floating point value.
Only 2 registers may be written at a time; that is, a single IEEE value. Currently the only supported
value is 85, to put the instrument into span (3), zero (2), cycle (1), or measure (0) mode.
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