Modern Moonshine Techniques Bill Owens
Modern Moonshine Techniques Bill Owens
Modern Moonshine Techniques Bill Owens
MOONSHINE
TECHNIQUES
34 illustrations
4 flow charts
2009
All rights reserved
Bill Owens
White Mule Press
Box 577
Hayward, CA 94541
ISBN 978-0-9824055-3-6
www.distilling.com
www.moonshineform.com
Congeners Impurities. These minor chemicals give liquor (spirits) distinctive character
and flavors. They are found in both heads and tails. May be considered desireable or
undesireable depending on quantity and type.
Cuts The process of separating different types of alcohol through the foreshots, heads,
hearts and tails cuts made during the final distillation run.
Density Meter Portable device that measures specific gravity, thus allowing the distiller
to make precise cuts.
Dephlegmator A small pre-condenser that sends distillate back to the pot. This process
increases the reflux and the purity of the spirit.
Dextrose Basic sugar also known as corn sugar. An optional base for distilling
moonshine.
DME Dried malt extract. When dissolved in water and fermented, can be distilled.
DSP A federally licensed distillery, known as a Distilled Spirits Plant.
Esters Fermented byproducts made by yeast action that contributes fruity characteristics,
aroma, and flavor to the wash.
Enzymes Proteins that assist conversion of starches into sugars that will ferment.
False Bottom In a mash tun the false bottom is a slotted copper pipe, the slots of
which allow wash to drain while holding back the grain.
Final gravity the density of the was after fermentation. Knowing the original and final
gravity of a wash allows you to determine the percentage of alcohol of the wash.
Flocculation The clumping and settling of yeast out of solution, forming a cake-like
substance in the bottom of the tank or tub.
Foreshots A small amount of low boiling distillate containing acetone, methanol, and
aldehyde volatiles. Catch and discard.
Fusel Oil A bitter oil found in tails. A liquid composed of amy and burly alcohols.
Heads Spirits from the beginning of the run that contain a high percentage of low boiling
alcohols such as aldehydes.
Infrared Thermometer Gun Instant reading thermometer device.
Low Wines The spirits collected from the first distillation.
Mash A mixture of ground malted grains and hot water.
Malt Sprouted dried grains. Malted grains contain enzymes that convert starches into
fermentable sugars.
Mash Tun A double-jacketed tank with a false bottom in which hot water and grains are
mixed.
NGS Neutral Grain Spirits (190+ proof alcohol). Most often produced from corn. Used
by distilling companies around the world for blending to produce vodka, gin and whiskey.
It is the workhorse of the commerical distillation industry.
Original gravity The density of the wash before fermentation.
Packing Copper mesh or copper Ts used in a stills column to increase the surface
area and thus the reflux and quality of the alcohol.
Parrot A device resembling a stylized bird that attaches to the still and floats the
hydrometer.
Proof A measurement of alcohols strength: In the US, proof is twice alcohol content at
60F. (i.e., 120 proof is 60% abv).
Pitch The process of adding yeast to the wash.
Plates: (or tray) Located horizontally at intervals in a column, often contain bubble caps
that enrich the reflux
Reflux Formed when vapors condense and re-vaporize in the column of a still.
Slop, Hot Hot, stinky, spent corn mash from the still.
Sparging At end of mashing, a process in which hot water is sprayed on, or run through,
the grain bed to extract additional sweet barley water.
Spirit Still A still designed to do the final distillation, producing finished whiskey.
Sweet Spot The head temperature between 174F and 180F. This range produces a
sweet tasting spirit and is considered the heart of the distillation run.
Stripping The process of running low abv wash through a still with no head or tail cuts
to remove alcohol that will be re-distilled.
TTB Alcohol and Tobacco Tax and Trade Bureau, formerly BATF.
Tails A distillate containing a high percentage of fusel oil and little alcohol.
Tub A 55-gallon plastic or stainless steel barrel used as a fermentation vessel.
Wash Fermented substrate containing alcohol.
Water Temperature Controller Device that allows cool water to flow through a
copper coil, controlling excess heat in a fermentation.
Introduction
Whiskey is simply distilled beer
To learn how to make whiskey you first have to brew beer. Go to amazon.com and
search brewing and you will find numerous books on this subject. The easy way,
however, is to take a home brewing class offered at most home brew shops. These shops
also sell brewing kits, malt extracts, dried malt extract (DME), malted barley, wheat, rye,
and flaked corn.
The next generation of distillers is going to come from the craft brewing industry since
they know the complex flavors found in barley make great beer and will make great
whiskey.
Modern Moonshine Techniques has three sections: First is how to use sugar to distill a
moonshine. Second, how to build an inexpensive corn cooker and make corn whiskey.
Finally, and most importantly, this book, with text and illustrations, shows how to build a
mash tun to create a grain whiskey wash. And, then instructions to distill that wash into
whiskey.
Finally, get your DSP from the TTB, your State (ABC) license and open an artisan
distillery. Then distill the grain whiskey here and put it into a barrel. It will, in a matter of
months, pick up flavor and color as it matures. And, if you leave your whiskey in a
charred oak barrel for two years, it becomes straight Bourbon whiskey. Craft distilleries
often drop the word straight and age their whiskey for less than one year.
Bill Owens
White Mule Press
Hayward, CA
USA
Chapter 1
Moonshine The Legend and the Law
Where the English went, they built a house; where the
Germans went, they built a barn; where the Scots-Irish
went, they built a whiskey still.
An old Appalachian proverb
With the rise of artisan distillation in the US, most producers have decided to focus on
typical spirits such as vodka, gin and rum, or more specialized spirits such as eau de vie or
malt whiskey. A few other distillers, however, are choosing to trade on a bit of legendary
history and produce moonshine.
The term moonshine was first used in Britain where it referred to employment or other
activities that took place late at night. In the US, however, it has always been associated
with illegal liquor that has been known under colloquial names such as white lightning,
popskull, corn liquor, rotgut, panthers breath, or, more simply, shine.
The practice of moonshining is inextricably tied to US history in numerous ways. After
the American Revolution the United States was strapped financially due to fighting a long
war. In an attempt to address this problem, a federal tax was levied on spirits. This did not
sit well with the newly liberated people who had just concluded a war to eliminate British
taxation. This gave rise to the practice of making distilled spirits clandestinely to
circumvent taxation.
Early on, this practice was a method of survival, not extra profit. If farmers experienced
a bad crop year, they could use their corn for making whiskey. Because this was a practice
of subsistence, the payment of tax on this product might mean they would be unable to
feed their families. Thus began the contentious relationship with federal agents who often
were attacked when they tried to collect the tax.
In 1794, things finally came to a head with the Whiskey Rebellion. A group of several
hundred managed to overtake the city of Pittsburgh, Pennsylvania. In reaction, George
Washington dispatched 13,000 militiamen to take back the city and jail the leaders. This
incident served as the first major test of authority for the fledgling federal government.
The battles between the US Congress and moonshiners continued to rage on. In the
1860s the government attempted to collect more excise taxes to fund the Civil War. In
response, a number of elements, including Ku Klux Klansmen, joined the moonshiners in
an attempt to fight back. The new alliances led to more brutality and incidents of
intimidation of local people who might reveal stills, and revenue of agents and their
families.
The Temperance movement then added these happenings to their arsenal on the march
towards prohibition.The states began to prohibit the sales of alcohol in the early 1900s,
and then complete national prohibition was established in 1920. Prohibitions enactment
provided the best possible scenario for moonshiners. With no legal means of obtaining
alcohol, demand grew exponentially with which the moonshiners could not keep up. In
response, the producers began using cheaper ingredients such as sugar and even watering
down their whiskey.
A large network of distribution was established with the assistance of organized crime.
To supply the illegal spirits to this network, young men in rural areas close to the still
operations delivered moonshine in highly modified, high performance cars. The
temptation was irresistible to these men, as the income they could make in a single night
was greater that a couple of months of honest work. What started as a transportation
method for moonshine gave birth to stock car racing which formalized into todays
NASCAR.
With the repeal of prohibition in 1933, the demand for moonshine declined rapidly,
returning the practice mostly back to areas concentrated in the Appalachian region of the
East Coast. Even today, there is illegal production of moonshine in these regions with
operations located in northern Georgia, western South and North Carolina and eastern
Tennessee. Due to the independent and strong willed character shared by most Americans,
most historians feel that moonshine will always be around in one form or another.
Today there are a few who have decided to produce moonshine legally. Not surprisingly,
these individuals are located in the same regions of the East Coast where the illegal
version is still made.
Q&A MOONSHINE:
THE EASY WAY FROM SUGAR
1. Moonshiners add sugar to moonshine because:
[a] It greatly increases the volume of the moonshine.
[b] Is an extremely cheap way to make moonshine.
[c] Fermenting and distilling sugar did not take a lot of skill on
the part of the distiller.
[d] None of the above.
[e] All of the above.
Chapter 5
How to Distill Moonshine From Sugar
YOU WILL NEED
Infrared thermometer gun (www.Amazon.com)
Wooden paddle (canoe or home made)
Three 55-gallon food grade drums (www.baylesscontainers.com)
Sump pump and 1 hoses (Home Depot)
3/4-inch soft copper tubing (local plumbing supply store)
Hydrometers & alcoholmeter (home brew stores)
Glass carboys, stainless steel collection pails, or stock pot
FERMENTATION
Mix 50 lbs. of sugar into 40 gallons of water.
Predict your original gravity (O.G.) from corn sugar. 1 lb. of corn sugar in 1 gallon of
water will give you a O.G. of 1.039. Take 50 lbs. of sugar and mix it into 40 gallons of
water. (50x39/40=48.75). Round up to 1.049. It will ferment out to 1.000 giving you 6%
abv. sugar wash. Single pass on a pot still will yield about 8 gallons of 30% abv alcohol
spirit.
The Process
Use a sump pump or bail to transfer the wash into the still, leaving behind as much
sediment as possible. Turn on the burner to the still and relax as it will take about 30-45
minutes to bring the wash up to temperature. Pure alcohol boils at 173F, but a 10 to 14%
abv wash will boil at a much higher temperaturea little over 190F. Most kettles dont
have a thermometer to monitor wash temperature, only vapor temperature at the still head.
This is unfortunate because the still head may not heat quickly, and many a boil-over has
happened because the operator did not listen to the sound of the kettle. The sizzle can be
heard before full boiling occurs, though it may be difficult to hear over the roar of the
burner. Turn the burner down to listen, then back up.
Watch the thermometer on the head of the still. When the needle hits 160F, turn down
the heat and turn on the water to the condenser. The still will recover, the temperature will
rise, and after a few minutes the distillate will start to spit and sputter as it comes out of
the condenser. Have the collection pail (jar) or pot ready. The first sputters from the still
are the foreshots. Cut about 1/2 cup and use it as solvent to clean auto parts.
At 174F the sputter of distillate from the condenser turns into a small stream. As the
still runs, record the distillate temperature, percent of alcohol and time since starting.
Collect the distillate in small jars as you learn. Smell and taste whats coming out of the
still as the temperature rises. By collecting in small jars, any mistake will not ruin a large
quantity of spirit. You will be able to go back and re-sample the jars and get a time-series
understanding of what the still is doing. Once you decide where the hearts begin and end,
you can combine those jars into a larger container and discard or re-distill the rest. The
point is to go slowly and keep records. This avoids making the same mistakes twice, and
you will make mistakes.
A 40-gallon wash on a single pass through a simple pot still should yield 10 gallons of
hearts at 100 proof alcohol. Lets call it a spirit whiskey.
How fast the still flows will depend on several factors:
The amount of wash
The amount of alcohol in the wash
The amount of heat that is being applied to the still
Size of the condenser
Foreshots: Collect the first 1/2 cup of distillate. It smells awful. Discard. The amount of
foreshots depends upon the quality of the wash.
Heads: Between 175F to 195F. Often distillers collect a generous amount of foreshots,
skip the heads, and switch to hearts.
Hearts: Between 196F to 201F collect 13 gallons. The run starts at 80% abv and is
stopped at 20% abv. The 13 gallons should contain 50% abv.
Tails: Dont collect above 203F. Tails have undesirable oils and esters. Some argue
there is a lot of flavor (congeners) in the tails and try to get everything out of them. A
hydrometer will tell you how much alcohol is coming out of the still. Do not collect below
20% abv. (Many whiskey distillery stop at 40% abv. A hydrometer reading will tell you
when to cut.) Collect the tails in a separate container for a future run. At 20% abv in the
distillate, the kettle contains only about 1.5 percent remaining alcohol. You have to
determine whether your time and the cost of energy are worth the effort to recover this
small amount of alcohol.
[Notes on distilling: At the end of a run the alcohol coming from the still has dropped and
water is picked-up as the boiling point goes higher. A small pot still will have
temperature spikes in the head. These spikes create fruit and spice like vapors such as
anise and banana. You can taste and smell these flavors. Cut and toss them.]
Double Distillation
Fermentation: Go back to the fermentation process and make two more 40 gallon
fermentations. You now have 120 gallons of 14% abv wash for stripping.
Stripping: Using the 120 gallons of wash make three fast stripping runs (dont make head
or tails cuts). From each run collect 15 gallons of 100 proof (3x15=45 gallons) in
preparation for the final spirits run or double distillation.
Double Distillation: Into the still add the 45 gallons of 100 proof from the stripping run
for the final distillation (where heads and tails will be cut). The final spirit run should
yield 15 gallons of 140 proof. Adjust with distilled or RO water to 80 proof for bottling.
[Note: Many distillers add a generous amount of water to the second run, extending the
length of the run, making it easier to make more precise cuts.]
Barreling
Barrel age your spirit in a bonded shed or barn, as a wooden building gives a good
summer and winter temperature variations. It is the temperature changes that aid in the
maturation process. Finally, using good clean water, cut the whiskey to 40% abv or 80
proof. You could also consider using oak chips to give color and flavor to the whiskey,
though this may require disclosure on your label.
PROFIT FROM SUGAR WASH MOONSHINE
Its cheap to make and distill.
90 lbs. of sugar at Costco is $59, yeast $17, water, $5, and labor $30
Total cost or raw material is $111
Fermentation producing 40 gallons of wash containing 14 abv
The hearts run (yield) from the still will be 13 gallons of 50 abv
Now, add 3.25 gallons of water to the 50 abv, making it 16.25
gallons of 40% abv (80 proof) for bottling, making 5x16.25=81
bottles (750 ml)
$16/bottle x 81 bottles = $1,300 gross revenue. Bottles sell for $25 at retail.
Raw cost of ingredients (sugar and yeast) per bottle is $111/107 = $1.37
Bottle, label, cap, capsule, and carton will add $2.50, raw cost of about $3.90
$16 wholesale - $3.90 cost is $12.10 margin per bottle
Now pay CA and US excise taxes - $2.80 /16 =17.5 percent
(against wholesale)
The $12.10 margin $2.80 tax = $9.30 x 81 = $750 net from distilling a
sugar wash
Barrel Aging (increases profitability)
6 months, assume angel share of .25 gallons. A dry climate increases abv.
12 gallons of spirit @ 50.5 percent cut with 2 gallons of water to get 40 percent
alcohol producing 70 bottles.
Retail price of $35, wholesale of $23 minus bottle & tax of $6.30 = $16.70
$16.70 x 70 = $1,169 net from the distilling run
Other Considerations:
A whiskey distiller often runs into the late (tail) fraction with head temperature reaching
202F at the high end. When aging whiskey tails are sometimes added back as they
soften in the oak barrel. Adding tails to a clear moonshine or unaged whiskey is avoided
as they contain esters giving the drinker a headache.
Q&A HOW TO BUILD A CORN COOKER
1. The biggest reason why mashes fail is:
[a] Because the distiller put too much barley into the mash.
[b] Because the pH was not adjusted to about 6.0.
[c] Because the distiller did not mix in enough water to the mash.
2. Around 145F, barley enzymes will begin to convert corn starch in sugar.
[a] True
[b] False
3. After you have pitched the Turbo yeast into the corn mash, you should:
[a] Walk away and leave the mash alone.
[b] Oxygenate the mash by bubbling air through it with a large
aquarium pump.
[c] Add 20 lbs. of 2-row malted barley to the mash.
4. Assuming you intend to do a double distillation, you will end up with what
percentage of low wine after your first stripping run?
[a] 65% abv.
[b] 10% abv
[c] 25% abv
5. If you have a direct fire still, it is strongly advisable to:
[a] Get rid of it immediately
[b] Allow solids into the kettle, so that they will produce interesting
flavors like banana or anise.
[c] Strain or filter the wash so that the solids dont burn and produce
off-flavors.
6. Before you can legally operate a still, you must first:
[a] Obtain your federal DSP (Distilled Spirits Plant) permit, as well as
state licenses.
[b] Practice by making a few trial runs on your still before applying for
your permits.
[c] Operate your still at night under the light of the moon.
[d] Send the government a sample of the spirit you have produced.
Chapter 7
I See the Future and its Whiskey
There are 165 craft distilleries in the US, of which 32 produce whiskey. In the future this
segment of the distilling industry will grow quickly because a new generation of distillers
has adapted the micro-brewers technique of creating a wort/wash using a mash tun. This
system of separating the grain from the fermentable liquids creates a bright clean beer
wash without phenol-releasing husks and grains. This is the system of producing distillers
wash that is used by Irish and Scottish distillers.
The new generation of distillers is using malted barley, wheat and rye to create new
styles of whiskeys. They shy away from corn because corn mash requires a cooking
vessel. Pound for pound, corn produces a thinner wash with lesser flavor. And, extracting
sugars from corn requires adding malt for enzymatic action. Making corn whiskey is time
consuming.
Many whiskey distillers cook, cool and ferment in the same vessel. Then the wash is
pumped directly into the still. This means 1/3 of the wash (in the still) is made up of husks
and other undesirables. This cooked corn mash yields about 6% abv and has a potential for
off-flavors. It is important to note that the corn wash has to be quickly removed from the
still to avoid pig slop aromas in the distillery.
In contrast, a distillery utilizing a brewers mash tun with a false bottom doesnt have
this problem. The mash tun allows you to drain and cool the grains. Then they are
shoveled out into waiting barrels and hauled away expeditiously by a local farmer.
The whiskey distilling process is often done using two stills: a larger pot for stripping,
and a smaller spirits still for cutting head and tails. This style of distilling is also done in
the brandy and rum industry.
Finally, a whiskey distiller does not need a tall column still with numerous plates. It can
be done on a pot still (no plates) or a still equipped with a short column with one or two
plates and a dephegmator (pre-condenser).
Which is better? A pot still doing double distillation, or a column still with plates? Both
can produce 70% abv/140 proof whiskey for barreling. Column still distillation is faster
than pot distillation, and both yield excellent results. The system doesnt matter because
whiskey has the magicit has the buzz.
HOW IT WORKS
The Mash Tun: This system uses a 200-quart (50-gallon) camping cooler as a mash tun.
It has been fitted with a false bottom that drains the sweet barley water while holding back
the grains. A 50-gallon mash tun can hold 30 gallons of water and 125 lbs. of grain.
Sparging requires 20 gallons of hot water.
There is little difference in the production of a beer wort and a whiskey wash. Both are
created in the mash tun using the simple infusion method of Time and Temperature. The
difference in the process is what happens to sweet barley water after it leaves the mash
tun. For the distiller, the barley water goes straight into the fermentation tank where it is
cooled and fermented. After fermentation it
is called wash and is then distilled into whiskey. Brewery wort runs into a kettle where it is
boiled with the addition of hops. After boiling it is cooled and fermentedand called beer.
AUXILIARY EQUIPMENT
Commercial water heater (ebay.com)
Wash temperature controller (www.Grainger.com)
50 feet of 3/4 L- Soft copper pipe
(coiled into heat exchanger)
Count-down digital timer or iPhone app
Infrared thermometer gun
(www.Testequipmentdepot.com)
High temperature water pump www.Granger.com
item or ebay.com
Sump pump and hoses for pumping wash to still.
(www.grainer.com)
Wooden paddle (www.Amazon.com)
Three 55-gallon plastic drums (www.bayleccontainers.com)
One 55-gallon stainless steel drum (www.surpluscenter.com)
Anton-Parr density meter DMA 35N (Anton-Paar.com)
(Instant specific gravity and alcohol reading)
PROCEDURE: SEVEN STEPS TO CREATE WASH
1. Striking: Adjust the temperature gauge on the water heater to 172F or use the pot
still and heat water to 172F. Use a high temperature water hose and strike by
transferring 30 gallons of hot water from the water heater to the mash tun filling it about
full. This water is called the foundation.
Use the thermometer gun to check temperature of the foundation water. You will notice
the water temperature has dropped 10F to 160F.
Note, if you are using the still to heat the foundation water, you will have to pump it to the
mash tun. Do not bucket it! Pumping hot water is also dangerous. If it splashes on your
skin, you will get a serious burn! Use gloves and caution when handling the pump and
hoses.
2. Mash-In: Once the foundation water is in the mash-tun, work quickly and add the
grains. The grain floats, so use a paddle and mix them into the foundation water. This is
called mashing-in. Stir for one minute or until the mash is lump free. Close the lid to the
tun, holding in the heat.
Malted barely, when mixed with hot water, will release enzymes within minutes that
convert the starch water into sugar water. Use the thermometer gun to take the mash-in
temperature reading for the log book. Mashing-in will also create a temperature loss of 8-
10F. During the mashing-in process, you can expect a temperature loss of 25-30F. The
final temperature of the mash should be around 152F. A low 130F or high 160F mash-in
is not a problem. The yields (alcohol) from the wash will be lower. Dont worry about it,
just keep going. You wont get it right on the first try.
If you didnt mash-in a perfect 152F, remember that 2-row barley malt is loaded with
enzymes and even with wide temperature variations, it will produce enzymes that convert
the starch water to sugar water. Now take a spoon and dip out some of the wash and taste
it. I promise it will be sweet. Close the lid to the mash tun to prevent heat loss. Note, most
distillers mash in at 144F.
3. Starch Conversion: Set the count-down timer for 40 minutes and walk away.
During the 40 minutes, starch conversion will continue.
The mash tuns at micro-breweries hold 2,000-5,000 lbs. of barley. They need to steam-
heat the tun and use mechanical rakes to insure a good mash in. The rakes also push the
grains out of the tun when sparging has finished. Small brewers stir the mash by hand and
use a shovel to dig the grains out the tun.
During the starch conversion period, take the time to write down in the logbook what
happened during the mash-in process. This ensures that you dont make the same mistakes
twice, and you will make mistakes. This is not a science project. Its a brewing project.
4. Sparge Water: During starch conversion the water heater will have recovered and
you again have 170F water. This water will be used for rinsing the grains. If you dont
have a water heater, sparge water can be heated in the pot still. You will only need 15
gallons, so heating the water in the pot still will only take a few minutes.
Sparging is a balancing act. Open the valve on the false bottom and start collecting the
sweet barley water. Next add the 170F sparge water to the grain bed covered with water. It
can be sprayed.
The balancing act is to add as much water to the mash-tun as sweet water runs out of the
bottom.
After a few minutes the mash will begin to settle. Do not mix. Collect 45 gallons of
sweet barley water for fermention. After collecting for whiskey mash, keep on collecting
the sweet water from the mash tun. It contains sugars from which you can make a small
batch of beer.
I suggest a short sparge of 15-20 gallons because you want to make a high gravity
wash. The more you sparge, the more dilute the wash, giving you less fermentable sugar.
Our goal for whiskey wash is 9% abv. A hydrometer reading will give you the potential
alcohol for fermentation with a starting gravity of 10.80. Note: Micro-brewers who make
barley wine seldom sparge because they want a create a beer that is 12% abv.
It will take about 30 minutes of sparging to collect 45 gallons for a 40 gallon wash. As
10 gallons of wash will be lost in cooling fermentation and pumping.
Grains sparge differently, and corn is the most difficult to work with. Use rice hulls in
the mash to provide a pathway for the sparge water. I suggest your corn whiskey mashes
contain 20 percent malted barley and 10 percent rice hulls. The barley will ensure good
enzyme action and the rice hulls will create mash that is thin enough to allow the wash to
run.
5. Cooling: The 45 gallons of wash has been collected, pumped, or bucketed into the
fermentation tank. If possible build a 4-foot platform for the mash tun. This way, the wash
from the tun can flow directly into a fermentation tank and there is no need to collect or
pump it.
The wash coming into the fermentation tank will be over 100F. Use the infrared
temperature gun to check the temperature of the wash. As soon as
the wash starts running to the fermentation tank, insert the copper coil and
start cooling.
Pitch the yeast when the wash has cooled to 70F.
[Note, wineries use flat stainless steel plates to control temperature during fermentation.]
6. Fermentation. Before pitching the yeast, record the original gravity of the wash. A
125 lb. malted barely mash should produce a wash with an O.G. of 1.070. After
fermentation the F.G should be 10.10, yielding a wash of 9-10% abv. Again, keep notes so
that you can correct any mistakes on the next mash-in. No one gets it right the first time.
In 4 to 6 hours after pitching the yeast, tiny bubbles will appear in the wash. In a few
more hours, fermentation will be rolling and you will be able to see that the wash is
moving around. As the wash ferments, it will give off heat. Use the copper coil to hold the
fermentation temperature at 70-75F. A high-temperature fermentation will create esters in
the wash. During distillation, these esters will create off-flavored spirits.
Do not cover the tank with a tight lid. A barley wash fermentation is very active and the
foam will push the lid off the tank and onto the floor, making a mess to clean up.
Once fermentation has slowed, you can use a loose lid to cover the tank. Use your eyes
and watch fermentation. When the fermentation bubbles have stopped (5-7 days), a bright
clean wash can be pumped directly to the still for fermentation. Try to not carry over any
yeast into the still.
7. Clean-up: Leave the lid to the mash-tun open for a couple of hours allowing the
grain to cool. Leave the false bottom drain open so the grain bed drains.
Once the grain bed has cooled, use a small plastic or wooden shovel and dig it out.
Spent grain can be fed to pigs or cows. However, it needs to be cut with 90% commercial
animal feed. Cows have multi-chambered stomachs and the sugar in the grains will
ferment, bloating and killing the cows. I have heard of pigs getting drunk and killing each
other.
WASH TEMPERATURE
CONTROLLER
(Grainger.com)
Parts:
1. Solenoid Valve 2 way (#4A700)
2. Solenoid Valve Coil 120 (#A706)
3. Controller PM6C1EHAAAA
4. RTD probe that can be inserted in to the wash
(Items 3 & 4 at www.instrumart.com)
A copper coil equipped with the regulator will allow
water to flow through the coil and keep a fermenting at
wash at 72F. The coil is a must when doing a high
gravity sugar fermentation. Without it, heat (90 to
100F) from the fermentation kills the yeast and yields a
stuck fermentation. High temperature fermentations also
produce an off-flavored wash.
Several years ago I made some beer and tossed 30 lbs. of spent grain in the backyard.
One year later it is still there. Worms wont eat spent grain unless it is cut with green
material and composted. It is a lot of work to compost spent grain. If you dont have a
farmer to come get the spent grains put them in a bag send them to the dump. This isnt
very GREEN but spent grains are hard to recycle. You may to pay to get rid of them
Now, back to the clean-up. After digging out the grains, use a rubber glove to remove
the slotted false bottom pipes. They will still be hot, so rinse with cold water and
disassemble. No soap or chemicals are necessary, just wipe and air dry everything,
including the tun. You can also use heads from a distillation to clean the mash tun. Again
use gloves.
Total set-up time to create strike water, mash-in, sparging, pitch yeast, and clean up is
about 3 hours.
In about 72 hours, the wash fermentation should be about 70 percent completed. Use the
hydrometer to check. The yeast is now starting to flocculate and to settle on the bottom of
the tank. It will form a one-inch thick cake slurry and can be collected for the next
fermentation. With a final gravity of 1.010 the wash will be almost clear. At this point,
drop a sump pump into tank and pump the wash into the pot still. If youre careful, very
little yeast will be pumped over.
If you distill on a regular basis you can re-pitch the yeast for numerous batches. Always
refrigerate the yeast between fermentations. Yeast is a single-cell organism and it doesnt
keep for months without feeding it sugar or fresh wash. Yeast is also cheap. If you just
distill once a month, start with fresh yeast on each fermentation.
You are now ready to distill a single malt whiskey.
*The ingredients for Straight Bourbon Whiskey and Bourbon Whiskeys are exactly the same. (CRF rules). What is
different? Straight whiskeys have to be stored in charred new American oak barrels for two years.
30 oz. of yeast.
[Important Note: When distilling malt whiskey it is very important to add the anti-foam
agent Fermcap-S to the wash before distilling. This prevents the wash from foaming out
of the still, and ending up in the parrot or collection pail.]
POT DISTILLATION OF MALT WHISKEY
Fill the still with 100 gallons of 9% abv wash. Most pot stills are direct-fired by
propane, so heat the still slowly to avoid scorching the wash. It will take about 60 minutes
to heat the wash to 173F. At this temperature alcohol vapors start boiling off the wash and
rise up and into the head of the still and into the condenser. Watch the head thermometer
on the still and you will see it spike from 165 to 173F as spirits spit and sputter as they
come out of the condenser...turn down the burner andturn on the water to the
condenser. This action will slow the vapor buildup in the head of the still and the spitting
and sputtering will stop. Toss this stuff. It will take another 15 minutes for the vapors to
build back up and head temperature to reach 174F. Again, the tube from the condenser
will surge and spit a few times before becoming a small but steady stream running into a
pail. Collect and toss the first 4-6 ounces before attaching the collection tube to the parrot
with a hydrometer. For a quick reading use a density meter.
THE 100-GALLON RUN
Foreshots: At 174F foreshots represent less than 2% of the distillate. Foreshots smell
foul. Use them as a weed killer or to power your lawn mower.
Heads: At 175 to 190F collect about 3 gallons. The abv will drop from 80 to 70%. Use
a density meter or hydrometer and record the alcohol content, so you can duplicate the
cuts at a later date. Use your nose and taste buds to assist in deciding where to cut your
spirits.
Hearts: At 190 to 198F collect 15 gallons. The abv will drop from 70 to 50% and
average out to 65% abv (130 proof). Many whiskey distillers dont collect hearts below
50% abv.
Tails: At 200 to 205F the abv will drop from 50% to 30%. Save these tails to be
redistilled since tails contain congeners that give whiskey its classic flavor. Note: At 30%
abv a spoon full of spirits will fail to ignite. (Dont try this at home.) Below 30% toss
everything.
DOUBLE DISTILLING
Ferment 8 bbls. or 240 gallons of 9% abv beer wash.
STRIPPING RUN
9% abv wash becomes 30% abv low wines.
No cuts.
Use Fermcap-S on all runs.
Make three 80 gallon stripping runs. Each run will yield
27 gallons of low wines.
The total amount collected, 81 gallons of 30% abv.
To the 81 gallons add 19 gallons of water (Water extends
the run allowing for better cuts).
Now you are ready to double distill 100 gallons of low wine.
SPIRIT RUN
100 gallons of low wines, becomes 50 gallons of 70% spirit
The run
Foreshots: The first 4-6 oz from the condenser contains aldehydes
and other undesirable elements. Collect and use as a cleaning agent.
Heads: Collect 10 gallons of 80 to 70 abv for re-distillation.
Hearts: Collect 50 gallons of 70% to 50% abv for barreling.
Tails: Collect 10 gallons 50% to 30% abv for redistilling.
Toss anything below 30% abv.
There is a great deal of aroma and flavor in the tails fractions. Retaining a limited
amount of the tails and then adding it back to the hearts adds complexity and depth. How
much to include or when to stop collection tails for blending back is largely subjective (by
taste) process that varies among distillers and their particular systems. You will need to
experiment to determine what works best in your situation. Most important is keeping a
record in a log book. Many distillers determine yields the old fashioned way, with an
alcoholameter. If you decide to do so, find one with a range of 60 to 120, rather that using
the widely available 0 to 200 models. The density meter gives faster results.
Note: At the end of the hearts run (50% abv) the alcohol coming out of the still is dropping
and water is picked up as the boiling point goes higher, creating different flavors. Pot stills
also often have temperature spikes in the head creating vapors with off-flavors of an anise
or banana. It will take more than one distillation to learn how to control the flow of spirits
from a pot still and collect the hearts from the sweet spot.
AGING
Age 6 months in a small, #4 char, new American oak barrel.
Experiment with toasted applewood and cherrywood chips.
Cut the spirits with distilled or reverse osmosis treated water.
If using tap water to dilute, use a tight filter to remove sediment.
It is best to barrel age the whiskey in a building with no insulation. This allows summer
and winter temperature variations to heat and cool the barrels ensuring a fast maturation. If
possible, set a few barrel out in the sun for a couple of months. Barley, rye and wheat
whiskiesunlike corn whiskeydont require years of aging to pick up flavor and color
from the barrel. Many believe that the flavor of corn whiskey comes from the barrel rather
than the malt.
A Column Still
This is a best effort to illustrate a column still.
Chapter 11
Using a Simple Column Still
A pot distillation can increase the concentration of a 10% abv wort/wash to a 55% abv
spirit. This first spirit is called low wines and before the second distillation it is diluted to
30% abv. This dilution will allow for accurate cuts during the second distillation by
increasing the run time. After the 30% abv low wines are distilled, a 70-75% abv spirit is
obtainable. In contrast, a pot still with a column with copper mesh packing and a
dephlegmator (also known as a pre-condenser) can take the same 10% abv wash and on a
single pass get a 60% abv or more spirit. Even more efficient is a column using trays
and/or bubble caps.
Distilling in a single run produces a different whiskey than one produced by double
distillation. This is because in double distillation, the dilution of the low wines with water
before the second run allows better removal of negative congeners since there is more
copper surface interaction and finer distillation control. This makes the spirit cleaner, less
hot, and lighter tasting. The inclusion of a column with a pot still will additionally increase
the ability of the distiller to control the congener content of the finished spirit with
extreme precision.
The resulting products from each method (pot vs. column) have desirable qualities. It is
up to the distiller to decide what process he or she wants to use and what style of whiskey
to produce. The deciding factor may be in the price of the still. A 250-gallon pot still with
a condenser runs about $150,000. A pot still with a column equipped with trays and
bubble caps costs over $250,000. Non-professionally made stills can cost 1/10 this amount
but require many engineering skills. A cheap 80-gallon pot still can be made for about
$5,000, but this may be at the sake of performance and efficiency and therefore is rarely
done for commercial use.
Many distillers, from Kentucky moonshiners to French cognac producers to German
brandy makers, have developed their own unique still designs to improve the efficiency of
a pot still. American moonshiners use a doubler, or a thumper keg. The French have a
large helmet characteristic of the alambic still, and the Germans produce highly
engineered stills with bubble plates.
While the equipment is different, the ultimate result of building a still that distills the
spirit twice (or more) is one that all these pioneers were developing. To achieve a second
distillation in a single run (using the column still), the vapor must condense briefly and
then evaporate again. This process is easy to understand as traditional distillers
accumulated their low wines so they would have a full still charge from which to perform
a second distillation a few days later.
More complicated to understand, but identical in theory, is the construction of a still that
automatically condenses, and then redistills, the spirit in a single run. American
moonshiners used the thumper keg to do this. The thumper was placed between the still
and the condenser, and was typically a pot 40 percent the size of the initial beer pot. The
steam alcohol vapors from the still are injected into a tank with a water bath. Initially all
of the vapors coming over from the still condense. As vapor subsequently continues to
enter the thumper, the heat is transferred to the water bath/condensed vapor mixture.
Finally the vapors will push their way through the bath when the temperature reaches
more than 160F and they will flow into the condenser. The use of thumpers, however, is
dangerous because pressure can build between the still and the thumper. This hazard can
lead to explosion of the thumper tank and can also cause a still to implode. It is not
recommended that any distillers use a pot still with a thumper. It will be rare that any
commercial distillers will be allowed to operate a thumper equipped still due to the lack of
ASME-rated safety devices. Instead, most artisan distillers have a pot still with four or
five plates in the column. The column pot still typically has plates equipped with bubble
cups and a deflegmator. This type of still is readily available. Some of the best whiskey in
the world is produced using a simple pot still with a condenser, but if you can invest in
equipment that allows for better efficiency and effectiveness it can reduce the production
and aging time of the whiskey. An ideal system would be one comprised of a pot still with
a 4-plate column, deflegmator, and a condenser.
THE COLUMN DISTILLATION PROCESS
At 173F, vapors from the wash begin to rise up the column and hit the copper mesh
packing or plates in the column. At the top of the column is a jacket or heat exchanger
(deplegmator/pre-condenser) through which cool water is circulated. The combination of
the surface area of the packing and the cool water heat exchange causes the rising vapors
to cool. The condensed vapor then cascades down the column and through the packing or
trays allowing it to fall back into the wash where it is re-heated. This process is called
reflux distillation. Some systems use the warmed water exiting the condenser to cool the
dephlegmator/pre-condenser. Although this can save some water, by using colder water
and slowing down the flow exiting the dephlegmator/pre-condenser, finer control of the
purity of the spirit can be achieved.
Soon reflux will push past the packing or trays and the dephlegmator/pre-condenser and
the system will be in balance. At this point the alcohol vapors from the wash will have
lined themselves up by their atomic weight with the lightest vapors (heads) coming off
first followed by the hearts and tails.
A typical whiskey second distillation run on a packed or plate column still should be
controlled to start running off between 80% and 75% abv and stopped between 64% abv
to 64.9% abv.
During the distilling process the distiller must be very careful not to over-cool the
dephlegmator/pre-condenser. Doing so with a non-safety equipped system will cause the
alcohol to condense quickly and possibly collapse the still. All distilling systems should be
equipped with a pressure and vacuum safety valve. In a safety-equipped system, over-
cooling of the dephelgmator/pre-condenser will only result in stopping the flow of spirit
from the condenser and will avoid disastrous results.
The distiller can control the percent of alcohol of the spirit by increasing or decreasing
the heat to the pot. If your distillation system includes a dephlegmator/pre-condenser, the
control is achieved by increasing or decreasing the amount of water running through it.
Increasing reflux = higher proof and purity, slower run. Decreasing reflux = lower proof
and purity, faster run.
Clean sweet spirits can be obtained by running a cold still. This is accomplished by
keeping the head temperature of the still under 180F. This is done by running a significant
amount of water through the dephlegmator/pre-condenser cooling the top portion of the
column which will increase condensation and thereby allowing greater reflux.
The head fraction collected on an average whiskey run will be about 21% of the total
alcohol. Hearts will be about 57%. The tails will be about 22%. Whiskey distillers re-
distill the tails because they contain very concentrated flavorful congeners, but typically
discard the head fraction.
The still must be cleaned after every use by flushing it with hot water, and weekly by
cleaning it with 2% caustic (sodium hydroxide) followed by a 2% citric acid wash.
CONCLUSION
Every distillery is different. Each decision, shape, style and size affects the final
product. The goal should be to produce a whiskey that is consistently reproducible from
batch to batch as efficiently as your system will allow.
An alternative use for local surplus is needed. With national trends of Eat Local, consume local and increases in spirit
consumption, the opportunity exists for locally produced value-added products for consumers and a void exists for a
locally produced premium 100 percent fruit brandy, Eau de Vie.
There is an increasing national trend of micro-distilling in the nation (3). Spirit consumption has risen every year the last
9 years (2,5). There are 2 micro-distillers operating in the state of Missouri: Augusta, St. Louis, and 1 near beginning
operation at Branson. Nationally there were 40 licensed makers in 2003 which grew to more than 150 in 2008 and many
more in the pipeline. (3) By adding value to our apples, as source material, distilling an eau de vie we could provide
added income directly to our orchard and locally push wholesale apple prices up. New uses for price-depressed apples
will help fruit producers with increased prices by putting pressure on base prices for the state, and distilling adds jobs in
manufacturing, construction, and sales. The distillery/orchard, as a destination, will also provide indirect economic
development potential for the rural community creating jobs for associated day trip activities, staycations. The micro-
distillery will provide an example for other producers in the state.
IV. STATEMENT OF OBJECTIVES
We would like to discover the increase in spirit consumption, and the size of the market not currently being met for local,
craft distilled product. The new wave of micro-distilling could provide rural jobs directly, tourism and support industries
jobs indirectly and a new market for Missouri apples for Bates, Clay, Caldwell, Carroll, Chariton, Lafayette, and Ray
counties. Bates, Chariton and Lafayette are the 3 largest orchard acres in the state and all counties are located in the
central western part of the state surrounding Kansas City.
It is already proven to be technically feasible (7,8),with over 150 registered micro-distillers nationally, 2 in Missouri.
Is regional distillation of apples to a eau de vie-style brandy potentially profitable, to what extent, and, if it is, what is the
path to implementing?
Phase 1
Feasibility study of the market situation
Raw material sources
Need for new useMidwest Fruit grower survey
Market demand for 100 percent fruit brandies
Consumer profile
Economic feasibility
Profit potential
Measure growth potential
Focus groups
Regional economic impact
Phase 2
Business plan
SWOT
Market plan
Production plan
Finance plan
Phase 3
Implementation
Presenting the plan to the bank
Technical merit Artisan distilling: 40 licensed makers in 2003 to more than 150 in 2008 (1-ADI)
Distilling currently being taught at Southwest Missouri State, Springfield and Michigan State University. At least 2
micro-distilleries operating in MO now.
Project specific qualifications of principals, subs: James D Pierce: BS in Horticulture at NWMS, 15 years growing fruits
and vegetables, several years of home juice/wine production, 1 year of juice production for market.
Potential for direct near-term commercial application of projects results:
According to the ADI forum, startup times are ranging from to 2-3 years. Our hope is that information gathered will
allow immediate application for funds and production/marketing to begin as soon as capital acquired.
Anticipated results: New product development for fruit and use of locally produced commodity to satisfy a market trend
creating new jobs and through competitive uses for apples push base price up and providing security to existing
orchards. A profitable product for Of The Earth.
Impact on MO ag producers: Increase demand for MO fruit mid- to long-term.
Impact on rural community economy: The states of Washington, Oregon, and Michigan have fledgling micro distillery
industries. Michigan expects a 400 million dollar contribution to its state economy. We expect to bring in new jobs
distilling, sales of value added product, and associated development. Send capital to surrounding counties producing
apples, increase county tax income, and the possibility of beginning a distilling trail along I-210, linking locally
produced ag products, value added products and associated increase in service, restaurants, fuel.
Job creation potential: Michigans expectations were a $400 million contribution to their state economy as a result of law
changes allowing microdistillation.
Of The Earth expects to create near-term 1-4 construction jobs, after production starts 1-2 in distilling and sales. The
market and our research will then determine growth for Of The Earth. Countywide or even statewide replication of
regional distilling businesses based on our findings could establish a state industry with results paralleling Michigan.
Capital investment:
Loader, bulk bins for harvest
Cost of building-restrooms, warehouse, production, office, sign.
Equipmentsink, 2 ton flatbed truck, tank wash, pallet jack, fruit mill, pulp pump, fermentation vessels, mash pump,
reflux still, holding tank, pulp disposal bins, bottle filler, labeler, pallets, cleaning equipment.
Office furnishingscomputer, business software, desk, file cabinet.
Tasting roomcounter, register, display shelves, glasses, sink, signage.
Actual costs are expected to come from preparing Business Plan with grant findings.
PLAN OF WORK
Key personnel
Patricia Pierce, James C. Pierce, and James D. Pierce
Consultants
EEMG, Kansas City, MO
Bill Owensindustry contact
FinancialWestbrook and Associates
Equipment Manufacturer contactedBavarian Breweries and Distilleries
Kris Berglund, Michigan State University
Week 1-8 (8 weeks)
Begin Phase 1, Feasibility study.
Begin interviewing operating micro distilleries and education research facilities about startup costs, equipment costs,
cost of production.
Week 9-13 (4 weeks)
Phase 2: build the business plan.
Week 14-17 (3 weeks)
Phase 3: Implement.
II. FACILITIES AND EQUIPMENT
Existing office, computer, and phone owned by Of The Earth.
VIII. CO-SPONSORS
None yet.
IX. REFERENCES
Bill Owens
Kris Berglund
1) Marilyn Odneal, SWMS, phone conversation 9/23/08.
2) http://articles.moneycentral.msn.com/Investing/Extra/BourbonBusinessBooms.aspx?GT1=33002
3) American Distilling Institute
4) Paul Peters, conversation 9/17/2008
5) Article, http://www.drinksmediawire.com/afficher_cdp.asp?id=1681&lng=2
<http://www.drinksmediawire.com/afficher_cdp.asp?id=1681&lng=2>
6) MO orchard statistics
http://www.nass.usda.gov/census/census02/volume1/mo/st29_2_030_030.pdf
7) ADI #92, Apples into Vodka
8) ADI#, Atchison Distiller, grains into whiskey
Literature Search
1) Article, MI state law change, expect 400 million economic impact http://news.msu.edu/story/5614
Of The Earth presently sells apples for fresh consumption at 1 local retail location and 1 local farmers market.
Production comes from 265 apple trees, 15 varieties, that are in their 13th year. There are 300 more apple trees of
various ages planted but not of bearing age. The farm sits on 3 parcels, 2 sited next to each other comprising 40 acres of
which 20 acres of pasture that could be planted to orchard. The 3rd parcel is a retail location where our greenhouse is
built along a main highway, I-210, a main thoroughfare to Kansas City, placing it 30 minutes from downtown Kansas
City.
Current orchard production is sold fresh with approximately 14 percent of total crop marketed through the Liberty
Farmers market, Lawson Farmers market, and at the greenhouse. Some culls are converted to juice. Fresh prices
average 50 cents per pound, $21 per bushel. Juice sells for $10 a gallon. A bushel yields 2 gallons, so, it takes 21.5
pounds of fruit, which nets 46.5 cents per pound. We lose 3.5 cents a pound by making juice.
Were selling 14 percent of the current fruit off producing trees, 185 bushel. Several varieties have turned out to not be
suited to our environment for the fresh market but would make juice. The confluence of limits of our own labor, excess
production, and the local fresh market demand are balanced.
There is less than 6 acres planted with potentially 25 acres to expand into but with prices at 2.52 for processors at
wholesale it makes the wholesale market consideration moot.
Our apple production, limited as it is, has outstripped our 3 marketing venues. Therefore, regional varietal eau de vie
production could add value and raise our gross revenues. Development of the equipment combined with the orchard and
eau de vie production as a tourist attraction will also increase income for the business. Regional varietal brandies open
the door to many locally small distilleries across the state. Creating jobs in operation, repair/maintenance, marketing,
orchards, and tourism.
1.) a
2.) d
Chapter 2
1.) b
2.) b
3.) c
Chapter 3
1.) d
2.) a
Chapter 4
1.) e
Chapter 5
1.) d
2.) b
3.) c
4.) b
5.) a
6.) c
7.) b
Chapter 6
1.) b
2.) a
3.) b
4.) c
5.) c
6.) a
Chapter 7
1.) e
2.) c
Chapter 8
1.) b
2.) a
3.) a
4.) c
Chapter 9
1.) b
2.) c
3.) a
4.) c
4.) c
Chapter 10
1.) a
2.) b
3.) b
4.) c
5.) a
6.) c
7.) a
8.) b
Chapter 11
1.) b
2.) a
3.) b
4.) c
5.) c
6.) b
7.) a
8.) c
9.) b