This document provides analytical data and information about 4-Hydroxy-DIPT (4-OH-DIPT), including its chemical structure, properties, analytical methods for identification like NMR, GC-MS, and FTIR spectroscopy. It describes key analytical data that allows for structural confirmation of this tryptamine compound, which is also known as iprocin or 4-hydroxy-N,N-diisopropyltryptamine. Additional online resources for more information are also referenced.
This document provides analytical data and information about 4-Hydroxy-DIPT (4-OH-DIPT), including its chemical structure, properties, analytical methods for identification like NMR, GC-MS, and FTIR spectroscopy. It describes key analytical data that allows for structural confirmation of this tryptamine compound, which is also known as iprocin or 4-hydroxy-N,N-diisopropyltryptamine. Additional online resources for more information are also referenced.
This document provides analytical data and information about 4-Hydroxy-DIPT (4-OH-DIPT), including its chemical structure, properties, analytical methods for identification like NMR, GC-MS, and FTIR spectroscopy. It describes key analytical data that allows for structural confirmation of this tryptamine compound, which is also known as iprocin or 4-hydroxy-N,N-diisopropyltryptamine. Additional online resources for more information are also referenced.
This document provides analytical data and information about 4-Hydroxy-DIPT (4-OH-DIPT), including its chemical structure, properties, analytical methods for identification like NMR, GC-MS, and FTIR spectroscopy. It describes key analytical data that allows for structural confirmation of this tryptamine compound, which is also known as iprocin or 4-hydroxy-N,N-diisopropyltryptamine. Additional online resources for more information are also referenced.
4-Hydroxy-DIPT The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. 3. QUALITATIVE DATA 3.1 NUCLEAR MAGNETIC RESONANCE Sample Preparation: Dilute analyte to ~5 mg/mL in base extracted CDCl3 containing TMS for 0 ppm reference. Instrument: 400 MHz NMR spectrometer Parameters: Spectral width: at least containing -3 ppm through 13 ppm Pulse angle: 90o Delay between pulses: 45 seconds 1
H NMR: 4-OH DIPT HCl Lot SF06008; CDCl3; 400MHz
TMS
10 9 8 7
CHCl3
6 5 4 3 2 1 0 1 2
22 2
12
0.75 0.50 0.25 0 1
7.00
Latest Revision: 1/5/2015
1 6.75
2 3.1
2 3.0
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12
2 2.9
2.8
1.050
1.000
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4-Hydroxy-DIPT The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. 3.2 GAS CHROMATOGRAPHY/MASS SPECTROMETRY Sample Preparation: Dilute analyte ~4 mg/mL methanol. Instrument: Column: Carrier Gas: Temperatures:
Agilent gas chromatograph operated in split mode with MS detector
DB-1 MS (or equivalent); 30m x 0.25 mm x 0.25 m Helium at 1 mL/min Injector: 280oC MSD transfer line: 280oC MS Source: 230 oC MS Quad: 150oC Oven program: 1) 100oC initial temperature for 1.0 min 2) Ramp to 300 oC at 12 oC/min 3) Hold final temperature for 9.0 min Split Ratio = 20:1, 1 L injected Mass scan range: 30-550 amu Threshold: 100 Tune file: stune.u Acquisition mode: scan 14.502 min EI Mass Spectrum: 4-OH-DIPT HCl Lot # SF06008
Injection Parameters: MS Parameters:
5 Intensity [x 10 ]
114
Retention Time:
1.5
40
80
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100
120
140
160
180
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200
220
240
260
245
229
215
199
174
160
130
104
86 91
146 60
77
65
EI+
56
43
0.5
30
72
1.0
260
m/z
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4-Hydroxy-DIPT The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. 3.3 INFRARED SPECTROSCOPY (FTIR) Insrument: Scan Parameters:
FTIR with diamond ATR attachment (1 bounce)
Number of scans: 32 Number of background scans: 32 Resolution: 4 cm-1 Sample gain: 8 Aperture: 150
735
40
490 582 661
50
843 968 1038 1130 1161 1261 1294 1350
60
1396 1433 1452 1589
3147
2669
3240
70
2943
%Transmittance
FTIR ATR (Diamond, 1 Bounce): 4-OH-DIPT HCl Lot SF06008
30 20 3000
1500
Wavenumber (cm-1)
490 517 582 604
634 661 694
756 785
843
968
1049 1038
1261
50
2000
1093 1130 1161
60
2500
1294 1319 1350
70
1396 1433 1452
1589
1506
%Transmittance
3500
735
40 30 20 1700
1600
1500
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1400
1300
1200
1100
1000
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900
800
700 Wavenumber (cm-1)
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4-Hydroxy-DIPT The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. 4. ADDITIONAL RESOURCES Forendex http://forendex.southernforensic.org/index.php/detail/index/1175 Wikipedia http://en.wikipedia.org/wiki/4-HO-DiPT
