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321-56738-21F

DEC. 2008

INSTRUCTION MANUAL
ELECTRONIC MOISTURE BALANCE
MOC-120H

READ AND UNDERSTAND THIS MANUAL BEFORE OPERATION.


SAVE THIS MANUAL.

RequestsFPL950701
 Provide this manual to the next user in the event that the instrument is transferred.
 To ensure safe operation, contact your Shimadzu Balance representative for installation, adjustment, or
reinstallation after moving the instrument to a different site.

NoticesFPL950701
 The content of this manual is subject, without notice, to modifications for the sake of improvement.
 Every effort has been made to ensure that the content of this manual was correct at the time of creation. However,
in the event that any mistakes or omissions are discovered, it may not be possible to correct them immediately.
 The copyright of this manual is owned by Shimadzu Corporation. Reproduction and duplication of whole or part of
the content without permission of the company are strictly prohibited.
 "Microsoft", "Windows", "Windows Vista" and "Excel" are registered trademarks of Microsoft Corporation of the
U.S.A. in the United States and other countries. All other company names and product names that appear in this
manual are trademarks or registered trademarks of the companies concerned. Note that TM and indications are
not used.
 The company names, organization names and product names in this manual are trademarks or registered
trademarks of the companies and organizations concerned.
 Shimadzu does not guarantee that the WindowsDirect communication function will operate without problems on all
PCs. Shimadzu will accept no responsibility for any trouble that arises as a result of using this function. You are
recommended to back up all important data and programs in advance.

2004-2008 Shimadzu Corporation. All rights reserved.

Declaration of Conformity
Manufacturers Name:

SHIMADZU CORPORATION
Analytical & Measuring Instruments Division
1, Nishinokyo-Kuwabara-cho, Nakagyo-ku,

Address :

Kyoto 604-8511, Japan


declares in sole responsibility that the following product
Product Name
Model Name
P/N

Electronic Moisture Balance


MOC-120H
321-63300-10

referred to in this declaration conforms with following directives and standards


Electromagnetic Compatibility 2004/108/EEC
EN61326-1:2006
Electrical equipment for measurement, control and laboratory use
EMC requirements
Low Voltage Directive 2006/95/EC
EN 61010-1:2001
Safety requirements for electrical equipment for measurement,
control and laboratory use
Part 1 : General requirements
The last two digits of the year in which CE marking was affixed for Low Voltage
Directive 2006/95/EC are 03.
Note 1) This declaration becomes invalid if technical or operational modifications are
introduced without manufacturers consent.
Note 2) This declaration is valid if this product is used alone or in combination with the
accessories of this product which are mentioned in attached Appendix 1 or
other instruments which fulfill with the requirement of mentioned directive.
Note3) Importer/Distributor and Authorised Representative in EU is as follows:
SHIMADZU EUROPA GmbH
Address :Albert-Hahn-Strasse 6-10, 47269 Duisburg, F.R. Germany

Quality Assurance Department


Analytical & Measuring Instruments Division
SHIMADZU CORPORATION

II

Action for Environment (WEEE)PL950701


To all user of Shimadzu equipment in the European Union:
Equipment marked with this symbol indicates that it was sold on or after 13th August 2005, which means it should
not be disposed of with general household waste. Note that our equipment is for industrial/professional use only.

Contact Shimadzu service representative when the equipment has reached the
end of its life.
They will advise you regarding the equipment take-back.
With your co-operation we are aiming to reduce contamination from waste electronic and
electrical equipment and preserve natural resource through re-use and recycling.
Do not hesitate to ask Shimadzu service representative, if you require further information.

WEEE Mark

III

Electronic Moisture Balance Safety NotesFPL950701


Improper use of the electronic moisture balance in violation of the following safety notes may result in death, injury or
damage to property due to fire, etc. Furthermore, the electronic moisture balance has high temperature components which
can cause burns if proper safety guidelines are not followed.

 Observe all safety guidelines


Carefully read and observe all safety notes included in this users manual.

 Do not use the unit if it appears to be malfunctioning


If you suspect a problem or malfunction in the unit, discontinue use and immediately have the unit inspected by certified
service personnel.

 Meanings of Warning Indicators and Symbols

The following symbols are used in this operating manual and product to prevent accidents from occurring as a result of
improper usage or handling. The meaning of each symbol is as described below.

Warning

Failure to observe these items may lead to death or injury to the user.

Caution

Failure to observe these items may lead to injury to the user or damage to property.

Note

Items which the user should be aware of in order to use the unit safety.

Caution Symbols

Fire Hazard

Burn Hazard

Electric Shock
Hazard

Prohibition Symbols

Prohibited

Symbol Requiring User Action

Do Not
Do not Expose
Disassemble
to Water

Required Disconnect Plug


Action from Electrical Outlet

Warning
Fire Hazard

Electric Shock Hazard

 Do not attempt to measure samples which may undergo dangerous chemical reactions when heated as doing so
may result in explosion or release of toxic gas.
 Do not place flammable materials near the electronic moisture balance.
Some parts of the electronic moisture balance become extremely hot during operation and could lead to fire if
flammable materials are placed nearby.
The heater inside the Electronic Moisture Balance reaches temperatures higher than the preset sample-heating
temperature.
The surface of the quartz tube of the heater reaches approximately 500C (900F) even during normal
measurements. In addition, the nickel-chromium resistance wire inside the heater reaches approximately 900C
(1700F) and is not airtight.
 Never use with any power source for which the product was not designed.
Application of excessively high voltage may result in overheating to malfunction or fire.
 Do not attempt to disassemble, modify or rebuild the electronic moisture balance.
Doing so may result in accident, electric shock, etc. If you believe the unit may be malfunctioning contact to an
authorized Shimadzu representative.
 Do not allow the unit to come in contact with water.
The electronic moisture balance is not waterproof. Do not allow water or other liquids to get into the units enclosure
as this may lead to electric shock or malfunction.

Caution
Burn Hazard

Electric Shock Hazard

 Do not touch the heat-dispersing component of the heater cover or sample pan with your bare hands, as doing so
might result in burns.
This electronic moisture balance is at high temperature during and immediately after making measurements,
When touching the unit, only use the specified control knobs and accessories.

IV

Follow operation instruction


 Correctly set draft shield, sample pan supporter, sample pan handler and sample pan.
 Hold the handle of heater lid when opening or closing heater lid.
 Use sample pan handler when removing sample pan.
 Never touch any metal parts of heater unit and surrounding parts when removing sample pan.
 Cool the unit down to ambient temperature in a safe location after measurement.
 Always make sure that the unit has cooled down sufficiently before covering it with a dust cover.

Warning on high temperature


 The shadowed parts become especially hot during measurement. Only handle the parts marked with circles when
operating.

Do not measure hazardous samples


 Use the Electronic Moisture Balance only for measuring the moisture content in a sample by moisture evaporation
through the heating process.
 Set the drying temperature within the safe temperature range of each sample.
 The heater inside the Electronic Moisture Balance reaches temperatures higher than the preset sample-heating
temperature.
The surface of the quartz tube of the heater reaches approximately 500C (900F) even during normal
measurements. In addition, the nickel-chromium resistance wire inside the heater reaches approximately 900C
(1700F) and is not airtight. Measurements of combustible or flammable samples pose a risk of fire.

 Do not measure any sample which might explode, ignite or produce toxic substances under high temperature.
 Do not measure any sample which might cause chemical reaction under high temperature.
 Do not measure any sample of unknown property.
 Do not measure any sample whose surface hardens or solidifies by heating causing high inner pressure.
 Immediately turn the power off if the sample should catch fire during measurement.
 Use with adequate ventilation and appropriate venting for sample type.

Do not place flammable objects near the unit


 The unit becomes very hot during and after measurements. Do not place any flammable objects near it as they may
catch fire.
 Do not place near any objects which are not heat resistant. They may be damaged or deformed.
 Never place anything on top of the heater unit.
 Immediately turn the power off and disconnect power cable when any emergency occurs, such as abnormal smell,
smoke or fire.

Key and Power Switch Operation


 Do not turn the power on while pressing any keys.
 Do not operate any keys except as instructed in this manual.
 Turn the power off and disconnect power cable when lightning is expected.

Emergency Stop
 [Start/Stop] key is always effective during measurement. Press it immediately when any danger or abnormality occurs.

Installation, Transportation and Storage


 Avoid locations subject to extremely high or low temperature, high humidity, direct sun light, electro-magnetic noise,
corrosive gas or dust.
 Install on a vibration-free, level surface.
 For transportation, hold the unit level as much as possible.
 Do not drop or impact the unit.
 Do not pull the cable - hold the connecter when disconnecting the power cable or RS-232C cable.
 Turn the power switch off and disconnect from the power source when not using for a long time or lighting is expected.

VI

Others
 After a power outage, turn the power back ON.
When a power outage occurs, the power is shut off automatically. Therefore, once turn off the power switch, then
begin operation from 7.1 "Turn on the power switch" ( page 12) again.
 Do not connect anything other than peripheral devices specified by Shimadzu to the moisture balance's connector.
If you do, the balance may stop working normally.
In order to avoid trouble, always connect peripheral devices in accordance with the directions in this manual.
 If you detect anything abnormal (e.g. a burning smell) disconnect the AC power cord immediately.
Continuing to use the balance with an abnormality could lead to fire or an electric shock.

VII

Contents
1. Introduction............................................................................................... 1
2. Description of Features and Principles of Operation ................................. 2
2-1 Principles of Operation ............................................................................................. 2
2-2 Features ................................................................................................................... 2
2-3 Applications (i.e., materials which can be measured) ............................................. 2

3. Specifications ........................................................................................... 3
4. Names of Individual Parts and Components ......................................... 4
4-1 Names of Parts of Main Unit .................................................................................... 4
4-2 Parts and Accessories .............................................................................................. 5

5. Display and Control Panel ....................................................................... 6


5-1 Display ...................................................................................................................... 6
5-2 Control Panel Operations ......................................................................................... 7

6. Assembly and Installation of Main Unit.................................................. 8


7. How to Conduct Measurements .............................................................. 12
8. Specifying Measuring Conditions........................................................... 15
8-1 Selecting Temperature Display Mode ...................................................................... 15
8-2 Types of Settings ...................................................................................................... 16
8-3 Descriptions of Individual Measuring Condition Settings ......................................... 16
8-3-1

Selecting the CONDITIONS (Measuring conditions storage area) ............. 17

8-3-2

Selecting the MODE (Measuring mode) ...................................................... 18

8-3-3

TEMP (Drying temperature) Setting ............................................................ 27

8-3-4

Bias Setting .................................................................................................. 28

9. Menu Settings ........................................................................................... 29


9-1 Types of Menu Settings ............................................................................................ 29
9-2 Descriptions of Individual Menu Items ..................................................................... 29
9-2-1

Selecting a measurement base and switching the % display ..................... 30

9-2-2

Specifying the type and format of output ..................................................... 31

9-2-3

Specifying sample codes ............................................................................. 34

9-2-4

Setting the date and time ............................................................................. 35

9-2-5

CAL (Balance calibration) ............................................................................ 36

9-2-6

Specifying a device ID ................................................................................. 37

9-2-7

Specifying a password ................................................................................. 38

10. Error Messages......................................................................................... 39


11. Precaution on Conducting Measurements ............................................ 40
12. Predictive Measurements ........................................................................ 41
12-1 A Description of Predictive Measuring ..................................................................... 41
12-2 Procedure for Obtaining Predicted Measurements.................................................. 43
12-2-1 Calculating the bias to be specified when operating in predictive
measurement mode ..................................................................................... 43
12-2-2 Evaluating Predictive measurements .......................................................... 45
12-2-3 Performing Predictive measurements ......................................................... 46

13. Temperature Calibration (Option required) ............................................ 47


14. Printing Output to a Printer (Option) ...................................................... 49
14-1 Printer Output Sample .............................................................................................. 49
14-2 Outputting Stored Measurement Data ..................................................................... 52

15. Computer Interface................................................................................... 53


15-1 RS-232C Interface Specifications ............................................................................ 53
15-2 Setting Up and Transmitting Data ............................................................................ 54
15-2-1 Connecting the RS-232C cable ................................................................... 54
15-2-2 MOC-120H settings ..................................................................................... 54
15-2-3 Setting Up the Computer ............................................................................. 54
15-2-4 Starting Up the Computer ............................................................................ 56
15-3 Computer Output Format ......................................................................................... 57

16. Maintenance .............................................................................................. 59


16-1 Performing Maintenance .......................................................................................... 59
16-2 Replacing Fuses ...................................................................................................... 60

17. Parts List ................................................................................................... 61

1. Introduction
Thank you for choosing the Shimadzu Electronic Moisture Balance MOC-120H. MOC-120H has high
reliability by employing the UniBloc cell, introduced for use in electronic balances by Shimadzu in 1989.
It provides WindowsDirect functions for transfer of measurement results to personal computer without
installing software. This and other various functions can be used to meet the operator's objectives.
In order to make full use of the functions and performance provided in the MOC-120H, please read this
instruction manual before using the balance and keep the manual for future reference.
For information on the following points, please contact your Shimadzu Balance representative.
 Product warranty
 After service

2. Description of Features and Principles of Operation


2-1 Principles of Operation
This unit determines the moisture and solid contents of samples by heating them using infrared
illumination and measuring changes in mass due to evaporation. This is referred to as the drying
loss method and is the simplest method for determining moisture content and thus mandated by
many public regulations related to measurement standards.

2-2 Features
 UniBloc sensor
The core mechanism of the internal precision balance is the UniBloc*1 cell which provides excellent responsiveness,
temperature characteristics, and shock resistance. This UniBloc*1 sensor ensures excellent reliability in moisture
content measurements over a long period of use.

 New Auto Taring Function


The MOC-120H comes with an internal Auto Taring Function which makes it possible to perform reset correction while
performing measurements, thus eliminating drift of the balance even when performing measurements over a long time
and making it possible to obtain extremely reliable measurements.

 Mid-infrared quartz heating lamp


The MOC-120H uses a mid-infrared quartz heating lamp (with a central wavelength of 2.6 m). This heater provides
excellent drying efficiency over a wide range of different types of sample, minimizes the differences in heating due to
the different colors of samples, and eliminates the overheating of sample surfaces, thus making it possible to obtain
ideal drying conditions.
Whats more, this heating lamp also provides a long service life 5 to 10 times greater (20,000 to 30,000 hours) than
older infrared or halogen lamps.

 A wide selection of measuring modes


The MOC-120H provides a wide selection of measuring modes (automatic operation mode, timed operation mode, highspeed drying mode, low-speed drying mode, stepped drying mode, and predictive measuring mode) which makes it
possible to perform measurements under the best drying condition for each sample.

 The ability to store measuring conditions


The MOC-120H provides 10 measuring conditions storage areas which may be used to store sets of measuring
conditions to be used for different types of samples, thus reducing the work of programming settings before each
measurement.

 Data memory
The MOC-120H is able to store up to 100 pieces of measurement data in memory, making it possible to output large
batches of data all at one time.

 Printer port
The MOC-120H is equipped with a printer port which may be used to connect to the optional printer, thus making it
possible to print out text or graph data showing final measurements or intermediate drying states while performing
measurements.

 The ability to display changes in moisture content (M) in a numeric and bar graph display
The change M in moisture content over 30-second intervals is displayed in a numeric and bar graph display, thus
making it easier to estimate when a measurement should be completed. This feature is also useful in helping to
determine measurement completion conditions.

2-3 Applications (i.e., materials which can be measured)


 Materials for which water is the only or main component which evaporates as a result of
heating
 Materials for which no dangerous chemical reactions or other changes occur as a result of
heating
* Measurements can be performed with virtually any material meeting these conditions.

3. Specifications
Measurement format

: Evaporation weight loss method (Heat drying and weight loss method)

Sample weight

: 0.5g - 120g

Minimum display

: Moisture content: 0.01%


Weight: 0.001 g
: Moisture content (wet base & dry base), weight, solid content

Measurable quantities

Reproducibility (Standard deviation)*1


: Samples with a weight of 5 g or higher less than 10g: 0.05% *1
Samples with a weight of 10 g or higher: 0.02% *1
Measurement modes

: Automatic operation mode


Timed operation mode (with measurement times of 1~240 minutes or
continuous measurement mode, with a maximum measurement time of
12 hours)
High-speed drying mode (may be used with either automatic or timed
operation mode)
Low-speed drying mode (may be used with either automatic or timed
operation mode)
Stepped drying mode (performs drying in 5 steps)
Predictive measuring mode

Heater temperature range : May be set within a range of 30 to 200C in 1C increments (sample
position temperature)
Display

: Backlit LCD display (137 x 43 mm)

External output

: RS-232C interface

Communications

: Allows for data output using WindowsDirect function

Storage of measurement conditions


: Allows for storage of 10 sets of measurement conditions
Data memory

: Allows for storage of 100 pieces of data

Temperature/humidity operating range


: 5~40C, maximum of 85% RH
Heat source

: Medium frequency infrared quartz heater (maximum 625W)

Power supply

: AC 100~120/220~240V (50/60 Hz)

Power consumption

: Maximum of 640W

Weight and external dimensions


: 4.5 kg, 220 x 415 x 190 mm (W x D x H)
Sample pan

: SUS sample pan (Diameter: 130 mm; Depth 13 mm)

Items included

: 2 sample pans, 2 sample pan handler, wind shield, sample pan


supporter, spoon, spatula, 2 spare 8A-fuses, 20 aluminum foil sheets,
power cord, three-prong plug adapter, Instruction manual

Optional equipment

: Printer set (includes DPU-414 printer, printer interface cable printer


paper 1roll, and AC adapter), printer paper (10 rolls), package of
aluminum foil sheets (500 sheets), RS-232C cable, Temperature
calibration kit

*1 When using Shimadzu standard samples and measuring conditions. It is not applied to and not
garanteed with all samples or conditions.

4. Names of Individual Parts and Components


4-1 Names of Parts of Main Unit

Heater lid

Handle (Observation window)

Heater
Temperature sensor

Wind shield

Sample pan
Sample pan handler
Display
Level
Control panel

Power switch

Power conversion switch

Power inlet

RS-232C port

Fuse holder

Height adjustment legs

4-2 Parts and Accessories

Sample pan (2)

Sample pan handler (2)

Wind shield

Sample pan supporter

Spoon and spatula (1 each)

Spare 8A-fuses (2)

Aluminum foil sheets (20)

Power cord

Three-prong plug adapter

Instruction manual

Protection Cover

5. Display and Control Panel


7

5-1 Display
1 2 3 D

0
4

G
Item

Display as it appears with the power on.


(All display items shown.)

Name

Description

Stability indicator

This indicator lights up when the balance is stable.

Measuring completion indicator

This indicator lights up when measuring has been completed.

Heater indicator

This indicator flashes whenever the heater is on.

Predictive measurement indicator

This indicator lights up when performing predictive measurements.

Preparatory measurement indicator

This indicator lights up when measuring has been completed after performing a preparatory
measurement.

Menu display (during menu selection)

Displays individual menu items in sequence each time the SELECT key is pressed after pressing the MENU key.

Measuring conditions display (during


condition setting)

Flashes to display individual items in sequence each time the SELECT key is pressed after pressing the
CONDITION key. Values may be specified for a given item when it is flashing.

Measuring conditions storage display*

Displays the reference number of the currently selected measuring conditions program.

Measuring mode display*

Displays the currently selected measuring mode.

Predictive measurement convergence


conditions display*

Displays the conditions for convergence of measured values when operating in predictive or
comparative mode. When operating in high-speed drying mode, used to display the conditions required
in order to maintain a temperature of 180C.

End conditions display*

Displays the currently selected end conditions. When the value is displayed as a percentage, it indicates
that measuring will end automatically, and when value is displayed in minutes, it indicates that
measuring will end when the specified amount of time is reached.

Drying temperature display*

Displays the currently selected drying temperature.

Bias display*

Displays the moisture (or solid) bias.

Moisture/Solid/Weight display

When measuring weight (i.e., when in idling mode), used to display the weight in grams. When
performing measurements, used to display the moisture content and solids content as percentages.
When measuring weight, this display is also used to display oL (overload) when the weight exceeds
the maximum measurable weight and to display oL (negative overload) when the weight does not
reach the minimum measurable weight.

Temperature display

When 'TT' mode is selected, displays the temperature near the heater with C symbol illuminated. When
'ST' mode is selected, displays the sample position temperature with C symbol blinking.
*Refer to 8.1 for the details of 'ST' and 'TT' modes.

Measuring time display

Displays the amount of elapsed time during measuring.

Change in moisture (solid) content


display

Displays the change M in moisture (or solid) content at 30-second intervals during measurement.

Change in moisture (solid) content


scale display

Displays the change M in moisture (or solid) content in scalar format. The scale may display a
maximum change of 2 percent/30 seconds.

* Items marked with an asterisk display as flashing items during condition setting.

5-2 Control Panel Operations


The control panel keys are used to perform the following operations.

MENU CONDITION

SELECT

Name

START/STOP

ENTER

TARE/RESET START/STOP

Operation
Used to start measuring or to abort a measuring operation.
Also used to turn off the alarm which sounds to indicate that a measuring operation has been
completed.

START/STOP key

TARE/RESET

Used to deduct the tare weight.


Also used to perform a reset after an error has occurred.
Also used to return to display of weight after completion of measurement.

TARE/RESET key

ENTER

Used to confirm currently selected settings during menu selection.


When further settings must be specified, pressing the ENTER key causes the next specifiable
item choice to be displayed.

ENTER key
Used to display the selectable items or for setting values during menu selection or condition setting.

SELECT
SELECT key
Used for numerical settings.
Pressing the
key causes the value to increase, and pressing the
decrease.
UP key / DOWN key
Used to enter and exit the measuring condition setting mode.

CONDITION
CONDITION key
Used to enter and exit the menu selection mode.

MENU
MENU key

key causes the value to

6. Assembly and Installation of Main Unit


1 Opening the package
Open the package and check to make sure all listed
items are included.

2 Installing the main unit


Place the main unit on a flat, stable surface where it
will not be subject to vibrations or exposed to drafts
or breezes.

3 Removing the protective sheet


When using the unit for the first time after purchase,
remove the protective sheet attached to pan
supporter column.

Pan supporter column


Protective sheet

4 Ensuring that the unit is level


Turn the two height adjustment legs located at both
sides of the lower rear of the unit to adjust until the
level bubble falls within the red circle.
* The level is located to the left of the control panel. The
instrument is level if the bubble appears in the center
of the red circle when viewed from directly above.
Not level

Height
adjustment
legs

Level

Level is located to the left of the control panel.

 Bubble
8

5 Installing the wind shield


Open the lid of the heater, hold the wind shield by the
knobs on the top, and place it on top of the pan
supporter column so that the two round holes in the
wind shield fit over the stays .
* Place the wind shield firmly into position so that it does
not come into contact with the black pan supporter
column located at the center of the weighing unit.

Wind shield
Knobs
Round
holes

Stays

Pan supporter column

6 Attaching the sample pan supporter


Place the sample pan supporter gently into the pan
supporter column at the center of the main unit. Make
certain that the round hole of the sample pan
supporter fits smoothly over the stay on pan
supporter column.

Sample pan supporter


Stay

Round hole
Pan supporter
column

7 Attaching the sample pan handler


Next, attach the sample pan handler. Make certain
that one of the grooves of the handler fit smoothly
over the projection located at the rear of the wind
shield.

Grooves

* The handle may be placed either to the left or right, in


the position you find easiest to use.

Stay

8 Placing the sample pan


Place the sample pan gently down onto sample pan
supporter.

9 Close the heater lid


Set the Protection Cover on the display.
Adhesive tapes are attached to the Protection Cover.

0 Connecting the power cord


Insert the female end of the power cord into the
power inlet located at the rear of the unit. Then,
attach the three-prong plug adapter to the power cord
plug and insert the plug into power socket.

A Connecting the printer (optional)


If you use the optional printer, connect the printer
with the provided printer interface cable. For
instructions on how to use the printer, see the
separately provided DPU-414 Printer Users Manual.
* Some parts must be oriented in a fixed direction for
assembly. Note that placing parts in the wrong
direction may prevent heater from closing or in
erroneous readings being obtained, and that you
should accordingly take care that all parts are put into
place in their proper positions.

100V
120V

* Note that an error will occur if this switch is not set to


a position matching the power source being used.

10

220V

B Checking the power settings


Check the power conversion switch located on the
rear of the main unit to make sure that it is set to the
proper voltage setting for your power source. If not,
turn the switch to the correct position.

240V

C Specifying the power voltage setting


The specifiable voltages differ depending on the
power setting with the power conversion switch
described in B.

Note: This setting must be done according to the power voltage available at the installation site.

 How to specify the power voltage setting


Step

Key(s) used

Display

Operating instructions
Turn on the power while holding the MENU key pressed down.

C-1

MENU

Note that you should not remove your finger from the MENU key
until a string of hyphens - - - - - are displayed.

Turn on power
A tone will sound, the display will light up with all items lit and then
change to display first CHE5 and then a string of hyphens (i.e., - - - -). At the bottom left of the display will be displayed the
currently specified power voltage.
C-2

C-4

C-5

SELECT

ENTER

When the voltage at the installation site is displayed, press the


ENTER key. The display will then change from CHE4 to CHE0 in
sequence with the specified voltage still displayed.

.....

C-3

If the power conversion switch is set to 100~120V, pressing the


SELECT key will cause the display to switch from 100V 110V
120V and back to 100V in sequence. If the power conversion
switch is set to 220~240V, pressing the SELECT key will cause the
display to switch from 220V 230V 240V and back to 220V in
sequence. Note that here a voltage of 120V has been specified.

A tone will then sound and the display will return to the regular
weight display.

11

7. How to Conduct Measurements


Before beginning measurement, check to make sure that there is nothing remaining in the sample
pan. Also be sure that all parts of the main unit are firmly fixed into place and be sure that the
heater lid has been closed firmly before starting to perform measurements.
Also be sure to check on a regular basis that the main unit is level and readjust the height adjustment legs if necessary. (See 6. Assembly and Installation of Main Unit on p. 8 for instructions on
how to do so.)

Operating instructions

Display

1 Turn on the power switch


*

Once the power voltage setting has been spcified (Step ~ in 6.), when the
power is turned on for the second or subsequent times, a tone will sound,
the display will light up with all items lit, the display will change to display
CHE4, CHE3, , CHE0 while the currently specified power setting is
displayed, and then a tone will sound again and the display will change to
weight reading display mode.

Note: It is recommended that you always turn on about half an hour before
use in order to obtain consistent measurements.

Display will show default settings at the


time of shipment. (See p. 17, 8-2-1
Selecting the CONDITIONS (Measuring
conditions storage area).)

2 Specifying settings
When performing measurements for the first time or when you wish to
change current settings before measuring, you should specify the settings
required for measuring at this time. (See 8. Specifying Measuring
Conditions on p. 15 and 9. Menu settings on p. 29 for instructions on how
to do so.)

3 Placing the sample pan in the tester


Open the heater lid, place the sample pan on the handler, and place the
handler into the tester, being sure when you do so that the grooves of the
handler fit smoothly over the projection located at the rear of the wind shield.
*

If you have already place the sample pan and handler into place as described in
6. Assembly and Installation of Main Unit, then proceed directly to the next
step.

When using an aluminum foil sheet or other wrapping material because of the
nature of the sample being measured, place it on top of the sample pan.

12

Operating instructions

Display

4 Performing a reset
Close the lid of the heater, check to make sure that the stability indicator ()
is being displayed, and then press the TARE/RESET key.
When ----- and TARE appear on the display, the sample pan moves
upward and downward. When a tone rings, then the reset is completed and
the display returns to 0.000 g .
*

Always be sure that the heater lid is closed when performing a reset. Also make
sure that the tester is not exposed to drafts or breezes or subjected to any
vibrations when a reset is being performed.

5 Placing a sample in the tester


Open the lid to the heater and place the sample inside.
Be sure to place the sample as flat as possible into the tester so that heat is
applied evenly to the sample during measurement. (See 11. Precaution on
Conducting Measurements for further information.)

6 Beginning measurement
Close the lid of the heater, check to make sure that the stability indicator ()
is being displayed, and then press the START/STOP key. The display will switch
from a display of the weight (i.e., grams) to a percentage display and the
measuring time will be displayed.
The heating indicator ( ) will start to flash and drying will begin.
*

There may be times when the stability indicator () is not displayed because of
external vibrations or drafts or breezes. While it is possible to perform
measurements at such times, there may be cases when it is impossible to
obtain accurate measurements at such times, and you should accordingly
always be sure to conduct measurements in a location as free as possible of
vibrations, drafts, breezes, or any other harmful influences.

*
*

Do not open the lid to the heater during measurement.


Note: During Measurement
During measurement, the sample pan supporter moves upward and
downward automatically once per minute (or once every 30 seconds
when near the end of the measuring time) for automatic taring. The
movement is indicated by servo motor noise.

13

Operating instructions

Display

7 Measuring time display


While a measurement is being performed, the amount of time elapsed
will be displayed in minutes.
*

The change in moisture content over each 30-second interval is displayed


numerically and in scalar format (where the scalar display may display a
maximum change of 2 percent/30 seconds).

Taring is performed automatically once per minute (or once every 30 seconds
when near the end of the measuring time) while measuring moisture content.

To stop measuring when in the midst of a measuring operation, press the


START/STOP

key.

8 Completion of measurement
When the measuring operation has been completed, the heating indicator
( ) will disappear, the measurement completed indicator ( ) will be
displayed, and a tone will ring for a period of 10 seconds. To turn off the
tone earlier, press the START/STOP key.
The results of the measurement will be displayed and remain on the display.
Pressing the ENTER key at this point causes Signature title to be printed. (See
14-1 Printer Output Sample)
9 Resetting the display
Pressing the TARE/RESET key at this point causes the display of the results of the
measurement (i.e., moisture content) to disappear and be replaced by a
display of the weight of the sample after drying.
*

Note that a reset cannot be performed until the completion tone has stopped
ringing.

0 Disposing of samples after measurement


Open the lid to the heater, raise the sample pan handler vertically from the
unit, remove the sample pan, and dispose of the sample.
*

Note that the sample and sample pan may be very hot and you should
accordingly be careful in handling them at this time.

A Getting ready to perform the next measurement


Leave the lid to the heater open to allow the tester to cool off. When
performing measurements one after the other, leave an interval of about 1-2
minutes between each measurement and make sure that the tester has
cooled down before proceeding to the next measurement. You should also
keep a spare (cooled) sample pan on hand to use in the next measurement.
(See 11. Precaution on Conducting Measurements on p. 40 for further
information.)
When ready, return to step 3 and begin the next measurement.
B Turning off the power
When all measurements have been completed, turn the power switch to the
off position. Also be sure to turn the power off whenever the tester is not in
use.

14

8. Specifying Measuring Conditions


When using this tester to measure moisture or solid content, it is necessary to first specify the conditions
(e.g., drying temperature or measuring mode) of the measurement. The settings to be specified are described below.
It is also possible to save sets of measuring conditions (i.e., drying temperature, measuring mode, and bias).

8-1 Selecting Temperature Display Mode


The temperature display that is used for drying temperature setting and temperature indication on the
main unit display can be selected from the following two modes.
[ST (Sample position Temperature)] mode
The temperature at the sample position is used for setting and displaying temperatures.
Sample position temperature is converted from the temperature detected by the thermistor near the
heater. The default setting is this mode.
TT (Thermistor Temperature)] mode
The temperature detected by the thermistor near the heater is used for setting and displaying
temperatures.
 How to select temperature display mode
Step

Key(s) used
SELECT

1
CONDITION

Display

Operating instructions
From the weight display, press SELECT key first and while holding it
down, press CONDITION key and keep pressing both keys for about 5
seconds.
Currently selected temperature display mode is indicated as
either 'TT' or 'ST' at the M display part.

Every time SELECT key is pressed, the display is switched between


'TT' and 'ST'. Press ENTER kkey while the desired temperature
display mode is shown.

SELECT

It returns to the weight display upon completion of setting


temperature display mode.

ENTER

The temperature display mode selected here is effective for all measurement modes.
Indication of currently set mode:
In the display, the C symbol blinks when the current setting is 'ST' mode and when the current
setting is 'TT' mode, the C symbol is illuminated without blinking.

15

8-2 Types of Settings


Setting
CONDITION

Display during
specification of setting

Description

CONDITION 0~9
(Measuring conditions
storage areas 0~9)

Used to select the area to store condition settings. There are 10 storage areas labeled from 0 to 9. (See 8-31 Selecting the CONDITIONS (Measuring conditions storage area).)

AUT
(AUTO: Standard drying &
Automatic ending mode)

In automatic operation mode, measuring is brought to a end whenever the change in moisture content over
two consecutive 30-second periods falls below the specified conditions for automatic ending. (For further
information, see 8-3-2 1) Specifying settings for AUTO (Automatic ending) mode.)

TIM
(TIME: Standard drying &
Timed ending mode)

In timed operation mode, measuring is ended when the elapsed time reaches the specified measuring time.
(For further information, see 8-3-2 2) Specifying settings for TIME (Timed operation) mode.)

RPD
(RAPID: High-speed drying
mode)

In high-speed drying mode, the sample is dried at a temperature of 180C until the amount of change in
moisture content over a 30-second interval falls below a specified value and then drying is continued at a
specified drying temperature. (For further information, see 8-3-2 3) Specifying settings for RAPID (Highspeed drying) mode.)

SLW
(SLOW: Low-speed drying
mode)

In low-speed drying mode, the temperature is raised more gradually than when performing measurements
under normal conditions, taking about 5 minutes from the time when measuring begins until the temperature
reaches the specified drying temperature. (For further information, see 8-3-2 4) Specifying settings for SLOW
(Low-speed drying) mode.)

STP
(STEP: Stepped drying
mode)

In stepped drying mode it is possible to specify a separate drying temperature and separate measuring time
over up to 5 step intervals. (For further information, see 8-3-2 5) Specifying settings for STEP (Stepped
drying) mode.)

CMP
(COMPARE: Preparatory
measuring mode for
Predictive mode)

Preparatory measuring mode is used for determining the bias (i.e., the difference between the measurement
corresponding to that obtained in automatic operation mode and the predicted measurement value) needed in
order to perform measurements in predictive measuring mode. (For further information, see 8-3-2 6)
Specifying settings for COMPARE (Preparatory measuring) mode.)

PRD
(PREDICT: Predictive
measuring mode)

In predictive measuring mode, the intermediate results of drying are used to predict future changes and to
calculate the result and thereby shorten the measurement time. (For further information, see 8-3-2 7)
Specifying settings for PREDICT (Predictive measuring) mode)

TEMP
(Drying
temperature)

OOO

This parameter may be used to specify the drying temperature. The temperature may be set
anywhere within a range of from from 30C to 200C in 1-degree increments. (30C to 180C in 'TT'
mode) (For further information, refer to 8-1 Selecting Temperature Display Mode, 13. Temperature
Calibration and 8-3-3 TEMP (Drying temperature).)

BIAS

O.OO

This parameter is used to specify a numeric value to be used to correct measurements for bias. A bias
anywhere in the range of from 9.99% to 9.99% may be specified in 0.01% increments. (For further
information, see 8.3.4 Bias.)

MODE
(Measuring
mode)

8-3 Descriptions of Individual Measuring Condition Settings


For a detailed description of individual measuring condition settings, see the instructions in subsection 8-2-1
and subsequent subsections.
1 To start specifying measuring condition settings:
Press the CONDITION key at a time when the display shows a weight reading.
2 If any password other than the default password of 0000 has been specified, then a PASS message will be displayed in
the weight display area. When this message is displayed, follow the instructions in 9.2.7 Specifying a password, to enter
the password. If the password entered is incorrect, the display will return to the weight display.
3 Selecting individual measuring conditions:
First a CONDITIONS message will flash on the display. Pressing the SELECT key at this time causes the flashing item to
change in sequence from MODE TEMP BIAS CONDITIONS and back to MODE each time the key is pressed.
When the item you wish to specify is flashing, press the ENTER key. Specify the settings for that item.
4 To finish specifying measuring condition settings:
Pressing the CONDITION key when any settings item is flashing causes the settings specified to take effect and causes the
display to return to the normal weight display.

16

8-3-1 Selecting the CONDITIONS (Measuring conditions storage area)


Below is described the procedure used to select the area in which measuring conditions are saved.
This operation causes the measuring mode, drying temperature, bias, and other currently specified
measuring conditions to be saved to the selected area.
* At the time of shipment, the following settings are stored in measuring conditions storage areas 0~9:
Measurement standard
Drying temperature
Measuring mode

: Wet Base
: 120C
: Standard drying & Automatic ending mode (Change in water content
of 0.05% over 30seconds)

 Specifying settings for the CONDITIONS (Measuring conditions storage area)


Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
key,
key and ENTER key to enter the password. Follow
the
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

The CONDITIONS display area will begin to flash.


3

ENTER

Press the
key or
key to select a measuring conditions
area number from 0 to 9. In this example, area number 5 is
selected.

Press the ENTER key. This will cause control to move to the
measuring conditions area number and the number will flash.

ENTER

SELECT

7
CONDITION

When the desired measuring conditions area number starts


flashing, press the ENTER key. The selected measuring conditions
area number will change from a flashing to a constantly lit display
and the CONDITIONS message will begin to flash instead.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu. To exit from specifying measuring
conditions settings, press the CONDITION key instead.

17

8-3-2 Selecting the MODE (Measuring mode)

1) Specifying settings for AUTO (Standard dryingAutomatic ending) mode


In this mode, measuring is brought to a end whenever the change in
Measurement (%)
moisture content over two consecutive 30-second periods (i.e., over a
period of 1 minute) falls below the specified conditions for automatic
Change in
ending. Automatic ending conditions may be specified in 0.01-percent
moisture
increments anywhere in a range from 0.01 to 0.1 percent. Specifying a
smaller percentage causes measurements to closely approach a point of content M
equilibrium, but more time is required for measurement. Specifying a
higher percentage lessens the amount of time required for measurement,
but measuring is stopped while there is still a wide variation in
measurements. The automatic ending conditions should be specified in
accordance with your objectives and the type of sample being measured.
Step

Key(s) used

Display

30 seconds

Measuring time

The MODE (measuring mode) setting is used to specify the conditions under which measuring is to be
completed. As shown in the table in subsection 8.1 Types of Settings, the mode may be set to automatic
operation mode, timed operation mode, or any one of five other modes.

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
the
key,
key and ENTER key to enter the password. Follow
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

The CONDITIONS display area will begin to flash. Press the SELECT
key until MODE begins to flash.

With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until AUT begins to flash.

SELECT

ENTER

Since AUT will already be flashing at the point, proceed directly


to the next step.

When AUT begins to flash, press the ENTER key. This will cause the
automatic end conditions (i.e., amount of change in moisture
content per 30 seconds) setting to become active and it begins
flashing.
key or
key to select the automatic end
Press the
conditions. Note that here we specify a setting of 0.10 percent.

ENTER

SELECT

9
CONDITION

When the desired automatic end conditions setting flashes, press


the ENTER key. The automatic end conditions setting will change
from a flashing to a constantly lit display and MODE will begin to
flash again.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the setting to be specified. To exit from
specifying measuring conditions settings, press the CONDITION key
instead.

18

2) Specifying settings for TIME (Standard drying & Timed ending) mode
In this mode, the measuring time is specified beforehand. When the specified measuring time is reached,
measuring is ended.
Measuring time may be specified in 1-minute increments anywhere in a range from 1 to 240 minutes or
measuring may be specified to be performed over a continuous period of 12 hours.

Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
the
key,
key and ENTER key to enter the password. Follow
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

The CONDITIONS display area will begin to flash. Press the SELECT
key until MODE begins to flash.

With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until TIM begins to flash.

SELECT

If TIM is already flashing, then proceed directly on to the next


step.

ENTER

When TIM flashes, press the ENTER key. This will cause the
measuring time settings to become active and the currently
specified measuring time to flash.
Press the
key or
key to select the desired measuring time.
Note that here a time of 30 minutes is specified.

ENTER

SELECT

9
CONDITION

When the desired measuring time flashes, press the ENTER key. The
specified measuring time will change from a flashing to a
constantly lit display and MODE will begin to flash instead.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu. To exit from specifying measuring
conditions settings, press the CONDITION key instead.

19

3) Specifying settings for RAPID (High-speed drying) mode


High-speed drying mode is useful for measuring samples with high levels of moisture content.
In high-speed drying mode, the sample is dried at 180C until the change M in moisture content over a 30second period becomes lower than setting, then drying will be continued at the specified drying temperature.
The RAPID M threshold specifies when high speed drying (180C) will end.
The threshold of RAIPID M may be specified in 0.1-percent increments anywhere in a range from 0.1 to 9.9
percent.
*

The actual time may vary depending on the specified temperature, but it generally takes about 2 minutes for the
temperature control to automatically shift from 180C to the specified temperature.

While specifying a lower RAPID M threshold lessens the amount of time required for measurement,
depending on the sample it may become burned making it impossible to obtain an accurate measurement.
Specifying a higher threshold shortens the time over which a temperature of 180C is maintained and
reduces the effects of rapid drying.
Either AUTO (automatic ending) or TIME (timed ending) may be specified to define the conditions under
which measuring is to be ended.

Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
key,
key and ENTER key to enter the password. Follow
the
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

The CONDITIONS display area will begin to flash. Press the SELECT
key until MODE begins to flash.

With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until RPD begins to flash.

SELECT

ENTER

If RPD is already flashing, then proceed directly on to the next


step.

When RPD flashes, press the ENTER key. This will cause the
numeric field next to RPD begin to flash.

Press the
key or
key to select the desired RAPID M
threshold value. Note that here a value of 0.7% is specified.

ENTER

When the desired threshold begins to flash, press the ENTER key.
The threshold will then be set and control will shift to the selection
of the ending conditions. The units area for timed ending mode
(min) or automatic ending mode (%) will begin to flash.

20

Step

Key(s) used

SELECT

ENTER

ENTER

Pressing the SELECT key will cause the units to switch between
minutes (min) and a percentage (%). Press the SELECT key until the
desired units are displayed.
When the desired unit flashes, press the ENTER key. This will cause
control to shift to the specification of the ending conditions and the
numerical field begins to flash.

When the desired ending condition flashes, press the ENTER key.
The rapid drying temperature that was previously specified will
begin to flash.
(Default setting is 180C for 'TT' mode, 200C for 'ST' mode.)
key or
key to set the desired rapid drying
Press the
temperature. Note that here a temperature of 140C is set.

Operating instructions

Press the
key or
key to set the value of the desired ending
condition. Note that here the timed ending of 20 minutes has been
specified.

Display

ENTER

SELECT

E
CONDITION

When the desired temperature flashes, press the ENTER key. The
specified ending conditions will then change from flashing to a
constantly lit display and MODE will begin to flash.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu. To exit from specifying measuring
conditions settings, press the CONDITION key instead.

21

4) Specifying settings for SLOW (Low-speed drying) mode


In low-speed drying mode, the temperature is raised more gradually than when performing measurements
under standard drying conditions, taking about 5 minutes until the temperature reaches the specified drying
temperature.
Either AUTO (automatic ending mode) or TIME (timed ending mode) may be specified to define the
condition under which measuring is to be ended.

Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
key,
key and ENTER key to enter the password. Follow
the
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until MODE begins to flash.

With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and the
currently specified mode to begin flashing.
Press the SELECT key repeatedly until SLW begins to flash.

SELECT

ENTER

SELECT

ENTER

If SLW is already flashing, then proceed directly on to the next


step.

When SLW flashes, press the ENTER key. Control will then shift to
specification of low-speed drying mode settings where the ending
condition must be specified. The units area for timed ending
mode (min) or automatic ending mode (%) will begin to flash.
Pressing the SELECT key will cause the units to switch between
minutes (min) and percentage (%). Press the SELECT key
repeatedly until the desired unit is displayed.
When the desired unit for the ending condition begins to flash,
press the ENTER key. This will cause control to shift to the
specification of the ending condition and the numerical field begins
to flash.
key or
key to set the desired ending condition.
Press the
Note that here a time of 20 minutes has been specified.

ENTER

SELECT

A
CONDITION

When the desired time or percentage flashes, press the ENTER key.
The specified ending condition will then change from flashing to a
constantly lit display and MODE will begin to flash.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.

22

5) Specifying settings for STEP (Stepped drying) mode


In stepped drying mode it is possible to specify separate drying conditions for up to a maximum of 5 steps.
Specifying a separate drying temperature and measuring time for each step makes it possible to determine
the optimum drying conditions for any sample type.
In Step 1, timed ending mode must be specified as the ending condition. In Step 2 and subsequent steps, it
is possible to select between either automatic ending mode or timed ending mode.
*

If automatic ending mode is selected in Step 2 or later, that step becomes the final step. When timed ending
mode is selected and a value of 0 is specified as the measuring time, the previous timed ending step becomes
the final step.

Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
the
key,
key and ENTER key to enter the password. Follow
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until MODE begins to flash.

With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until STP begins to flash.

SELECT

ENTER

If STP is already flashing, then proceed directly on to the next


step.

When STP flashes, press the ENTER key. This will cause STP to
change from a flashing to a constantly lit display. Control will shift
to the specification of the measuring time for Step 1, and the
measuring time will flash.

key or
key to select the desired measuring time.
Press the
The measuring time may be specified in 1-minute increments in a
range anywhere from 1 to 240 minutes. Note that here a time of
20 minutes has been specified for Step 1.

When the desired measuring time flashes, press the ENTER key. The
measuring time will change from a flashing to a constantly lit
display, control will shift to the specification of the drying
temperature, and the drying temperature will begin to flash.

ENTER

key or
key to select the desired drying
Press the
temperature. The drying temperature may be specified in 1degree increments in a range from 30C to 200C (30C to 180C
in 'TT' mode). Note that here a temperature of 105C has been
specified for Step 1.

When the desired drying temperature flashes, press the ENTER key.
The step displayed will change from STP 1 to STP 2 and the
units area for timed ending mode (min) or automatic ending
mode (%) will begin to flash.

ENTER

23

Step

Key(s) used

SELECT

ENTER

Display

Operating instructions
Pressing the SELECT key will cause the units to switch between
minutes (min) and a percentage (%). Press the SELECT key until the
desired unit is displayed.
When the desired unit for the ending condition begins to flash,
press the ENTER key. This will cause control to shift to the
specification of the ending condition of Step 2 and the numerical
field will flash.
*

Note that this step becomes the final step if automatic ending
mode (i.e., a percentage) is specified here.

Press the
key or
key to select the desired ending
conditions. Note that here the timed ending at 20 minutes has
been specified. (Also note that if automatic ending mode has
been selected, a value from 0.01 to 0.1 percent may be specified
in 0.01-percent increments.
C

ENTER

Note that the previous step becomes the final step if timed
ending mode is selected and a measuring time of 0 is specified
here.

Note that continuous drying (i.e., a drying time of 12 hours)


cannot be specified in this mode. The maximum drying time for
each step is 240 minutes.

When the desired ending condition begin to flash, press the ENTER
key. This will cause the display of the ending condition to change
from a flashing to a constantly lit display, for control to shift to the
specification of the drying temperature for Step 2, and the drying
temperature will begin to flash.

key or
key to select the desired drying
Press the
temperature. Note that here a temperature of 100C has been
specified.

When the desired drying temperature is displayed, press the ENTER


key. The step displayed will change from STP 2 to STP 3 and
control will shift to the specification of ending condition. Go back
to step A and repeat all subsequent steps up to this step until
settings have been specified for all the drying steps.

.....

ENTER

ENTER

SELECT

H
CONDITION

When the settings for the final drying step have been specified,
MODE will begin to flash.

If you wish to specify other measuring conditions settings, press


the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.

24

Note: Read Section 12 before use of this part.


6) Specifying settings for COMPARE (Preparatory measuring) mode
Preparatory measuring mode is used to calculate the bias (i.e., the difference between the measurement
results which would be obtained in Standard drying & Automatic ending mode and predictive measuring
mode) needed for predictive measurements.
Prior to predictive measurements, this mode should be used first to seek the bias. (For further information,
see  Preparatory measuring mode and  Predictive measuring mode.)
Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
the
key,
key and ENTER key to enter the password. Follow
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until MODE begins to flash.

With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until CMP begins to flash.

SELECT

ENTER

If CMP is already flashing, then proceed directly on to the next


step.

When CMP flashes, press the ENTER key. CMP will change from a
flashing to a constantly lit display and you will next be required to
specify the predicted value convergence range settings (see 
Predicted value convergence range(section 12)). The current
setting for the predicted value convergence range will begin to flash.

key or
key to specify the desired value. Any
Press the
value of 0.1 to 9.9 percent in increments of 0.1 percent may be
specified. Note that here a value of 0.5% has been selected.

When the desired value is displayed, press the ENTER key. The
display of the predicted value convergence range will change from
a flashing to a constantly lit display, and control will shift to the
automatic ending settings, and the setting specifying the degree of
change in moisture content over a 30-second period will begin to flash.

ENTER

key or
key to select the desired automatic
Press the
ending condition. Automatic ending condition may be specified in
0.01-percent increments anywhere in a range from 0.01 to 0.1
percent. Note that here a value of 0.05% has been selected.

When the desired automatic ending condition has been selected,


press the ENTER key. The specified setting will change from a
flashing to a constantly lit display, and MODE will begin to flash.

ENTER

SELECT

A
CONDITION

If you wish to specify other measuring conditions settings, press


the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.

25

Note: Read Section 12 before use of this part.


7) Specifying settings for PREDICT (Predictive measuring) mode
Predictive measuring mode is used to predict the change in moisture content and calculate the predicted
final measurement before drying has been completed. Thus measuring time can be saved. Note that some
materials have properties which make it difficult to obtain accurate predictions. Measurements in preparatory
measuring mode must be performed to check the precision of measurement and determine the possible
effectiveness of Predictive Measurement in terms of shortening the measuring time.

Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
key,
key and ENTER key to enter the password. Follow
the
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until MODE begins to flash.

With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until PRD begins to flash.

SELECT

ENTER

If PRD is already flashing, then proceed directly on to the next


step.

When PRD flashes, press the ENTER key. PRD will then change
from a flashing to a constantly lit display and you will next be
required to specify the predicted value convergence range
settings (see  Predicted value convergence range). The
current setting for the predicted value convergence range will
begin to flash.
key or
key to select the desired automatic
Press the
ending condition. Automatic ending condition may be specified in
0.01-percent increments anywhere in a range from 0.1 to 9.9
percent. Note that here a value of 0.5% has been selected.

ENTER

SELECT

9
CONDITION

When the desired automatic ending condition has been selected,


press the ENTER key. The specified setting will change from a
flashing to a constantly lit display, and MODE will begin to flash.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.

26

8-3-3 TEMP (Drying temperature) Setting


The following describes the procedure to specify the drying temperature in conducting
measurements.
While the default drying temperature is 120C, depending on the type of sample, its moisture content,
or other conditions the proper drying temperature may vary. To find the proper drying temperatures
for different types of materials, conduct repeated measurements until you find the correct
temperature to use for each material.
The drying temperature may be set within the range from 30C to 200C (from 30C to 180C in 'TT'
mode) in 1-degree increments.
* Note that the drying temperature refers not to the temperature of the sample but the temperature of the
temperature sensor. The actual temperature of samples during drying may vary depending on the color
of the sample, its moisture content, or the type or form of the sample.
* Generally speaking, drying is performed more quickly when a higher drying temperature is specified,
but if the temperature specified is too high it might result in the sample becoming burned, thus making
it impossible to obtain accurate measurements.

 Specifying settings for the TEMP (Drying temperature)


Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
key,
key and ENTER key to enter the password. Follow
the
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

With the TEMP indicator flashing, press the ENTER key. This will
cause control to shift to specification of the drying temperature
and the currently specified drying temperature to begin to flash.
Press the
key or
key to select the desired drying
temperature. Note that here a temperature of 105C has been
specified.

The CONDITIONS display area will begin to flash. Press the SELECT
key until TEMP begins to flash

ENTER

SELECT

7
CONDITION

When the desired drying temperature flashes, press the ENTER key.
The display of the specified temperature will change from a
flashing to a constantly lit display and the TEMP indicator will
begin to flash instead.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.

27

8-3-4 Bias Setting


When necessary, measurements can be corrected with bias. A bias anywhere in the range of from
9.99% to 9.99% may be specified in 0.01% increments. A bias should be specified in cases such
as below described.
 There are cases where measurement results with the MOC-120H fail to meet with expected
(standard) values as moisture measurements are the result of various conditions. The bias may be
set to adjust the measured value by the MOC-120H to the expected (standard) value. Thus,the
measured value using the MOC-120H can be treated to be equivalent to the existing (standard)
measuring methed.
In most cases it is possible to match the expected (standard) values by optimizing the measuring
conditions, but when such conditions would cause the sample to be burned, cause the time
required too long, or result in other problems, a bias should be specified.

 When using more than one moisture balance unit, there may be cases where it is impossible to
obtain identical measurements even when the same measuring conditions are used because
of small differences in the surrounding environment. In such cases, set the bias of the unit that
is to serve as the standard to zero and set the bias of the other units set to account for any
such differences.
For information on how to specify the bias when operating in predictive measurement mode, see,
12-2-1 Calculating the bias to be specified when operating in predictive measurement mode.

 How to set the bias


Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the CONDITION key.

CONDITION

If a password has been specified, the message PASS will be


displayed to indicate that the password should be entered. Use
key,
key and ENTER key to enter the password. Follow
the
the instructions under step 7 in 9-2-7 Specifying a password to
set or delete a password.

SELECT

ENTER

With the BIAS indicator flashing, press the ENTER key. Control will
then shift to the bias specification, and the currently specified bias
value will begin to flash.
Press the
key or
key to select the desired bias. Note that
here a bias of 0.2% has been specified.

The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until BIAS begins to flash.

ENTER

SELECT

7
CONDITION

When the desired bias is displayed, press the ENTER key. The
display of the specified bias will change from a flashing to a
constantly lit display, and BIAS will begin to flash instead.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.

28

9. Menu Settings
MOC-120H provides the capability to specify and select between different measurement bases,
data output formats, and other menu settings. All desired settings should be specified before
conducting measurements.
The procedure used when changing menu settings is the same as the procedure used when
specifying menu settings for the first time. Note that menu settings are automatically internally
saved, and that there is no need to specify menu settings before each measurement.

9-1 Types of Menu Settings


Menu

Menu display (Menu items)

UNIT
(Measurement
base)

OUTPUT
(Measurement
data output)

Step 2

Step 1

minimum display (%)

MW (Wet base)
MD (Dry base)
SOL (Solid)

CAL
(Calibration)

0.01
0.1

Step 1

Step 2

Step 3

PC

30S (30 secs.)

(Output to computer)

1M (1 min.)

TBL (Output in
tabular format to printer)

2M (2 min.)

GRP (Output as

10M (10 min.)

.%

graph to printer)

FIN (Final result)

.%

5M (5 min.)



CODE
(Sample code)
DATE
(Date & time)

Description
Used to select one of three possible measurement bases.
It is also possible to switch % display.
(For further information, see 9-2-1 Selecting a
measurement base and switching % display)
Used to specify the format in which data is to be output to
a printer or computer. The user may select the external
device to which output is sent and the format in which
data is to be output.
When graph output (GRP) has been selected, it is also
possible to specify the minimum and maximum values to
be used in the range of measurements. (For further
information, see 9-2-2 Specifying the type and format of
output)
Used to specify the sample code to be output to printer or
computer. (For further information, see 9-2-3 Specifying
sample codes)

Step 1

Step 2

Step 3

Step 4

YMD

Year

Month/Day

Time

MDY

Month/Day

Year

Time

DMY

Day/Month

Year

Time

Used to set the internal clock. This date and time is output
as the Measurement time printed together with any
output data to a printer or computer. (For further
information, see 9-2-4 Setting the date and time)
Used to calibrate the balance. (For further information,
see 9-2-5 CAL (Balance calibration))

WCAL (Balance calibration)

* In addition to these settings, it is also possible to specify other settings such as the device ID (see 9-2-6
Specifying a device ID) or password (see 9-2-7 Specifying a password").

9-2 Descriptions of Individual Menu Items


Descriptions of individual menu items are given in subsection 9-2-1 and below.
Menu operation
1 Calling up menu settings: To call up menu settings, press the MENU key from the weight display.
2 Selecting individual menu items: When the MENU key is pressed, the menu item UNIT will light up. Pressing
the SELECT key here causes the menu item lit up to change from UNIT OUTPUT CODE DATE
CAL and back to UNIT in sequence each time the SELECT key is pressed. When the item for which you wish
to specify settings is displayed, press the ENTER key. The settings for the selected item may then be specified.
3 Exiting from menu settings: Pressing the MENU key when any menu item is currently lit up exits from menu
settings mode and returns to the regular weight display.

29

9-2-1 Selecting the measurement base and switching the % display


1) Selecting the measurement base

This menu item is used to specify what measurement base is to be used in measurements. There are
three different types of bases: wet base, dry base, and solid. The type of base specified should be
selected in accordance with the sample being measured.
Type

Menu display

Formula

Description

Wet Base

MW

WD
x 100 (%)
W

Percentage of evaporated moisture weight with


respect to the weight before drying.

Dry Base

MD

WD
x 100 (%)
D

Percentage of evaporated moisture weight with


respect to the weight after drying.

Solid

SOL

D
x 100 (%)
W

Percentage of residual weight after drying with


respect to the weight before drying.

Notation used in formulas:


W: Wet weight before measurement
D: Dry weight after measurement
(While measurement is being performed, the weight at each point in time is
used as the dry weight in calculating measurements.)
2) Switching the minimum display of percentage

This menu item is used to switch the minimum display of the measurement result between 0.1% and 0.01%.
 How to select a measurement base
Step

Key(s) used

MENU

Operating instructions
With the display displaying the weight in grams, press the
key.

MENU

The UNIT menu item will light up and the currently selected
measurement base will be displayed.

Display

ENTER

Press the ENTER key. This will cause control to shift to specification
of UNIT settings and for the currently selected measurement
base to begin to flash.

SELECT

Press the SELECT key until the desired measurement base is


displayed. The flashing item will change from MW MD
SOL and back to MW again in sequence each time the SELECT key
is pressed. Note that here wet base (MW) has been selected.

ENTER

SELECT

ENTER

SELECT

8
MENU

When the desired measurement base flashes, press the


The currently selected % display begins to flash.

ENTER

key.

Press the SELECT key until the desired % display is displayed. The
flashing item will change from 0.01 to 0.1 and back to 0.01
again in sequence each time the SELECT key is pressed. Note that
here % display (0.1) has been selected.
When the desired % display flashes, press the ENTER key. The
display of the selected measurement base will change from a
flashing to a constantly lit display and control will return to step 2.
If you wish to specify other menu settings, press the SELECT key to
select the desired menu item. If you wish to exit from specifying
menu settings, press the MENU key.

30

9-2-2 Specifying the type and format of output


The MOC-120H may be connected to the optional printer or computer so that measurement data can
be output.

1 There are three types of output formats as shown in the table below.
External device

Output format

Menu display

Description

Computer

Numeric

PC

This is the setting which should be selected


when using the Windows Direct Function or
some other software to output data through the
RS-232C interface.

Printer

Numeric

TBL

This setting causes numeric output to the


optional printer.

Graph

GRP

This setting causes graph output to the optional


printer.

2 Any one of the six output intervals shown below may be selected to specify the frequency at which output is
to be generated.
The output interval specifies the amount of time which is allowed to elapse during measurement before the
next set of output is generated. When there is no need to view intermediate data, FIN may be selected so
that only the final results are output.
*

FIN should never be selected when graph output has been selected when operating in preparatory measuring
mode as that would result in no predicted measurements being output.
Output interval

Menu display

Every 30 seconds

30S

Every minute

1M

Every 2 minutes

2M

Every 5 minutes

5M

Every 10 minutes

10M

Final results only

FIN

3 When graph output has been selected, it is possible to specify the maximum and minimum values of the
range of values to be measured in 5-percent increments.
Measurement base
Wet base (%), Solid (%)

Range of values to be measured


Minimum: From 0 to (Maximum 5%) (Specified in 5-percent increments; may be
set to any value from 0~95%.)
Maximum: From (Minimum +5%) to 100 (Specified in 5-percent increments; may
be set to any value from 5~100%.)

Dry base (%)

Minimum: From 0 to (Maximum 5%) (Specified in 5-percent increments; may be


set to any value from 0~495%.)
Maximum: From (Minimum +5%) to 500 (Specified in 5-percent increments; may
be set to any value from 5~500%.)

31

 How to specify the output format to be used


Step

Key(s) used

MENU

Display

Operating instructions
With the display displaying the weight in grams, press the
key.

MENU

Press the SELECT key until the OUTPUT menu item is displayed.
2

SELECT

ENTER

SELECT

ENTER

Press the ENTER key. This will cause control to shift to the output
settings and cause the currently selected output format to flash.

Press the SELECT key until the desired output format is displayed.
Pressing the SELECT key here causes the menu item lit up to change
from TBL GRP PC and back to TBL in sequence each
time the SELECT key is pressed. Note that here TBL has been
selected.
When the desired output format begins flashing, press the ENTER
key. This will cause control to shift to the specification of the
output interval and the currently specified interval flashes.

SELECT

Press the SELECT key until the desired output interval is displayed.
Pressing the SELECT key here causes the menu item lit up to change
from 30S 1M 2M 5M 10M FIN and back to
30S in sequence each time the SELECT key is pressed. Note that
here an interval of 1M has been selected.

ENTER

When the desired output interval flashes, press the ENTER key. The
next step to be performed here differs depending on the output
format specified in step 4.

SELECT

7
MENU

Procedure when TBL has been selected:


The currently specified output format will be displayed and the
control will return to the format step 2. If you wish to specify other
menu settings, press the SELECT key to select the desired menu. If
you wish to exit menu settings, press the MENU key.
Procedure when GRP has been selected:
Control will shift to the specification of the range of data output
(described in step 8 to B).

32

Specifying the range of measurement values to be used (when GRP has been selected)
Step

Key(s) used

Press the
key or
key until the desired lower limit is
displayed. Note that here a value of 5% has been selected.

ENTER

When the desired lower limit flashes, press the ENTER key. This will
cause the upper limit of the range of data output begin to flash.

Press the
key or
key until the desired upper limit is
displayed. Note that here a value of 20% has been selected.

ENTER

Operating instructions
The currently selected lower limit of the range of data output will
begin to flash.

Display

SELECT

MENU

When the desired upper limit flashes, press the ENTER key. The
currently specified output format will be displayed and the display
will return to the state shown in step 2.
If you wish to specify other menu settings, press the SELECT key. If
you wish to exit from specifying menu settings, press the MENU key.

33

9-2-3 Specifying sample codes


This section describes how to specify sample codes to be used when outputting measurements to
the optional printer or a computer. Sample codes may be specified as 4-character codes.
 Any digit from 0 to 9, and letter from A to Z, or a hyphen _ may be specified as the value of
the first or second character of the code.
 Only digits from 0 to 9 may be specified as the value of the third and fourth character and the
code.
* The digits in the third and fourth characters of the code are automatically increased by 1 after each
measurement, with the value returning to 00 when it would otherwise exceed a value of 99.

 How to specify sample codes


Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the MENU key.

MENU

Press the SELECT key until the CODE menu item is displayed.
2

SELECT

ENTER

Press the
key or
key to select a digit from 0 to 9 or a
letter from A to Z. Note that here A has been selected.

Press the ENTER key. Control will then shift to the specification of the
sample code and the first character of the currently selected
sample code will flash.

ENTER

ENTER

When the desired character has been displayed, press the ENTER
key. The first character will be fixed and the second character will
flash.
Repeat steps 4 and 5 until the fourth character has been
specified.
When the fourth character has been specified, press the ENTER key.
The sample code just specified will then be displayed and the
display will return to the step 2.

SELECT

If you wish to specify other menu settings, press the SELECT key.
To exit from specifying menu settings, press the MENU key instead.

MENU

34

9-2-4 Setting the date and time


This section describes how to set the date and time. Also note that the date and time of measurement are output whenever measurement data is output to the optional printer or a computer.

 How to set the date


Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the MENU key.

MENU

Press the SELECT key until the DATE menu item is displayed.
2

SELECT

ENTER

SELECT

ENTER

ENTER

ENTER

ENTER

ENTER

Press the ENTER key. This will cause control to shift to DATE output
format setting and the currently selected output format to be
displayed.

ENTER

SELECT

The output format will be displayed in the order YMD (year,


month, day, and time), MDY (month, day, year, and time), and
DMY (day, month, year, and time).

Press the SELECT key until the desired output format is displayed.
Each time the SELECT key is pressed the display will change from
YMD MDY DMY and back to YMD again. Note that here
YMD has been specified.
When the desired output format is displayed, press the ENTER key.
This will cause control to shift to the specification of the year and
the currently specified 2-digit value flashes. Press the
key or
key to display the correct 2-digit year.
Pressing the ENTER key causes the year to be set and control to shift
key or
key to
to the specification current month. Press the
select the correct 2-digit month.
Pressing the ENTER key causes the month to be set and control to
key or
key
shift to the specification of the date. Press the
to display the correct 2-digit day.
Pressing the ENTER key causes the date to be set and control to shift
to the specification of the 2-digit value for the hour. Press the
key or
key to select the correct 2-digit hour.
Pressing the ENTER key causes the hour to be set and control to shift
to the specification of the 2-digit value for the minutes. Press the
key or
key to select the correct 2-digit minutes.
Pressing the ENTER key causes the minutes to be set and only
DATE to be displayed. (The clock will start counting from 0
seconds from the moment when the ENTER key is pressed.)
If you wish to specify other menu settings, press the SELECT key.
To exit from specifying menu settings, press the MENU key instead.

MENU

35

9-2-5 CAL (Balance calibration)


The internal balance of the MOC-120H may be calibrated at two points: at the 0 and 100grams. The
MOC-120H may also be connected to a printer to make it possible to automatically generate
calibration records in compliance with GLP, GMP, and ISO standards.
* The power to the unit should be turned on at least 30 minutes before calibration is performed in order to
ensure accurate calibration.
* The MOC-120H is extremely sensitive to interference from drafts, breezes, vibration, and other
disturbances in the surrounding environment, and care should be taken to ensure that there is no such
interference before performing calibration.
* It is impossible to calibrate the balance accurately immediately after performing measurements or at
any other time when the heater lid is hot. Allow the temperature of the heater lid to cool down to
ambient temperature before performing calibration.
* The weights used should consist of standard OIML weights or some other type of non-magnetic Class 1
weights. (The use of Class E2 or Class E1 weights is recommended.)
* When placing the weight on the sample pan, it should be placed in the center of it.
* The heater lid must be closed during calibration to prevent influence of drafts or air flow, and the height
of the weights used should be such that they do not come into contact with the temperature sensor or
heater.
* If you wish to abort a calibration already in progress, press the TARE/RESET key. An Abort message will be
displayed and the display will return to the weight in grams.

 Scale calibration procedure


Step

Key(s) used

Display

Operating instructions
With the display of the weight in grams, press the MENU key.

MENU

Press the SELECT key until the CAL menu item is displayed.
2

SELECT

ENTER

SELECT

4
ENTER

ENTER

ENTER

Press the ENTER key. This will cause the calibration settings to be
displayed and the setting 100.000 to flash.

If you wish to change the value of the weight to be used, then


press the SELECT key. This will cause the displayed value to stop
key or
key to enter a value for
flashing. Next, press the
the weight. Pressing the ENTER key then causes the specified weight
value to flash.
Open the heater lid and place a calibration weight of the specified
weight value on sample pan. Closing the heater lid and pressing the
ENTER key causes - - - - to be displayed, 100-gram calibration to
come to an end, and then a flashing value of 0.000 to be
displayed.

With the value 0.000 flashing, open the heater lid and remove
the calibration weight.
Closing the heater lid and pressing the ENTER key causes - - - - to
be displayed, 0-point calibration to come to an end, and then an
END message to be displayed.
*

If the unit is connected to the optional printer, a calibration record


will be automatically printed out.

After a few seconds, the display will return to the regular weight
display.

36

9-2-6 Specifying a device ID


This section describes how to specify the device ID output when outputting data to the optional
printer or a computer. The device ID is an 8-character ID which may be set using the following
characters: digits from 0 to 9, letters from A to Z, and hyphens .

 How to specify a device ID


Step

Key(s) used
SELECT

Display

Operating instructions
From the weight display, press the SELECT key and hold the SELECT key
down while pressing the MENU key.

MENU

The first through fourth characters of the device ID will be


displayed with the first character flashing. The indicator id will be
displayed in the center of the display.

Press the
key or
key to select the desired character for
the first character (i.e., a digit from 0 to 9, a letter from A to Z, or
a hyphen). Note that here the letter A has been selected.

ENTER

ENTER

Repeat steps 3 and 4 until the fourth character has been


specified. Note that here ABCD has been specified.
When the fourth character has been specified, press the ENTER key.
The fifth through eighth characters of the device ID will then be
displayed with the first of these four characters flashing.

Just as with the first four characters, repeat steps 3 and 4 until
the eighth character has been specified. Note that here 123
has been specified.

When the desired character is displayed, press the ENTER key. The
first character will be specified and the second character will flash.

ENTER

When the eighth character has been specified, press the


The display will then return to the regular weight display.

37

ENTER

key.

9-2-7 Specifying a password


In order to prevent the specified measuring conditions from being modified unexpectedly, a password may be specified to prevent other users from changing the specified conditions. The password is 4 characters in length and may be set using the following characters: digits from 0 to 9,
letters from A to Z, and hyphen.
If any password other than the default password of 0000 is set, then whenever the CONDITION key is
pressed to specify measuring conditions PASS is displayed and the user is required to enter the
password.

 How to specify a password


Step

Key(s) used

Display

ENTER

Operating instructions
From the weight display, press the
down while pressing the MENU key.

ENTER

key and hold the

ENTER

key

MENU

The default password of 0000 will be displayed with the first


character of the password flashing. The indicator SEt will be
displayed in the weight display area.

Press the
key or
key to select the desired character (i.e., a
digit from 0 to 9, a letter from A to Z, or a hyphen). Note that here
the letter 1 has been selected.

ENTER

Repeat steps 3 and 4 until the fourth character has been


specified. Note that here a value of 1234 has been specified.

When the desired character is displayed, press the ENTER key. The
first character will be set and the second character will flash.

ENTER

When the fourth character has been specified, press the ENTER key.
The display will then return to the regular weight display.

[Deleting or modifying an existing password]

ENTER

7
MENU

ENTER

To delete or modify an existing password, press the ENTER key and


hold the ENTER key down while pressing the MENU key from the weight
display. The indicator PASS will be displayed in the weight
display area and the first character of the default password 0000
will begin to flash. Repeat steps 3 and 4 until you have entered
the current password.
When the 4-character password has been entered, press the ENTER
key. The indicator SEt will be displayed in the weight display
area. The value 0000 will be displayed in the password area with
the first character flashing; repeat steps 3 to 6 to specify a new
password.
To delete a password, enter 0000 as the new password.

38

10. Error Messages


If any of the following error messages is displayed, follow the procedures described below to
check for the cause and take appropriate action.
If the error cannot be removed, contact your Shimadzu representative.
Message

Action to be taken

Description
The protective sheet has not
been removed.

Remove protective sheet located under the pan supporter


column. (See item 3 in 6. Assembly and Installation of Main
Unit on p. 9 for instructions.)

The sample is too light (i.e.,


under 0.5 grams).

The minimum weight which may be measured by the MOC-120H


is 0.5 grams. Measure again using a sample with a weight of 0.5
grams or greater. Press the TARE/RESET key to make the error
message disappear.

The sample is too heavy (i.e.,


over 120 grams).

The maximum weight which may be measured by the MOC-120H


is 120 grams. Measure again using a sample with a weight of
120 grams or smaller. Press the TARE/RESET key to make the error
message disappear.

Er201

Invalid moisture content value


(Occurs when weight increases
by more than 0.1 grams)

This error is displayed when a sample is added during


measurement. Press the TARE/RESET key to make the error message
disappear.

Invalid moisture content value


(Occurs when weight being
measured is less than 1 grams)

Press the

Er202

Balance communications error

Turn off the power and then turn the power on again.

Invalid calibration weight

Use a calibration weight of the correct weight value.

Instability during balance


calibration

Perform balance calibration again with the MOC-120H placed on


a flat, stable surface not subject to the effects of external
vibration, drafts, or breezes.

Power error

Turn the power off, make sure that the power conversion switch
located on the back is set to the correct position.

Er102

Er103

Er104

Er401
Er501

Er502

Er701

TARE/RESET

key to make the error message disappear.

If any of the following errors are displayed, contact your Shimadzu representative.
Message
Er301
Er302
Er303

Er305
Er306
Er601
Er602
Er603
Er802

Description
Temperature sensor failure
Heater overheated
This error indicates the existence of an extremely hazardous condition. Turn the power off
immediately and contact your Shimadzu representative.
Heater control failure
Heater lid is open during measurement (for 15 sec.).
Lift mechanism failure

Internal clock failure

39

11. Precaution on Conducting Measurements


 Precaution on conducting multiple measurements in succession
Placing a sample on the sample pan which is already warm may cause moisture from the sample to
evaporate before measuring is begun and causes errors in measurement result. Always be sure to
use a cool sample pan when performing a subsequent measurement.
Allow an even amount of time to elapse between measurements, as errors may occur if the
temperature of the balance mechanism varies.
* Two sample pans and two sample pan handlers are provided for use when conducting multiple
measurements in succession.

 Use of sample pan and aluminum foil sheets


It is impossible to obtain accurate measurements if any of the last measured sample remains on the
sample pan. To avoid errors, either wipe the sample pan clear of any remaining sample (see 15.
Maintenance on p. 58 for further instructions) or use disposable aluminum foil sheets.
* Twenty disposable aluminum foil sheets are included with the unit.

 Quantity and placement of powdered, particulate and viscous sample materials


Samples cannot be heated properly if they are not placed flatly. Placing samples in mounds or in
layers of varying thickness may result in the highest points being burned. accurate measurements.
The precision of measurement improves when the samples are flatly and evenly placed and the
amount of sample are larger. However, too large sample amount results in uneven heating. Make
certain samples are placed correctly.
Proper placement

Incorrect placement

 Measuring liquid samples


Since most liquid samples harden and become sticky after drying, it is recommended to use the
aluminum foil sheets when measuring such samples. Note that the aluminum foil sheet is waterwettable, thus making it possible to obtain wide and even sample placement and effective in
shortening measuring times and obtaining accurate measurements.
Depending on the sample, the use of sand to speed up drying (Silica sand or ocean sand with a
mesh of 20 or so).

40

12. Predictive Measurements


12-1 A Description of Predictive Measuring
Electronic moisture balance can be used to measure the moisture content of a wide range of materials. This is the most important feature not found in other types of moisture testers.
However, because moisture balance operates by heating samples to evaporate the moisture content, it
takes a fair amount of time to obtain results. MOC-120H has a feature that not only reduces measuring
times but also brings the method to adjust partial drying measurement results to those obtained with a
standard method of measuring. The feature is called predictive measuring mode.
In predictive measurement:
(1) The final moisture content is predicted while drying is still in progress.
(2) Three additional settings must be specified before measuring: the drying temperature, the
predicted value convergence range, and bias.
(3) Only sample materials which produce what are usually referred to as S-shaped drying curves
can be measured.
The bias may also be used to correct for differences in measurements obtained with other moisture content testers.

 Drying temperature
Since the measurements obtained in predictive measuring mode are treated as comparable to the
measurements obtained by automatic operation mode, the drying temperature should be set to
the same temperature as in automatic operation mode.

 Predicted value convergence range


When measuring in predictive operating mode, the predicted values are internally calculated every
30 seconds, and while variation occurs in the calculated values the degree of variation becomes
smaller as time elapses. The range of variation in moisture content specified in order to confirm a
predicted value as the final is referred to as the predicted value convergence range. The MOC120H treats the predicted value as final when the range of variation falls within the predicted
value convergence range
The predicted value convergence range may be set to a value anywhere from 0.1 to 9.9 percent.
Specifying a higher value for the predicted value convergence range causes the final predicted
value to be determined quickly. On the other hand, the specification of a higher value may also
result in greater degree of error. It is possible to obtain more precise sets of predicted values by
specifying lower values. This takes longer to determine the final predicted value. The predicted
value convergence range should be specified according to your objectives. Note that the default
setting for the MOC-120H is a value of 0.5 percent.

 Bias
Bias is used to adjust the predictive measurement. On the MOC-120H, a bias of anywhere from
9.99 to +9.99 percent may be specified. When performing a preparatory (COMPARE) measurement, the MOC-120H automatically indicates the most appropriate bias to be used to correct
measurements to match those obtained in automatic operation mode.

 Bias can be used for correction against other methods


When seeking the bias to perform correction against another method, the bias should be reset to
zero and then a number of samples with known moisture contents have to be measured with
predictive measurements and the average difference between the known moisture contents and
the predicted moisture contents should then be specified as the bias.
41

 Preparatory measuring mode


In preparatory measuring mode, predicted measurements are displayed while measuring is in
progress and measuring is halted under the same conditions as when operating in automatic
operation mode. The difference between the measured values of automatic operation mode and
pedictive measuring mode is displayed as the necessary bias.
In order to obtain accurate predicted measurements, it is recommended to perform at least 5
preparatory measurements and take the average to determine the bias.
You should also take care in terms of the amount of the sample and the way the sample material
is placed onto the sample pan. They must be the same every time and laid out as evenly as
possible.

 Predictive measuring mode


Prior to predictive measurements, specify the same drying temperature, predicted value convergence range, and bias as calculated from preparatory measurements.
Note that measuring is halted if no predicted measurement has been calculated after 30 minutes
have elapsed after starting the measurement.

42

12-2 Procedure for Obtaining Predicted Measurements


1) Use preparatory measuring mode to obtain the appropriate bias value for the predictive measurement. (See 12-2-1 Calculating the bias to be specified when operating in predictive measurement mode for instructions.)
2) Use the bias obtained in preparatory measuring mode in step 1) to perform the measurement,
and evaluate the predicted measurement. (See 12-2-2 Evaluating predicted measurements
for instructions.)
3) Measure in predictive measuring mode. (See 12-2-3 Preforming predictive measurements for
instructions.)

12-2-1 Calculating the bias to be specified when operating in predictive measurement mode
Step

Display

Operating instructions
Set the mode to preparatory measuring mode. (See 8-2-2 6) Specifying
settings for preparatory measuring mode for instructions.)

Specify the desired predicted value convergence range. In the example shown
here, a range of 0.5% is specified.
2

Note that the predicted value convergence range specified affects the amount of
time required for measurement and the accuracy of predictive measurements,
and that you should specify a range according to your objectives.

Specify the automatic halting conditions to be used (e.g., 0.05%).

Specify the drying temperature to be used. (For further information, see 8-2-3
TEMP (Drying temperature).) In the example shown here, a temperature of
120C is specified.
Set the bias to 0.00%. (See 8-2-4 Bias for further information.)

.....

Place the sample onto the sample pan and begin measurement. (In the
example shown here, the initial weight is 10.478 grams.)
6

.....

When the final predicted value has been calculated, it will be displayed. (In the
example shown here, the measuring time was 7 minutes and the predicted
measurement is 15.8 percent.)

43

Step

Operating instructions

Display

Completion of measurement
Measuring will be completed when the conditions specified for automatic
operation mode have been met. When measuring is completed, the bias will be
displayed in the bias display area.
8

[Measurement results]
Bias is + 0.60 (= 16.40 (Automatic operation mode value) 15.80 (Predicted
measurement))
Automatic operation mode measurement
Predicted measurement

Without changing any of the conditions used in steps 1 through 5, repeat


steps 6 through 8 to measure again 5 times or more and calculate the
average bias.
The average bias may then be used to specify the bias to be used in predictive
measuring mode.
*

If the bias varies greatly from one time to the next when performing repeated
measurements, predicted measurement cannot be obtained, and you should
measure in automatic operation mode or in some other mode instead.

If you wish to use the calculated bias to evaluate predicted measurements,


follow the procedure described in 12-2-2 Evaluating predicted measurements.
If you wish to use the calculated bias to actually perform predictive
measurements, follow the procedure described in 12-2-3 Performing predictive
measurements.

44

12-2-2 Evaluating predicted measurements


Step

Display

Operating instructions
With the mode set to preparatory measuring mode, set the bias obtained by
the procedure described in 12.2.1. In the example shown here, a bias of 0.60
percent has been specified. (For information on how to set the bias, see 8-2-4
Bias.)
*

Do not change any other settings (i.e., the predicted value convergence range
and drying temperature) at this time.

.....

Place the sample onto the sample pan and begin measurement. (In the
example shown here, the initial weight is 10.478 grams.)
2

....

When the predicted measurement result has been obtained, a predicted


measurement adjusted by the specified bias (here a bias of 0.60%) will be
displayed. (In the example shown here, the measuring time was 7 minutes and
the predicted measurement is 16.10 percent.)

Completion of measurement
Measuring will be completed when the conditions specified for automatic
operation mode have been met.
Measurement results
Bias is + 0.90
4

( = 16.40 (Automatic operation mode value) 15.50 (Predicted measurement when


*

bias is 0.))
Note that the specified bias (0.60%) does not affect the bias displayed here.

Automatic operation mode measurement


Predicted measurement adjusted using specified bias of 0.60%
= 15.50 (i.e., predicted measurement when bias is 0) + 0.60 (i.e., specified bias)

Without changing any of the specified in step 1, repeat steps 2 through 4 to


measure again 5 times or more and obtain a comparison of the values between
automatic operation mode and predictive measurement mode.
If the difference between the two sets of values is within an allowable range,
then the specified bias may be judged to be an appropriate one. If the
difference between the two sets of values exceeds allowable levels, then the
average bias from the comparison just performed should be calculated and
specified as the new bias. The evaluation process should be performed again.
*

If the difference between the two sets of values exceeds allowable levels and
the bias varies sharply over repeated measurements, it is assumed that
predictive measurement cannot be properly performed. You should measure in
automatic operation mode or in some other mode instead.

45

12-2-3 Preforming predictive measurements


Step

Display

Operating instructions
Set the mode to predictive measuring mode. Refer to 8.2.2 7 Specifying
settings for PREDICT (Predictive measuring) mode for instructions.

Specify the same settings for the predicted value convergence range and
drying temperature as those used in preparatory measuring mode (subsections
12.2.1 and 12.2.2).
Example:
Predicted value convergence range: 0.5%
Drying temperature:
120C

Set the bias obtained through the procedures described in 12.2.1 and 12.2.2
(shown here as 0.60%). (See 8-2-4 Biasfor setting.)

.....

Place the sample onto the sample pan and begin measurement. (In the
example shown here, the initial weight is 10.213 grams.)
4

Completion of measurement
The predicted measurement will then be displayed.

46

13. Temperature Calibration (Option required)


Temperature calibration can be performed with the optional temperature calibration kit. The
calibration record meeting with GLP/GMP/ISO requirements can be automatically produced
with the optional printer.

Caution
Do not touch heater cover and the sensor probe or holder of temperature calibration kit during
temperature calibration as they become very hot. Touching these parts may cause serious burning.
 The environmental conditions such as ambient temperature and air movement affect temperature calibration.
Perform temperature calibration without surrounding air movement and under the same conditions as when
performing measurements.
 Press the TARE/RESET key to discontinue a once started temperature calibration. "Abort" is displayed and it returns to
the weight display.
 For the operation of digital thermometer of temperature calibration kit, refer to its instruction manual.

Installation of Temperature Calibration Kit (Option)


1 Assembling temperature calibration kit:
Insert the sensor probe into the brackets on the
holder as shown in the figure.
Place the end of sensor probe in the bracket in
holders center.

Holder
Sensor probe

Brackets

2 Open heater cover and place the temperature


calibration kit over the sample pan as shown in the
figure.
(Fit the hole of holder to stay of main unit as shown in
the figure.)

Hole

Stay

3 Confirm heater cover is completely closed and sensor


probe is fitting in the notch of heater cover.
Notch

47

Temperature calibration procedure


The following temperature calibration procedure can be entered only when 'ST' mode is selected
as temperature display mode (Refer to 8.1). Verify that the C symbol in the display is blinking,
which indicates that currently selected mode is 'ST' mode.
Install temperature calibration kit and switch on digital thermometer in advance.
Step

Key(s) used

Display

Operating instructions
Press the MENU key at the weight display.

MENU

Press the SELECT key repeatedly until 'CAL' is displayed.


2

SELECT

Press the
3

ENTER

key. 'BAL' is displayed.

ENTER

Press the SELECT key repeatedly until 'TEMP' is displayed.


4

SELECT

ENTER

Press the ENTER key. It moves to the display for inputting the
temperature for temperature calibration, and "100C" blinks.

Make up the figure of the desired temperature for temperature


,
keys. Select a temperature close to
calibration with the
the most frequently used temperature. Temperature from 50C to
180C can be selected. Note that the set temperature here is the
heater temperature*.

Verify heater cover is completely closed. Then, press the [START]


key. It heats it up to the temperature that the heater set for the
calibrating to begin. Turn on the temperature display of the
temperature calibration kit.

START/STOP

START/STOP

The temperature in heater cover reaches stability in about 15


minutes. Press START/STOP key when both temperatures on the main
unit and digital thermometer have been stabilized.
Input the temperature indicated on the digital thermometer with
,
keys.
the

Press ENTER key. First "-----", and then "END" is displayed.


Temperature calibration is then complete.
0

ENTER

The temperature calibration report is automatically output if the


optional printer or a computer is connected.
Wait until it returns to the weight display automatically.
A

* Select a temperature about 20C lower than the sample position temperature. Set 80C if 100C at the sample
position is desired.

48

14. Printing Output to a Printer (Option)


The MOC-120H may be connected to the optional printer to output measurement data. Output
includes data consisting of intermediate or final measurements, sample codes, and measurement times.

14-1 Printer Output Sample


 Output of final results of more than one measurement
[Tabular output (TBL)]
Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D207300000
Device ID
: ABCD-123
Time of measurement : 2003/08/08
Measuring conditions storage area : 0
Measurement standard : Wet base
Temperature display mode : Output only when
'ST' mode is selected
Measurement mode : Automatic operation mode
Drying temperature : 110C
Automatic ending conditions : 0.05%

Sample code
Time of measurement
Measured value (%)

Signature title
* When the measurement is complete, press
the ENTER key. This will cause it to be printed.

[Graph output (GRP)]

Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D207300000
Device ID
: ABCD-123
Time of measurement : 2003/08/08
Measuring conditions storage area : 0
Measurement standard : Dry base
Measurement mode : Timed operation mode
Drying temperature : 110C
Measurement time : 10 mins.

Sample code
Time of measurement
Measurement graph

49

 Output of the intermediate and final values of a single measurement


[Tabular output (TBL)]

Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D207300000
Device ID
: ABCD-123
Sample code
: C-01
Date & time of measurement : 2003/08/08, 15:24
Measuring conditions storage area : 0
Measurement standard : Dry base
Temperature display mode : Output only when
'ST' mode is selected
Measurement mode : Preparatory measuring mode
Drying temperature : 110C
Automatic ending conditions : 0.05%
Predicted value convergence range : 0.5

Elapsed measuring time


Changes in drying temperature
Changes in weight
Measured value (%)

Predicted measurement

* Note on the decimal precision of printed weight data


Although the minimum weight which may be displayed by the MOC-120H is 0.001 grams, weights are
printed to a precision of 4 decimal points because the values printed consist of averages from 7
measurements taken over each 30-second interval for each set of weight data output.

50

 Output of the intermediate and final values of a single measurement


[Graph output (GRP)]
Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D207300000
Device ID
: ABCD-123
Sample code
: B-20
Date & time of measurement : 2003/08/08, 15:07
Measuring conditions storage area : 0
Measurement standard : Dry base
Temperature display mode : Output only when
'ST' mode is selected
Measurement mode : Preparatory measuring mode
Drying temperature : 110C
Automatic ending conditions : 0.05%
Predicted value convergence range : 0.5
Wet Mass

: 5.6892g

Elapsed measuring time


Changes in drying temperature
Measured value (%)

Predicted measurement

Dry Mass

51

: 4.8637g

 Output of report of balance calibration

Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D207300000
Device ID
: ABCD-123
Date & time of measurement : 2003/08/08, 15:17
Reference
Before calibration
After calibration
Signature title

: 100.000g
: 100.004g
: 100.000g

Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D412345678
Device ID
: 00000000
Date & time of measurement : 2004/11/22, 16:09
Reference
Before calibration
After calibration
Signature title

: 105C
: 101C
: 105C

14-2 Outputting Stored Measurement Data


The MOC-120H can store up to 100 sets of previous measurements data, and the stored data can
be output to the optional printer or a computer. To output this data:
1 Follow the directions given on p. 31 in 9-2-2 Specifying the type and format of output to set
the output format to either TBL or PC.
2 From the weight display, press the SELECT key and hold the SELECT key down while pressing the START/STOP
key.
3 The data will then be output in order beginning from the most recently measured data. To stop
printing while printing is still in progress, press the START/STOP key.

52

15. Computer Interface


The RS-232C interface may be used to connect the MOC-120H to a computer.

15-1 RS-232C Interface Specifications


Interface type

: RS-232C

Communications method : Asynchronous communication


Baud rate

: 2400 bps

Data bits

: 8 bits

Parity

: None

Stop bits

: 1 bit

Connector

: Female D-SUB9 pins

Pin assignment

:
5

4
9

Pin number

Direction

3
8

2
7

1
6

Description
Not used

Output

TXD

Input

RXD

Not used

GND

Not used

Not used

Not used

Not used

Frame

Shield

53

15-2 Setting Up and Transmitting Data


15-2-1 Connecting the RS-232C cable
With the power to the MOC-120H and the computer both turned off, connect the RS-232C cable.
Connect the RS-232C cable to the RS-232C port located at the rear of the MOC-120H and tighten
the screws at both sides of the connector. Follow the same procedure to connect the RS-232C
cable to the computer. If the MOC-120H has been moved, make sure that the MOC-120H is
readjusted the level. (See 6. Assembly and Installation of Main Unit on p. 9 for instructions.)

15-2-2 MOC-120H settings


Turn on the power to the MOC-120H and set the measurement data output format to PC. (See
9-2-2 Specifying the type and format of output on p. 31 for instructions.)

15-2-3 Setting Up the Computer


(leave the balance unplugged)
1 Turn ON the power to the computer and start
Windows*.
2 Click Start, choose Settings, and Control
Panel.
3 Select Accessibility Options.
4 Verify that there are no check marks for any items
on all five tabs including General.

5 Put a check mark at Support Serialkey device in


the General tab. This should be the only check
mark on all the tabs of Accessibility Options unless
Administrative options appears in the General
tab. Put check marks at both the items of Administrative options to maintain the settings even after
restarting Windows.
6 Open Settings.
7 Select the serial port corresponding to the RS232C port of your personal computer. (Serial port:
any one of COM1 to 4. Usually, COM1)

54

8 Select a Baud rate of 300.


9 Click OK.
10 Click Apply and wait.
11 Click OK.

55

15-2-4 Starting Up the Computer


Turn on the power to the computer and when Windows has started up open the Microsoft Excel or
whatever software is to be used to read in data.
* For instructions on how to use your computer, operating system (Microsoft Windows), or software
being used, see the user manuals provided with them.
* The Microsoft Windows name and logo are the trademarks and registered trademarks of Microsoft
Corporation.

56

15-3 Computer Output Format


Interface type

: RS232C

Numeric output format : JIS (ASCII)


Delimiter code

: 0x09 (tab)

Delimiter

: 0x0D (CR) + 0x0A(LF)

 Title output format at time of start of measurement


(Underscore characters (i.e., ) are used below to indicate blanks (i.e., 20 in hexadecimal)
_SHIMADZU-CORP + delimiter
_Model_:_MOC-120H + delimiter
_SN_:_ + _XX (10-byte Serial No.) + delimiter
_ID_:_ + _XX (8-byte ID) + delimiter
_Date/Time_:_ + XX (2-byte year) + . + XX (2-byte month) + . + XX (2-byte day) + / +
XX (2-byte hour) + : + XX (2-byte minutes) + delimiter
_Condition_:_ + X (1-byte condition number) + delimiter
_Unit_:_ + Wet Base Moist. or Dry Base Moist. or Solid Content + delimiter
"_Temp_mode_:_"+"Sample_plate_tem.," (Output only when 'ST' mode is selected)
 Automatic operation format
_Mode_:_Auto
_Setting Temp._:_ + XXX (3-byte temperature setting) delimiter
_Auto Stop Cond._:_ + X.XX (4-byte automatic ending conditions setting) + delimiter
 Timed operation format
_Mode_:_Time
_Setting_Temp._:_ + XXX (3-byte temperature setting) + delimiter
_Drying_Time_:_ + XXX (3-byte drying time setting) + delimiter
 High-speed drying format
_Mode_:_Rapid
_Setting_Temp._:_ + XXX (3-byte temperature setting) + delimiter
Automatic operation: Auto Stop Cond._:_ + X.XX (4-byte automatic ending conditions
setting) + delimiter
Timed operation: Drying Time_:_ + XXX (3-byte drying time setting) + delimiter
_Delta M_:_ + X.X (3-byte 200C maintenance condition setting) + delimiter
 Low-speed drying format
_Mode_:_Slow
_Setting Temp._:_ + XXX (3-byte temperature setting) + delimiter
Automatic operation: Auto Stop Cond._:_ + X.XX (4-byte automatic ending conditions
setting) + delimiter
Timed operation: Drying Time_:_ + XXX (3-byte drying time setting) + delimiter

57

 Stepped mode format


_Mode_:_Step
tab + Temp + tab + Time + delimiter
The following output then appears the same number of times as the number of specified steps:
_Step + X (1-byte step number) + tab + XXX (3-byte temperature setting) + tab +
XXX (3-byte drying time setting) + delimiter
 Comparative mode format
_Mode_:_Compare
_Setting Temp._:_ + XXX (3-byte temperature setting) + delimiter
_Auto Stop Cond._:_ + X.XX (4-byte automatic halting conditions setting) + delimiter
_Pred. Tol._:_ + X.X (Predicted value convergence range) + delimiter
 Predictive mode format
_Mode_:_Predict
_Setting Temp._:_ + XXX (3-byte temperature setting) + delimiter
_Auto Stop Cond._:_ + X.XX (4-byte automatic halting conditions setting) + delimiter

 Measurement output format


tab + Time (min.) + tab + Temp. (C) + tab + Weight (g) + tab + Moist (%) + delimiter

 Intermediate measurement output format


tab + XXX.X (5-byte measuring time) + tab + XXX (3-byte sample pan temperature) + tab +
XXX.XXXX (8-byte sample weight) + tab + Moisture content XXX.XX (6-byte moisture content)
+ delimiter

 Final measurement output format


* + tab + XXX.X (5-byte measuring time) + tab + XXX (3-byte sample pan temperature) + tab
+ XXX.XXXX (8-byte sample weight) + tab + Moisture content XXX.XX (6-byte moisture content) + delimiter

58

16. Maintenance
16-1 Performing Maintenance
Turn the power off and disconnect the power cable. Allow the heater and other parts
cool down to ambient temperature before performing maintenance.

Removing and reinstalling parts and components


Remove the sample pan, then the sample pan handler, sample pan supporter, and wind shield in
this order.
See 6. Assembly and Installation of Main Unit on p. 9 for instructions on how to install parts and
components.

(1) Wipe away any dust or residue of spilled samples.

(2) Maintenance of the main unit


 Use a soft, dry cloth to wipe away any dirt or soil.
 Avoid applying strong pressure when wiping even if you find dirt or soiling difficult to remove.
 If you find it particularly difficult to remove dirt or soiling, wet a cloth in water or in water with a
small amount of neutral detergent, wring the cloth thoroughly, and wipe. Next, rinse the cloth in
water and wring it out to remove any detergent and wipe again and then allow to dry.

(3) Maintenance of parts and accessories


 Remove the spoon, spatula, sample pan, and wind shield from the main unit and wash in water
with a soft sponge.
 Reattach to the main unit and wait until they completely dry before using the unit again.

* When using detergents, be sure to follow the instructions for use provided with the detergent.
* Never use paint thinner, benzene, or any volatile cleaning agents or any abrasive cleansers or
polishes.
* Never use wire brushes or other hard cleaning tools.

59

16-2 Replacing Fuses


1 Turn the power off and disconnect the power cord from the unit.
2 The fuse holder is located at the rear of the unit. Insert a slot screwdriver or similar
tool from the top of the fuse holder and pull the fuse holder towards you.
3 Remove the fuses from the fuse holder and check if any are burned out.
4 If there are no burned-out fuses, return the fuse holder to its original position. Replace burned-out fuse(s) with spare fuse(s) (8A).
5 Return the fuse holder to its original position in the main unit.
6 Insert the power cord back into the main unit.
*

Should the fuse(s) blow out repeatedly after replacement, contact your Shimadzu
representative.

60

17. Parts List


Standard Accessories
Item

Part number

Sample Pan

321-63314

Sample Pan Handler

321-63315

Wind Shield

321-63316

Sample Pan Supporter

321-63317

Spoon Spatula Set

321-63318

Fuse, 8A, 2 pcs Set

321-63319

Description

Aluminum Foil Sheet 10 pcs Set

See below for order

Protection Cover

See below for order

Optional Accessories and Consumables List


Item

Part number

Description

Electronic Printer (W/O AC Adapter)

321-64125

AC Adapter should be separately


ordered. Connection cable and
Thermal Printer Paper 1 roll are
included.

AC Adapter 120V

321-63306-05

For Electronic Printer.

AC Adapter 230V

321-63306-04

For Electronic Printer.

Thermal Printer Paper (10 roll set)

321-63306-08

RS-232C Cable

321-63308

Temperature calibration kit

321-64130

Aluminum Foil Sheet 500 pcs set

321-63320-02

Protection Cover 5 pcs set

321-64193

Digital thermometer (321-64136)

61

Holder (321-64131)

 Specifications of Printer cable and RS-232C communication cable

Printer cable P/N:321-63307

MOC-120H

Printer Side

Side

D-sub9P

D-sub9P

Plug

Plug

4
5

4
SIGNAL
GND

RS-232C Cable P/N:321-63308


MOC-120H

PC Side

Side

D-sub9P

D-sub9P

Socket

Plug

4
5

6
SIGNAL
GND

62

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