Moc IM
Moc IM
Moc IM
DEC. 2008
INSTRUCTION MANUAL
ELECTRONIC MOISTURE BALANCE
MOC-120H
RequestsFPL950701
Provide this manual to the next user in the event that the instrument is transferred.
To ensure safe operation, contact your Shimadzu Balance representative for installation, adjustment, or
reinstallation after moving the instrument to a different site.
NoticesFPL950701
The content of this manual is subject, without notice, to modifications for the sake of improvement.
Every effort has been made to ensure that the content of this manual was correct at the time of creation. However,
in the event that any mistakes or omissions are discovered, it may not be possible to correct them immediately.
The copyright of this manual is owned by Shimadzu Corporation. Reproduction and duplication of whole or part of
the content without permission of the company are strictly prohibited.
"Microsoft", "Windows", "Windows Vista" and "Excel" are registered trademarks of Microsoft Corporation of the
U.S.A. in the United States and other countries. All other company names and product names that appear in this
manual are trademarks or registered trademarks of the companies concerned. Note that TM and indications are
not used.
The company names, organization names and product names in this manual are trademarks or registered
trademarks of the companies and organizations concerned.
Shimadzu does not guarantee that the WindowsDirect communication function will operate without problems on all
PCs. Shimadzu will accept no responsibility for any trouble that arises as a result of using this function. You are
recommended to back up all important data and programs in advance.
Declaration of Conformity
Manufacturers Name:
SHIMADZU CORPORATION
Analytical & Measuring Instruments Division
1, Nishinokyo-Kuwabara-cho, Nakagyo-ku,
Address :
II
Contact Shimadzu service representative when the equipment has reached the
end of its life.
They will advise you regarding the equipment take-back.
With your co-operation we are aiming to reduce contamination from waste electronic and
electrical equipment and preserve natural resource through re-use and recycling.
Do not hesitate to ask Shimadzu service representative, if you require further information.
WEEE Mark
III
The following symbols are used in this operating manual and product to prevent accidents from occurring as a result of
improper usage or handling. The meaning of each symbol is as described below.
Warning
Failure to observe these items may lead to death or injury to the user.
Caution
Failure to observe these items may lead to injury to the user or damage to property.
Note
Items which the user should be aware of in order to use the unit safety.
Caution Symbols
Fire Hazard
Burn Hazard
Electric Shock
Hazard
Prohibition Symbols
Prohibited
Do Not
Do not Expose
Disassemble
to Water
Warning
Fire Hazard
Do not attempt to measure samples which may undergo dangerous chemical reactions when heated as doing so
may result in explosion or release of toxic gas.
Do not place flammable materials near the electronic moisture balance.
Some parts of the electronic moisture balance become extremely hot during operation and could lead to fire if
flammable materials are placed nearby.
The heater inside the Electronic Moisture Balance reaches temperatures higher than the preset sample-heating
temperature.
The surface of the quartz tube of the heater reaches approximately 500C (900F) even during normal
measurements. In addition, the nickel-chromium resistance wire inside the heater reaches approximately 900C
(1700F) and is not airtight.
Never use with any power source for which the product was not designed.
Application of excessively high voltage may result in overheating to malfunction or fire.
Do not attempt to disassemble, modify or rebuild the electronic moisture balance.
Doing so may result in accident, electric shock, etc. If you believe the unit may be malfunctioning contact to an
authorized Shimadzu representative.
Do not allow the unit to come in contact with water.
The electronic moisture balance is not waterproof. Do not allow water or other liquids to get into the units enclosure
as this may lead to electric shock or malfunction.
Caution
Burn Hazard
Do not touch the heat-dispersing component of the heater cover or sample pan with your bare hands, as doing so
might result in burns.
This electronic moisture balance is at high temperature during and immediately after making measurements,
When touching the unit, only use the specified control knobs and accessories.
IV
Do not measure any sample which might explode, ignite or produce toxic substances under high temperature.
Do not measure any sample which might cause chemical reaction under high temperature.
Do not measure any sample of unknown property.
Do not measure any sample whose surface hardens or solidifies by heating causing high inner pressure.
Immediately turn the power off if the sample should catch fire during measurement.
Use with adequate ventilation and appropriate venting for sample type.
Emergency Stop
[Start/Stop] key is always effective during measurement. Press it immediately when any danger or abnormality occurs.
VI
Others
After a power outage, turn the power back ON.
When a power outage occurs, the power is shut off automatically. Therefore, once turn off the power switch, then
begin operation from 7.1 "Turn on the power switch" ( page 12) again.
Do not connect anything other than peripheral devices specified by Shimadzu to the moisture balance's connector.
If you do, the balance may stop working normally.
In order to avoid trouble, always connect peripheral devices in accordance with the directions in this manual.
If you detect anything abnormal (e.g. a burning smell) disconnect the AC power cord immediately.
Continuing to use the balance with an abnormality could lead to fire or an electric shock.
VII
Contents
1. Introduction............................................................................................... 1
2. Description of Features and Principles of Operation ................................. 2
2-1 Principles of Operation ............................................................................................. 2
2-2 Features ................................................................................................................... 2
2-3 Applications (i.e., materials which can be measured) ............................................. 2
3. Specifications ........................................................................................... 3
4. Names of Individual Parts and Components ......................................... 4
4-1 Names of Parts of Main Unit .................................................................................... 4
4-2 Parts and Accessories .............................................................................................. 5
8-3-2
8-3-3
8-3-4
9-2-2
9-2-3
9-2-4
9-2-5
9-2-6
9-2-7
1. Introduction
Thank you for choosing the Shimadzu Electronic Moisture Balance MOC-120H. MOC-120H has high
reliability by employing the UniBloc cell, introduced for use in electronic balances by Shimadzu in 1989.
It provides WindowsDirect functions for transfer of measurement results to personal computer without
installing software. This and other various functions can be used to meet the operator's objectives.
In order to make full use of the functions and performance provided in the MOC-120H, please read this
instruction manual before using the balance and keep the manual for future reference.
For information on the following points, please contact your Shimadzu Balance representative.
Product warranty
After service
2-2 Features
UniBloc sensor
The core mechanism of the internal precision balance is the UniBloc*1 cell which provides excellent responsiveness,
temperature characteristics, and shock resistance. This UniBloc*1 sensor ensures excellent reliability in moisture
content measurements over a long period of use.
Data memory
The MOC-120H is able to store up to 100 pieces of measurement data in memory, making it possible to output large
batches of data all at one time.
Printer port
The MOC-120H is equipped with a printer port which may be used to connect to the optional printer, thus making it
possible to print out text or graph data showing final measurements or intermediate drying states while performing
measurements.
The ability to display changes in moisture content (M) in a numeric and bar graph display
The change M in moisture content over 30-second intervals is displayed in a numeric and bar graph display, thus
making it easier to estimate when a measurement should be completed. This feature is also useful in helping to
determine measurement completion conditions.
3. Specifications
Measurement format
: Evaporation weight loss method (Heat drying and weight loss method)
Sample weight
: 0.5g - 120g
Minimum display
Measurable quantities
Heater temperature range : May be set within a range of 30 to 200C in 1C increments (sample
position temperature)
Display
External output
: RS-232C interface
Communications
Power supply
Power consumption
: Maximum of 640W
Items included
Optional equipment
*1 When using Shimadzu standard samples and measuring conditions. It is not applied to and not
garanteed with all samples or conditions.
Heater lid
Heater
Temperature sensor
Wind shield
Sample pan
Sample pan handler
Display
Level
Control panel
Power switch
Power inlet
RS-232C port
Fuse holder
Wind shield
Power cord
Instruction manual
Protection Cover
5-1 Display
1 2 3 D
0
4
G
Item
Name
Description
Stability indicator
Heater indicator
This indicator lights up when measuring has been completed after performing a preparatory
measurement.
Displays individual menu items in sequence each time the SELECT key is pressed after pressing the MENU key.
Flashes to display individual items in sequence each time the SELECT key is pressed after pressing the
CONDITION key. Values may be specified for a given item when it is flashing.
Displays the reference number of the currently selected measuring conditions program.
Displays the conditions for convergence of measured values when operating in predictive or
comparative mode. When operating in high-speed drying mode, used to display the conditions required
in order to maintain a temperature of 180C.
Displays the currently selected end conditions. When the value is displayed as a percentage, it indicates
that measuring will end automatically, and when value is displayed in minutes, it indicates that
measuring will end when the specified amount of time is reached.
Bias display*
Moisture/Solid/Weight display
When measuring weight (i.e., when in idling mode), used to display the weight in grams. When
performing measurements, used to display the moisture content and solids content as percentages.
When measuring weight, this display is also used to display oL (overload) when the weight exceeds
the maximum measurable weight and to display oL (negative overload) when the weight does not
reach the minimum measurable weight.
Temperature display
When 'TT' mode is selected, displays the temperature near the heater with C symbol illuminated. When
'ST' mode is selected, displays the sample position temperature with C symbol blinking.
*Refer to 8.1 for the details of 'ST' and 'TT' modes.
Displays the change M in moisture (or solid) content at 30-second intervals during measurement.
Displays the change M in moisture (or solid) content in scalar format. The scale may display a
maximum change of 2 percent/30 seconds.
* Items marked with an asterisk display as flashing items during condition setting.
MENU CONDITION
SELECT
Name
START/STOP
ENTER
TARE/RESET START/STOP
Operation
Used to start measuring or to abort a measuring operation.
Also used to turn off the alarm which sounds to indicate that a measuring operation has been
completed.
START/STOP key
TARE/RESET
TARE/RESET key
ENTER
ENTER key
Used to display the selectable items or for setting values during menu selection or condition setting.
SELECT
SELECT key
Used for numerical settings.
Pressing the
key causes the value to increase, and pressing the
decrease.
UP key / DOWN key
Used to enter and exit the measuring condition setting mode.
CONDITION
CONDITION key
Used to enter and exit the menu selection mode.
MENU
MENU key
Height
adjustment
legs
Level
Bubble
8
Wind shield
Knobs
Round
holes
Stays
Round hole
Pan supporter
column
Grooves
Stay
100V
120V
10
220V
240V
Note: This setting must be done according to the power voltage available at the installation site.
Key(s) used
Display
Operating instructions
Turn on the power while holding the MENU key pressed down.
C-1
MENU
Note that you should not remove your finger from the MENU key
until a string of hyphens - - - - - are displayed.
Turn on power
A tone will sound, the display will light up with all items lit and then
change to display first CHE5 and then a string of hyphens (i.e., - - - -). At the bottom left of the display will be displayed the
currently specified power voltage.
C-2
C-4
C-5
SELECT
ENTER
.....
C-3
A tone will then sound and the display will return to the regular
weight display.
11
Operating instructions
Display
Once the power voltage setting has been spcified (Step ~ in 6.), when the
power is turned on for the second or subsequent times, a tone will sound,
the display will light up with all items lit, the display will change to display
CHE4, CHE3, , CHE0 while the currently specified power setting is
displayed, and then a tone will sound again and the display will change to
weight reading display mode.
Note: It is recommended that you always turn on about half an hour before
use in order to obtain consistent measurements.
2 Specifying settings
When performing measurements for the first time or when you wish to
change current settings before measuring, you should specify the settings
required for measuring at this time. (See 8. Specifying Measuring
Conditions on p. 15 and 9. Menu settings on p. 29 for instructions on how
to do so.)
If you have already place the sample pan and handler into place as described in
6. Assembly and Installation of Main Unit, then proceed directly to the next
step.
When using an aluminum foil sheet or other wrapping material because of the
nature of the sample being measured, place it on top of the sample pan.
12
Operating instructions
Display
4 Performing a reset
Close the lid of the heater, check to make sure that the stability indicator ()
is being displayed, and then press the TARE/RESET key.
When ----- and TARE appear on the display, the sample pan moves
upward and downward. When a tone rings, then the reset is completed and
the display returns to 0.000 g .
*
Always be sure that the heater lid is closed when performing a reset. Also make
sure that the tester is not exposed to drafts or breezes or subjected to any
vibrations when a reset is being performed.
6 Beginning measurement
Close the lid of the heater, check to make sure that the stability indicator ()
is being displayed, and then press the START/STOP key. The display will switch
from a display of the weight (i.e., grams) to a percentage display and the
measuring time will be displayed.
The heating indicator ( ) will start to flash and drying will begin.
*
There may be times when the stability indicator () is not displayed because of
external vibrations or drafts or breezes. While it is possible to perform
measurements at such times, there may be cases when it is impossible to
obtain accurate measurements at such times, and you should accordingly
always be sure to conduct measurements in a location as free as possible of
vibrations, drafts, breezes, or any other harmful influences.
*
*
13
Operating instructions
Display
Taring is performed automatically once per minute (or once every 30 seconds
when near the end of the measuring time) while measuring moisture content.
key.
8 Completion of measurement
When the measuring operation has been completed, the heating indicator
( ) will disappear, the measurement completed indicator ( ) will be
displayed, and a tone will ring for a period of 10 seconds. To turn off the
tone earlier, press the START/STOP key.
The results of the measurement will be displayed and remain on the display.
Pressing the ENTER key at this point causes Signature title to be printed. (See
14-1 Printer Output Sample)
9 Resetting the display
Pressing the TARE/RESET key at this point causes the display of the results of the
measurement (i.e., moisture content) to disappear and be replaced by a
display of the weight of the sample after drying.
*
Note that a reset cannot be performed until the completion tone has stopped
ringing.
Note that the sample and sample pan may be very hot and you should
accordingly be careful in handling them at this time.
14
Key(s) used
SELECT
1
CONDITION
Display
Operating instructions
From the weight display, press SELECT key first and while holding it
down, press CONDITION key and keep pressing both keys for about 5
seconds.
Currently selected temperature display mode is indicated as
either 'TT' or 'ST' at the M display part.
SELECT
ENTER
The temperature display mode selected here is effective for all measurement modes.
Indication of currently set mode:
In the display, the C symbol blinks when the current setting is 'ST' mode and when the current
setting is 'TT' mode, the C symbol is illuminated without blinking.
15
Display during
specification of setting
Description
CONDITION 0~9
(Measuring conditions
storage areas 0~9)
Used to select the area to store condition settings. There are 10 storage areas labeled from 0 to 9. (See 8-31 Selecting the CONDITIONS (Measuring conditions storage area).)
AUT
(AUTO: Standard drying &
Automatic ending mode)
In automatic operation mode, measuring is brought to a end whenever the change in moisture content over
two consecutive 30-second periods falls below the specified conditions for automatic ending. (For further
information, see 8-3-2 1) Specifying settings for AUTO (Automatic ending) mode.)
TIM
(TIME: Standard drying &
Timed ending mode)
In timed operation mode, measuring is ended when the elapsed time reaches the specified measuring time.
(For further information, see 8-3-2 2) Specifying settings for TIME (Timed operation) mode.)
RPD
(RAPID: High-speed drying
mode)
In high-speed drying mode, the sample is dried at a temperature of 180C until the amount of change in
moisture content over a 30-second interval falls below a specified value and then drying is continued at a
specified drying temperature. (For further information, see 8-3-2 3) Specifying settings for RAPID (Highspeed drying) mode.)
SLW
(SLOW: Low-speed drying
mode)
In low-speed drying mode, the temperature is raised more gradually than when performing measurements
under normal conditions, taking about 5 minutes from the time when measuring begins until the temperature
reaches the specified drying temperature. (For further information, see 8-3-2 4) Specifying settings for SLOW
(Low-speed drying) mode.)
STP
(STEP: Stepped drying
mode)
In stepped drying mode it is possible to specify a separate drying temperature and separate measuring time
over up to 5 step intervals. (For further information, see 8-3-2 5) Specifying settings for STEP (Stepped
drying) mode.)
CMP
(COMPARE: Preparatory
measuring mode for
Predictive mode)
Preparatory measuring mode is used for determining the bias (i.e., the difference between the measurement
corresponding to that obtained in automatic operation mode and the predicted measurement value) needed in
order to perform measurements in predictive measuring mode. (For further information, see 8-3-2 6)
Specifying settings for COMPARE (Preparatory measuring) mode.)
PRD
(PREDICT: Predictive
measuring mode)
In predictive measuring mode, the intermediate results of drying are used to predict future changes and to
calculate the result and thereby shorten the measurement time. (For further information, see 8-3-2 7)
Specifying settings for PREDICT (Predictive measuring) mode)
TEMP
(Drying
temperature)
OOO
This parameter may be used to specify the drying temperature. The temperature may be set
anywhere within a range of from from 30C to 200C in 1-degree increments. (30C to 180C in 'TT'
mode) (For further information, refer to 8-1 Selecting Temperature Display Mode, 13. Temperature
Calibration and 8-3-3 TEMP (Drying temperature).)
BIAS
O.OO
This parameter is used to specify a numeric value to be used to correct measurements for bias. A bias
anywhere in the range of from 9.99% to 9.99% may be specified in 0.01% increments. (For further
information, see 8.3.4 Bias.)
MODE
(Measuring
mode)
16
: Wet Base
: 120C
: Standard drying & Automatic ending mode (Change in water content
of 0.05% over 30seconds)
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
ENTER
Press the
key or
key to select a measuring conditions
area number from 0 to 9. In this example, area number 5 is
selected.
Press the ENTER key. This will cause control to move to the
measuring conditions area number and the number will flash.
ENTER
SELECT
7
CONDITION
17
Key(s) used
Display
30 seconds
Measuring time
The MODE (measuring mode) setting is used to specify the conditions under which measuring is to be
completed. As shown in the table in subsection 8.1 Types of Settings, the mode may be set to automatic
operation mode, timed operation mode, or any one of five other modes.
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
The CONDITIONS display area will begin to flash. Press the SELECT
key until MODE begins to flash.
With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until AUT begins to flash.
SELECT
ENTER
When AUT begins to flash, press the ENTER key. This will cause the
automatic end conditions (i.e., amount of change in moisture
content per 30 seconds) setting to become active and it begins
flashing.
key or
key to select the automatic end
Press the
conditions. Note that here we specify a setting of 0.10 percent.
ENTER
SELECT
9
CONDITION
18
2) Specifying settings for TIME (Standard drying & Timed ending) mode
In this mode, the measuring time is specified beforehand. When the specified measuring time is reached,
measuring is ended.
Measuring time may be specified in 1-minute increments anywhere in a range from 1 to 240 minutes or
measuring may be specified to be performed over a continuous period of 12 hours.
Step
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
The CONDITIONS display area will begin to flash. Press the SELECT
key until MODE begins to flash.
With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until TIM begins to flash.
SELECT
ENTER
When TIM flashes, press the ENTER key. This will cause the
measuring time settings to become active and the currently
specified measuring time to flash.
Press the
key or
key to select the desired measuring time.
Note that here a time of 30 minutes is specified.
ENTER
SELECT
9
CONDITION
When the desired measuring time flashes, press the ENTER key. The
specified measuring time will change from a flashing to a
constantly lit display and MODE will begin to flash instead.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu. To exit from specifying measuring
conditions settings, press the CONDITION key instead.
19
The actual time may vary depending on the specified temperature, but it generally takes about 2 minutes for the
temperature control to automatically shift from 180C to the specified temperature.
While specifying a lower RAPID M threshold lessens the amount of time required for measurement,
depending on the sample it may become burned making it impossible to obtain an accurate measurement.
Specifying a higher threshold shortens the time over which a temperature of 180C is maintained and
reduces the effects of rapid drying.
Either AUTO (automatic ending) or TIME (timed ending) may be specified to define the conditions under
which measuring is to be ended.
Step
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
The CONDITIONS display area will begin to flash. Press the SELECT
key until MODE begins to flash.
With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until RPD begins to flash.
SELECT
ENTER
When RPD flashes, press the ENTER key. This will cause the
numeric field next to RPD begin to flash.
Press the
key or
key to select the desired RAPID M
threshold value. Note that here a value of 0.7% is specified.
ENTER
When the desired threshold begins to flash, press the ENTER key.
The threshold will then be set and control will shift to the selection
of the ending conditions. The units area for timed ending mode
(min) or automatic ending mode (%) will begin to flash.
20
Step
Key(s) used
SELECT
ENTER
ENTER
Pressing the SELECT key will cause the units to switch between
minutes (min) and a percentage (%). Press the SELECT key until the
desired units are displayed.
When the desired unit flashes, press the ENTER key. This will cause
control to shift to the specification of the ending conditions and the
numerical field begins to flash.
When the desired ending condition flashes, press the ENTER key.
The rapid drying temperature that was previously specified will
begin to flash.
(Default setting is 180C for 'TT' mode, 200C for 'ST' mode.)
key or
key to set the desired rapid drying
Press the
temperature. Note that here a temperature of 140C is set.
Operating instructions
Press the
key or
key to set the value of the desired ending
condition. Note that here the timed ending of 20 minutes has been
specified.
Display
ENTER
SELECT
E
CONDITION
When the desired temperature flashes, press the ENTER key. The
specified ending conditions will then change from flashing to a
constantly lit display and MODE will begin to flash.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu. To exit from specifying measuring
conditions settings, press the CONDITION key instead.
21
Step
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until MODE begins to flash.
With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and the
currently specified mode to begin flashing.
Press the SELECT key repeatedly until SLW begins to flash.
SELECT
ENTER
SELECT
ENTER
When SLW flashes, press the ENTER key. Control will then shift to
specification of low-speed drying mode settings where the ending
condition must be specified. The units area for timed ending
mode (min) or automatic ending mode (%) will begin to flash.
Pressing the SELECT key will cause the units to switch between
minutes (min) and percentage (%). Press the SELECT key
repeatedly until the desired unit is displayed.
When the desired unit for the ending condition begins to flash,
press the ENTER key. This will cause control to shift to the
specification of the ending condition and the numerical field begins
to flash.
key or
key to set the desired ending condition.
Press the
Note that here a time of 20 minutes has been specified.
ENTER
SELECT
A
CONDITION
When the desired time or percentage flashes, press the ENTER key.
The specified ending condition will then change from flashing to a
constantly lit display and MODE will begin to flash.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.
22
If automatic ending mode is selected in Step 2 or later, that step becomes the final step. When timed ending
mode is selected and a value of 0 is specified as the measuring time, the previous timed ending step becomes
the final step.
Step
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until MODE begins to flash.
With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until STP begins to flash.
SELECT
ENTER
When STP flashes, press the ENTER key. This will cause STP to
change from a flashing to a constantly lit display. Control will shift
to the specification of the measuring time for Step 1, and the
measuring time will flash.
key or
key to select the desired measuring time.
Press the
The measuring time may be specified in 1-minute increments in a
range anywhere from 1 to 240 minutes. Note that here a time of
20 minutes has been specified for Step 1.
When the desired measuring time flashes, press the ENTER key. The
measuring time will change from a flashing to a constantly lit
display, control will shift to the specification of the drying
temperature, and the drying temperature will begin to flash.
ENTER
key or
key to select the desired drying
Press the
temperature. The drying temperature may be specified in 1degree increments in a range from 30C to 200C (30C to 180C
in 'TT' mode). Note that here a temperature of 105C has been
specified for Step 1.
When the desired drying temperature flashes, press the ENTER key.
The step displayed will change from STP 1 to STP 2 and the
units area for timed ending mode (min) or automatic ending
mode (%) will begin to flash.
ENTER
23
Step
Key(s) used
SELECT
ENTER
Display
Operating instructions
Pressing the SELECT key will cause the units to switch between
minutes (min) and a percentage (%). Press the SELECT key until the
desired unit is displayed.
When the desired unit for the ending condition begins to flash,
press the ENTER key. This will cause control to shift to the
specification of the ending condition of Step 2 and the numerical
field will flash.
*
Note that this step becomes the final step if automatic ending
mode (i.e., a percentage) is specified here.
Press the
key or
key to select the desired ending
conditions. Note that here the timed ending at 20 minutes has
been specified. (Also note that if automatic ending mode has
been selected, a value from 0.01 to 0.1 percent may be specified
in 0.01-percent increments.
C
ENTER
Note that the previous step becomes the final step if timed
ending mode is selected and a measuring time of 0 is specified
here.
When the desired ending condition begin to flash, press the ENTER
key. This will cause the display of the ending condition to change
from a flashing to a constantly lit display, for control to shift to the
specification of the drying temperature for Step 2, and the drying
temperature will begin to flash.
key or
key to select the desired drying
Press the
temperature. Note that here a temperature of 100C has been
specified.
.....
ENTER
ENTER
SELECT
H
CONDITION
When the settings for the final drying step have been specified,
MODE will begin to flash.
24
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until MODE begins to flash.
With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until CMP begins to flash.
SELECT
ENTER
When CMP flashes, press the ENTER key. CMP will change from a
flashing to a constantly lit display and you will next be required to
specify the predicted value convergence range settings (see
Predicted value convergence range(section 12)). The current
setting for the predicted value convergence range will begin to flash.
key or
key to specify the desired value. Any
Press the
value of 0.1 to 9.9 percent in increments of 0.1 percent may be
specified. Note that here a value of 0.5% has been selected.
When the desired value is displayed, press the ENTER key. The
display of the predicted value convergence range will change from
a flashing to a constantly lit display, and control will shift to the
automatic ending settings, and the setting specifying the degree of
change in moisture content over a 30-second period will begin to flash.
ENTER
key or
key to select the desired automatic
Press the
ending condition. Automatic ending condition may be specified in
0.01-percent increments anywhere in a range from 0.01 to 0.1
percent. Note that here a value of 0.05% has been selected.
ENTER
SELECT
A
CONDITION
25
Step
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until MODE begins to flash.
With the MODE display flashing, press the ENTER key. This will
cause control to shift to measuring mode selection and for the
currently specified measuring mode to begin flashing.
Press the SELECT key repeatedly until PRD begins to flash.
SELECT
ENTER
When PRD flashes, press the ENTER key. PRD will then change
from a flashing to a constantly lit display and you will next be
required to specify the predicted value convergence range
settings (see Predicted value convergence range). The
current setting for the predicted value convergence range will
begin to flash.
key or
key to select the desired automatic
Press the
ending condition. Automatic ending condition may be specified in
0.01-percent increments anywhere in a range from 0.1 to 9.9
percent. Note that here a value of 0.5% has been selected.
ENTER
SELECT
9
CONDITION
26
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
With the TEMP indicator flashing, press the ENTER key. This will
cause control to shift to specification of the drying temperature
and the currently specified drying temperature to begin to flash.
Press the
key or
key to select the desired drying
temperature. Note that here a temperature of 105C has been
specified.
The CONDITIONS display area will begin to flash. Press the SELECT
key until TEMP begins to flash
ENTER
SELECT
7
CONDITION
When the desired drying temperature flashes, press the ENTER key.
The display of the specified temperature will change from a
flashing to a constantly lit display and the TEMP indicator will
begin to flash instead.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.
27
When using more than one moisture balance unit, there may be cases where it is impossible to
obtain identical measurements even when the same measuring conditions are used because
of small differences in the surrounding environment. In such cases, set the bias of the unit that
is to serve as the standard to zero and set the bias of the other units set to account for any
such differences.
For information on how to specify the bias when operating in predictive measurement mode, see,
12-2-1 Calculating the bias to be specified when operating in predictive measurement mode.
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the CONDITION key.
CONDITION
SELECT
ENTER
With the BIAS indicator flashing, press the ENTER key. Control will
then shift to the bias specification, and the currently specified bias
value will begin to flash.
Press the
key or
key to select the desired bias. Note that
here a bias of 0.2% has been specified.
The CONDITIONS display area will begin to flash. Press the SELECT
key repeatedly until BIAS begins to flash.
ENTER
SELECT
7
CONDITION
When the desired bias is displayed, press the ENTER key. The
display of the specified bias will change from a flashing to a
constantly lit display, and BIAS will begin to flash instead.
If you wish to specify other measuring conditions settings, press
the SELECT key to select the menu.
To exit from specifying measuring conditions settings, press the
CONDITION key instead.
28
9. Menu Settings
MOC-120H provides the capability to specify and select between different measurement bases,
data output formats, and other menu settings. All desired settings should be specified before
conducting measurements.
The procedure used when changing menu settings is the same as the procedure used when
specifying menu settings for the first time. Note that menu settings are automatically internally
saved, and that there is no need to specify menu settings before each measurement.
UNIT
(Measurement
base)
OUTPUT
(Measurement
data output)
Step 2
Step 1
MW (Wet base)
MD (Dry base)
SOL (Solid)
CAL
(Calibration)
0.01
0.1
Step 1
Step 2
Step 3
PC
(Output to computer)
1M (1 min.)
TBL (Output in
tabular format to printer)
2M (2 min.)
GRP (Output as
.%
graph to printer)
.%
5M (5 min.)
CODE
(Sample code)
DATE
(Date & time)
Description
Used to select one of three possible measurement bases.
It is also possible to switch % display.
(For further information, see 9-2-1 Selecting a
measurement base and switching % display)
Used to specify the format in which data is to be output to
a printer or computer. The user may select the external
device to which output is sent and the format in which
data is to be output.
When graph output (GRP) has been selected, it is also
possible to specify the minimum and maximum values to
be used in the range of measurements. (For further
information, see 9-2-2 Specifying the type and format of
output)
Used to specify the sample code to be output to printer or
computer. (For further information, see 9-2-3 Specifying
sample codes)
Step 1
Step 2
Step 3
Step 4
YMD
Year
Month/Day
Time
MDY
Month/Day
Year
Time
DMY
Day/Month
Year
Time
Used to set the internal clock. This date and time is output
as the Measurement time printed together with any
output data to a printer or computer. (For further
information, see 9-2-4 Setting the date and time)
Used to calibrate the balance. (For further information,
see 9-2-5 CAL (Balance calibration))
* In addition to these settings, it is also possible to specify other settings such as the device ID (see 9-2-6
Specifying a device ID) or password (see 9-2-7 Specifying a password").
29
This menu item is used to specify what measurement base is to be used in measurements. There are
three different types of bases: wet base, dry base, and solid. The type of base specified should be
selected in accordance with the sample being measured.
Type
Menu display
Formula
Description
Wet Base
MW
WD
x 100 (%)
W
Dry Base
MD
WD
x 100 (%)
D
Solid
SOL
D
x 100 (%)
W
This menu item is used to switch the minimum display of the measurement result between 0.1% and 0.01%.
How to select a measurement base
Step
Key(s) used
MENU
Operating instructions
With the display displaying the weight in grams, press the
key.
MENU
The UNIT menu item will light up and the currently selected
measurement base will be displayed.
Display
ENTER
Press the ENTER key. This will cause control to shift to specification
of UNIT settings and for the currently selected measurement
base to begin to flash.
SELECT
ENTER
SELECT
ENTER
SELECT
8
MENU
ENTER
key.
Press the SELECT key until the desired % display is displayed. The
flashing item will change from 0.01 to 0.1 and back to 0.01
again in sequence each time the SELECT key is pressed. Note that
here % display (0.1) has been selected.
When the desired % display flashes, press the ENTER key. The
display of the selected measurement base will change from a
flashing to a constantly lit display and control will return to step 2.
If you wish to specify other menu settings, press the SELECT key to
select the desired menu item. If you wish to exit from specifying
menu settings, press the MENU key.
30
1 There are three types of output formats as shown in the table below.
External device
Output format
Menu display
Description
Computer
Numeric
PC
Printer
Numeric
TBL
Graph
GRP
2 Any one of the six output intervals shown below may be selected to specify the frequency at which output is
to be generated.
The output interval specifies the amount of time which is allowed to elapse during measurement before the
next set of output is generated. When there is no need to view intermediate data, FIN may be selected so
that only the final results are output.
*
FIN should never be selected when graph output has been selected when operating in preparatory measuring
mode as that would result in no predicted measurements being output.
Output interval
Menu display
Every 30 seconds
30S
Every minute
1M
Every 2 minutes
2M
Every 5 minutes
5M
Every 10 minutes
10M
FIN
3 When graph output has been selected, it is possible to specify the maximum and minimum values of the
range of values to be measured in 5-percent increments.
Measurement base
Wet base (%), Solid (%)
31
Key(s) used
MENU
Display
Operating instructions
With the display displaying the weight in grams, press the
key.
MENU
Press the SELECT key until the OUTPUT menu item is displayed.
2
SELECT
ENTER
SELECT
ENTER
Press the ENTER key. This will cause control to shift to the output
settings and cause the currently selected output format to flash.
Press the SELECT key until the desired output format is displayed.
Pressing the SELECT key here causes the menu item lit up to change
from TBL GRP PC and back to TBL in sequence each
time the SELECT key is pressed. Note that here TBL has been
selected.
When the desired output format begins flashing, press the ENTER
key. This will cause control to shift to the specification of the
output interval and the currently specified interval flashes.
SELECT
Press the SELECT key until the desired output interval is displayed.
Pressing the SELECT key here causes the menu item lit up to change
from 30S 1M 2M 5M 10M FIN and back to
30S in sequence each time the SELECT key is pressed. Note that
here an interval of 1M has been selected.
ENTER
When the desired output interval flashes, press the ENTER key. The
next step to be performed here differs depending on the output
format specified in step 4.
SELECT
7
MENU
32
Specifying the range of measurement values to be used (when GRP has been selected)
Step
Key(s) used
Press the
key or
key until the desired lower limit is
displayed. Note that here a value of 5% has been selected.
ENTER
When the desired lower limit flashes, press the ENTER key. This will
cause the upper limit of the range of data output begin to flash.
Press the
key or
key until the desired upper limit is
displayed. Note that here a value of 20% has been selected.
ENTER
Operating instructions
The currently selected lower limit of the range of data output will
begin to flash.
Display
SELECT
MENU
When the desired upper limit flashes, press the ENTER key. The
currently specified output format will be displayed and the display
will return to the state shown in step 2.
If you wish to specify other menu settings, press the SELECT key. If
you wish to exit from specifying menu settings, press the MENU key.
33
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the MENU key.
MENU
Press the SELECT key until the CODE menu item is displayed.
2
SELECT
ENTER
Press the
key or
key to select a digit from 0 to 9 or a
letter from A to Z. Note that here A has been selected.
Press the ENTER key. Control will then shift to the specification of the
sample code and the first character of the currently selected
sample code will flash.
ENTER
ENTER
When the desired character has been displayed, press the ENTER
key. The first character will be fixed and the second character will
flash.
Repeat steps 4 and 5 until the fourth character has been
specified.
When the fourth character has been specified, press the ENTER key.
The sample code just specified will then be displayed and the
display will return to the step 2.
SELECT
If you wish to specify other menu settings, press the SELECT key.
To exit from specifying menu settings, press the MENU key instead.
MENU
34
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the MENU key.
MENU
Press the SELECT key until the DATE menu item is displayed.
2
SELECT
ENTER
SELECT
ENTER
ENTER
ENTER
ENTER
ENTER
Press the ENTER key. This will cause control to shift to DATE output
format setting and the currently selected output format to be
displayed.
ENTER
SELECT
Press the SELECT key until the desired output format is displayed.
Each time the SELECT key is pressed the display will change from
YMD MDY DMY and back to YMD again. Note that here
YMD has been specified.
When the desired output format is displayed, press the ENTER key.
This will cause control to shift to the specification of the year and
the currently specified 2-digit value flashes. Press the
key or
key to display the correct 2-digit year.
Pressing the ENTER key causes the year to be set and control to shift
key or
key to
to the specification current month. Press the
select the correct 2-digit month.
Pressing the ENTER key causes the month to be set and control to
key or
key
shift to the specification of the date. Press the
to display the correct 2-digit day.
Pressing the ENTER key causes the date to be set and control to shift
to the specification of the 2-digit value for the hour. Press the
key or
key to select the correct 2-digit hour.
Pressing the ENTER key causes the hour to be set and control to shift
to the specification of the 2-digit value for the minutes. Press the
key or
key to select the correct 2-digit minutes.
Pressing the ENTER key causes the minutes to be set and only
DATE to be displayed. (The clock will start counting from 0
seconds from the moment when the ENTER key is pressed.)
If you wish to specify other menu settings, press the SELECT key.
To exit from specifying menu settings, press the MENU key instead.
MENU
35
Key(s) used
Display
Operating instructions
With the display of the weight in grams, press the MENU key.
MENU
Press the SELECT key until the CAL menu item is displayed.
2
SELECT
ENTER
SELECT
4
ENTER
ENTER
ENTER
Press the ENTER key. This will cause the calibration settings to be
displayed and the setting 100.000 to flash.
With the value 0.000 flashing, open the heater lid and remove
the calibration weight.
Closing the heater lid and pressing the ENTER key causes - - - - to
be displayed, 0-point calibration to come to an end, and then an
END message to be displayed.
*
After a few seconds, the display will return to the regular weight
display.
36
Key(s) used
SELECT
Display
Operating instructions
From the weight display, press the SELECT key and hold the SELECT key
down while pressing the MENU key.
MENU
Press the
key or
key to select the desired character for
the first character (i.e., a digit from 0 to 9, a letter from A to Z, or
a hyphen). Note that here the letter A has been selected.
ENTER
ENTER
Just as with the first four characters, repeat steps 3 and 4 until
the eighth character has been specified. Note that here 123
has been specified.
When the desired character is displayed, press the ENTER key. The
first character will be specified and the second character will flash.
ENTER
37
ENTER
key.
Key(s) used
Display
ENTER
Operating instructions
From the weight display, press the
down while pressing the MENU key.
ENTER
ENTER
key
MENU
Press the
key or
key to select the desired character (i.e., a
digit from 0 to 9, a letter from A to Z, or a hyphen). Note that here
the letter 1 has been selected.
ENTER
When the desired character is displayed, press the ENTER key. The
first character will be set and the second character will flash.
ENTER
When the fourth character has been specified, press the ENTER key.
The display will then return to the regular weight display.
ENTER
7
MENU
ENTER
38
Action to be taken
Description
The protective sheet has not
been removed.
Er201
Press the
Er202
Turn off the power and then turn the power on again.
Power error
Turn the power off, make sure that the power conversion switch
located on the back is set to the correct position.
Er102
Er103
Er104
Er401
Er501
Er502
Er701
TARE/RESET
If any of the following errors are displayed, contact your Shimadzu representative.
Message
Er301
Er302
Er303
Er305
Er306
Er601
Er602
Er603
Er802
Description
Temperature sensor failure
Heater overheated
This error indicates the existence of an extremely hazardous condition. Turn the power off
immediately and contact your Shimadzu representative.
Heater control failure
Heater lid is open during measurement (for 15 sec.).
Lift mechanism failure
39
Incorrect placement
40
Drying temperature
Since the measurements obtained in predictive measuring mode are treated as comparable to the
measurements obtained by automatic operation mode, the drying temperature should be set to
the same temperature as in automatic operation mode.
Bias
Bias is used to adjust the predictive measurement. On the MOC-120H, a bias of anywhere from
9.99 to +9.99 percent may be specified. When performing a preparatory (COMPARE) measurement, the MOC-120H automatically indicates the most appropriate bias to be used to correct
measurements to match those obtained in automatic operation mode.
42
12-2-1 Calculating the bias to be specified when operating in predictive measurement mode
Step
Display
Operating instructions
Set the mode to preparatory measuring mode. (See 8-2-2 6) Specifying
settings for preparatory measuring mode for instructions.)
Specify the desired predicted value convergence range. In the example shown
here, a range of 0.5% is specified.
2
Note that the predicted value convergence range specified affects the amount of
time required for measurement and the accuracy of predictive measurements,
and that you should specify a range according to your objectives.
Specify the drying temperature to be used. (For further information, see 8-2-3
TEMP (Drying temperature).) In the example shown here, a temperature of
120C is specified.
Set the bias to 0.00%. (See 8-2-4 Bias for further information.)
.....
Place the sample onto the sample pan and begin measurement. (In the
example shown here, the initial weight is 10.478 grams.)
6
.....
When the final predicted value has been calculated, it will be displayed. (In the
example shown here, the measuring time was 7 minutes and the predicted
measurement is 15.8 percent.)
43
Step
Operating instructions
Display
Completion of measurement
Measuring will be completed when the conditions specified for automatic
operation mode have been met. When measuring is completed, the bias will be
displayed in the bias display area.
8
[Measurement results]
Bias is + 0.60 (= 16.40 (Automatic operation mode value) 15.80 (Predicted
measurement))
Automatic operation mode measurement
Predicted measurement
If the bias varies greatly from one time to the next when performing repeated
measurements, predicted measurement cannot be obtained, and you should
measure in automatic operation mode or in some other mode instead.
44
Display
Operating instructions
With the mode set to preparatory measuring mode, set the bias obtained by
the procedure described in 12.2.1. In the example shown here, a bias of 0.60
percent has been specified. (For information on how to set the bias, see 8-2-4
Bias.)
*
Do not change any other settings (i.e., the predicted value convergence range
and drying temperature) at this time.
.....
Place the sample onto the sample pan and begin measurement. (In the
example shown here, the initial weight is 10.478 grams.)
2
....
Completion of measurement
Measuring will be completed when the conditions specified for automatic
operation mode have been met.
Measurement results
Bias is + 0.90
4
bias is 0.))
Note that the specified bias (0.60%) does not affect the bias displayed here.
If the difference between the two sets of values exceeds allowable levels and
the bias varies sharply over repeated measurements, it is assumed that
predictive measurement cannot be properly performed. You should measure in
automatic operation mode or in some other mode instead.
45
Display
Operating instructions
Set the mode to predictive measuring mode. Refer to 8.2.2 7 Specifying
settings for PREDICT (Predictive measuring) mode for instructions.
Specify the same settings for the predicted value convergence range and
drying temperature as those used in preparatory measuring mode (subsections
12.2.1 and 12.2.2).
Example:
Predicted value convergence range: 0.5%
Drying temperature:
120C
Set the bias obtained through the procedures described in 12.2.1 and 12.2.2
(shown here as 0.60%). (See 8-2-4 Biasfor setting.)
.....
Place the sample onto the sample pan and begin measurement. (In the
example shown here, the initial weight is 10.213 grams.)
4
Completion of measurement
The predicted measurement will then be displayed.
46
Caution
Do not touch heater cover and the sensor probe or holder of temperature calibration kit during
temperature calibration as they become very hot. Touching these parts may cause serious burning.
The environmental conditions such as ambient temperature and air movement affect temperature calibration.
Perform temperature calibration without surrounding air movement and under the same conditions as when
performing measurements.
Press the TARE/RESET key to discontinue a once started temperature calibration. "Abort" is displayed and it returns to
the weight display.
For the operation of digital thermometer of temperature calibration kit, refer to its instruction manual.
Holder
Sensor probe
Brackets
Hole
Stay
47
Key(s) used
Display
Operating instructions
Press the MENU key at the weight display.
MENU
SELECT
Press the
3
ENTER
ENTER
SELECT
ENTER
Press the ENTER key. It moves to the display for inputting the
temperature for temperature calibration, and "100C" blinks.
START/STOP
START/STOP
ENTER
* Select a temperature about 20C lower than the sample position temperature. Set 80C if 100C at the sample
position is desired.
48
Sample code
Time of measurement
Measured value (%)
Signature title
* When the measurement is complete, press
the ENTER key. This will cause it to be printed.
Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D207300000
Device ID
: ABCD-123
Time of measurement : 2003/08/08
Measuring conditions storage area : 0
Measurement standard : Dry base
Measurement mode : Timed operation mode
Drying temperature : 110C
Measurement time : 10 mins.
Sample code
Time of measurement
Measurement graph
49
Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D207300000
Device ID
: ABCD-123
Sample code
: C-01
Date & time of measurement : 2003/08/08, 15:24
Measuring conditions storage area : 0
Measurement standard : Dry base
Temperature display mode : Output only when
'ST' mode is selected
Measurement mode : Preparatory measuring mode
Drying temperature : 110C
Automatic ending conditions : 0.05%
Predicted value convergence range : 0.5
Predicted measurement
50
: 5.6892g
Predicted measurement
Dry Mass
51
: 4.8637g
Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D207300000
Device ID
: ABCD-123
Date & time of measurement : 2003/08/08, 15:17
Reference
Before calibration
After calibration
Signature title
: 100.000g
: 100.004g
: 100.000g
Maker
: SHIMADZU CORP
Model
: MOC-120H
Serial number
: D412345678
Device ID
: 00000000
Date & time of measurement : 2004/11/22, 16:09
Reference
Before calibration
After calibration
Signature title
: 105C
: 101C
: 105C
52
: RS-232C
: 2400 bps
Data bits
: 8 bits
Parity
: None
Stop bits
: 1 bit
Connector
Pin assignment
:
5
4
9
Pin number
Direction
3
8
2
7
1
6
Description
Not used
Output
TXD
Input
RXD
Not used
GND
Not used
Not used
Not used
Not used
Frame
Shield
53
54
55
56
: RS232C
: 0x09 (tab)
Delimiter
57
58
16. Maintenance
16-1 Performing Maintenance
Turn the power off and disconnect the power cable. Allow the heater and other parts
cool down to ambient temperature before performing maintenance.
* When using detergents, be sure to follow the instructions for use provided with the detergent.
* Never use paint thinner, benzene, or any volatile cleaning agents or any abrasive cleansers or
polishes.
* Never use wire brushes or other hard cleaning tools.
59
Should the fuse(s) blow out repeatedly after replacement, contact your Shimadzu
representative.
60
Part number
Sample Pan
321-63314
321-63315
Wind Shield
321-63316
321-63317
321-63318
321-63319
Description
Protection Cover
Part number
Description
321-64125
AC Adapter 120V
321-63306-05
AC Adapter 230V
321-63306-04
321-63306-08
RS-232C Cable
321-63308
321-64130
321-63320-02
321-64193
61
Holder (321-64131)
MOC-120H
Printer Side
Side
D-sub9P
D-sub9P
Plug
Plug
4
5
4
SIGNAL
GND
PC Side
Side
D-sub9P
D-sub9P
Socket
Plug
4
5
6
SIGNAL
GND
62