Astm G57 - 95a
Astm G57 - 95a
Astm G57 - 95a
causing current to flow, and the voltage drop between the inner
electrodes is measured using a sensitive voltmeter. Alternatively, the resistance can be measured directly. The resistivity,
r, is then:
1. Scope
1.1 This method covers the equipment and procedures for
the field measurement of soil resistivity, both in situ and for
samples removed from the ground, for use in the control of
corrosion of buried structures.
1.2 To convert cm (metric unit) to metre (SI unit), divide by
100.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
r,Vcm 5 2p aR ~a in cm!
5 191.5 aR~a in ft!
where:
a = electrode separation, and
R = resistance, V.
Using dimensional analysis, the correct unit for resistivity is
ohm-centimetre.
3.3 If the current-carrying (outside) electrodes are not
spaced at the same interval as the potential-measuring (inside)
electrodes, the resistivity, r is:
2. Terminology
2.1 Definition:
2.1.1 resistivitythe electrical resistance between opposite
faces of a unit cube of material; the reciprocal of conductivity.
Resistivity is used in preference to conductivity as an expression of the electrical character of soils (and waters) since it is
expressed in whole numbers.
2.1.2 Resistivity measurements indicate the relative ability
of a medium to carry electrical currents. When a metallic
structure is immersed in a conductive medium, the ability of
the medium to carry current will influence the magnitude of
galvanic currents and cathodic protection currents. The degree
of electrode polarization will also affect the size of such
currents.
b
r, Vcm 5 95.76 b R/ 1 2 b 1 a
where:
b = outer electrode spacing, ft,
a = inner electrode spacing, ft, and
R = resistance, V.
or:
b
r, Vcm 5 p b R/ 1 2 b 1 a
where:
b = outer electrode spacing, cm,
a = inner electrode spacing, cm, and
R = resistance, V.
3.4 For soil contained in a soil box similar to the one shown
in Fig. 1, the resistivity, r, is:
r, Vcm 5 R A/a
where:
R = resistance, V,
A = cross sectional area of the container perpendicular to
the current flow, cm2, and
a = inner electrode spacing, cm.
1
This method is under the jurisdiction of ASTM Committee G01 on Corrosion
of Metals, and is the direct responsibility of Subcommittee G01.10 on Corrosion in
Soils.
Current edition approved April 15, 1995. Published June 1995. Originally
published as G 57 78. Last previous edition G 57 95.
Copyright ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
G 57
FIG. 1 Typical Connections for Use of Soil Box with Various Types of Instruments
4. Apparatus
4.1 At-Grade Measurements in situ:
4.1.1 The equipment required for field resistivity measurements to be taken at grade consists of a current source, a
suitable voltmeter, ammeter, or galvanometer, four metal
electrodes, and the necessary wiring to make the connections
shown in Fig. 2.
4.1.2 Current SourceAn ac source, usually 97 Hz, is
preferred since the use of dc will cause polarization of most
metal electrodes, resulting in error. The current can be provided
by either a cranked ac generator or a vibrator-equipped dc
source. An unaltered dc source can be used if the electrodes are
abraded to bright metal before immersion, polarity is regularly
G 57
tive of the soil of interest, in the electrode span. Conductive
structures such as pipes and cables should not be within 12 a of
the electrode span unless they are at right angles to the span.
6.1.2 Select electrode spacings with regard to the structure
of interest. Since most pipelines are installed at depths of from
1.5 to 4.5 m (5 to 15 ft), electrode spacings of 1.5, 3.0, and 4.5
m (5, 10, and 15 ft) are commonly used. The a spacing should
equal the maximum depth of interest. To facilitate field
calculation of resistivities, spacings of 1.58, 3.16, and 4.75 m
(5.2, 10.4, and 15.6 ft), which result in multiplication factors of
1000, 2000, and 3000, can be used when a d-c vibratorgalvanometer instrument is used.
6.1.3 Impress a voltage across the outer electrodes. Measure
the voltage drop across the inner electrodes and record both the
current and voltage drop if a separate ammeter and voltmeter
are used. Where a resistivity meter is used, read the resistance
directly and record.
6.1.4 Make a record of electrode spacing, resistance or
amperes and volts, date, time, air temperature, topography,
drainage, and indications of contamination to facilitate subsequent interpretation.
6.2 Soil Sample Measurement:
6.2.1 Soil samples should be representative of the area of
interest where the stratum of interest contains a variety of soil
types. It is desirable to sample each type separately. It will also
be necessary to prepare a mixed sample. The sample should be
reasonably large and thoroughly mixed so that it will be
representative. The soil should be well-compacted in layers in
the soil box, with air spaces eliminated as far as practicable.
Fill the box flush to the top and take measurements as
previously detailed (6.1.3). The meter used may limit the upper
range of resistivity, which can be measured. In such cases, the
resistivity should be recorded as <10 000 Vcm, etc.
6.2.2 The measured resistivity will be dependent on the
degree of compaction, moisture content, constituent solubility,
and temperature. The effect of variations in compaction and
moisture content can be reduced by fully saturating the sample
before placing it in the box. This can be done by preparing a
stiff slurry of the sample, adding only sufficient water to
produce a slight amount of surface water, which should be
allowed to evaporate before the slurry is remixed and placed in
the box. Where available, use ground water from the sample
excavation for saturation. Otherwise, use distilled water. If the
soil resistivity is expected to be below 10 000 Vcm, local tap
water can be used without introducing serious error. Some soils
absorb moisture slowly and contain constituents that dissolve
slowly, and the resistivity may not stabilize for as much as 24
h after saturation. The saturated measurement will provide an
approaching minimum resistivity, and can be usefully compared with as-received resistivity measurements. Surplus
water should not be poured off as this will remove soluble
constituents.
6.2.3 Temperature correction will not be required if measurement is made in-the-ditch or immediately after the sample
is taken. If samples are retained for subsequent measurement,
correct the resistivity if the measurement temperature is
substantially different from the ground temperature. Correction
b
r,Vcm 5 95.76 b R / 1 2 b 1 a
where:
b = outer electrode spacing, ft,
a = inner electrode spacing, ft, and
R = resistance, V.
or:
b
r,Vcm 5 pb R / 1 2 b 1 a
where:
b = outer electrode spacing, cm
a = inner electrode spacing, cm, and
R = resistance, V.
4.2.3 The dimensions of the box can be established so that
resistivity is read directly from the voltmeter without further
calculation. The box should be readily cleanable to avoid
contamination by previous samples.
5. Standardization
5.1 Periodically check the accuracy of resistance meters
using a commercial resistance decade box. Meter error should
not exceed 5 % over the range of the instrument. If error
exceeds this limit, prepare a calibration curve and correct all
measurements accordingly. A soil box can be calibrated using
solutions of known resistivity. Solutions of sodium chloride
and distilled water with resistivities of 1000, 5000, and 10 000
Vcm are recommended for this purpose. These solutions
should be prepared under laboratory conditions using a commercial conductivity meter, itself calibrated to standard solutions at 20C (68F).2
6. Field Procedures
6.1 At-Grade Measurements:
6.1.1 Select the alignment of the measurement to include
uniform topography over the limits of the electrode span. Do
not include large nonconductive bodies such as frozen soil,
boulders, concrete foundations, etc., which are not representa2
Handbook of Chemistry and Physics, 41st ed., The Chemical Rubber Co., p.
2606.
G 57
random resistivities are measured over a plant site, these can
best be displayed on a plot plan or similar layout. In either case,
use pedological surveys in the planning and interpretation of
any extensive survey. Measurements could be made in each
soil classification under a variety of drainage conditions to
simplify survey planning.
7.1.2 If resistivity information is required to assess the
requirement for corrosion control measures, it is recommended
that the tests be made on a true random basis. Since the number
of soil sections that could be inspected is essentially unlimited,
infinite population characteristics can be used to simplify
statistical treatment. Risk and error must be arbitrarily selected
to allow determination of the number of measurements. A risk
of 5 % of an error greater than 100 Vcm should be suitable for
most situations. The error limit should be about 10 % of the
anticipated mean resistivity. Where mean or median values
cannot be estimated with reasonable accuracy, sequential
sampling techniques can be employed.
7.2 InterpretationInterpretation of the results of resistivity surveys will largely depend on the experience of the persons
concerned. The mean and median resistivity values will indicate the general corrosivity of the soil. Sharp changes in
resistivity with distance and appreciable variations in moisture
content and drainage are indicative of local severe conditions.
24.5 1 T
40
where:
T
= soil temperature, C, and
RT = resistivity at T C.
A nomograph for this correction is shown in Fig. 3.3
7. Planning and Interpretation
7.1 Planning:
7.1.1 Surveys may be conducted at regular or random
intervals. The former method is suited to graphical presentation
and plotting resistivity versus distance, and will identify
gradients and abrupt changes in soil condition. The latter
method permits precise mathematical treatment, such as cumulative probability analysis. This method permits the determination of the probability of the presence of a soil with a
resistivity equal to or greater than a particular value.4 Where
FIG. 3 Nomogram or Conversion Chart for Reducing Soil Paste Resistance in ohms at a Particular Temperature as Measured in the
Bureau of Soils Cup, to Resistance at 15.6C (60F)
G 57
TABLE 1 Statistics from Multi-participant Evaluation of Wenner
Four Electrode Soil Resistivity MeasurementA
Electrode spacing, m
Average measured resistance
Average resistivity, V - cm
Repeatability standard deviation, V - cm
Repeatability coefficient variation, Cv, %
Reproducibility standard deviation, S, V - cm
Reproducibility coefficient of variation, Cv, %
8. General
8.1 It should be recognized that subsurface conditions can
vary greatly in a short distance, particularly where other buried
structures have been installed. Surface contamination tends to
concentrate in existing ditches with surface run-off, appreciably lowering the resistivity below the natural level. Since a
pipeline ditch cannot be included in the span of at-grade
measurements, soil box samples should be obtained where the
opportunity exists. To evaluate contamination effects when a
new route is being evaluated, soil samples can be obtained at
crossings of existing pipelines, cables, etc, or by intentional
sampling using soil augers.
8.2 Other field resistivity measurement techniques and
equipment are available. These commonly use two electrodes
mounted on a prod that is inserted in the soil-at-grade in an
excavation or a driven or bored hole. The two-electrode
technique is inherently less accurate than the four-electrode
method because of polarization effects, but useful information
can be obtained concerning the characteristics of particular
strata. More precise procedures may be employed in laboratory
investigations and these should be defined in reporting the
results. Where resistivity information is included in published
information, the measurement techniques used should be
defined.
Site No. 1
Site No. 3
6.1
10.9
41 700
2 300
5.5
6 900
16.5
1.5
62.6
59 900
4 700
7.8
10 000
16.6
A
Evaluation in Chester, New Jersey on May 28, 1993. Triplicate soil resistivity
measurements by seven participants each using different meters.
10. Keywords
10.1 four electrodes method; soil resistivity
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