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    The document summarizes an experiment on determining the water of hydration in sodium carbonate decahydrate (Na2CO3·10H2O). It provides the observations and measurements taken, including the mass of hydrate and anhydrous salt samples before and after heating. Calculations determine the moles of anhydrous salt and water present, and the moles of water per mole of hydrate. The % water in the hydrate is calculated to be 81%. Questions at the end ask to calculate the % water in other hydrates and determine the moles of water in one mole of the hydrate from experimental measurements and the molar mass of the anhydrous salt.

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    Ex 4

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    3a2d
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    The document summarizes an experiment on determining the water of hydration in sodium carbonate decahydrate (Na2CO3·10H2O). It provides the observations and measurements taken, including the mass of hydrate and anhydrous salt samples before and after heating. Calculations determine the moles of anhydrous salt and water present, and the moles of water per mole of hydrate. The % water in the hydrate is calculated to be 81%. Questions at the end ask to calculate the % water in other hydrates and determine the moles of water in one mole of the hydrate from experimental measurements and the molar mass of the anhydrous salt.

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    The document summarizes an experiment on determining the water of hydration in sodium carbonate decahydrate (Na2CO3·10H2O). It provides the observations and measurements taken, including the mass of hydrate and anhydrous salt samples before and after heating. Calculations determine the moles of anhydrous salt and water present, and the moles of water per mole of hydrate. The % water in the hydrate is calculated to be 81%. Questions at the end ask to calculate the % water in other hydrates and determine the moles of water in one mole of the hydrate from experimental measurements and the molar mass of the anhydrous salt.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as DOC, PDF, TXT or read online from Scribd
    Download as doc, pdf, or txt
    178 views2 pages

    Ex 4

    Uploaded by

    3a2d
    The document summarizes an experiment on determining the water of hydration in sodium carbonate decahydrate (Na2CO3·10H2O). It provides the observations and measurements taken, including the mass of hydrate and anhydrous salt samples before and after heating. Calculations determine the moles of anhydrous salt and water present, and the moles of water per mole of hydrate. The % water in the hydrate is calculated to be 81%. Questions at the end ask to calculate the % water in other hydrates and determine the moles of water in one mole of the hydrate from experimental measurements and the molar mass of the anhydrous salt.

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    ‫بسم ال الرحمن الرحيم‬

    Name: ayedzahran
    Group:
    Day:

    Experiment 4
    "Water of hydration"
    _________________________________________________________________

    I. Observations and results:

    Unknown number Na2CO3010H2O


    Molar mass of anhydrous salt 106 g/mol
    Mass of crucible 123.52 g
    Mass of crucible and hydrate 124.97 g
    Mass of crucible and residue after heating 123.80
    Mass of hydrate 1.43 g (1)
    Mass of anhydrous salt 0.28 g
    Mass of water of anhydrous salt 1.17 g (3)
    Moles of anhydrous salt 0.00175 mol (4)
    Moles of water 0.065 mol (5)
    Moles of water per 1 mol hydrate 3.887 mol
    % water in the hydrate 81% (6)
    Molar mass of hydrate 176 g/mol (7)

    II. Calculation:

    (1) Mass of hydrate = 124.95-123.52=1.43 g

    (2) Mass of anhydrous salt =123.80-123.52 =0.28 g

    (3) Mass of water of anhydrous salt =124.97 g -123.80=1.17 g

    (4) n =m/M=0.28 /106= 0.00175 mol

    (5) n= m/M=1.17 /18=0.065 mol

    (6) %water= (mwater/msample)*100%= (1.17 /1.43)*100%=81%

    (7) In hydrate (anhydrous salt : water) ,that’s mean the ratio between

    anhydrous salt and water in hydrate as (0.00175: 0.065) or (1:38.23) ,from


    the ratio the hydrate is Na2CO304H2O ,and molar mass is 176 g/mol
    III. Answer the following questions:
    1. What percent by weight of water is in alum KAI(SO4)2.12H2O
    Take sample of hydrate
    ,nhydrate =m/M =100\474=0.211 mol
    1 mole hydrate === 12 mole water
    0.211 mol === ??
    Moles of water =2.532 mol
    Mass of water =n*M =2.532*18 =45.576 g
    %water = (mwater/msample)*100% = (45.576/100)*100%=45.576%

    2. A solid hydrate weighting 2.691 g was heated to drive off the water .A solid
    anhydrate residue remained which weighed 2.259 g /Calculate the percent by
    mass of water in the hydrate .If the anhydrous residue has a molar mass of 282
    g/mol how many moles of water contained in one mole of hydrous salt?
    ,mwater = mhydrate-manhydrate=2.692-2.259=0.432 g
    %water =(mwater/msample)*100% =(0.432/2.691)*100% =16%
    ,nanhydrate = m/M=2.259/282 =0.008 mol
    , nwater = 0.432/18=0.024 mol
    0.008 mol ===== 0.024 mol
    1 mol ===== ??
    , nwater =3 mol in one mole of hydrous

    Not: For experiment number , For calculation number , For the solution of
    answers .

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