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Bi(NO 3) 3 • 5H 2 O/MgSO 4 was developed as an efficient and green reagent for the nitration of aromatic compounds under mechanochemistry (or ball milling) condition. While aromatics with weak activating groups such as phenyl could be... more
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    •   6  
      ChemistryMechanochemistryBall MillGreen Reagent
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    •   20  
      Chemical EngineeringEvolutionary BiologyBiophysicsChemistry
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    •   14  
      EngineeringMaterials ScienceSpectroscopyRaman Spectroscopy
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    •   11  
      EngineeringChemical EngineeringMaterials ScienceMechanochemistry
In this work, a mechanochemical route was proposed for the synthesis of the PrBaMn2O5+δ (PMBO) double layered perovskite phase. The mechanochemical reaction between Pr6O11, BaO2, and MnO powders with cationic stoichiometric ratios of... more
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      Chemical EngineeringMaterials ScienceNanomaterialsMedicine
In this work, a mechanochemical process using high-energy milling conditions was employed to synthesize La0.8Sr0.2Ga0.8Mg0.2O3-δ (LSGM) powders from the corresponding stoichiometric amounts of La2O3, SrO, Ga2O3, and MgO in a short time.... more
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    •   11  
      EngineeringMaterials ScienceSinteringMaterials
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    •   13  
      Materials ScienceTransmission Electron MicroscopyMechanochemistryPhotocatalysis
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    •   8  
      Materials EngineeringCondensed Matter PhysicsMaterials ScienceSolar Cell
Mechanochemistry is becoming an established method for the sustainable, solidphase synthesis of scores of nano-materials and molecules, ranging from active pharma-1
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      Materials ScienceChemistryNanoparticleNanotechnology
Mechanochemistry is a possible route to synthesize calcium deficient hydroxyapatite (CDHA) with an expected molar calcium-tophosphate (Ca/P) ratio 70.01. To optimize the experimental conditions of CDHA preparation from dicalcium phosphate... more
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      Materials ScienceBiomaterialsKineticsHydroxyapatite
The possibility for hydrothermal processes to take place under the action of mechanical pulses that arise in mechanical activators is considered for the system: a solid substance-water. Experimental data are presented on the... more
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      Mechanical EngineeringChemical EngineeringMaterials SciencePowder technology
In RbSn2Br5 halide, prepared by mechano-chemistry, the 5s2 lone electron pairs of Sn2+ were located from NPD and SXRD data. Among the thermoelectric properties, a huge Seebeck coefficient and an extremely low thermal conductivity are... more
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      Materials EngineeringMaterials ScienceInorganic ChemistryHalide
In this study we demonstrate the synthesis of quaternary semiconductor nanocrystals of stannite Cu 2 FeSnS 4 /rhodostannite Cu 2 FeSn 3 S 8 (CFTS) via mechanochemical route using Cu, Fe, Sn and S elements as precursors in one-pot... more
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    •   13  
      Materials ScienceTransmission Electron MicroscopyMechanochemistryPhotocatalysis
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    •   8  
      MultidisciplinaryMechanochemistrySurface modificationDensity Functional Theory
While the synthesis of nanographenes has advanced greatly in the past few years, development of their atomically precise functionalization strategies remains rare. The ability to modify the carbon scaffold translates to controlling,... more
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    •   8  
      MultidisciplinaryMechanochemistrySurface modificationDensity Functional Theory
This work presents results of the study of bioresorbable lactide/glycolide/trimethylene carbonate terpolymers exhibiting the shape memory properties. Infrared spectroscopy and second derivative spectra were used to explain the character... more
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One approach to mitigate the crisis of plastic waste is "chemical upcycling", in which waste plastic is converted into products with higher economic value. Towards this goal, several metal-catalyzed post-functionalization of polymers have... more
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      BiochemistryChemistryOrganic ChemistryPolymer Chemistry
A new cocrystal of pyrazinamide with oxalic acid was prepared mechanochemically and characterized by PXRD, Raman spectroscopy, solid-state NMR spectroscopy, DTA-TG, and SEM. Based on powder X-ray diffraction data the structure was solved.... more
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      ChemistryOrganic ChemistryRaman SpectroscopyPowder Diffraction
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      ChemistryMechanochemistryOrganic Process Development
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    •   6  
      ChemistryCatalysisBiodieselMechanochemistry
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      ChemistryMedicinePolymerizationMechanochemistry
Polymer mechanochemistry has traditionally been employed to study the effects of mechanical force on one or two chemical bonds within a polymer. It is underexploited for the scalable synthesis of wholly new materials by activating bonds... more
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      Materials ScienceChemistryMedicinePolymerization
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      MechanochemistryGrinding
Harnessing mechanical force to modulate material properties and enhance biomechanical functions is essential for advancing smart materials and bioengineering. Polymer mechanochemistry provides an emerging toolkit to unlock unconventional... more
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    • Mechanochemistry
The regularities of the mechanical activation of hexagonal boron nitride are analyzed using the X ray diffraction, IR spectroscopy, transmission electron microscopy, dynamic light scattering, and adsorp tion methods. At the initial state... more
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      PhysicsMaterials ScienceChemistryTransmission Electron Microscopy
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      PhysicsMaterials ScienceOpticsChemistry
Coupled evolution of a high-pressure phase (HPP) and dislocations, including dislocation pileups and dislocations generated due to phase transformation (PT), under compression and shear of a nanograined bicrystal, is considered as a model... more
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      EngineeringMaterials ScienceMaterials ChemistrySolid Mechanics
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      PhysicsHigh PressureKineticsMechanochemistry
A simple multiscale (nano-, micro-and macro-) continuum thermodynamic theory for strain-induced phase transitions (PTs) and chemical reactions (CRs), as well as closed form solutions were developed which explain a number of... more
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      Materials ScienceThermodynamicsPlasticityHigh Pressure
Harnessing mechanical force to modulate material properties and enhance biomechanical functions is essential for advancing smart materials and bioengineering. Polymer mechanochemistry provides an emerging toolkit to unlock unconventional... more
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    • Mechanochemistry
Direct access to the protonated merocyanine forms of two substituted spiropyrans by mechanosynthesis or sonochemistry was explored. The compounds were formed by the condensation reaction of the methyleneindolium iodide salt with... more
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      ChemistryPhotochemistryMedicinePhotochromism
Phthalimides have been successfully synthesized in the solid state by grinding (or kneading) of substituted phthalic anhydride and aniline derivatives. Selected products and intermediates were crystallized and characterized by... more
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      Materials EngineeringChemistryInorganic ChemistryMechanochemistry
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      Materials EngineeringChemical EngineeringCondensed Matter PhysicsMaterials Science
In this study, iron oxide nanoparticles (NPs) were successfully prepared from three different reactive systems by using mechanochemical synthesis. The effect of using iron salts with different oxidation state and the addition of metallic... more
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      Materials EngineeringChemical EngineeringCondensed Matter PhysicsMaterials Science
This paper is a collection of selected contributions of the 1st International Workshop on Mechanochemistry of Metal Hydrides that was held in Oslo in May 2018. In this paper, the recent developments in the use of mechanochemistry to... more
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      EngineeringMaterials ScienceMetallurgyMaterials
The reaction by melt mixing at 220 °C of the antihyperglycemic drug metformin hydrochloride 1 with dehydrated sodium succinate yields efficiently the organic salt [MET]2[SUC] 2 (H-MET+= metforminium and SUC2- = succinate). Solid state... more
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      ChemistryCrystallographyGreen ChemistryDiabetes
Angabe der unten stehenden Digitalobjekt-Identifizierungsnummer (DOI) zitiert werden. Die deutsche Übersetzung wird gemeinsam mit der endgültigen englischen Fassung erscheinen. Die endgültige englische Fassung (Version of Record) wird... more
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      ChemistryMedicineMechanochemistryBioluminescence
High-energy ball milling was applied to prepare powder samples by treating copper or copper oxides with magnesium or magnesium oxide. The five samples thus prepared were characterized by physical methods. According to X-ray diffraction... more
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      Chemical EngineeringChemistryInorganic ChemistryCatalysis
Eugenol is a phenylpropanoid with antifungal activity, with its anti-Candida activity being extensively studied. It has been proposed that eugenol generates oxidative stress and lipid peroxidation in Candida albicans. The products of... more
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      ChemistryCandida albicansEugenolpropiedades fisicoquímicas
Original Research Article MgO@SiO2 nanocomposite was synthesized using solvent-free mechanochemical route and its information was confirmed by UV-visible and FTIR analysis. The antibacterial and antifungal study of MgO@SiO2 nanocomposite... more
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      MechanochemistryAntimicrobial activity
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      ChemistryGreen ChemistryMechanochemistryCHEMICAL SCIENCES
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      Materials SciencePhotovoltaicsMaterialsHalide
In an attempt to establish the structures of the product formed in the reaction of PdCl2 and diphenylacetylene in polar organic solvents, the reactions were carried out in alcohols, acetonitrile and tetrahydrofuran at room temperature.... more
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      Materials ScienceChemistryCatalysisMechanochemistry
When an elastomeric material is deformed and subjected to temperatures above some characteristic value T cr (near 100 • C for natural rubber), it undergoes time and temperature dependent chemical changes consisting of scission and... more
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      Mechanical EngineeringCivil EngineeringApplied MathematicsMaterials Science
Mechanochemistry is becoming an established method for the sustainable, solid-phase synthesis of scores of materials and molecules, ranging from active pharmaceutical ingredients to materials for cleantech. Yet we are still lacking a good... more
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    •   8  
      PhysicsMaterials ScienceNanoparticleNanomaterials
The standard methodology for the synthesis of oligonucleotides is the solid-phase method. Here, we report the first case of mechanochemistry being directly applied to synthesising a dinucleotide on a soluble support. While... more
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      ChemistryIonic LiquidIonic LiquidsMechanochemistry
In an attempt to establish the structures of the product formed in the reaction of PdCl2 and diphenylacetylene in polar organic solvents, the reactions were carried out in alcohols, acetonitrile and tetrahydrofuran at room temperature.... more
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      Materials ScienceChemistryCatalysisMechanochemistry
Discrete (discontinuous) mechanochemical synthesis of titanium nitride was experimentally investigated. The experimental results show that mechanical activation intensifies the chemical conversion in the Ti-N system, and the discrete... more
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      Materials ScienceTitaniumMechanochemistryTitanium nitride
Olaparib (OLA) is an insoluble targeting antitumor drug for the treatment of ovarian cancer. Herein, polyamorphism of OLA was systematically studied aiming to improve its solubility and dissolution properties. Three amorphous forms of OLA... more
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      MorphologyNMR SpectroscopyCrystallizationEvaporation
This review paper deals with the application of broad possibilities of mechanochemistry in mineral processing, extractive metallurgy, chemical engineering, building industry, coal industry, materials engineering, agriculture, pharmacy and... more
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      EngineeringMaterials ScienceMetallurgyWaste Management