Is 419-1967 - Putty For Use On Window Frames
Is 419-1967 - Putty For Use On Window Frames
Is 419-1967 - Putty For Use On Window Frames
Indian Standard
SPECIFICATION FOR
PUTTY, FOR USE ON WINDOW FRAMES
(First Revision)
Seventh Reprint JULY 2007
(Incorporating Amendment No. 1 and Including Amendment Nos. 2, 3, 4 & 5)
UDC 691.585
© Copyright 1971
BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
Gr 2 September 1967
AMENDMENT NO. 5 MAY 2004
TO
IS 419 : 1967 SPECIFICATION FOR PUTTY, FOR
USE ON WINDOW FRAMES
( First Revision )
1)
Method of sampling and test for paints, varnishes and related products : Part 8 Tests for
pigments and other solids, Section 1 Residue on sieve (third revision).
2)
Method of sampling and test for paints, varnishes and related products : Part 2 Tests on
liquid paints (chemical examination), Section 1 Water content (third revision).
3)
Method of sampling and test for paints, varnishes and related products : Part 6 Durability
tests on paint films. Section 2 Keeping properties (third revision).
(CHD 20)
1
AMENDMENT NO. 4 OCTOBER 1997
TO
IS 419 : 1967 SPECIFICATION FOR PUTTY, FOR USE
ON WINDOW FRAMES
( First Revision )
( Page 4, clause 3.2) — Substitute the following for the existing clause:
'3.2 Composition — The material shall consist of mainly whiting and linseed
oil if necessary, varnish and suitable additives may be added in the formulation
of putty. The material shall be mixed in such proportions as to form a paste
which shall comply with the requirements of this standard.'
( Amendment No. 2, clause 3.2.1 ) — Insert at the end 'when tested as per
Appendix A'.
( Page 4, clause 3.3.1, line 4 ) — Substitute the words 'Appendix B' for
'Appendix A'.
( Page 6, Appendix A ) — Substitute the words 'Appendix B' for 'Appendix
A' and renumber the subsequent clauses.
( Page 6, clause 6.2 ) — Insert the following appendix after Note under
clause 6.2:
'APPENDIX A
(Clause 3.2.1)
A-1 DETERMINATION OF CALCIUM CARBONATE CONTENT
A-1.0 General — The calcium carbonate content is determined volumetrically,
using standard potassium permanganate solution.
A-1.1 Reagents
A-1.1.1 Standard Potassium Permanganate Solution (0.1 N) — Dissolve 3.2 g
of potassium permanganate in 1 000 ml of water and allow it to stand for 8 to 14
days. Siphon off the clear supernatant solution into dark-coloured glass
stoppered bottle. Weigh accurately about 3.3 g of sodium oxalate, previously
dried for a few hours at 100 ± 2°C and cooled over fused calcium chloride in a
desiccator. Dissolve it in water and make up the solution to exactly 500 ml.
Transfer 25 ml of sodium oxalate solution to a conical flask, add 50 ml of water
and 10 ml of dilute sulphuric acid (1:1 by volume). Heat the solution to about
60°C and titrate with potassium permanganate solution.
1
Amend No. 4 to IS 419 : 1967
where
M = mass in g of sodium oxalate in 100 ml of solution, and
V= volume in ml of potassium permanganate required for titration
against 25 ml of sodium oxalate solution.
A-1.1.2 Bromine Water
A-1.1.3 Ammonium Oxalate Solution — saturated.
A-1.1.4 Dilute Hydrochloric Acid — Add one volume of concentrated
hydrochloric acid [ see IS 265 : 1993 Hydrochloric acid — Specification
(fourth revision ) ] to four volumes of water.
A-1-2 Procedure — Transfer about 0.2 g of accurately weighed whiting, dried
as described in 7 of IS 33 : 1976 'Inorganic pigments and extenders for paints
— Methods of sampling and test ( third revision )' to a beaker. Dissolve the
whiting in about 20 ml of dilute hydrochloric acid. Digest for 10 minutes on a
steam bath, dilute to 150 ml, filter and wash the residue with water. Add a few
millilitres of bromine water, heat to boiling and make the boiling solution
ammoniacal. Filter off the residue, wash it thoroughly and reduce the filtrate by
evaporation to 200 ml. To the slightly ammoniacal solution, heated to boiling,
add an excess of hot ammonium oxalate solution. Continue boiling till the
precipitate becomes granular. Allow to stand for one hour, filter and wash with
hot water. Pierce the apex of the filter paper with a stirring rod and wash the
precipitate into beaker with hot water. Pour warm dilute sulphuric acid through
the paper and wash it a few times with warm acid. Add about 30 ml of dilute
sulphuric acid, dilute to about 250 ml, heat to 60°C and titrate with standard
potassium permanganate solution.
A-1.3 Calculation
2
Amend No. 4 to IS 419 : 1967
A-1.4 The carbon dioxide content shall also be estimated by a suitable method.
This shall not be less than the equivalent value for calcium carbonate (CaCO3)
content.'
(CHD 020)
3
AMENDMENT NO. 3 OCTOBER 1992
TO
IS 419 : 1967 SPECIFICATION FOR PUTTY, FOR USE
ON WINDOW FRAMES
( First Revision )
(Page 5, Table 1, Sl No. 2, col 3) — Substitute '1.5' for '1.0'.
(CHD 020)
1
AMENDMENT NO. 2 SEPTEMBER 1989
TO
IS : 419 - 1967 SPECIFICATION FOR PUTTY, FOR
USE ON WINDOW FRAMES
( First Revision )
( Page 4, clause 3.2 ) — Insert the following after 3.2:
'3.2.1 The calcium carbonate content of extracted pigment, from putty,
shall be not less than 80 percent.'
( C D C 8)
1
IS : 419 - 1967
( Superseding IS : 420 - 1953 )
Indian Standard
SPECIFICATION FOR
PUTTY, FOR USE ON WINDOW FRAMES
( First Revision )
Paints and Allied Products Sectional Committee, CDC 8
Chairman Representing
SHRI W. E. NORRIS Goodlass Nerolac Paints Private L t d , Bombay
Vice-Chairman
SHRI S. S. N A Y U D U Solar Paint & Varnish Manufacturing Co,
Calcutta
Members
SHRI H. N. RAMACHAR ( Alternate to
Shri W. E. N o r r i s )
DR J. S. A G G A R W A L Regional Research Laboratory, Hyderabad
D R M . A. S I V A S A M B A N ( Alternate )
SHRI P. C. CHANDA P. G. Chanda & Co Ltd, Calcutta
SHRI K. K. C H O W D H R Y Ministry o f Defence ( R & D )
SHRI I . D . S I N G H ( Alternate)
SHRI B. K. D A S GUPTA Ministry o f Defence ( R & D )
SHRI I . D . S I N G H (Alternate)
SHRI R. C. D A S GUPTA National Test House, Calcutta
SHRI S. K . BOSE (Alternate)
DEPUTY DIRECTOR R E S E A R C H Railway Board ( Ministry of Railways )
(CHEMICALS)
S H R I L . R . F I A L H O ( Alternate)
DIRECTOR Indian Lac Research Institute, Ranchi
SENIOR SCIENTIFIC OFFICER ( Alternate)
D I R E C T O R O F SCIENTIFIC R E - Naval Headquarters
SEAECH (NAVY)
S H R I K. S. GANESAN T h e Hyderabad Allwyn Metal Works Ltd,
Hyderabad
S H R I I S H W A R S I N G H ( Alternate)
DR J O S E P H GEORGE Central Building Research Institute, Roorkee
SHRI G . W . K A P S E ( Alternate)
( Continued on page 2 )
1
IS : 419 - 1967
( Continued from page 1 )
Members Representing
SHRI K. MADHAVAN NAIR Travancore T i t a n i u m Products Ltd, Trivandrum
S H R I B. R A M A M U R T H I ( Alternate )
S H R I T. K. S. MANI Addisons Paints and Chemicals Ltd, Madras
S H R I M. B. S A T Y A N A R A Y A N A (Alternate)
S H R I P. G. V. R A M A N A N Indian Aluminium Co Ltd, Calcutta
S H R I H . S. C H A W L A ( Alternate)
SHRI M. N. RAO Indian Paint Association, Calcutta
S H R I B. V. D A L A L ( Alternate)
SHRI R. K. ROKADE T h e Premier Automobiles Ltd, Bombay
S H R I P. K. D E S H P A N D E (Alternate)
SHRI N. K. S E N Development Commissioner, Small Scale Indus-
tries
S H R I P. R . M A L H A N ( Alternate)
S H R I K N. R. S H A R M A Directorate General of Technical Development
S U P E R I N T E N D I N G SURVEYOR OF Central Public Works Department, New Delhi
W O R K S (I)
SURVEYOR OF W O R K S ( I Alternate)
S H R I Y. S. SWAMY I. C. I. ( I n d i a ) Private Ltd, Calcutta
S H R I H . J . M I S T R Y (Alternate)
DR S A D G O P A L , Director General, ISI ( Ex-officio Member)
Director ( C h e m )
Secretary
SHRI M. S. SAXENA
Deputy Director ( Chem ), ISI
(Continued on page 8)
2
IS : 419 - 1967
Indian Standard
SPECIFICATION FOR
PUTTY, FOR USE ON WINDOW FRAMES
( First Revision )
0. F O R E W O R D
0.1 This Indian Standard (First Revision) was adopted by the Indian
Standards Institution on 30 June 1967, after the draft finalized by the Paints
and Allied Products Sectional Committee had been approved by the Chemical
Division Council.
0.2 This standard was first published in 1953 when it covered putty for use
on wooden frames. At the time of revision of this standard, the concerned
Sectional Committee decided to enlarge its scope to cover putty for use on
metal frames also, which was covered by IS : 420-1953*, Consequently,
this standard supersedes IS : 420-1953* which has since been withdrawn.
0.3 In drawing up the amalgamated revision, adequate consideration has
been given to stipulate various requirements independent of approved sample.
With the formulation of a specification for whiting for putty ( see IS : 2468-
1963†) reference to this standard has been given in the composition of the
material. Performance test for consistency has been improved by making it
more objective. All other changes found necessary as a result of experience
gained through the use of the standard have also been effected.
0.3.1 Full alignment of JSS 3070 'Specification for putty' issued by the
Department of Standardization, Ministry of Defence, Government of India,
has also been achieved with this revised standard.
0.4 For residue on sieve, IS Sieves conforming to IS : 460-1962‡ arc prescribed.
Where IS Sieves are not available, other equivalent standard sieves as judged
by aperture size may be used.
0.5 This standard is one of a series of Indian Standard specifications for fillers,
stoppers and putties.
*Specification for putty, for use on metal frames.
†Specification for whiting for putty.
‡Specification for test sieves (revised).
3
IS : 419 - 1967
1. SCOPE
1.1 This standard prescribes the requirements and the methods of sampling
and test for putty for use in fixing glass panes on wood and metal frames and
for filling splits, cracks and holes in wood or metal.
2. TERMINOLOGY
2.1 For the purpose of this standard, the definitions given under 2 of
IS : 85-1950†, in IS : 1303-1963‡ and the following shall apply:
Setting time — The time taken for the putty to convert itself into
cohesive mass which does not yield to specified pressure applied after
a specified drying time.
3. REQUIREMENTS
3.1 Form and Condition — The material shall be homogeneous paste and
shall be free from grit and other visible impurities.
3.2 Composition — The material shall consist only of whiting (conforming
to IS : 2468-1963§), linseed oil, raw ( conforming to IS : 75-1950||) and
suitable varnish medium in such proportions as to form a paste which shall
comply with the requirements of this standard.
3.3 Consistency — The material, after thorough working in hands, shall
have good plastic quality without sliminess or stickiness that would render it
difficult to handle and apply.
3.3.1 In addition, it shall work readily and smoothly under a palette knife
without crumbling or cracking and, after being moulded in place, it shall
convert itself into a cohesive mass which does not yield to specified pressure
applied after 72 hours as prescsibed in Appendix A.
3.4 The material shall also comply with the requirements given in Table 1.
*Rules for rounding off numerical values ( revised ).
†Methods of test for oil pastes for paints.
‡Glossary of terms relating to paints ( revised ).
§Specification for whiting for putty.
||Specification for linseed oil, raw, for paints. ( Since revised ).
4
I S : 419 - 1967
4.2.2 The use of the Standard Mark is governed by the provisions of the Bureau
of Indian Standards Act, 1986 and the Rules and Regulations made thereunder.
The details of conditions under which the licence for the use of Standard Mark
may be granted to manufactures or producers may be obtained from the Bureau
of Indian Standards.
5. SAMPLING
5.1 Representative samples of the material shall be drawn as prescribed in 3
of LS : 85-1950*.
5
IS : 419 - 1967
6. TEST METHODS
6.1 Tests shall be conducted as prescribed in Appendix A and IS : 85-1950*.
References to Appendix A and IS : 85-1950* are given in 3.3.1 and col 4 of
Table 1 respectively.
6.2 Quality of Reagents — Unless specified otherwise, pure chemicals and
distilled water (see IS : 1070-1960†) shall be employed in the test.
NOTE — 'Pure chemicals' shall mean chemicals that do not contain impurities
which affect the results of analysis.
APPENDIX A
( Clause 3.3.1 )
DETERMINATION OF SETTING TIME
A-0. GENERAL
A-0.1 Outline of the Method — The putty applied to a specified thickness
over a metal panel is subjected to pressure test after stipulated period and
layers examined for deformity.
A-1. APPARATUS
A-1.1 Apparatus for Setting T i m e Test — as shown in Fig. 1.
A-2. PROCEDURE
A-2.1 Apply the material on two clean metal panels of 60 × 60 mm size to
give a thickness of 5 mm. Allow the putty to dry for 72 hours. At the end of
this period, superimpose the two panels, so that the putty layers are under
contact and place on table A. Lower the steel ball B and plunger C to the
centre of the metal panels and place a weight of 500 g on top of the plunger.
Maintain the pressure on the plunger for 5 minutes. At the end of the 5
minutes period, separate the panels and examine for deformation,
A-2.1.1 The material shall be deemed to have passed the test if putty
layers do not get deformed under this load.
*Methods of test for oil pastes for paints.
†Specification for water, distilled quality ( revised ) ( Since revised ).
6
IS : 419-1967
7
IS : 419 - 1967
( Continued from page 2 )
Convener Representing
SHRI R. C. D A S GUPTA National Test House, Calcutta
Members
S H R I P. K. ADHIKARL Indian Paint Association, Calcutta
D E P U T Y DIRECTOR RESEARCH Railway Board ( Ministry of Railways )
( CHEM )
SHRI O. L. GUPTA Ministry of Defence ( D G I )
S H R I S. S. MAYUDU Solar Paint & Varnish Manufacturing Co,
Calcutta
SHRI M. N. RAO Indian Paint Association, Calcutta
Regional Offices:
Central : Manak Bhavan, 9 Bahadur Shah Zafar Marg, NEW DELHI 110002 2323 7617
*Eastern : 1/14 CIT SchemeVII M, V.I.P. Road, Kankurgachi, KOLKATA 700054 2337 8662
Northern : SCO 335-336, Sector 34-A, CHANDIGARH 160022 260 9285
Southern : C.I.T. Campus, IV Cross Road, CHENNAI 600113 2254 1984
†Western : Manakalaya, E9, MIDC, Behind Marol Telephone Exchange, 2832 9295
Andheri (East), MUMBAI 400093
Branch Offices:
'Pushpak', Nurmohamed Shaikh Marg, Khanpur, AHMEDABAD 380001 560 1348
Peenya Industrial Area, 1st Stage, Bangalore-Tumkur Road, BANGALORE 839 4955
Commercial-cum-Office Complex, Opp. Dushera Maidan, Arera Colony, 242 3452
Bittan Market, BHOPAL 462016
62-63, Ganga Nagar, Unit VI, BHUBANESHWAR 751001 240 3139
5th Floor, Kovai Towers, 44 Bala Sundaram Road, COIMBATORE 641018 221 0141
SCO 21, Sector 12, Faridabad 121007 229 2175
Savitri Complex, 116 G.T. Road, GHAZIABAD 201001 286 1498
53/5 Ward No. 29, R.G. Barua Road, 5th By-lane, Apurba Sinha Path, 245 6508
GUWAHATI 781003
5-8-56C, L.N. Gupta Marg, Nampally Station Road, HYDERABAD 500001 2320 1084
Prithavi Raj Road, Opposite Bharat Overseas Bank, C-Scheme, JAIPUR 302001 222 3282
11/418 B, Sarvodaya Nagar, KANPUR 208005 223 3012
Sethi Bhawan, 2nd Floor, Behind Leela Cinema, Naval Kishore Road, 261 8923
LUCKNOW 226001
H. No. 15, Sector-3, PARWANOO, Distt. Solan (H.P.) 173220 235 436
Plot No A-20-21, Institutional Area, Sector 62, Goutam Budh Nagar, NOIDA 201307 240 2206
Patliputra Industrial Estate, PATNA 800013 226 2808
Plot Nos. 657-660, Market Yard, Gultkdi, PUNE 411037 2427 4804
"Sahajanand House" 3rd Floor, Bhaktinagar Circle, 80 Feet Road, 237 8251
RAJKOT 360002
T.C. No. 2/275 (1 & 2), Near Food Corporation of India, Kesavadasapuram-Ulloor Road,
Kesavadasapuram, THIRUVANANTHAPURAM 695004 255 7914
1st Floor, Udyog Bhavan, VUDA, Siripuram Junction, VISHAKHAPATNAM-03 271 2833
*Sales Office is at 5 Chowringhee Approach, P.O. Princep Street, KOLKATA 700072 355 3243
†Sales Office (WRO) Plot No. E-9, MIDC, Rd No. 8, Behind Telephone Exchange,
Andheri (East), Mumbai-400 0093 2832 9295