ASC Winter06 JOT P44-55
ASC Winter06 JOT P44-55
ASC Winter06 JOT P44-55
Quantity (per
plugs were 1.5” in diameter and 2” in length, and were Composition Properties Value
barrel)
cleaned with toluene by leaching technique prior to use.
Make-up
Basic core properties such as air permeability, grain volume 0.98 bbl Density 65 lb/ft3
Water
and grain density were determined. The mineralogy of the
Defoamer 0.01gal PV 12-15 cP
selected cores was determined using their end cuttings by x-
ray diffraction. The major mineral found in all the cores 20-25
XC-Polymer 1.0 lb YP
lb/100ft2
was calcite, 90-98 wt.%.
The cores were prepared according to the standard
Dextrid 4.0 lb 10 sec gel 4 lb/100ft2
practices and re-saturated to represent expected reservoir Lime 0.50 lb 10 min gel 8 lb/100ft2
conditions. Base and return permeability of cores were CaCO3
15.0 lb pH 10
determined to Haradh oil at Swir. In some cases, Haradh “fine”
formation water, which was collected from the separation CaCO3
8.0 lb API Filtrate 6 mL/30min
plant, was also used for this purpose. The oil was filtered “medium”
twice, first to 5µm at ambient conditions and later to 15µm Table 1. Composition and properties of the DIF collected from a rig in
at cold conditions (4°C) using a filter press. The formation increment-2.
water was filtered through 0.45µm Miller filter paper.
Resaturated cores were brought to irreducible brine
saturation, before determining the base permeability, by
injecting oil through them for more than 15 hours at low
flow rates (0.2 mL/min.). Steps followed in return-
permeability testing were as follows:
• Established reference permeability of the core to oil (or
brine) at Swir.
• Circulated the drill-in fluid across the face of the core
for 30 minutes at dynamic conditions at 200 psi
overbalance.
• The same core was exposed to drill-in fluid for 16
hours at static conditions at the same overbalance.
• Circulated cleanup fluids, as necessary, each for 30
Photo 1. Residual filter cake after wash with acidic brine.
minutes across the face of the core.
100
100
Cumulative Volume Under %
Cumulative Volume Under, %
Fine particles 80
80 D 50 = 11µm
60
60
D 50=34.55µm
40
40
Medium particles
D 50 = 137 µm 20
20
0
0
1 10 100 1000 10000 1 10 100 1000 10000
Particle size, µm Particle size, µm
Fig. 2. PSD for neat, fine and medium, calcium carbonate. Fig. 4. PSD of the DIF with high quantity of fines.
Retained Permeability, %
80
592 mD
80 518 mD
60
40
40
100 120
Cumulative Volume Under %
63.5 mD
Retained Permeability, %
100
80
80 48 mD
60
60
40
40 21 mD
20 DIF with 8:15 , fine to medium.
20
DIF with 15:8 fine to medium.
0
1 10 100 1000 10000
0
Particle Size, μm Base After enzymes Surfactant
Fig. 6. Comparison of PSD of muds with different loadings of carbonate. Fig. 8. Permeability of the core after cleanup.
Table 3. Composition of the DIF with high quantity of fine. Table 5. Composition of the enzyme solution used in tests.
R E C O M M E N D AT I O N S
S I M E T R I C C O N V E R S I O N FA C T O R S
The following recommendations are made for the drill-in
cP x 1.0* E-03 = Pa.s
fluids in the density range of 62 or higher:
ft x 3.048* E-01 = m
• Apply the drill-in fluid formulations as given in Table 7
°F (°F-32)/1.8 = °C
per density requirement.
bbl x 1.589873 E-01 = m3
• Monitor the PSD of the DIF during drilling.
in. x 2.54* E+00 = cm
• Maintain the system properties during drilling by
mL x 1.0* E+00 = cm3
frequent quality checks.
lbm x 4.535924 E-01 = kg
• Dilute the mud to avoid change of density.
psi x 6.894757 E+00 = kPa
• Circulate filtered/solids-free NaCl brine upon
completing the drilling operations.
*Conversion factor is exact
• Spot recommended polymer breaker enzymes with pH
of the carrier fluid in the range of 6.
REFERENCES
• Implement the drilling practices as per the guidelines
given.
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