Astm B163 (2001)

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Designation: B 163 – 01 An American National Standard

Standard Specification for


Seamless Nickel and Nickel Alloy Condenser and Heat-
Exchanger Tubes1
This standard is issued under the fixed designation B 163; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.

This standard has been approved for use by agencies of the Department of Defense.

1. Scope E 29 Practice for Using Significant Digits in Test Data to


1.1 This specification2 covers seamless tubes of nickel and Determine Conformance with Specifications5
nickel alloys, as shown in Table 1, for use in condenser and E 76 Test Methods for Chemical Analysis of Nickel-Copper
heat-exchanger service. Alloys6
1.2 This specification covers outside diameter and average E 112 Test Methods for Determining the Average Grain
wall, or outside diameter and minimum wall tube. Size4
1.2.1 The sizes covered by this specification are 3 in. (76.2 E 140 Hardness Conversion Tables for Metals4
mm) and under in outside diameter with minimum wall E 1473 Test Methods for Chemical Analysis of Nickel,
thicknesses of 0.148 in. (3.76 mm) and under, and with average Cobalt, and High-Temperature Alloys7
wall thicknesses of 0.165 in. (4.19 mm) and under. 2.2 Federal Standards:8
1.3 Tube shall be furnished in the alloys and conditions as Fed. Std. No. 102 Preservation, Packaging and Packing
shown in Table 2. For small diameter and light wall tube Levels
(converter sizes), see Appendix X2. Fed. Std. No. 123 Marking for Shipment (Civil Agencies)
1.4 The values stated in inch-pound units are to be regarded Fed. Std. No. 182 Continuous Identification Marking of
as the standard. The values given in parentheses are for Nickel and Nickel-Base Alloys
information only. 2.3 Military Standard:8
1.5 The following safety hazards caveat pertains only to the MIL-STD-129 Marking for Shipment and Storage
test method portion, Section 12, of this specification. This 3. Terminology
standard does not purport to address all of the safety concerns,
if any, associated with its use. It is the responsibility of the user 3.1 Definitions:
of this standard to establish appropriate safety and health 3.1.1 average diameter, n—average of the maximum and
practices and determine the applicability of regulatory limita- minimum outside diameters, as determined at any one cross
tions prior to use. section of the tube.
3.1.2 tube, n—hollow product of round or any other cross
2. Referenced Documents section having a continuous periphery.
2.1 ASTM Standards: 4. Ordering Information
B 622 Specification for Seamless Nickel and Nickel-Cobalt
Alloy Pipe and Tube3 4.1 It is the responsibility of the purchaser to specify all
B 880 Specification for General Requirements for Chemical requirements that are necessary for the safe and satisfactory
Check Analysis Limits for Nickel, Nickel Alloys and performance of material ordered under this specification.
Cobalt Alloys3 Examples of such requirements include, but are not limited to,
E 8 Test Methods for Tension Testing of Metallic Materials4 the following:
E 18 Test Methods for Rockwell Hardness and Rockwell 4.1.1 Alloy (Table 1).
Superficial Hardness of Metallic Materials4 4.1.2 Condition (Temper) Table 3 and Appendixes X1 and
X2.
4.1.2.1 If annealed ends for stress relieved tubing are
1
This specification is under the jurisdiction of ASTM Committee B02 on desired, state length of end to be annealed and whether or not
Nonferrous Metals and Alloys and is the direct responsibility of Subcommittee one end or both ends are to be annealed.
B02.07 on Refined Nickel and Cobalt and Their Alloys.
Current edition approved June 10, 2001. Published August 2001. Originally
5
published as B 163 – 41 T. Last previous edition B 163 – 98a. Annual Book of ASTM Standards, Vol 14.02.
2 6
For ASME Boiler and Pressure Vessel Code applications see related Specifi- Annual Book of ASTM Standards, Vol 03.05.
7
cation SB-163 in Section II of that Code. Annual Book of ASTM Standards, Vol 03.06.
3 8
Annual Book of ASTM Standards, Vol 02.04. Available from Standardization Documents Order Desk, Bldg. 4 Section D, 700
4
Annual Book of ASTM Standards, Vol 03.01. Robbins Ave., Philadelphia, PA 19111-5094, Attn: NPODS.

Copyright © ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.

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TABLE 1 Chemical Requirements
Composition,%

Alloy Manga- Colum-


Molyb- Sulfur, Chro- Alum- Titan- Phos- Zircon- Tung-
Nickel Copper Iron nese, CarbonA SiliconA Cerium Yttrium Boron Cobalt bium
denum max mium inum ium phorus ium sten
max (Nb)
Nickel UNS N02200 99.0 minB 0.25 max ... 0.40 max 0.35 0.15 max 0.35 0.01 ... ... ... ... ... ... ... ... ... ... ...
Low-carbon Nickel
B
UNS N02201 99.0 min 0.25 max ... 0.40 max 0.35 0.02 max 0.35 0.01 ... ... ... ... ... ... ... ... ... ... ...
Nickel-copper alloy
UNS N04400 63.0 minB 28.0 to 34.0 ... 2.5 max 2.0 0.3 max 0.5 0.024 ... ... ... ... ... ... ... ... ... ... ...
Nickel-chromium-iron 14.0 to
alloy UNS N06600 72.0 minB 0.5 max ... 6.0 to 10.0 1.0 0.15 max 0.5 0.015 17.0 ... ... ... ... ... ... ... ... ... ...
Nickel-chromium-iron 58.0 to 21.0 to 1.0 to
alloy UNS N06601 63.0 1.0 max ... remainderA 1.0 0.10 0.5 0.015 25.0 1.7 ... ... ... ... ... ... ... ... ...
Nickel-chromium-iron 27.0 to
B
alloy UNS N06690 58.0 min 0.5 max ... 7.0 to 11.0 0.5 0.05 max 0.5 0.015 31.0 ... ... ... ... ... ... ... ... ... ...

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Nickel-chromium-iron 0.15 to 24.0 to 1.8 to 0.1 to 0.020 0.01 to 0.05 to
alloy UNS N06025 balanceB 0.1 max ... 8.0 to 11.0 0.15 0.25 0.5 0.010 26.0 2.4 0.2 max ... 0.10 0.12 ... ... ... ...
Alloy UNS N06045 45.0 min 0.3 max ... 21.0 to 25.0 1.0 0.05 to 2.5 to 0.010 26.0 to ... ... 0.020 0.03 to ... ... ... ... ... ...
0.12 3.0 29.0 max 0.09
Nickel-chromium-iron-
aluminum alloy 0.20 to 24.0 to 2.4 to 0.01 to 0.02 0.01 to 0.01 to

COPYRIGHT American Society for Testing and Materials


UNS N06603 balanceB 0.5 max ... 8.0 to 11.0 15.0 0.40 0.5 max 0.010 26.0 3.0 0.25. max ... 0.10 0.15 ... ... ... ...
Low-carbon nickel-
chromium-molybdenum-
tungsten alloy 15.0 to 19.0 to 0.02 to 0.04 3.0 to
UNS N06686 balanceB ... 17.0 5.0 max 0.75 0.010 0.08 0.02 23.0 ... 0.25 max ... ... ... ... ... ... 4.4
Nickel-iron-chromium 35.0 to 0.50 max 2.50 max remainderB 1.5 max 0.02 to 1.0 0.03 23.0 to 0.40 ... 0.15 to ... ... ... 0.010 3.0 max 0.4 to 2.50

2
alloy UNS N08120 39.0 0.10 max max 27.0 max 0.30 max 0.9 max
Nickel-iron-chromium 30.0 to 0.75 max ... 39.5 minB 1.5 0.10 max 1.0 0.015 19.0 to 0.15 to 0.15 to ... ... ... ... ... ... ... ...
alloy UNS N08800 35.0 23.0 0.60 0.60
B 163

B
Nickel-iron-chromium 30.0 to 0.75 max ... 39.5 min 1.5 0.05 to 1.0 0.015 19.0 to 0.15 to 0.15 to ... ... ... ... ... ... ... ...
alloy UNS N08810 35.0 0.10 23.0 0.60 0.60
Nickel-iron-chromium 30.0 to 0.75 max ... 39.5 minB 1.5 0.06 to 1.0 0.015 19.0 to 0.15 to 0.15 to ... ... ... ... ... ... ... ...
alloy UNS N08811 35.0 0.10 23.0 0.60C 0.60C
Nickel-iron-chromium 30.0 to 0.50 max ... 39.5 minB 1.50 0.10 max 1.00 0.015 19.0 to ... 0.75 to ... ... ... ... ... ... ... ...
alloy UNS N08801 34.0 22.0 1.5
Nickel-iron-chromium-
molybdenum-copper 38.0 to 2.5 to 19.5 to 0.6 to
alloy UNS N08825 46.0 1.5 to 3.0 3.5 22.0 minB 1.0 0.05 max 0.5 0.03 23.5 0.2 max 1.2 ... ... ... ... ... ... ... ...
A
Maximum unless range is given.
B
Element shall be determined arithmetically by difference.
C
Alloy UNS N08811: Al + Ti, 0.85 − 1.20.
B 163
TABLE 2 Alloy and Conditions 5. Chemical Composition
Alloy Condition
5.1 The material shall conform to the composition limits
Nickel UNS N02200 and specified in Table 1.
low-carbon nickel UNS N02201 annealed or stress-relieved
Nickel-copper alloy UNS N04400 annealed or stress-relieved 5.2 If a product (check) analysis is performed by the
Nickel-chromium-iron-aluminum purchaser, the material shall conform to the product (check)
alloy UNS N06603 annealed
Nickel-chromium-iron-aluminum
analysis per Specification B 880.
alloy UNS N06601 annealed
Nickel-chromium-iron alloy 6. Mechanical Properties and Other Requirements
UNS N06600 annealed
Low-carbon nickel-chromium- 6.1 Mechanical Properties—The material shall conform to
molybdenum-tungsten alloy UNS the mechanical properties specified in Table 3.
N06686 solution annealed
Nickel-chromium-iron alloy 6.2 Hardness—When annealed ends are specified for tubing
UNS N06690 annealed in the stress-relieved condition (see Table 3), the hardness of
Nickel-chromium-iron alloy
UNS N06045 annealed
the ends after annealing shall not exceed the values specified in
Nickel-iron-chromium alloy Table 3.
UNS N08120A annealed or cold-worked 6.3 Flare—A flare test shall be made on one end of each
Nickel-iron-chromium alloy
UNS N08800A annealed or cold-worked random length tube after final heat treatment. In the case of
Nickel-iron-chromium alloy stress-relieved tubing with annealed ends, the test shall be
UNS N08810A annealed made prior to, or subsequent to, annealing of the ends, at the
Nickel-iron-chromium alloy
UNS N08811A annealed option of the manufacturer.
Nickel-iron-chromium alloy 6.3.1 The flare test shall consist of flaring a test specimen
UNS N08801 annealed
Nickel-iron-chromium-molybdenum-
with an expanding tool having an included angle of 60° until
copper alloy UNS N08825 annealed the specified outside diameter has been increased by 30 %. The
Nickel-chromium-iron alloy flared specimen shall not exhibit cracking through the wall.
UNS N06025 annealed
A
6.4 Grain Size—A transverse sample representing full-wall
Alloy UNS N08800 is normally employed in service temperatures up to and
including 1100°F (593°C). Alloys UNS N08810, UNS N08811, and UNS N08120
thickness of annealed alloys UNS N08120, UNS N08810 and
are normally employed in service temperatures above 1100°F (539°C) where UNS N08811 shall conform to an average grain size of ASTM
resistance to creep and rupture is required, and it is annealed to develop controlled No. 5 or coarser.
grain size for optimum properties in this temperature range.
6.5 Hydrostatic Test:
4.1.3 Finish. 6.5.1 Each tube with an outside diameter 1⁄8 in. (3.2 mm)
4.1.4 Dimensions—Outside diameter, minimum or average and larger and tubes with wall thickness of 0.015 in. (0.38 mm)
wall thickness (in inches, not gage number), and length. and over shall be tested by the manufacturer to an internal
4.1.5 Fabrication Operations: hydrostatic pressure of 1000 psi (6.9 MPa) provided that the
4.1.5.1 Cold Bending or Coiling. fiber stress calculated in accordance with the following equa-
4.1.5.2 Packing. tion does not exceed the allowable fiber stress, S, indicated
4.1.5.3 Rolling or Expanding into Tube Sheets. below. The tube shall show no evidence of leakage.
4.1.5.4 Welding or Brazing—Process to be employed. P 5 2St/D
4.1.5.5 Pressure Requirements—If other than required by
6.5. where:
4.1.5.6 Ends—Plain ends cut and deburred will be fur- P = hydrostatic test pressure, psi (MPa),
nished. S = allowable fiber stress for material in the condition
4.1.6 Supplementary Requirements—State nature and de- furnished, as follows:
tails. t = minimum wall thickness, in. (mm); equal to the
4.1.7 Certification—State if certification is required (Sec- specified average wall minus the permissible “minus”
tion 15). wall tolerance, Table 4 and Table X2.2, or the specified
4.1.8 Samples for Product (Check) Analysis—Whether minimum wall thickness, and
samples for product (check) analysis shall be furnished. D = outside diameter of the tube, in. (mm).
4.1.9 Purchaser Inspection—If purchaser wishes to witness 6.5.2 When so agreed upon between the manufacturer and
tests or inspection of material at place of manufacture, the the purchaser, tube may be tested to 11⁄2 times the above
purchase order must so state indicating which tests or inspec- allowable fiber stress.
tions are to be witnessed (Section 13). 6.5.3 When stress-relieved tubes with annealed ends are to
4.1.10 Small-Diameter and Light-Wall Tube (Converter be tested hydrostatically, such pressure testing shall be done
Sizes)—See Appendix X2. prior to annealing of the ends of the tube.

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B 163
TABLE 3 Mechanical Properties of Tubes
Yield Strength Elongation in 2 in. Rockwell Hardness
Tensile Strength,
Material and Condition (0.2 % Offset), or 50 mm (or 4 D) min, (or equivalent) for
min, ksi (MPa)
min, psi (MPa) % annealed endsA
NickelUNS N02200:
Annealed 55 (379) 15 (103) 40 ...
Stress-relieved 65 (448) 40 (276) 15 B65 max
Low-carbon nickelUNS N02201:
Annealed 50 (345) 12 (83) 40 ...
Stress-relieved 60 (414) 30 (207) 15 B62 max
Nickel-copper alloyUNS N04400:
Annealed 70 (483) 28 (193) 35 ...
Stress-relieved 85 (586) 55 (379) 15 B75 max
Nickel-chromium-iron alloys:
Annealed alloy UNS N06600 80 (552) 35 (241) 30 ...
Annealed alloy UNS N06601 80 (552) 30 (207) 30 ...
Annealed alloy UNS N06690 85 (586) 35 (241) 30 ...
Annealed alloy UNS N06045 90 (620) 35 (240) 35 ...
Annealed alloy UNS N06025 98 (680) 39 (270) 30 ...
Annealed alloy UNS N06603 94 (650) 43 (300) 25 ...
Low-carbon nickel-chromium-molybdenum-tungsten alloy:
Solution annealed UNS N06686 100 (690) 45 (310) 45 ...
Nickel-iron-chromium alloys:
Annealed alloy UNS N08120 90 (620) 40 (276) 30 ...
Annealed alloy UNS N08800 75 (517) 30 (207) 30 ...
Annealed alloy UNS N08801 65 (448) 25 (172) 30 ...
Cold-worked alloy UNS N08800 83 (572) 47 (324) 30 ...
Annealed alloy UNS N08810 65 (448) 25 (172) 30 ...
Annealed alloy UNS N08811 65 (448) 25 (172) 30 ...
Nickel-iron-chromium-molybdenum-copper-
alloy:
Annealed UNS N08825 85 (586) 35 (241) 30 ...
A
Rockwell or equivalent hardness values apply only to the annealed ends of stress-relieved tubing. Caution should be observed in using the Rockwell test on thin
material, as the results may be affected by the thickness of specimen. For thickness under 0.050 in. (1.27 mm) the use of the Rockwell superficial or the Vickers hardness
test is suggested. For hardness conversions for nickel and high-nickel alloys see Hardness Conversion Tables E140.

TABLE 4 Permissible Variations in Outside Diameter and Wall Thickness of Condenser and Heat Exchanger Tubes

NOTE 1—The tolerances in the table apply to individual measurements of outside diameter and include out-of-roundness (ovality), and apply to all
materials and all conditions, except that for thin wall tubes having a nominal wall of 3 % or less of the outside diameter, the mean outside diameter shall
comply with the permissible variations of the above table and individual measurements (including ovality) shall conform to the plus and minus values
of the table with the values increased by 1⁄2 % of the nominal outside diameter.
NOTE 2—Eccentricity—The variation in wall thickness in any one cross section of any one tube shall not exceed plus or minus 10 % of the actual
(measured) average wall of that section. The actual average wall is defined as the average of the thickest and thinnest wall of that section.
NOTE 3—For tolerances of small diameter and light wall tube (converter sizes) see Appendix X2 (Table X2.2).
Permissible VariationsA
Outside Diameter, in. (mm) Wall Thickness,%
Material Nominal Outside Diameter, in. (mm)
Average Wall Minimum Wall
+ −
+ − + −
UNS N02200, UNS N02201, ⁄ to 5⁄8 (12.7 to 15.9), excl
12 0.005 (0.13) 0 12.5 12.5 25.0 0
and UNS N04400
5⁄8 to 11⁄2 (15.9 to 38.1), incl 0.005 (0.13) 0.005 (0.13) 10.0 10.0 20.0 0
over 11⁄2 to 3 (38.1 to 76.2), incl 0.010 (0.25) 0.010 (0.25) 10.0 10.0 22.0 0

UNS N06600, UNS N06601, UNS ⁄ to 5⁄8 (12.7 to 15.9), excl


12 0.005 (0.13) 0.005 (0.13) 12.5 12.5 25.0 0
N06690,
UNS N06045, UNS N06025, UNS
N06603, UNS N08800,
UNS N08810, UNS N08811, UNS
N08801,
UNS N08825, and UNS N08120
UNS N06686 5⁄8 to 11⁄2 (15.9 to 38.1), incl 0.0075 (0.19) 0.0075 (0.19) 10.0 10.0 20.0 0
over 11⁄2 to 3 (38.1 to 76.2), incl 0.010 (0.25) 0.010 (0.25) 10.0 10.0 22.0 0
A
Wall variations as indicated above are applicable only to the wall as ordered, for instance, to minimum or to average wall, but not to both.

psi MPa Stress-relieved nickel-copper alloy UNS N04400 21 200 146.2


Annealed low-carbon nickel UNS N02201 8 000 55.2 Annealed nickel-chromium-iron alloy UNS N06600 20 000 137.9
Stress-relieved low-carbon nickel UNS N02201 15 000 103.4 Annealed nickel-chromium-iron alloy UNS N06601 20 000 137.9
Annealed nickel UNS N02200 10 000 68.9 Annealed nickel-chromium-iron alloy UNS N06690 21 200 146
Stress-relieved nickel UNS N02200 16 200 111.7 Annealed nickel-chromium-iron alloy UNS N06045 22 500 155
Annealed nickel-copper alloy UNS N04400 17 500 120.6 Annealed nickel-chromium-iron alloy UNS N06025 24 500 169

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B 163
Solution annealed low-carbon nickel-chromium- 25 000 172 10. Number of Tests
molybdenum-tungsten alloy UNS N06686
Annealed nickel-chromium-iron-aluminum alloy
10.1 Chemical Analysis—One test per lot.
UNS N06603 24 000 165 10.2 Mechanical Properties—One test per lot.
Annealed nickel-iron-chromium alloy UNS N08120 22 500 155 10.3 Hardness—A representative sample consisting of 3 %
Annealed nickel-iron-chromium alloy UNS N08800 18 700 128.9
Annealed nickel-iron-chromium alloy UNS N08810 16 600 114.4 of each lot of tubes with annealed ends (see 9.1.2).
Annealed nickel-iron-chromium alloy UNS N08811 16 600 114.4 10.4 Grain Size—One test per lot.
Annealed nickel-iron-chromium alloy UNS N08801 16 600 114.4 10.5 Flare—One end of each random length tube.
Annealed nickel-iron-chromium-molybdenum copper alloy
UNS N08825 21 000 144.8
Cold-worked nickel-iron-chromium alloy UNS N08800 20 700 142.7
11. Specimen Preparation
11.1 Tension Test:
7. Dimensions and Permissible Variations 11.1.1 Tension test specimens shall be taken from material
7.1 Outside Diameter and Wall Thickness—The permissible in the final condition (temper) and tested in the direction of
variations in the outside diameter and wall thickness of tube fabrication.
shall not exceed those prescribed in Table 4 and Table X2.2, as 11.1.2 Whenever possible, all tubes shall be tested in full
applicable. (See also Table 5 and Table 6.) tubular size. When testing in full tubular size is not possible,
7.2 Length—When tube is ordered cut-to-length, the length longitudinal strip specimens, or the largest possible round
shall not be less than that specified, but a variation of plus 1⁄8 specimen, shall be used. In the event of disagreement when full
in. (3.2 mm) will be permitted, except that for lengths over 30 tubular testing is not possible, a longitudinal strip specimen
ft (9.1 m), a variation of plus 1⁄4 in. (6.4 mm) will be permitted. with reduced gage length as contained in Test Methods E 8
7.3 Straightness—Material shall be reasonably straight and shall be used.
free of bends or kinks. 11.1.3 In the case of stress-relieved tubes furnished with
annealed ends, the tension test shall be made on the stress-
8. Workmanship, Finish, and Appearance relieved tubes prior to annealing the ends.
8.1 The material shall be uniform in quality and temper, 11.2 Hardness Test:
smooth, commercially straight, and free of injurious imperfec- 11.2.1 Stress-Relieved Tubing with Annealed Ends—The
tions. hardness test may be made on the inside of the tube near the
end or on a specimen cut from the end, at the option of the
9. Sampling
manufacturer. The test shall be made on the inside of the
9.1 Lot—Definition: specimen.
9.1.1 A lot for chemical analysis shall consist of one heat.
9.1.2 A lot for mechanical properties, hardness, and grain 12. Test Methods
size testing shall consist of all material from the same heat, 12.1 The chemical composition, mechanical, and other
nominal size (excepting length), and condition (temper). properties of the material as enumerated in this specification
9.1.2.1 Where material cannot be identified by heat, a lot shall be determined, in case of disagreement, in accordance
shall consist of not more than 500 lb (230 kg) of material in the with the following methods:
same condition (temper) and size. Test ASTM Designation
9.2 Test Material Selection: Chemical Analysis E 76, E1473
Tension E8
9.2.1 Chemical Analysis—Representative samples shall be Rounding Procedure E 29
taken during pouring or subsequent processing. Rockwell Hardness E 18
9.2.1.1 Product (check) analysis shall be wholly the respon- Grain Size E 112
Hardness Conversion E 140
sibility of the purchaser.
9.2.2 Mechanical Properties, Hardness, and Grain Size— 12.2 The measurement of average grain size may be carried
Samples of the material to provide test specimens for mechani- out by the planimetric method, the comparison method, or the
cal properties, hardness, and grain size shall be taken from such intercept method described in Test Methods E 112. In case of
locations in each lot as to be representative of that lot. dispute the “referee” method for determining average grain

TABLE 5 Alloy,A Condition, Tube Size, and Bend Radii Limitations


Minimum Bend Radius, in.
(mm)
Tube OD, in. (mm) Average Tube Wall, in. (mm)B
Annealed Stress-Relieved
Condition Condition
Up to 1⁄2 (12.7), incl 0.046 to 0.057 (1.17 to 1.45), incl 13⁄16(30.2) 11⁄4(31.8)
Up to 1⁄2(12.7), incl Over 0.057 to 0.120 (1.45 to 3.05), incl 1 (25.4) 11⁄8 (28.6)
Over 1⁄2 to 5⁄8(12.7 to 15.9), incl 0.037 to 0.057 (0.94 to 1.45), incl 13⁄16(30.2) 11⁄4(31.8)
Over 1⁄2 to 5⁄8(12.7 to 15.9), incl Over 0.057 to 0.120 (1.45 to 3.05), incl 1 (25.4) 13⁄16(30.2)
Over 5⁄8 to 3⁄4(15.9 to 19.0), incl 0.049 to 0.057 (1.24 to 1.45), incl 11⁄4(31.8) 11⁄2(38.1)
Over 5⁄8 to 3⁄4(15.9 to 19.0), incl Over 0.057 to 0.109 (1.45 to 2.77), incl 13⁄16 (30.2) 11⁄4(31.8)
Over 3⁄4 to 1 (19.0 to 25.4), incl 0.049 to 0.058 (1.24 to 1.47), incl 2 (50.8) 4 (101.6)
Over 3⁄4 to 1 (19.0 to 25.4), incl Over 0.058 to 0.109 (1.47 to 2.77), incl 13⁄4(44.5) 21⁄4(57.2)
A
Applies for all alloys except alloy UNS N08810, alloy UNS N08801, and UNS N08811.
B
To determine the bend radius applicable to minimum wall tubing, compute the corresponding average wall from the wall tolerances in Table 4, then use Table 5.

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B 163
TABLE 6 Alloys, Size Ranges, and Yield Strength for Higher Yield Strength Tubes
Size Range, in. (mm) 0.2 % Yield Strength, ksi (MPa)
Alloys
OD Wall Thickness Minimum Maximum
Nickel-chromium-iron Alloy UNS N06600 ⁄
14 to ⁄
78 (6.35 to 22.23) Up to 0.100 (2.54) 40 (276) 65 (448)
Nickel-chromium-iron Alloy UNS N06601 1⁄4 to 7⁄8 (6.35 to 22.23) Up to 0.100 (2.54) 40 (276) 65 (449)
Nickel-iron-chromium Alloy UNS N08800 1⁄4 to 7⁄8 (6.35 to 22.23) Up to 0.100 (2.54) 40 (276) 65 (448)
Nickel-chromium-iron Alloy UNS N06690 1⁄4 to 7⁄8 (6.35 to 22.23) Up to 0.100 (2.54) 40 (276) 65 (448)

size shall be the planimetric method. dissatisfaction with the results of the tests, the manufacturer
12.3 For purposes of determining compliance with the may make claim for a rehearing within that time.
specified limits for requirements of the properties listed in the
following table, an observed value or a calculated value shall 15. Certification
be rounded as indicated below, in accordance with the round- 15.1 When specified in the purchase order or contract, a
ing method of Practice E 29: manufacturer’s certification shall be furnished to the purchaser
Test
Rounded Unit for Observed stating that material has been manufactured, tested, and in-
or Calculated Value
Chemical composition, hardness, nearest unit in the last right-hand place of
spected in accordance with this specification, and that the test
and tolerances (when expressed figures of the specified limit results on representative samples meet specification require-
in decimals) ments. When specified in the purchase order or contract, a
Tensile strength, yield strength nearest 1000 psi (6.9 MPa)
Elongation nearest 1 %
report of the test results shall be furnished.
Grain size:
0.0024 in. (0.060 mm) or larger nearest multiple of 0.0002 in. (0.005 mm) 16. Product Marking
less than 0.0024 in. (0.060 mm) nearest multiple of 0.0001 in. (0.002 mm)
16.1 Each bundle or shipping container shall be marked
13. Inspection with the name of the material; condition (temper); this speci-
13.1 Inspection of the material shall be made as agreed upon fication number; the size; gross, tare, and net weight; consignor
between the manufacturer and the purchaser as part of the and consignee address; contract or order number; or such other
purchase contract. information as may be defined in the contract or order.

14. Rejection and Rehearing 17. Keywords


14.1 Material not conforming to this specification or to 17.1 seamless tube; UNS N02200; UNS N02201; UNS
authorized modifications will be subject to rejection. N04400; UNS N06025; UNS N06045; UNS N06600; UNS
14.2 Samples tested in accordance with this specification N06601; UNS N06603; UNS N06686; UNS N06690; UNS
that represent rejected material shall be preserved for not less N08120; UNS N08800; UNS N08801; UNS N08810; UNS
than three weeks from the date of the test report. In case of N08811; UNS N08825

SUPPLEMENTARY REQUIREMENTS

S1. U-BENT TUBES

The following supplementary requirements shall apply when U-bent tubes are specified by the
purchaser in the inquiry, contract, or order.

S1.1 Limitation of Supplementary Requirements for Centerline Bend Radius (R), in. (mm) Tolerance, in. (mm)
U-Bent Tubes Up to 18 (457), incl 1⁄16(1.6)

Over 18 to 30 (457 to 762), incl 3⁄32 (2.4)

S1.1.1 The requirements for U-bent tubes included in this Over 30 to 36 (762 to 914), incl 1⁄8 (3.2)

supplement are limited to the alloys, conditions (tempers), tube


S1.2.2 Diameter of Tube in U-Bent Section—Neither the
outside diameter (OD), and wall thickness ranges and bend
major, nor the minor outside diameter of the tube at any one
radii listed in Table 5.
cross section included within the points of tangency of the bend
S1.2 Permissible Variations in Dimensions (Fig. S1) shall deviate from the nominal diameter prior to bending by
S1.2.1 Leg Spacing—The leg spacing, measured between more than 10 %.
the points of tangency of the bend to the legs shall not vary S1.2.3 Wall Thickness of Tube in U-Bent Section—The wall
from the value (2R − specified tube OD) by more than the thickness of the tube at the apex of the U-bent section shall be
amounts shown below where R is the specified centerline bend not less than the value determined by the following equation:
radius: TF 5 T~2R! / ~2R 1 D!

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FIG. S1 Bent Portion of U-Tube

Specified Length (L), ft (m) Tolerance (all Plus), in. (mm)


Up to 20 (6.1), incl 1⁄8 (3.2)
where: Over 20 to 30 (6.1 to 9.1), incl 5⁄32 (4.0)
TF = thickness after bending, in. (mm), Over 30 to 60 (9.1 to 18.3), incl 1⁄4 (6.4)

T = minimum permissible thickness of tube wall prior to Over 60 (18.3) 3⁄8 (10.0)

bending, in. (mm) S1.2.4.1 The difference in the length of the tube legs shall
R = centerline bend radius, in. (mm), and not be greater than 1⁄8 in. (3.2 mm).
D = nominal outside diameter of the tube, in. (mm).
S1.2.5 Squareness of Ends—The end of any tube may
When specified by the purchaser, proof of conformance to depart from square by not more than the following amounts:
this requirement shall be obtained by bending a tube specimen, Tube OD, in. (mm) Tolerance, in. (mm)
representative of the material offered, to the scheduled radius Up to 5⁄8 (15.9), incl 0.010 (0.25)
Over 5⁄8 (15.9) 0.016 (0.41)
of bend, cutting the tube at the apex of the bend, measuring the
S1.3 Hydrostatic Test
tube wall at the cross section of this apex section, and
comparing the measured value with the calculated value of TF. S1.3.1 When specified by the purchaser, the hydrostatic test
shall be performed after bending. The minimum holding time
S1.2.4 Length of U-Bend Tube Legs—The length of the tube at pressure shall be 5 s.
legs as measured from the point of tangency of the bend and S1.3.1.1 When hydrostatic testing is performed after bend-
the tube leg to the end of the tube leg shall not be less than that ing, such testing will not be required on straight length tubes
specified, but may exceed the specified values by the following prior to bending.
amounts: S1.3.1.2 The required fiber stress for computing hydrostatic
test pressure shall be 26 600 psi (183.3 MPa).

S2. HIGH YIELD STRENGTH TUBES


The following supplementary requirements shall apply when high yield strength tubes are specified by the purchaser in the
inquiry, contract, or purchase order.

S2.1 Limitations of Supplementary Requirements for meet the higher yield strength.
High Yield Strength Tubes
S2.1.1 The requirements for higher yield strength tubes S2.4 Annealing
included in this supplement are limited to the alloys, tube S2.4.1 Tubing is to be furnished in the annealed condition.
outside diameter (OD), and wall thickness ranges listed in In order to meet the higher yield strength requirement, it may
Table 6. be necessary to control the final annealing parameters so as to
S2.2 Higher Yield Strength preclude large grain sizes.
S2.2.1 The 0.2 % yield strength shall be as listed in Table 6.
S2.5 Marking Requirements
All other mechanical properties shall be as listed in Table 3.
S2.5.1 In addition to the marking requirements of SB-163,
S2.3 Degree of Cold Work the marking shall include the letters HYS signifying higher
S2.3.1 No additional cold working over and above that yield strength.
normally required for these alloys shall be used in order to

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S3. COILED OR UNSTRAIGHTENED TUBING

The following supplementary requirements shall apply when coiled or unstraightened tubing is specified by the purchaser in the inquiry,
contract, or purchase order.

S3.1 Unstraightened Tubing S3.1.2 On the certification and wherever the grade designa-
S3.1.1 When the purchaser specifies coiled or unstraight- tion for unstraightened tubing appears, it shall be identified
ened tubing after final heat treatment, the tensile specimens with the suffix letter “U” (for example, UNS N06600–U).
may be machine straightened prior to testing.

S4. U.S. GOVERNMENT

The following supplementary requirements shall apply only when specified by the purchaser in the inquiry, contract, or order, for agencies
of the U.S. Government.

S4.1 Referenced Documents cation in accordance with Fed. Std. No. 182 except that the
S4.1.1 The following documents of the issue in effect on ASTM specification number and the alloy number shall be
date of material purchased form a part of this specification to used.
the extent referenced herein: Fed. Std. No. 102, Fed. Std. No.
123, Fed. Std. No. 182, and MIL-STD-129. S4.4 Preparation for Delivery

S4.2 Quality Assurance S4.4.1 Preservation, Packaging, Packing:


S4.2.1 Responsibility for Inspection: S.4.4.1.1 Military Agencies—The material shall be sepa-
S4.2.1.1 Unless otherwise specified in the contract or pur- rated by size, composition, grade or class and shall be
chase order, the manufacturer is responsible for the perfor- preserved and packaged, level A or C, packed level A, B, or C
mance of all inspection and test requirements specified. Except as specified in the contract or purchase order.
as otherwise specified in the contract or purchase order, the S4.4.1.2 Civil Agencies—The requirements of Fed. Std. No.
manufacturer may use his own or any other suitable facilities 102 shall be referenced for definitions of the various levels of
for the performance of the inspection and test requirements packaging protection.
unless disapproved by the purchaser at the time the order is S4.4.2 Marking:
placed. The purchaser shall have the right to perform any of the
S4.4.2.1 Military Agencies—In addition to any special
inspections or tests set forth when such inspections and tests
are deemed necessary to ensure that the material conforms to marking required by the contract or purchase order, marking
prescribed requirements. for shipment shall be in accordance with MIL-STD-129.
S4.4.2.2 Civil Agencies—In addition to any special marking
S4.3 Identification Marking required by the contract or purchase order, marking for
S4.3.1 The material shall be properly marked for identifi- shipment shall be in accordance with Fed. Std. No. 123.

APPENDIXES

(Nonmandatory Information)

X1. CONDITION AND FINISHES NORMALLY SUPPLIED

X1.1 Scope stresses, with a thin, light to medium-dark surface.


X1.1.1 This appendix lists the conditions and finishes in X1.2.3 Stress Relieved with Annealed Ends—Same as
which tube (other than converter sizes) are normally supplied. X1.2.2 except with annealed ends.
These are subject to change and the manufacturer should be
consulted for the latest information available. X1.3 Low-Carbon Nickel UNS N02201
X1.2 Nickel UNS N02200 X1.3.1 Annealed—Similar to X1.2.1
X1.2.1 Annealed—Soft, with a dull matte finish. X1.3.2 Stress Relieved— Similar to X1.2.2
X1.2.2 Stress Relieved—Thermally treated below the an- X1.3.3 Stress-Relieved With Annealed Ends—Same as
nealing temperature to relieve the major portion of the internal X1.3.2 except with annealed ends.

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X1.4 Nickel-Copper Alloy UNS N04400 side diameter may have a bright finish when material is
X1.4.1 Annealed—Soft with a dull matte finish. annealed in protective atmosphere; otherwise, the inside diam-
X1.4.2 Stress Relieved— Thermally treated below the an- eter is supplied descaled as necessary.
nealing temperature to relieve the major portion of the internal X1.5.2 Annealed and Pickled (Not Ground)—Outside and
stresses resulting from cold drawing, with a thin, light to inside diameter will have dull, matte (pickled) surfaces.
medium-dark surface.
X1.4.3 Stress-Relieved With Annealed Ends—Same as
X1.4.2 except with annealed ends.
X1.5 Nickel-Chromium-Iron Alloy UNS N06600, Nickel-
Chromium-Iron Alloy UNS N06601, Nickel-
Chromium-Iron Alloy UNS N06690, Nickel-
Chromium-Iron Alloy UNS N06045, Nickel-
Chromium-Iron Alloy UNS N06025, Nickel-Iron-
Chromium Alloys (UNS N08120, UNS N08800, UNS
N08810, UNS N08811, and UNS N08801), and
Nickel-Iron-Chromium-Molybdenum-Copper Alloy
UNS N08825
X1.5.1 Annealed and Ground Outside Diameter—The in-
TABLE X2.1 Mechanical PropertiesA of Small Diameter and Light Wall Tube
Rockwell
Yield Strength
Tensile Strength, Elongation in 2 in. HardnessC
Material (0.2 % offset),B
ksi (MPa) or 50 mm, min, % (Scale as
min, ksi (MPa)
Indicated)
Nickel UNS N02200:
AnnealedD 80 (552) max 15 (103) 33 B75, max
Half-hardE 80 (552) min 40 (276) 12 B75 to B90
Full hardF 95 (655) min 75 (517) 4 B90 to C30
Low-carbon nickel
UNS N02201:
AnnealedD 70 (483) max 12 (83) 35 B62, max
Half-hardE 70 (483) min 30 (207) 12 B70 to B85
Full hardF 85 (586) min 65 (448) 4 B80 to B95
Nickel-copper alloy
UNS N04400:
AnnealedD 90 (621) max 28 (193) 32 B80, max
Half-hardE 85 (586) min 55 (379) 12 B75 to B97
Full hardF 110 (758) min 90 (621) 3 B95 to C27
Nickel-chromium-iron alloy
UNS N06600:
AnnealedDG 80 (552) to 110 (758) 35 (241) 30 B92, max
Half-hardE 105 (724) min 55 (379) 13 B90 to B98
Full-hardF 130 (896) min 105 (724) 4 C19 to C34
UNS N06601:
AnnealedD,G 80 (552) to 110 (758) 30 (207) 30 B92 max
Half-hardE 105 (724) min 55 (379) 13 B90 to B98
Full-hardF 130 (896) min 105 (724) 4 C19 to C34
UNS N06690:
AnnealedD,G 85 (586) to 115 (793) 35 (241) 30 B92 max
Half-hardE 105 (724) min 55 (379) 13 B90 to B98
Full-hardF 130 (896) min 105 (724) 4 C19 to C34
Nickel-iron chromium alloy
UNS N08800:
AnnealedDG 75 (517) to 100 (689) 30 (207) 30 B95, max
Half-hardE 105 (724) 60 (414) 13 B93 to C26
Full hardF 130 (896) 105 (724) 4 C24 to C38
Nickel-iron chromium-molyb-
denum-copper alloy
UNS N08825:
AnnealedDG 85 (586) to 115 (793) 35 (241) 30 B90 max
Half-hardE 105 (724) min 75 (517) 15 B90 to C25
Full-hardF 125 (862) min 100 (689) 5 C25 to C35
A
Not applicable to outside diameters under 1⁄8in. (3.2 mm) and to wall thicknesses under 0.015 in. (0.38 mm).
B
See 12.3.
C
Hardness values, indicative of tensile strength, are shown for information only. All tests are subject to confirmation by tension tests. For hardness conversions, see
Hardness Conversion Tables E140.
D
This condition is sometimes designated as “No. 1 Temper.”
E
This condition is sometimes designated as “No. 2 Temper.”
F
This condition is sometimes designated as “No. 3 Temper.”
G
The minimum tensile strength value applies only to tubing in straight lengths.

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X2. CONVERTER SIZES

X2.1 Small diameter and light wall tube in outside diam- and the manufacturer should be consulted as to the various
eters 11⁄4 in. (31.8 mm) and under all wall thicknesses may be outside diameters and wall thicknesses that may be furnished.
furnished in the following conditions or tempers when so Material shall be clean and scale-free. Such material shall
specified. The material is furnished in a limited range of sizes conform to the applicable requirements indicated in Table X2.1
and Table X2.2.

TABLE X2.2 Permissible Variations for Small Diameter and Light Wall Tube (Converter Sizes)

NOTE 1—Ovality, Normal Wall Tube:


As-Drawn (No. 2 and 3) Tempers—Ovality will be held within the outside diameter tolerances shown in the table.
Annealed (No. 1) Temper—Ovality will be held within 2 % of the theoretical average outside diameter.
NOTE 2—Ovality Light Wall Tube:
As-Drawn (No. 2 and 3) Tempers—Ovality will be held within 2 % of the theoretical average outside diameter.
Annealed (No. 1) Temper—Ovality will be held within 3 % of the theoretical average outside diameter.
NOTE 3—Wall Tolerances, Light Wall Tube—The plus and minus wall tolerance shown in the table shall apply down to and including 0.005 in. (0.13
mm) in wall thickness. For wall thicknesses less than 0.005 in. the tolerance shall be plus and minus 0.0005 in.
NOTE 4—Random Lengths:
(a) Where nominal random lengths on tubing 1⁄8 in. and larger in outside diameter are specified, a length tolerance of plus and minus 31⁄2 ft (1.1 m) applies
to the nominal length. This is a total spread of 7 ft. (2.1 m).
(b) Random lengths in sizes 1⁄8 in. (3.2 mm) and larger in outside diameter shall be subject to a length range from 5 to 24 ft (1.5 to 7.3 m). Long random
lengths are subject to a range from 15 to 22 ft (4.6 to 6.7 m).
(c) Random lengths in sizes up to, but not including, 1⁄8 in. in outside diameter, and fragile light wall tubes over this outside diameter are subject to the
length range from 1 to 15 ft (0.3 to 4.6 m).
NOTE 5—Cut Lengths—Tolerances on cut lengths shall be as follows:
NOTE 6—Straightness—Round tubing is subject to a straightness tolerance of one part in 600 (equivalent to a depth of arc of 0.030 in. (0.76 mm) in
any 3 ft (0.9 m) of length).
NOTE 7—Eccentricity—Eccentricity (as defined in Table 4, Note 2) shall be limited to plus or minus 10 % of the specified wall or calculated average
wall.
NOTE 8—When specified, the tolerance spread may be applied as desired. However, when not specified the tolerances shown below will apply. It should
be noted that inside diameter tolerances are based upon the outside diameter range.
Permissible Variations, in.
Length, ft Tube Size, in.
Over Under
U.S. Customary Units
Under 1 Up to 1.250, incl ⁄
1 32 0
1 to 4, incl Up to 1.250, incl ⁄
1 16 0
Over 4 to 10, incl Up to 1.250, incl 3⁄32 0
Over 10 Up to 1.250, incl 3⁄16 0
Metric Units
Permissible Variations, mm
Length, m Tube Size, mm
Over Under
Under 0.3 Up to 31.75, incl 0.794 0
0.3 to 1.2, incl Up to 31.75, incl 1.59 0
1.2 to 3.0, incl Up to 31.75, incl 2.38 0
Over 3.0 Up to 31.75, incl 4.76 0
Outside Diameter, in. Inside Diameter, in. Wall Thickness,%
Specified Outside Diameter, in.
+ − + − + −
U.S. Customary Units
Under 3⁄32 0.002 0 0 0.002 10 10
to 3⁄16(0.1875), excl 0.003 0 0 0.003 10 10
3⁄16 to 1⁄2(0.500), excl 0.004 0 0 0.004 10 10
1⁄2 to 11⁄4(1.250), incl 0.005 0 0 0.005 10 10
Millimetres
Under 2.38 0.051 0 0 0.051 10 10
2.38 to 4.76, excl 0.076 0 0 0.076 10 10
4.76 to 12.70, excl 0.102 0 0 0.102 10 10
12.70 to 31.8, incl 0.127 0 0 0.127 10 10

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with any item mentioned in this standard. Users of this standard are expressly advised that determination of the validity of any such
patent rights, and the risk of infringement of such rights, are entirely their own responsibility.

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if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM Headquarters. Your comments will receive careful consideration at a meeting of the responsible
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