Fraass Ezperiment
Fraass Ezperiment
Fraass Ezperiment
Ramza A. Guiling
Ozair O. Malic
Nadzmyra Zyra B. Tabao
Sonaya H.U. Amanoden
Abdulhakeem M. Panggaga
January 2024
1
Chapter 1
Rationale
countries, and it is considered a weed due to its invasive nature. However, recent studies
have shown that cogon grass can be a promising alternative source of paper, which can
help reduce the reliance on traditional paper sources such as trees. Despite its reputation
production. Investigating the performance of cogon grass in this context could pave the
way for a more ecologically sound paper production method, thereby contributing to
Pena (2021) stated that the Philippines is one of the countries that has a high
potential for cogon grass as an alternative source of paper due to the abundance of the
grass in the country. However, there is still a need to conduct further research to
determine the feasibility and viability of using cogon grass for paper production. This is
where this experimental research comes in, as it aims to investigate the performance of
According to Madung, Soloi, Majid, & Sarjadi (2022), since the principal source
of paper, trees, has become scarce due to the annual increase in demand for paper, non-
woody plants have emerged as an alternative fiber in the paper-making process. Because
imperata cylindrica has a high cellulose content and a low lignin level, it is used as a
The process of making paper using cogon grass involves several steps, including
harvesting and cleaning the grass, pulping the grass to extract the cellulose fibers, and
The primary objective of this study was to comprehensively assess the potential
experiments and analyzing the physical and chemical properties of cogon grass fibers,
this research aimed to determine its sustainability for papermaking processes. The
findings from this investigation contributes to essential insights into the feasibility,
ecologically friendly option in the realm of paper sourcing and manufacturing, potentially
reducing the demand for conventional paper sources like pine trees while promoting
sustainable practices.
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This study was established and aimed to test the performance of Cogon Grass
1. What are the qualitative properties that the paper from Cogon Grass have in terms
of:
1.2 Texture?
2. What are the quantitative properties that the paper from Cogon Grass have in
terms of:
2.1 Grammage;
Conceptual Framework
The conceptual framework of this study illustrates the different concepts of the
an alternative source of paper. The independent variable is the use of Cogon Grass. It
alternative source of paper, in terms of: the qualitative and quantitative properties of
Dependent Variable
Quantitative Properties:
Independent Variable
Color
Texture
cylindrica) as an alternative source of paper that was found in an area after entering the
Agus Bridge 1 (Banggolo Bridge), Marawi City, Lanao del Sur, Philippines. This study
was delimited to Cogon Grass as an alternative source of paper and examining its
paper. The grass paper produced was then subjected to examination and determination of
its qualitative properties, in terms of color and texture, and quantitative properties, in
terms of grammage, coefficient of friction, burst index, burst strength, tensile index, and
tensile strength. The location where the Cogon Grass originated and its condition, its age
and duration of expiration is beyond the scope of the study. This study excluded the
comparison of cogon grass paper to commercial paper as this study was only focused on
something beneficial for everyday use. This study can make use of an invasive plant to
produce an alternative to paper. This study can be a great help to benefit the following
individuals:
Community. This study can be a great benefit to the community that has massive
growth of cogon grass; they can make use of the cogon grass by producing paper out of
it. It will not only help discard unwanted grass, but it can also be utilized and contributed
to the community.
Farmers. This study can help the farmers profit from turning the invasive Cogon
Grass around their areas into paper. This can help them with financial benefits.
Paper Industry. This could give them information about the potential of Cogon
Grass as an alternative source of wood-free paper. They can utilize the cogon grass into
Future Researchers. The findings of this research may be a helpful guide for
them and their future research. They can use this study as their reference for their
research and pave the way for more clarified studies on this similar field.
Definition of Terms
. In this study, it is referred to as the average of the burst test of the paper made
(Testronix, accessed 9 January 2024). In this study, it is referred to as the maximum load
the paper made from cogon grass can withstand before it ruptures.
Cogon Grass. It is an invasive grass with stiff stalks and saw-toothed leaves that
quickly takes over any bit of land (Pena, 2021). In this study, it is the experimental
friction force to normal force (Zhang, 2016). In this study, it is referred to as the
minimum force required to start the paper made from cogon grass moving on a surface by
Color. It is the aspect of any element that may be expressed in terms of hue,
radiation of a specific wavelength range visible to the human eye (Nassau, 2024). In this
the weight of paper, although it is also commonly applied to polymers and fabrics (Label
Planet, accessed 6 January 2024). In this study, it is referred to as the weight of paper
different types of paper grades (Adams, 2023). In this study, it is referred to as the
Tensile Strength. It is the highest stress a material can withstand before breaking
when allowed to be stretched or pulled (Pal et al., 2022). In this study, it is the maximum
load that the paper made from cogon grass can support before it fractures.
January 2024). In this study, it is referred to as the tactile surface consistency of paper
Chapter 2
This chapter presents a view of literature and studies related to this study of the
source of paper, including foreign and local literature and studies. It also discusses the
Related Literature
Cogon Grass
Miller (2003) stated that Cogon Grass is a perennial, rhizomatous grass (Poaceae)
that grows approximately 2 to over 4 feet in height. The leaves are about an inch wide,
have a prominent white midrib, and end in a sharp point. Leaf margins are finely toothed
and are embedded with silica crystals. The lower surface of the leaf blade is often hairy
near the base; the upper is hairless. The white plume-like flowers are arranged in a
silvery, cylindrical, branching structure, or panicle, about 3-11 inches long and 1½ inches
wide. Cogon grass reproduces both vegetatively and from seed. In spring, a single plant
can produce up to 3000 seeds per seed head that may be carried great distances by the
wind. Vegetative spread of cogon grass is aided by its tough and massive rhizomes that
may remain dormant for extended periods of time before sprouting. Rhizomes can grow
from
As defined by Matic Hub (n.d.), with its long stem-less clumps of up to 1.5m leaf
blades; its extensive rhizome root system; and its feathery white flowers over productive
seeding capability, and its allelopathic tendencies – cogon sucks nutrients and insinuates
Asia but has now spread to other regions of the world. It is a perennial grass that can
grow up to two meters tall and has long, narrow leaves. Cogon grass is known for its fast
growth rate, aggressive root system, and high tolerance to various environmental
conditions. It reproduces through rhizomes, which can grow up to one meter deep in the
soil, making it difficult to control. The plant is known to alter soil properties, reduce
biodiversity, and increase the risk of wildfires. However, its abundance and fast growth
rate make it a potential source of raw material for paper production (Kumar, Barrett, &
Kaewkuekool, 2015).
Fiber Pulp
Research studies have shown that Cogon Grass can be used as a source of pulp
and paper. The cellulose content of cogon grass is about 45%, which is comparable to
other commercial pulpwood. The lignin content of cogon grass is low, which makes it
easier to break down the plant material into fibers during the pulping process. However,
the high silica content of cogon grass can pose challenges in the pulping process, as it can
Paper
manufacturing is amongst the most intense CO2-emitting industries. Grass Paper has
mined nature for an alternative plant-fiber material derived from grass, preserving natural
forest resources. The first grass paper on the market has a premium look and feel, with
Grass fiber, together with wood pulp and recycled paper, has the potential to
become the paper industry's third raw material supply. It cannot completely replace virgin
fibers or recycled pulp (wood), but it can currently account for up to 50% of the fiber
content in the finished product. Grass fiber can also be up to 70% less expensive than
wood pulp. Grass fiber provides industry with a more sensitive and gentle way to treat
forest resources. "I believe grass and wood is the perfect symbiosis when it comes to
paper products and packaging in the near future," Schatzschneider said. Furthermore,
grass fibers provide farmers with an extra cash stream when it comes to abandoned
pasture hay, which is currently being burned or used to fill biogas plants (Cordis, 2020).
Grammage
Grammage is the mass of a sheet of paper divided by its area, and it is expressed
in grams per square meter (g/m2). Grammage is an important factor in determining the
selling price of paper. Other paper qualities, such as bursting strength, thickness, and
volume, are specified in terms of grammage. Mass per unit area is also known as basis
weight in the United States. The basis weight is determined by the weight in pounds of a
ream of paper of a specified size and quantity, which is normally 500 sheets but can be
480 sheets. The grammage of paper is primarily controlled by the loading of fiber stock
onto the paper machine, but it is also influenced by fillers, coatings, sizing, and the
Coefficient of Friction
According to Arthurs, Anthony, & Christopher (2005), friction is the force that
opposes the relative motion of two objects in contact. It is a vector quantity. Friction
always acts in the opposite direction of slippage and is always parallel to the two surfaces
11
in contact. The force that opposes the commencement of motion is known as static
friction. Kinetic friction is the friction that exists between moving things. The force of
friction is directly proportional to the size of the normal force and is determined by the
Tensile Index
A tensile tester is used to measure the test strip at a steady rate of elongation.
tissue, crepe paper, copier paper, medical paper, carton board, and liner boards were
among the materials he tested. Tensile index = tensile strength per grammage, expressed
as Nm/g. The tensile energy absorbed is estimated from the area under the
load/elongation curve in addition to the maximum tensile load and elongation. This is the
result of the work done in breaking the test strip. Tensile energy absorption units are
Tensile Strength
required to break a strip of paper sheet. It is one of the most essential fundamental
physical features of paper and paperboard. Tensile strength varies depending on fiber
direction. Tensile strength is assessed in both directions because the fiber orientation
differs between machine direction (MD) and cross direction (CD). Machine direction
refers to the direction of the paper web running on the machine, whereas cross direction
refers to the direction perpendicular to the paper sheet running on the machine during
paper production. It's higher in the machine direction than in the cross direction. It is
The tensile strength test of paper sheet is like the tensile strength test of other
materials, but the manner of expression is different. Tensile strength is usually expressed
in terms of load per unit cross-sectional area, however in the paper sector it is reported in
terms of load per unit of the test specimen. If the tensile strength of paper is low, the
quality of the paper is low and must be improved by enhancing several factors (Ahmed,
2019).
Related Studies
The following research studies were already conducted and were useful while
conducting the study, for some of their methods were adapted by the researchers.
Cogon Grass
A research study of Aripin (2014), stated that the global demand for wood fiber
has increased due to increasing population and new applications for wood fiber.
Therefore, to supplement the limited wood fiber resources, non-wood fibers have been
introduced as alternatives in pulp and paper-based industries. The objective of this study
is to determine the potential of cassava peel, cocoa pod husk, cogon grass and oil palm
leaf as alternative fibers for pulp in paper-based industries based on its chemical, physical
and mechanical properties. The mechanical strength of hand sheet produced (tensile,
burst, tear and fold) was investigated according to the TAPPI test method. To propose the
suitability of the studied plants as alternative fiber resources as pulp in papermaking, the
obtained results are compared to other published literatures from wood resources.
Although cogon grass contains shorter fibre than oil palm leaf, the handsheet product
showed the highest tensile (45.06 Nm/g), burst (3.90 kPa. m 2/g) and tear (2.17 mN. m
13
2/g) indices when compared to oil palm leaf (12.08 Nm/g, 0.95 kPa. m 2/g and 1.80 mN.
m 2/g) and published wood resources. From SEM images, handsheet of cogon grass
contains compact, straight, and smooth fibres. In conclusion, apart from the chemical,
pulp, physical and mechanical properties and the surface morphology of the cocoa pod
husk, cogon grass and oil palm leaf sheets indicate that they are suitable to be used as
alternative fibers for pulp and paper-based industries with cogon grass being the best.
Fiber Pulp
The study by Tamrin, Pratama, Purnomo, & Davitri (2017) stated, the
investigation of aquatic and dry land weeds as fibers resources for paper making was
carried out. The selected fiber resources of aquatic weeds were water hyacinth
(Eicchornia crassipes) and water chestnuts (Eleocharis dulcis), and blady grass
(Imperata cylindrica) as the selected dry land weed. Research was designed as a factorial
completely randomized design with two factors. The first factor was fibers origin
(Eicchornia crassipes, Imperata cylindrica, Eleocharis dulcis) and the second factor was
the fibers pulp slurry concentrations (30%, 50%, and 70% v/v). Results showed that the
fibers origin and fibers pulp slurry concentration had significant effect on the tensile
strength, mass density, water absorption, and frictional resistance of paper. The
interaction between the fiber’s origin and fibers pulp slurry concentration had significant
effect on tensile strength, frictional resistance, water absorption; but had no significant
effect on mass density of paper. The paper that was made of 70% (v/v) of water hyacinth
fiber pulp slurry showed the best characteristics with the tensile strength of 3.65 kgf mm-
1, mass density of 0.87 g cm-3, water absorption of 0.235 g cm-2, and frictional
Paper
The study of Kassim, Aripin, Ishak, & Zainulabidin (2015) stated that the
increasing demand in wood fiber consumptions especially in pulp and paper making has
pushed forward the search for alternative fiber resources. Non-wood derived fiber could
annual plants are good potential fiber resources for pulp and paper making. The objective
of this study is to determine the suitability of cogon grass as an alternative fiber for pulp
and paper making by analyzing its chemical and surface morphological properties.
Technical Association of the Pulp and Paper Industry (TAPPI) Tests, Kurscher-Hoffner
and Chlorite methods. Scanning electron microscopy (SEM) was used to visualize the
surface morphology of the cogon grass fibre. Results obtained indicate that the
holocellulose (64.93%) content is comparable with other published non-woods and the
lignin (5.67%) content is favorably the lowest. Based on the chemical and surface
Grammage
According to Bloch, Engin, & Sampson (2019), in this study, they showed how
the structure of sheet surfaces affects the porosity profile and hence the sheet thickness
microtomographic analysis. Furthermore, despite their higher porosity, they also showed
15
that the mean pore height in low grammage sheets is lower than that in higher grammage
sheets, meaning that pore heights in surface layers are lower than those in the bulk.
Coefficient of Friction
between dry metal surfaces attributes it to tiny minute welds or adhesions between the
surfaces and proposes that the friction force is uniquely defined for a particular pair of
surfaces by the normal load alone. It is shown here that this cannot be true in general and
that some additional operating conditions must be defined. Experiments show that one
such feasible condition is the sliding speed, so that the friction force is a function of both
the normal load and the sliding speed. It is noted that speed can influence friction force in
two ways: first, by the ensuing shear strain rate in the area of the welded junction, and
Tensile Index
According to Chauhan and Bhardwaj (2014), inorganic fillers, the second most
filler particles and fibers. The impacts of filler content and preflocculation on the filler
bondability factor estimated based on first-pass ash retention and paper strength
parameters such as the tensile, Z-direction tensile, and composite tensile indexes are
discussed in this article. Talc filler preflocculated with 0.1-0.8% doses of cooked cationic
starch based on the dry weight of the filler was put in paper to achieve filler
16
concentrations ranging from 15 to 24 percent. For all studies, the filler bondability factor
(FBF) and other tensile properties of paper were determined and studied. FBF and paper
strength decreased as filler content in paper increased, but increased when preflocculated
filler was added. At a filler content of 24%, preflocculated filler resulted in increases in
Tensile Strength
theories regarding tensile strength of steel paper do not take into account the tensile
stiffness. Another issue is the micromechanical input. Few factors have a definite
None of the existing ideas link tensile strength to bonding degree or bonding value that
Chapter 3
METHODOLOGY
This chapter includes all about the tools and procedures and covers the analysis
and techniques that the researchers utilized and found useful. This presents the study's
setting, the methods used to acquire the data, and the data analytic techniques used to
Research Design
experimental design is an intelligent method of selecting input combinations for the aim
of decreasing the number of computer model runs for data analysis, inversion problems,
and input uncertainty evaluation (Mishra & Datta-Gupta, 2018). This study harvested,
utilized, and produced cogon grass as paper to determine its efficiency as a paper. The
Cogon Grass (Imperata cylindrica) paper was tested by researchers to learn its
private household with an open area and access to direct sunlight that was needed for the
experiment. This residence is situated in Purok 1, Basak Malutlut, Marawi City, Lanao
18
del Sur, 9700, Philippines. This neighborhood is comprised of different families mainly
from the Meranao tribe. A household in this neighborhood may be home to nuclear
families and even to clans. This residence was chosen because it has the needed utilities
Research Instrument
This segment includes the ingredients and materials needed for the production of
cogon grass paper. The following is the list of all the materials and tools that will be used
Table 1
List of all the Materials and Equipment that will be used in the Study.
cylindrica) as paper. The researchers began their data collection as soon as they had the
materials that are needed. The procedure for this experiment was observed in the video
“Kanami Koronadal – Cogon Paper Making”, as well as observed significant steps from
other related studies, and was applied in this experiment to make Cogon Grass (Imperata
cylindrica) as an alternative source of paper. After the experiment, the Cogon Grass as
of paper, in terms of the qualitative and quantitative properties of cogon grass as source
cogon grass paper. The step-by-step procedure and process is listed below.
To begin with, the Cogon Grass was harvested and collected. Exposure to direct
sunlight was requisite to the harvested grass to dry for a week. The color of the grass
turned brown or fully dried after a week of exposure from the sunlight, ensuring there
was no moisture found in the grass. The grass was removed from its stem and cut for
about 1 to 2 inches long. The cut grass was placed on the kitchen scale to measure its
mass.
The dried grass was soaked in a large basin with sodium bicarbonate for it to be
easier to process and made the grass pulp appear. After 30 minutes, the soaked grass was
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strained from the solution of sodium bicarbonate and water. In a boiling water-filled
cauldron, the grass was cooked for 5 hours long that made it tender. Five hours of
cooking has pass and the grass was let sit to cool down before rinsing. The cooked grass
was rinsed under running water twice to remove any toxins that were may be present
during cooking. The grass pulp was pounded using a pestle and mortar. The pounded
grass was then granulated using a commercial blender and grinded again but using a food
processor for even finer pieces. The grinded cogon grass was bleached in a water-filled
basin with chlorine to brighten its color. After 2 hours of bleaching, the bleached grass
pulp was rinsed multiple times under running water to remove the remains of chlorine
lingering to it.
In a basin, the binding agents, starch and potassium alum, were mixed in water.
The bleached cogon grass pulp was gradually added onto the mixture of binding
agent and stirred. The Silk screen was soaked in the mixture to gather pulp then
removed after accumulating the desired amount. The silk screen was wrapped in a dry
cloth; flipped together to make the dry cloth face downwards and silk screen facing
upwards. Excess water on the silk screen was discarded by gently dabbing a dry
sponge on top of the screen multiple times. Ensuring that the paper pulp was
transferred onto the cloth, the silk screen was gently removed. A rolling pin was used
to spread and flatten the surface of the pulp. The pulp on dry cloth was blow dried for
at least 10 minutes. Then the pulp was ironed by layering it with dry cloth on top to
ensure it does not burn from the hot flat iron. the ironed pulp was exposed to direct
sunlight to ensure no moisture was present and to fully dry the pulp. After the pulp
24
was dried, it was detached from the cloth that it was transferred to. The cogon grass
The researchers will analyze the qualitative properties of cogon grass paper in
terms of colors and textures. The researchers will meticulously examine the texture of the
cogon grass paper using their sense of touch. The researchers will flash a light onto the
paper using their mobile phones to scrutinize the texture of cogon grass paper through its
appearance. To assess the color of the grass, the researchers will use the Color Grab
Software installed on their mobile phones to determine the color of the paper,
The researchers will measure the quantitative property of cogon grass paper in
terms of grammage. In this analysis, scissors, digital weighing scale and tape measure are
required. To begin with, the researchers will trim the cogon grass paper into similar sizes.
A digital weighing scale is needed in this analysis to determine the grams of each cogon
grass paper. Each cogon grass paper is scaled by the researchers using this device while
ensuring to tare the scale. Next, the length and width of the cogon grass paper will be
measured by the researchers using a tape measure. Lastly, the area of each cogon grass
paper is calculated using the garnered data. The researchers will apply this technique to
The researchers will assess another quantitative property of the cogon grass paper
Spring Balance is used to measure the friction force of the cogon grass paper, and
marbles used as the load for this measurement. Firstly, the cogon grass paper is lain on a
flat surface. Marbles filled an empty pencil pouch to act as the load. The weight of the
load is calculated. Then, the newton meter is attached to the pencil pouch that has
marbles and is placed on the other end of the cogon grass paper. Next, the newton meter
is gently pulled across the opposite end of the cogon grass paper to measure the stability
The researchers will gauge the quantitative property of cogon grass paper in terms
of tensile index. Tensile index was used to measure and compare the inherent strengths of
The researchers will evaluate the quantitative property of cogon grass paper in
terms of tensile strength. In this method, the researchers required the cogon grass paper,
marbles, a small disposable cellophane, an inch sized binder clips, and digital weighing
scale. The researchers will cut the cogon grass paper to make paper strips that has the size
of 0.5 inch in width and 6 inches in length. Both ends of the paper has binder clips in it,
one hanging on the wall and the other carrying the weight. Marbles were gradually added
onto the cellophane to measure the load a cogon grass paper can withstand until it can no
In accordance with the objectives of this study and the statement of the problem,
the data that the researchers will gather will be subjected to tabulation, statistical analysis,
and interpretation. These analyses tend to show the patterns present in studies. The data
will be computed and analyzed using statistical tools to answer the problem of the study.
1. Grams per Square Meter. It is used to determine the grams of each paper
Where:
10000 = Constant
100 = Constant
Formula:
Where:
F = Frictional Force
N = Normal Force
Formula:
Where:
Nm = Tensile Strength
g/m2 = Grammage
4. Tensile Strength. It is used to measure the maximum load that a material can
support without fracture when being stretched, divided by the original cross-
the collected research data in a systematic and logical manner to properly assess
(imperata cylindrica) paper. This statistic measures the mean, median, mode, and
the central tendency of the provided information by the researchers, of the central
data.
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