PD Cen TR 13233-2007
PD Cen TR 13233-2007
PD Cen TR 13233-2007
13233:2007
Incorporating
corrigendum no. 1
Advanced technical
ceramics — Notations
and symbols
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PD CEN/TR 13233:2007
National foreword
English Version
This Technical Report was approved by CEN on 25 December 2006. It has been drawn up by the Technical Committee CEN/TC 184.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
© 2007 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TR 13233:2007: E
worldwide for CEN national Members.
CEN/TR 13233:2007
Contents Page
Foreword ............................................................................................................................................................. 3
1 Scope...................................................................................................................................................... 4
2 Normative references ........................................................................................................................... 4
3 Symbols, units and notations.............................................................................................................. 4
3.1 General symbols ................................................................................................................................... 4
3.2 Symbols and notations specific to ceramic matrix composites ...................................................... 4
3.3 Symbols, definitions and units............................................................................................................ 7
Bibliography ..................................................................................................................................................... 17
2
CEN/TR 13233:2007
Foreword
This document (CEN/TR 13233:2007) has been prepared by Technical Committee CEN/TC 184
“Advanced technical ceramics”, the secretariat of which is held by BSI.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such
patent rights.
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CEN/TR 13233:2007
1 Scope
This Technical Report defines the symbols to be used to represent physical, mechanical and thermal
characteristics, as determined by methods described in relevant CEN publications, for advanced
technical ceramics, including ceramic matrix composites. It is a guide for writing the symbols of
quantities of these materials to avoid confusion in reporting measurements and characteristics of
products.
Where possible, the definitions are in accordance with the relevant parts of ISO 31 and ISO 80000. In
addition the symbols used in undertaking measurements of these characteristics are also defined.
2 Normative references
Not applicable.
Contrary to monolithic materials, continuous fibre reinforced ceramic matrix composites show a
directional dependence in their thermal and mechanical properties, because of their anisotropic
nature. A specific set of standards different from those for monolithic materials is required in order to
characterize these properties, both at room temperature and at the anticipated high application
temperatures. To allow adequate representation of the directional dependence, a notation convention
is needed to identify the reinforcement directions in a right-hand orthogonal coordinate system for
purposes of sampling test pieces and for the presentation of results.
The use of the subscripts 1, 2, 3 attached to the symbols used for mechanical properties makes it
possible to define the mechanical characteristics of a material along one of its principal directions. The
use of the subscripts (12, 13, 23) attached to the symbols used for mechanical properties makes it
possible to give a material characteristics in one of the principal planes, for example:
Figures 1 to 4 give examples of denotation on long fibre ceramic matrix composite materials.
4
CEN/TR 13233:2007
Figure 1 — Schematic diagram of a 1D material (see 3.2 for reference to axes 1, 2 and 3)
Figure 2 — Schematic diagram of a 2D material (see 3.2 for reference to axes 1, 2 and 3)
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CEN/TR 13233:2007
Figure 4 — Schematic diagram of a 3D material (see 3.2 for reference to axes 1, 2 and 3)
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CEN/TR 13233:2007
Tables 1 to 4 give symbols, definitions and units generally used for quantities referred to in standards
for advanced technical ceramics.
NOTE The quantities listed are referred to in the standards given in the final column of each table, although
it is possible that the corresponding symbols have not been used. In this case, it is anticipated that they will be
incorporated in the next revision of the standard.
7
8
Table 1 — Symbols related to physical quantities
Physical quantities
Quantity Symbol Definition Unit Remark Relevant EN,
ENV or
CEN/TS
3
Density ρ Ratio of the mass of a body to its volume kg/m Applies to true density 623-2, 725-7,
of powders 1159-2
CEN/TR 13233:2007
3
Apparent density ρa Ratio of the mass of the body to its total kg/m Applies to compacted 725-10
volume powders
3
Bulk density ρb Ratio of the mass of the dry material of a kg/m Applies also to tapped 623-2, 725-8,
porous body to its volume bulk density of 1389
powders
Linear density t Ratio of the mass of a multifilament tow to its Tex Tex is the mass in 1007-2
length grams per 1 000 m
Porosity P Ratio of the total volume of pores in a - 623-2, 1389
porous body to its total volume
Apparent porosity Pa Ratio of the volume of open pores to total - 623-2, 1389
volume
Grain size gmli Mean linear intercept grain size determined µm 623-2
either by the line or circle method applied to
micrographs of polished cross-sections
Phase volume fraction Vf,j Fractional volume of phase of type j - 623-5
determined from micrographs of polished
cross-sections
Table 2 — Symbols related to geometrical quantities of test pieces
Geometrical quantities
Quantity Symbol Definition Unit Remark Relevant EN,
ENV or
CEN/TS
Length
Total length l, lt Total length of the test piece mm 843-1, 843-2
Initial length l0 Initial length of test piece in thermal mm 821-1
expansion measurement
Gauge length L0 Initial distance between reference points on mm 658-1, 658-2,
the test piece in the calibrated length 1892, 1893
Distance between outer rollers La Outer support span in three or four-point mm In flexural strength and 658-3
bending configuration modulus testing
Distance between inner rollers Li Inner loading span in four-point bending mm In flexural strength and 821-1, 843-1,
configuration modulus testing 843-2, 843-3,
658-3
2
Cross-section A Cross-section area mm
2
Initial cross-section area A0 Initial cross-section area of the test piece mm 1892
within the calibrated length at test
temperature
NOTE 1 When the material is protected by a surface treatment, two initial cross-section areas can be defined:
2
Apparent cross-section area A0,a Geometrical area of the cross-section mm 1893
2
Effective cross-section area A0,e Geometrical area corrected by a factor, to mm 1893
account for the presence of a surface
treatment
Distance between notches L In inter-laminar shear testing, the spacing mm 658-4, 1894
between opposed notches
Width and thickness
Width b Width of a test piece (normal to loading mm 658-3, 843-1,
direction in flexure) 843-2, 1892
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CEN/TR 13233:2007
10
Geometrical quantities
Quantity Symbol Definition Unit Remark Relevant EN,
ENV or
CEN/TS
NOTE 2 When the material is protected by a surface treatment, two widths can be defined :
Apparent width ba Geometrical width mm 1893
Effective width be Geometrical width corrected by a factor to mm 1893
CEN/TR 13233:2007
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12
Table 3 — Symbols related to mechanical quantities
Mechanical quantities
Quantity Symbol Definition Unit Remark Relevant EN,
ENV or
CEN/TS
Deformation
CEN/TR 13233:2007
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14
Mechanical quantities
Quantity Symbol Definition Unit Remark Relevant EN,
ENV or
CEN/TS
In plane shear strength τm Ratio of the maximum force applied to the MPa 658-4, 658-5,
initial cross-section area 658-6, 12289
NOTE 1 The symbols listed here for mechanical quantities at rupture (strength and strain) have a first subscript indicating the type of test (t for tensile, c for compressive, f for
CEN/TR 13233:2007
flexure).
A second subscript, m is added to indicate the maximum value. Other subscripts may be added to refer to test conditions (for example temperature). These additional subscripts
are set between brackets.
EXAMPLE 1 σt, m (1500)(vacuum) = tensile strength at 1 500 °C under vacuum
Elastic properties
ˆElastic modulus tension/compression E Slope of the linear part of the stress strain GPa 658-1, 658-2,
(Young 's modulus)‰ curve when the linear part starts at the origin 1892, 12289
Elastic modulus in shear G Slope of the linear part of the shear stress GPa 843-2
strain curve when the linear part starts at the
origin
NOTE 2 When the material is protected by a surface treatment, two types of mechanical quantities can be considered to determi
ne whether the apparent or effective cross-
section area is used:
The subscript 'a' for apparent is added when the apparent cross-section area is used.
The subscript 'e' for effective is added when the effective cross-section area is used.
EXAMPLE 2 σt,m,e = effective tensile strength
Proportionality Coefficient Or Pseudo Modulus
ˆProportionality coefficien t in Ep (σ1,σ2) Slope of a linear portion of the stress strain GPa The quantity is used for 658-1, 658-2,
tension/compressi on ‰ curve between 2 values (σ1, σ2) materials which do not 1892, 12289
have a linear behaviour
Proportionality coefficient in shear Gp (τ1 , τ2) Slope of a linear portion of the shear GPa
at the origin
stress shear strain curve between 2 values
ˆ(τ 1, τ 2 ) ‰
Poisson ratio ν Ratio of lateral strain to axial strain in axially - 843-2
τ
stressed body
Mode of vibration n Modal analysis is used to characterize -
resonant vibration in machinery and
structures. A mode of vibration is defined
by the three parameters: modal frequency,
Mechanical quantities
Quantity Symbol Definition Unit Remark Relevant EN,
ENV or
CEN/TS
modal damping value and mode shape.
Flexural frequency ff Recorded flexural vibration frequency of Hz 843-2
struck or resonating test piece
Torsional frequency ft Recorded torsional vibration frequency of Hz 843-2
struck or resonating test piece
Longitudinal wave sound velocity νl Velocity of a compression wave transmitted m/s Used in computation of 843-2
through a material moduli in ultrasonic
Transverse wave sound velocity Velocity of a shear wave transmitted through m/s testing
νt
a material
Ultrasonic pulse width τ Duration of an ultrasonic pulse transmitted s 843-2
through a material
15
CEN/TR 13233:2007
16
Table 4 — Symbols related to thermal quantities
Thermal quantities
Quantity Symbol Definition Unit Remark Relevant
EN, ENV or
CEN/TS
Linear thermal expansion ∆L Positive or negative change in one mm 821-1, 1159-
dimension that occurs when a material is 1
CEN/TR 13233:2007
Bibliography
[1] EN 623-1:2006, Advanced technical ceramics — Monolithic ceramics — General and textural
properties — Part 1: Determination of the presence of defects by dye penetration
[2] EN 623-2:1993, Advanced technical ceramics — Monolithic ceramics — General and textural
properties — Part 2: Determination of density and porosity
[3] EN 623-3:2001, Advanced technical ceramics — Monolithic ceramics — General and textural
properties — Part 3: Determination of grain size and size distribution (characterized by the
Linear Intercept Method)
[4] EN 623-4:2004, Advanced technical ceramics — Monolithic ceramics — General and textural
properties — Part 4: Determination of surface roughness
[5] ENV 623-5:2002, Advanced technical ceramics — Monolithic ceramics — General and
textural properties — Part 5: Determination of phase volume fraction by evaluation of
micrographs
[12] EN 725-1:1997, Advanced technical ceramics — Methods of test for ceramic powders — Part
1: Determination of impurities in alumina
[13] ENV 725-2:1994, Advanced technical ceramics — Methods of test for ceramic powders —
Part 2: Determination of impurities in barium titanate
[14] EN 725-3:2007, Advanced technical ceramics — Methods of test for ceramic powders — Part
3: Determination of the oxygen content of non-oxides by thermal extraction with a carrier gas
[15] EN 725-4:2006, Advanced technical ceramics — Methods of test for ceramic powders — Part
4: Determination of oxygen content in aluminium nitride by XRF analysis
[16] EN 725-5:2007, Advanced technical ceramics — Methods of test for ceramic powders — Part
5: Determination of particle size distribution
17
CEN/TR 13233:2007
[17] EN 725-6:1996, Advanced technical ceramics — Methods of test for ceramic powders — Part
6: Determination of the specific surface area [withdrawn – see also EN ISO 18757]
[18] EN 725-7:1995, Advanced technical ceramics — Methods of test for ceramic powders — Part
7: Determination of the absolute density [withdrawn – see also EN ISO 18753]
[19] EN 725-8:2006, Advanced technical ceramics — Methods of test for ceramic powders — Part
8: Determination of tapped bulk density
[20] EN 725-9:2006, Advanced technical ceramics — Methods of test for ceramic powders — Part
9: Determination of un-tapped bulk density
[21] EN 725-10:1997, Advanced technical ceramics — Methods of test for ceramic powders —
Part 10: Determination of compaction properties
[22] EN 725-11:2006, Advanced technical ceramics — Methods of test for ceramic powders —
Part 11: Determination of densification on natural sintering
[23] EN 725-12:2001, Advanced technical ceramics — Methods of test for ceramic powders —
Part 12: Chemical analysis of zirconia
[28] CEN/TS 820-5:2004, Advanced technical ceramics — Methods of testing monolithic ceramics
— Thermo-mechanical properties — Part 5: Determination of elastic moduli at elevated
temperatures
18
CEN/TR 13233:2007
[38] ENV 1006:2003, Advanced technical ceramics — Monolithic ceramics — Guidance on the
selection of test pieces for the evaluation of properties
[39] EN 1007-1:2002, Advanced technical ceramics — Ceramic composites — Methods of test for
reinforcements — Part 1: Determination of size content
[40] EN 1007-2:2002, Advanced technical ceramics — Ceramic composites — Methods of test for
reinforcements — Part 2: Determination of linear density
[41] EN 1007-3:2002, Advanced technical ceramics — Ceramic composites — Methods of test for
reinforcements — Part 3: Determination of filament diameter and cross-section area
[42] EN 1007-4:2004, Advanced technical ceramics — Ceramic composites — Methods of test for
reinforcements — Part 4: Determination of tensile properties of filaments at ambient
temperature
[43] EN 1007-5:2003, Advanced technical ceramics — Ceramic composites — Methods of test for
reinforcements — Part 5: Determination of distribution of tensile strength and of tensile strain
to failure of filaments within a multifilament tow at ambient temperature
[44] ENV 1007-6:2002, Advanced technical ceramics — Ceramic composites — Methods of test
for reinforcements — Part 6: Determination of tensile properties of filaments at high
temperature
[45] EN 1071-1:2003, Advanced technical ceramics — Methods of test for ceramic coatings — Part
1: Determination of coating thickness by contact probe filometer
[46] EN 1071-2:2002, Advanced technical ceramics — Methods of test for ceramic coatings — Part
2: Determination of coating thickness by the crater grinding method
[47] EN 1071-3:2005, Advanced technical ceramics — Methods of test for ceramic coatings — Part
3: Determination of adhesion and other mechanical failure modes by a scratch test
[48] EN 1071-4:2006, Advanced technical ceramics — Methods of test for ceramic coatings — Part
4: Determination of chemical composition by electron probe microanalysis (EPMA)
[49] ENV 1071-5:1995, Advanced technical ceramics — Methods of test for ceramic coatings —
Part 5: Determination of porosity
[50] ENV 1071-6:2002, Advanced technical ceramics — Methods of test for ceramic coatings —
Part 6: Determination of the abrasion resistance of coatings by a micro-abrasion wear test
[51] CEN/TS 1071-7:2003, Advanced technical ceramics — Methods of test for ceramic coatings
— Part 7: Determination of hardness and Young's modulus by instrumented indentation
testing
[52] CEN/TS 1071-8:2004, Advanced technical ceramics — Methods of test for ceramic coatings
— Part 8: Rockwell indentation test for evaluation of adhesion
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CEN/TR 13233:2007
[53] CEN/TS 1071-9:2004, Advanced technical ceramics — Methods of test for ceramic coatings
— Part 9: Determination of fracture strain
[54] CEN/TS 1071-10:2004, Advanced technical ceramics — Methods of test for ceramic coatings
— Part 10: Determination of coating thickness by cross sectioning
[55] CEN/TS 1071-11:2005, Advanced technical ceramics — Methods of test for ceramic coatings
— Part 11: Determination of internal stress by the Stoney formula
[64] ENV 12212:1995, Advanced technical ceramics — Unified method for classification
20
CEN/TR 13233:2007
[71] ENV 12923-2:2001, Advanced technical ceramics — Monolithic ceramics — Part 2: Oxidation
test
[75] ENV 14226:2002, Advanced technical ceramics — Test methods for ceramic powders —
Determination of calcium, magnesium, iron and aluminium in silicon nitride by using flame
atomic absorption spectroscopy (FAAS) or inductively coupled plasma atomic emission
spectroscopy (ICP-AES)
[76] ENV 14232:2003, Advanced technical ceramics — Terms, definitions and abbreviations
[79] CEN/TS 14425-1:2003, Advanced technical ceramics — Test methods for determination of
fracture toughness of monolithic ceramics — Part 1: Guide to test method selection
[80] CEN/TS 14425-3:2003, Advanced technical ceramics — Test methods for determination of
fracture toughness of monolithic ceramics — Part 3: Chevron notched beam (CNB) method
[81] CEN/TS 14425-5:2004, Advanced technical ceramics — Test methods for determination of
fracture toughness of monolithic ceramics — Part 5: Single-edge vee-notch beam (SEVNB)
method
[82] EN ISO 15732:2005, Fine ceramics (advanced ceramics, advanced technical ceramics) —
Test method for fracture toughness of monolithic ceramics at room temperature by single edge
pre-cracked beam (SEPB) method (ISO 15732:2003)
[83] EN ISO 18753:2005, Fine ceramics (advanced ceramics, advanced technical ceramics) —
Determination of absolute density of ceramic powders by pyknometer (ISO 18753:2004)
[84] EN ISO 18756:2005, Fine ceramics (advanced ceramics, advanced technical ceramics) —
Determination of fracture toughness of monolithic ceramics at room temperature by the
surface crack in flexure (SCF) method (ISO 18756:2003)
[85] EN ISO 18757:2005, Fine ceramics (advanced ceramics, advanced technical ceramics) —
Determination of specific surface area of ceramic powders by gas adsorption using the BET
method (ISO 18757:2003)
[87] ISO 80000-3:2006 Quantities and units — Part 3: Space and time
21
PD CEN/TR
13233:2007
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