CoA P873870

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CERTIFIED REFERENCE MATERIAL

Acetaldehyde [CAS:75-07-0] 1000 ug/ml in Water
Lot N: XXXXXX Ref N: P873870 Certification Date:XXXXXX

Barcode: XXXXXXXX
Component Certified Value* CAS Chemical Formula

and uncertainty [µg/ml]
Acetaldehyde 1002.3 ± 9.3 75-07-0 C2H4O
* WQP 5.15.1/2 The certified value was obtained gravimetrically and confirmed experimentally by GC/MS or HPLC
Density 0.996 g/cm3 at 20°C
Starting Material Purity, Batch

Acetaldehyde 99.6% (41340639)
Storage Conditions: Store in a freezer at -18°C or below
Expiry Date: XXXXXXXXXX

Concept of Certification and traceability statement:
This certified reference material is produced by gravimetric measurement and dissolving the individual substances in Water .
The reported expanded uncertainty of measurement is stated as the standard uncertainty of measurement multiplied by the coverage factor k = 2, which for a
normal distribution corresponds to a coverage probability of approximately 95%. The standard uncertainty of measurement has been determined in
accordance with EA 4/02 and incorporates the uncertainties of the raw-material purity, the mass and the volume.
The metrological traceability is defined as the “property of a measurement result whereby the result can be related to a reference through a documented
unbroken chain of calibrations, each contributing to the measurement uncertainty”.
The metrological traceability is ensured through gravimetric measurement and dissolving of certified reference material/s (traceable to SI) from
laboratories/producers, accredited according to ISO 17034.
The measurement results are traceable to SI. All analytical balances used for the preparation of the solution are calibrated yearly under an in-house
procedure with class E1 and class E2 analytical weights, traceable to SI (DKD), and are checked daily.
Class A laboratory glassware is used.
The results from temperature measurement are traceable to SI. The thermometers used for solution's calibration are calibrated from an ISO 17025 accredited
laboratory. The ambient conditions are controlled with a hygrometer calibrated from an ISO 17025 accredited laboratory.
Both, purity of the starting materials and solvent, were checked using appropriate analytical instrument.
Intended use: For Laboratory Use Only

This CRM is intended for:
Calibration of TLC, GC/FID, GC/TCD, GC/ECD, GC/MS, GC/MS/MS, LC/UV, LC/MS and LC/MS/MS
Validation of analytical methods
Preparation of “working reference samples”
Detection limit and linearity studies
This statement is not intended to restrict the use for other purposes.
Instructions for the correct use of this certified reference material:

This CRM can be used directly or can be diluted in an appropriate solvent. Only a clean class A glassware should be used. Do not pipet from container.
Obtained concentration (in mg/l) after dilution is a result from the multiplication of certified value of CRM concentration and the CRM's volume used for
dilution and divided into the flask's volume used for dilution. For quantitative analysis, we recommend analyzing this mixture separately, without mixing it with
other solutions, to ensure accurate results for every compound.
Stability and storage:

This CRM is with a guaranteed stability until ±5% of the certified concentration for a period of 24 months. Stability is guaranteed of an unopened original
packaging stored, as written in the section: Storage Conditions. Even if the product is stable at normal laboratory conditions, in order to increase its stability,
we highly recommend it to be stored in a refrigerator.
The product should be used shortly after opening to avoid concentration changes due to evaporation. Warranty does not apply to a product stored after
opening.
Hazardous situation:
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The normal laboratory safety precautions should be observed when working with this RM. Further details for the handling of this RM are available in a safety
data sheet.
Level of homogeneity
This solution was mixed according to an in-house procedure (MQP 5.13.1) and is guaranteed to be homogeneous.
To ensure sufficient homogeneity of the sample prior to use thoroughly mix by inversion or sonicate.
Names of certifying officers:
Laboratory: Margarita Dimitrova
Manager: Krassimira Taralova
This document QF 5.17.1/1 version 1 is designed and the certified value(s) and uncertainty(ies) are determined in accordance with ISO Guide 31, ISO Guide
35,and Eurachem / CITAC Guides
This certificate relates solely to the lot number given above.

All processes (including generating of this certificate) are completely controlled by the specialized Computer-Aided-Manufacturing (CAM) software.
This Certified Reference Material was produced under a quality management system that is:
- Registered to ISO 9001 Quality Management System (Lloyd's Register Quality Assurance Ltd Cert No 0039638)
- Accredited according to ISO/IEC 17025 – Testing (ANAB Cert No AT-1836)
- Accredited according to ISO 17034 - Reference Material Producer (ANAB Cert No AR-1835)
Additional Information
Gravimetric Data
Component Purity Source Weighed Final Bulk/ Concen- Chemist

% Lot No quantity, g quantity, Standard tration ID
kg.10-3 Solution mg/kg
lot No
Acetaldehyde 99.6 41340639 0.5698 2.9951 91650665 189483 AS
91650665 1.3224 249.072 XXXXXXXX 1006.02 PA

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CERTIFIED REFERENCE MATERIAL

Lot N: XXXXXX Ref N: P873870 Certification Date:XXXXXX

Component Certified Value* CAS Chemical Formula

Density 0.996 g/cm3 at 20°C

Starting Material Purity, Batch

Storage Conditions: Store in a freezer at -18°C or below

Expiry Date: XXXXXXXXXX

Intended use: For Laboratory Use Only

Instructions for the correct use of this certified reference material:

Stability and storage:

Names of certifying officers:

Laboratory: Margarita Dimitrova

Manager: Krassimira Taralova

This certificate relates solely to the lot number given above.

Component Purity Source Weighed Final Bulk/ Concen- Chemist

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