REV. DATE BY CHK APP.

CLIENT: HMEL REFINERY

0 Jan-23 NA MB MB
1 May-23 NA MB MB
LOCATION: BATHINDA, PUNJAB
2 May-23 NA MB MB
IC4 PRODUCTION FROM ISOM STAB.
PROJECT: Column Process Datasheet
REFLUX STREAM
1 EQUIPMENT TAG#: 504-C-002
2 SERVICE: Deethanizer Column
3 OPERATING DESIGN
4 PRESSURE kg/cm2G kg/cm2G
5 Top (Note-1) 10.0 / 12.8 / 12.8 / 12.8
31.0
6 Bottom (Note-1) 10.2 / 13.0 / 13.0 / 13.0
7 TEMPERATURE °C °C
8 Top (Note-1) 58.1 / 68.9 / 75.4 / 67.0
122
9 Bottom (Note-1) 114.8 / 111.1 / 115.1 / 114.3
10
11 SHELL / TRAYS /
12 HEADS PACKINGS
13 MATERIAL CS SS-304
14 CORR. ALLOW. 3.0 mm -
15 SERVICE FLUID Hydrocarbon
16 DENSITY @ BOTTOM (Note-2) kg/m³
17 INSULATION HOT
18 LINING N/A
19
20 NOTES:
21 1) Values are provided for Case1 / Case 2 / Case 3 / Case 4
22 2) Refer to the attached stream summary for flowrate
23 and fluid physical properties at each nozzle
24 3) Streams 123 and 124 are based on 30wt% vaporization in the
25 reboiler. Actual circulation rate to be determined by DEC.
26 4) DEC to evaluate the thickness of insulation.
27
28
29
30
Refer attached sketch
31
32
33
34
35 NOZZLE SUMMARY
36 NOZZ. SIZE NO. SERVICE
37 I1 2" (Existing 1 Feed In
38 I2 2" (Existing) 1 Reflux In
39 I3 8" (Existing) 1 Reboiler Return
40 01 6" (Existing) 1 Vapor Out
41 02 6" (Existing) 1 Liq To reboiler
42 MH1-2 18" (Existing) 2 Manhole
43
44 P1-P5 NOTE-12,9 5 Pressure Indicator
45 T1 NOTE-12,9 1 1 Temperature Controller
46 T2-T6 NOTE-12,9 5 Temperature Indicator
51
52 V 2" 1 Vent
53 UC 2" 1 Utility Connection
54
55
56
57
58
59
60
61
62
63
64
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the prior written consent of DWC Innovations LLC.

134 of 346
 820 I.D.
EXISTING VESSEL
01

NOTES
T.L.
1. REMOVE EXISTING TRAYS, SEAL PAN AND REPLACE WITH
PACKING AS SHOWN IN SKETCH. USE EXISTING SUPPORT
RINGS. NO WELDING ON VESSEL SHELL ALLOWED. IF ANY
NOTE 9 WELDING IS REQUIRED, VENDOR TO CONTACT LICENSOR.
1000

I2 2. PACKING:
TYPE: KOCH-GLITSCH FLEXIPAC 350Y OR EQUAL
VOLUME: 0.72 m³ BED #1 ; 3.49 m³ BED #2 (4.21m³ TOTAL)
LD-1 EXIST. T#18
NOTE 5 3. DELETED 1
450

EXIST. T#17
4. GRID-TYPE PACKED BED SUPPORT WITH MIN. 95% OPEN
AREA. GRID SUPPORT TO BE DESIGNED FOR SUM OF (a)
1350

BED #1 PACKING BULK DENSITY PLUS (b) LIQUID HOLDUP = 0.25 m³/m³

EXIST. T#14 5. LIQUID DISTRIBUTOR DESIGN PER VENDOR. DISTRIBUTOR

RANGE = 110-50% ALL CASES. RISER (VAPOR) AREA TO BE
MH- MIN. 15% OF COLUMN AREA.
I1 NOTE 8
1200

1 1
6. ALLOWABLE PRESSURE DROP FOR INTERNALS = 0.20 kg/cm2
LD-2 EXIST. T#13
NOTE 5 7. WITH EXISTING VORTEX BREAKER
600

EXIST. T#12
8. REPLACE EXISTING FEED DISTRIBUTOR WITH NEW FEED
14200

DISTRIBUTOR. DISTRIBUTOR DESIGN BY VENDOR.

6600

BED #2
9. REMOVE INLET DEFLECTOR BAFFLE FOR NOZZLE “12” AND
EXIST. T#1
1

REPLACE WITH NEW DISTRIBUTOR. DESIGN BY PACKING

VENDOR.
1350

I3
2 MAY-23 Issued for BEP NA MB MB
400

NHLL
1 MAY-23 Issued for BEP NA MB MB
140

0 Jan-23 Issued for BEP NA MB MB

LAH
Rev. Date Modification By Chk Appr.
1070
1350

LAL

NLLL
MH-
300

2
T.L. HMEL REFINERY
BHATINDA, PUNJAB
02

NOTE 7
COLUMN SKETCH
504-C-002 DEETHANIZER

DWG No: DWG-504-C-002-001

136 of 346
 REV. DATE BY CHK APP.
CLIENT: HMEL REFINERY
0 Jan-23 NA MB MB
LOCATION: BATHINDA, PUNJAB 1 Jun-23 KM NA MB
Hydraulic Loading (Case - 1)
IC4 PRODUCTION FROM ISOM Deethanizer Column
PROJECT:
STAB. REFLUX STREAM 504-C-002

Vapor to / From Tray Liquid From / to Tray

Temp Pressure Flow Flow Molecular Density Viscosity Temp Flow Flow Density Viscosity Surface
Stage T P Weight Volume Weight at P.T at P.T T Weight Volume at P.T at P.T Tension
Description
3 3 3 3
ºC kg/cm2G kg/h Act_m /s kg/m CP ºC kg/h Act_m /hr kg/m CP dyn/cm

BED#1 TOP 62.1 10.0000 1,243 0.0138 52.3 25.074 0.00960 54.4 1,018 2.02 503.92 0.1139 6.30

BED#1 BTM 76.9 10.0280 1,370 0.0136 59.0 28.076 0.00969 80.6 1,145 2.23 514.50 0.1119 6.24

BED#2 TOP FEED 93.0 10.0350 2,092 0.0207 60.4 26.776 0.00990 76.9 5,867 10.89 539.01 0.1253 7.65

BED#2 BTM 114.8 10.2100 3,646 0.0335 69.0 30.279 0.00985 110.2 7,422 14.73 503.81 0.0996 5.30

Confidential information of DWC Innovations LLC. This information is to be held in confidence. Disclosure, Reproduction OR other use of this document is prohibited without the prior written consent of DWC
Innovations LLC.

137 of 346
 REV. DATE BY CHK APP.
CLIENT: HMEL REFINERY
0 Jan-23 NA MB MB

LOCATION: BATHINDA, PUNJAB

Stream Summary
IC4 PRODUCTION FROM ISOM
PROJECT:
STAB. REFLUX STREAM
[Case - 1]
Stream No. (Nozzle Name) 117 (I1) 118 (01) 121 (I2) 123 (02) 124 (I3)
125 (02)
De-
Vapors
2 Phase ethanizer
From De-
Feed to De- Reboiler Column
ethanizer Reflux to Liquid to
ethanizer outlet to Bottoms to
Stream Description Units Column to Column Reboiler
Column Column iC4
Condenser 504-C-002 504-E-013
[504-C- 504-C-002 Column
[504-E-
002] [503-C-
012]
004]
Phase
Total
Temperature C 50.6 58.1 40.6 114.8 117.5 115.2
Pressure kg/cm2G 10.0 10.0 15.0 10.2 10.2 13.0
Vap. Frac on Mass Basis - 0.0019 1.0000 0.0000 0.0000 0.2934 0.0000
Mass Flow kg/hr 4,000.3 1,177.3 952.5 12,541.9 12,541.9 3,775.4
Molecular Weight - 68.78 50.32 52.68 71.45 71.45 71.45
Vapor Phase
Mass Flow kg/hr 7.6 1,177.3 - - 3,679.2 -
Actual Volume Flow m3/h 0.8 48.7 - - 120.5 -
Molecular Weight - 22.85 50.32 - - 69.86 -
Molar Flow kgmole/h 0.33 23.40 - - 52.66 -
Mass Density kg/m3 9.490 24.190 - - 30.530 -
Viscosity cP 0.014 0.010 - - 0.010 -
Z Factor - 0.971 0.817 - - 0.777 -
Liquid Phase
Mass Flow kg/hr 3,992.6 - 952.5 12,541.9 8,862.7 3,775.4
Actual Volume Flow m3/h 6.9 - 1.9 24.9 17.6 7.5
Molar Flow kgmole/h 57.8 - 18.1 175.5 122.9 52.8
Molecular Weight - 69.05 - 52.68 71.45 72.13 71.45
Mass Density kg/m3 579.7 - 513.5 503.9 503.8 504.4
Viscosity cP 0.163 - 0.120 0.098 0.098 0.098
Surface Tension dyne/cm 10.86 - 7.11 5.25 5.22 5.22
Confidential information of DWC Innovations LLC. This information is to be held in confidence. Disclosure, Reproduction or other use of this document is prohibited without the prior written
consent of DWC Innovations LLC.

138 of 346
 REV. DATE BY CHK APP.
CLIENT: HMEL REFINERY
0 Jan-23 NA MB MB
LOCATION: BATHINDA, PUNJAB 1 Jun-23 KM NA MB
Hydraulic Loading (Case - 2)
IC4 PRODUCTION FROM ISOM Deethanizer Column
PROJECT:
STAB. REFLUX STREAM 504-C-002

Vapor to / From Tray Liquid From / to Tray

Temp Pressure Flow Flow Molecular Density Viscosity Temp Flow Flow Density Viscosity Surface
Stage T P Weight Volume Weight at P.T at P.T T Weight Volume at P.T at P.T Tension
Description
3 3 3 3
ºC kg/cm2G kg/h Act_m /s kg/m CP ºC kg/h Act_m /hr kg/m CP dyn/cm

BED#1 TOP 73.6 12.8000 3,072 0.0265 52.5 32.166 0.01000 62.9 2,915 5.92 492.24 0.1015 5.70

BED#1 BTM 86.5 12.8280 3,604 0.0276 58.4 36.220 0.01006 89.4 3,447 7.06 487.98 0.0964 4.98

BED#2 TOP FEED 98.7 12.8350 4,843 0.0375 59.4 34.554 0.01022 86.5 9,488 18.76 505.85 0.1042 5.83

BED#2 BTM 111.1 13.0100 6,467 0.0490 63.3 36.686 0.01019 107.7 11,112 23.08 481.44 0.0905 4.34

Confidential information of DWC Innovations LLC. This information is to be held in confidence. Disclosure, Reproduction OR other use of this document is prohibited without the prior written consent of DWC
Innovations LLC.

139 of 346
 REV. DATE BY CHK APP.
CLIENT: HMEL REFINERY
0 Jan-23 NA MB MB

LOCATION: BATHINDA, PUNJAB

Stream Summary
IC4 PRODUCTION FROM ISOM
PROJECT:
STAB. REFLUX STREAM
[Case - 2]
Stream No. 117 (I1) 118 (01) 121 (I2) 123 (02) 124 (I3)
125 (02)
De-
Vapors
2 Phase ethanizer
From De-
Feed to De- Reboiler Column
ethanizer Reflux to Liquid to
ethanizer outlet to Bottoms to
Stream Description Units Column to Column Reboiler
Column Column iC4
Condenser 504-C-002 504-E-013
[504-C- 504-C-002 Column
[504-E-
002] [503-C-
012]
004]
Phase
Total
Temperature C 50.5 68.9 40.6 111.1 113.0 111.1
Pressure kg/cm2G 12.8 12.8 17.8 13.0 13.0 13.0
Vap. Frac on Mass Basis - 0.0006 1.0000 0.0000 0.0000 0.2931 0.0000
Mass Flow kg/hr 4,801.7 2,738.0 2,581.4 21,967.3 21,967.3 4,645.1
Molecular Weight - 63.78 49.87 50.96 65.39 65.39 65.39
Vapor Phase
Mass Flow kg/hr 2.8 2,738.0 - - 6,439.7 -
Actual Volume Flow m3/h 0.2 90.3 - - 174.6 -
Molecular Weight - 22.03 49.87 - - 63.90 -
Molar Flow kgmole/h 0.13 54.91 - - 100.78 -
Mass Density kg/m3 11.517 30.318 - - 36.886 -
Viscosity cP 0.014 0.010 - - 0.010 -
Z Factor - 0.966 0.784 - - 0.743 -
Liquid Phase
Mass Flow kg/hr 4,798.9 - 2,581.4 21,967.3 15,527.5 4,645.1
Actual Volume Flow m3/h 8.5 - 5.0 45.5 32.2 9.6
Molar Flow kgmole/h 75.2 - 50.7 335.9 235.1 71.0
Molecular Weight - 63.85 - 50.96 65.39 66.03 65.39
Mass Density kg/m3 562.1 - 512.3 482.5 482.6 482.5
Viscosity cP 0.146 - 0.114 0.090 0.090 0.090
Surface Tension dyne/cm 9.91 - 7.22 4.32 4.30 4.32
Confidential information of DWC Innovations LLC. This information is to be held in confidence. Disclosure, Reproduction or other use of this document is prohibited without the prior written
consent of DWC Innovations LLC.

140 of 346
 REV. DATE BY CHK APP.
CLIENT: HMEL REFINERY
0 Jan-23 NA MB MB
LOCATION: BATHINDA, PUNJAB 1 Jun-23 KM NA MB
Hydraulic Loading (Case - 3)
IC4 PRODUCTION FROM ISOM Deethanizer Column
PROJECT:
STAB. REFLUX STREAM 504-C-002

Vapor to / From Tray Liquid From / to Tray

Temp Pressure Flow Flow Molecular Density Viscosity Temp Flow Flow Density Viscosity Surface
Stage T P Weight Volume Weight at P.T at P.T T Weight Volume at P.T at P.T Tension
Description
3 3 3 3
ºC kg/cm2G kg/h Act_m /s kg/m CP ºC kg/h Act_m /hr kg/m CP dyn/cm

BED#1 TOP 79.3 12.8000 2,099 0.0178 54.1 32.719 0.01010 68.3 2,007 4.06 494.70 0.1031 5.73

BED#1 BTM 87.1 12.8280 2,547 0.0188 59.9 37.719 0.01007 93.3 2,454 5.01 490.10 0.0966 4.99

BED#2 TOP FEED 103.5 12.8350 3,752 0.0280 60.9 35.079 0.01028 87.1 8,457 16.45 514.09 0.1078 6.20

BED#2 BTM 115.1 13.0100 5,563 0.0416 64.7 37.180 0.01024 111.6 10,269 21.30 482.14 0.0898 4.30

Confidential information of DWC Innovations LLC. This information is to be held in confidence. Disclosure, Reproduction OR other use of this document is prohibited without the prior written consent of DWC
Innovations LLC.

141 of 346
 REV. DATE BY CHK APP.
CLIENT: HMEL REFINERY
0 Jan-23 NA MB MB

LOCATION: BATHINDA, PUNJAB

Stream Summary
IC4 PRODUCTION FROM ISOM
PROJECT:
STAB. REFLUX STREAM
[Case - 3]
Stream No. 117 (I1) 118 (01) 121 (I2) 123 (02) 124 (I3)
125 (02)
De-
Vapors
2 Phase ethanizer
From De-
Feed to De- Reboiler Column
ethanizer Reflux to Liquid to
ethanizer outlet to Bottoms to
Stream Description Units Column to Column Reboiler
Column Column iC4
Condenser 504-C-002 504-E-013
[504-C- 504-C-002 Column
[504-E-
002] [503-C-
012]
004]
Phase
Total
Temperature C 50.6 75.4 40.5 115.1 117.1 115.1
Pressure kg/cm2G 12.8 12.8 17.8 13.0 13.0 13.0
Vap. Frac on Mass Basis - 0.0005 1.0000 0.0000 0.0000 0.2932 0.0000
Mass Flow kg/hr 4,797.6 1,802.5 1,710.2 18,952.8 18,952.8 4,705.3
Molecular Weight - 65.58 51.54 53.10 66.84 66.84 66.84
Vapor Phase
Mass Flow kg/hr 2.2 1,802.5 - - 5,557.1 -
Actual Volume Flow m3/h 0.2 58.6 - - 148.5 -
Molecular Weight - 19.87 51.54 - - 65.33 -
Molar Flow kgmole/h 0.11 34.97 - - 85.06 -
Mass Density kg/m3 10.301 30.770 - - 37.422 -
Viscosity cP 0.014 0.010 - - 0.010 -
Z Factor - 0.974 0.784 - - 0.741 -
Liquid Phase
Mass Flow kg/hr 4,795.4 - 1,710.2 18,952.8 13,395.7 4,705.3
Actual Volume Flow m3/h 8.4 - 3.3 39.3 27.7 9.7
Molar Flow kgmole/h 73.0 - 32.2 283.5 198.5 70.4
Molecular Weight - 65.65 - 53.10 66.84 67.49 66.84
Mass Density kg/m3 568.6 - 523.4 482.7 482.7 482.7
Viscosity cP 0.151 - 0.122 0.089 0.089 0.089
Surface Tension dyne/cm 10.30 - 7.84 4.27 4.24 4.27
Confidential information of DWC Innovations LLC. This information is to be held in confidence. Disclosure, Reproduction or other use of this document is prohibited without the prior written
consent of DWC Innovations LLC.

142 of 346
 REV. DATE BY CHK APP.
CLIENT: HMEL REFINERY
0 Jan-23 NA MB MB
LOCATION: BATHINDA, PUNJAB 1 Jun-23 KM NA MB
Hydraulic Loading (Case - 4)
IC4 PRODUCTION FROM ISOM Deethanizer Column
PROJECT:
STAB. REFLUX STREAM 504-C-002

Vapor to / From Tray Liquid From / to Tray

Temp Pressure Flow Flow Molecular Density Viscosity Temp Flow Flow Density Viscosity Surface
Stage T P Weight Volume Weight at P.T at P.T T Weight Volume at P.T at P.T Tension
Description
3 3 3 3
ºC kg/cm2G kg/h Act_m /s kg/m CP ºC kg/h Act_m /hr kg/m CP dyn/cm

BED#1 Top 71.5 12.8000 2,299 0.0201 51.7 31.840 0.00998 61.2 2,197 4.48 490.31 0.0998 5.59

BED#1 BTM 87.1 12.8280 2,732 0.0206 59.1 36.895 0.01006 90.4 2,631 5.37 489.73 0.0963 5.01

BED#2 TOP FEED 101.0 12.8350 3,835 0.0294 60.0 34.682 0.01025 87.1 7,933 15.56 509.79 0.1052 5.97

BED#2 BTM 114.3 13.0100 5,428 0.0406 64.4 37.142 0.01022 111.0 9,525 19.78 481.46 0.0894 4.28

Confidential information of DWC Innovations LLC. This information is to be held in confidence. Disclosure, Reproduction OR other use of this document is prohibited without the prior written consent of DWC
Innovations LLC.

143 of 346
 REV. DATE BY CHK APP.
CLIENT: HMEL REFINERY
0 Jan-23 NA MB MB

LOCATION: BATHINDA, PUNJAB

Stream Summary
IC4 PRODUCTION FROM ISOM
PROJECT:
STAB. REFLUX STREAM
[Case - 4]
Stream No. 117 (I1) 118 (01) 121 (I2) 123 (02) 124 (I3)
125 (02)
De-
Vapors
2 Phase ethanizer
From De-
Feed to De- Reboiler Column
ethanizer Reflux to Liquid to
ethanizer outlet to Bottoms to
Stream Description Units Column to Column Reboiler
Column Column iC4
Condenser 504-C-002 504-E-013
[504-C- 504-C-002 Column
[504-E-
002] [503-C-
012]
004]
Phase
Total
Temperature C 50.5 67.0 40.6 114.3 116.2 114.3
Pressure kg/cm2G 12.8 12.8 17.8 13.0 13.0 13.0
Vap. Frac on Mass Basis - 0.0005 1.0000 0.0000 0.0000 0.2938 0.0000
Mass Flow kg/hr 4,198.9 2,065.0 1,963.3 18,461.2 18,461.2 4,097.3
Molecular Weight - 65.06 49.38 50.36 66.40 66.40 66.40
Vapor Phase
Mass Flow kg/hr 1.9 2,065.0 - - 5,424.2 -
Actual Volume Flow m3/h 0.2 68.3 - - 145.1 -
Molecular Weight - 19.80 49.38 - - 65.03 -
Molar Flow kgmole/h 0.10 41.82 - - 83.41 -
Mass Density kg/m3 10.262 30.236 - - 37.373 -
Viscosity cP 0.014 0.010 - - 0.010 -
Z Factor - 0.975 0.783 - - 0.740 -
Liquid Phase
Mass Flow kg/hr 4,197.0 - 1,963.3 18,461.2 13,036.9 4,097.3
Actual Volume Flow m3/h 7.4 - 3.9 38.3 27.1 8.5
Molar Flow kgmole/h 64.4 - 39.0 278.0 194.6 61.7
Molecular Weight - 65.12 - 50.36 66.40 66.98 66.40
Mass Density kg/m3 566.8 - 509.3 481.9 481.8 481.9
Viscosity cP 0.149 - 0.111 0.089 0.088 0.089
Surface Tension dyne/cm 10.18 - 7.05 4.24 4.21 4.24
Confidential information of DWC Innovations LLC. This information is to be held in confidence. Disclosure, Reproduction or other use of this document is prohibited without the prior written
consent of DWC Innovations LLC.

144 of 346