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    Lab 7

    Uploaded by

    connie
    The document contains data from a titration experiment measuring pH and volume of NaOH added. As NaOH is added, pH increases gradually at first then more rapidly, leveling off after 16 mL NaOH. The first derivative curve shows the rate of pH change peaking around 16 mL NaOH then decreasing as the reaction nears completion. Overall, the data shows the typical curve for a titration reaction as the analyte is gradually neutralized then reaches the equivalence point where excess titrant is added.

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    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd

    Lab 7

    Uploaded by

    connie
    15 views11 pages
    The document contains data from a titration experiment measuring pH and volume of NaOH added. As NaOH is added, pH increases gradually at first then more rapidly, leveling off after 16 mL NaOH. The first derivative curve shows the rate of pH change peaking around 16 mL NaOH then decreasing as the reaction nears completion. Overall, the data shows the typical curve for a titration reaction as the analyte is gradually neutralized then reaches the equivalence point where excess titrant is added.

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    Lab7

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    The document contains data from a titration experiment measuring pH and volume of NaOH added. As NaOH is added, pH increases gradually at first then more rapidly, leveling off after 16 mL NaOH. The first derivative curve shows the rate of pH change peaking around 16 mL NaOH then decreasing as the reaction nears completion. Overall, the data shows the typical curve for a titration reaction as the analyte is gradually neutralized then reaches the equivalence point where excess titrant is added.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Download as xlsx, pdf, or txt
    15 views11 pages

    Lab 7

    Uploaded by

    connie
    The document contains data from a titration experiment measuring pH and volume of NaOH added. As NaOH is added, pH increases gradually at first then more rapidly, leveling off after 16 mL NaOH. The first derivative curve shows the rate of pH change peaking around 16 mL NaOH then decreasing as the reaction nears completion. Overall, the data shows the typical curve for a titration reaction as the analyte is gradually neutralized then reaches the equivalence point where excess titrant is added.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Download as xlsx, pdf, or txt
    of 11

    volume (mL)pH volume (mL)p

    0 4.61 0
    1 4.63 1
    2 4.74 2
    3 4.8 3
    4 4.86 4
    5 4.92 5
    6 4.99 6
    7 5.05 7
    8 5.12 8
    9 5.18 9
    10 5.25 10
    11 5.33 11
    12 5.41 12
    13 5.5 13
    14.1 5.6 14.1
    15 5.71 15
    16.1 5.91 16.1
    16.5 5.97 16.5
    17 6.1 17
    17.5 6.29 17.5
    17.7 6.37 17.7
    17.9 6.47 17.9
    18.1 6.64 18.1
    18.3 7.13 18.3
    18.5 8.91 18.5
    18.7 9.89 18.7
    18.9 10.14 18.9
    19.1 10.35 19.1
    19.3 10.5 19.3
    19.5 10.54 19.5
    19.7 10.64 19.7
    20 10.7 20
    20.5 10.82 20.5
    21 10.9 21
    21.5 10.96 21.5
    22 11.01 22
    22.5 11.06 22.5
    23 11.1 23
    23.5 11.13 23.5
    24 11.16 24
    24.5 11.18 24.5
    first derivative

    0.02 fi rst derivati ve curve


    0.11 10
    0.06
    8.90000
    0.06 9
    0.06
    0.07 8
    0.06
    0.07
    7
    0.06
    0.07
    6
    0.08
    0.08
    5
    pH

    0.09
    0.09090909
    4
    0.12222222
    0.18181818
    3
    0.15
    0.26
    2
    0.38
    0.4
    0.5 1

    0.85
    2.45 0
    0 5 10 15 20
    8.9
    volume of NaOh added
    4.9
    1.25
    1.05
    0.75 pH vs Volume
    0.2
    12
    0.5
    0.2
    0.24 10
    0.16
    8.91
    0.12
    0.1 8
    0.1
    0.08
    6
    0.06
    pH

    0.06
    0.04
    4

    2
    6

    pH
    4

    0
    0 5 10 15 20

    Volume of NaOh added


    derivati ve curve

    8.90000000000003

    15 20 25 30

    volume of NaOh added

    H vs Volume

    8.91
    15 20 25 30

    Volume of NaOh added


    volume (mL)pH volume (mL)pfirst derivative
    0 3.8 0
    0.7 3.72 0.7 -0.11428571
    1.7 3.8 1.7 0.08
    2.7 3.96 2.7 0.16 12

    3.7 4.11 3.7 0.15


    4.7 4.22 4.7 0.11
    5.7 4.34 5.7 0.12 10

    6.7 4.43 6.7 0.09


    7.7 4.52 7.7 0.09
    8.7 4.63 8.7 0.11 8

    9.7 4.73 9.7 0.1


    10.7 4.84 10.7 0.11
    11.8 4.95 11.8 0.1 6

    Ph
    12.7 5.08 12.7 0.14444444
    13.2 5.14 13.2 0.12
    13.4 5.16 13.4 0.1 4
    13.6 5.2 13.6 0.2
    13.8 5.24 13.8 0.2
    14 5.26 14 0.1 2
    14.2 5.3 14.2 0.2
    14.4 5.34 14.4 0.2
    14.7 5.41 14.7 0.23333333 0
    0
    14.9 5.46 14.9 0.25
    15.1 5.53 15.1 0.35
    15.3 5.6 15.3 0.35
    15.5 5.7 15.5 0.5
    15.7 5.78 15.7 0.4
    15.8 5.83 15.8 0.5
    15.9 5.91 15.9 0.8
    16 5.98 16 0.7
    16.1 6.1 16.1 1.2
    16.2 6.25 16.2 1.5
    16.3 6.45 16.3 2
    16.4 7.07 16.4 6.2
    16.5 8.5 16.5 14.3
    16.6 9.05 16.6 5.5
    16.8 9.52 16.8 2.35
    17 9.75 17 1.15
    17.2 9.94 17.2 0.95
    17.7 10.16 17.7 0.44
    18.2 10.29 18.2 0.26
    19.2 10.45 19.2 0.16
    20.2 10.55 20.2 0.1
    21.2 10.62 21.2 0.07
    22.2 10.69 22.2 0.07
    23.2 10.71 23.2 0.02
    pH vs Volume
    12

    10

    8.5
    8

    7.07

    6
    Ph

    0
    0 5 10 15 20

    volume of Naoh added

    fi rst derivati ve
    16

    14 14.2999999999998

    12

    10

    8
    ph

    0
    0 5 10 15 20
    -2
    volume of naoh added
    4

    0
    0 5 10 15 20
    -2
    volume of naoh added
    8.5

    7.07

    15 20 25

    14.2999999999998

    15 20 25
    15 20 25

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