Manual FXL

Translation of the Original Instructions
FOUNDRY-MASTER uäáåÉ
Version: 1.2GB/2013-11-25
Document number: 6000000164
Oxford Instruments Analytical GmbH

Wellesweg 31
47589 Uedem/Germany
Phone: +49 (0) 2825 9383-0
Fax: +49 (0) 2825 9383-100
E-mail: [email protected]
Web: www.oxford-instruments.com
All rights reserved
This document may only be used by the recipient for the intended purpose. It shall not be reproduced in whole
or in part or translated into another language without prior written consent.
Right to technical changes reserved.
© 2013 Oxford Instruments Analytical GmbH

Preface FOUNDRY-MASTER Xline
Preface
To ensure smooth operation, we have drawn up these practical operating instructions.
We explicitly point out that Oxford Instruments Analytical GmbH does not assume
responsibility for damage or losses resulting from the disregard of these operating
instructions or the misuse of the products described herein.
These operating instructions are protected by copyright.
Upon request, they are available in other languages and can also be supplied on CD
(Acrobat® Reader 7.0).
Our products are subject to continuous further development — technical changes are
reserved.
Uedem, November 2013
Version: 1.2GB/2013-11-25 © 2013 Oxford Instruments Analytical GmbH

Table of contents FOUNDRY-MASTER Xline
Table of contents
1 Notes regarding the use of these operating instructions.................................................................... 1

1.1 Validity of the operating instructions .......................................................................................... 1
1.2 Pictograms and signal words ..................................................................................................... 2
1.2.1 Hazard symbols .......................................................................................................... 2
1.2.2 Symbols for personal protective equipment................................................................ 2
1.2.3 Information symbol ..................................................................................................... 2
2 Intended use and misuse ....................................................................................................................... 3
3 General safety instructions .................................................................................................................... 5

3.1 Safety instructions for work on the electrical system ................................................................. 7
3.2 Personnel qualification ............................................................................................................... 8
4 Description of the Instrument .............................................................................................................. 11

4.1 Function ................................................................................................................................... 11
4.2 Components and operating controls ........................................................................................ 13
4.2.1 Spectrometer components........................................................................................ 14
4.2.2 Operating controls, displays and ports of the spectrometer ..................................... 15
4.3 Technical data.......................................................................................................................... 16
5 Scope of delivery, transport, set-up and installation......................................................................... 17

5.1 Scope of delivery...................................................................................................................... 17
5.2 Transport.................................................................................................................................. 18
5.2.1 Transport lock ........................................................................................................... 18
5.2.2 Transport .................................................................................................................. 18
5.3 Set-up....................................................................................................................................... 19
5.4 Installation ................................................................................................................................ 20
6 Putting into service ............................................................................................................................... 23
7 Quick start.............................................................................................................................................. 27
7.1 Analysing in spark mode (argon) ............................................................................................. 27
7.2 Flowcharts for analysis and recalibration ................................................................................. 30
7.2.1 Start and sequence of a check measurement in spark mode................................... 30
7.2.2 Recalibrating "Full" ................................................................................................... 31
7.2.3 Recalibrating "Type" ................................................................................................. 32
7.2.4 Performing an analysis ............................................................................................. 33
Version: 1.2GB/2013-11-25 -I- © 2013 Oxford Instruments Analytical GmbH

FOUNDRY-MASTER Xline Table of contents
8 WASLab software .................................................................................................................................. 35

8.1 Start screen.............................................................................................................................. 36
8.2 Utilities...................................................................................................................................... 37
8.2.1 Enter password ......................................................................................................... 38
8.2.2 Options ..................................................................................................................... 39
8.2.3 Passwords ................................................................................................................ 41
8.2.4 Delete files ................................................................................................................ 42
8.2.5 Select analysis program ........................................................................................... 43
8.2.6 Firmware status ........................................................................................................ 43
8.2.7 Service ...................................................................................................................... 44
8.3 Readout mode / settings grade identification ........................................................................... 45
8.3.1 Recall stored analysis ............................................................................................... 46
8.3.2 Repeated measuring ................................................................................................ 46
8.3.3 Grade options ........................................................................................................... 47
8.3.4 Print/store options..................................................................................................... 48
8.4 Description of the analysis screens.......................................................................................... 49
8.4.1 Select analysis program ........................................................................................... 49
8.4.2 Analysis window (vertical)......................................................................................... 50
8.4.3 Analysis window (horizontal) .................................................................................... 51
8.4.4 Short description of the function buttons .................................................................. 52
8.5 Analysing samples ................................................................................................................... 60
8.5.1 Disabling a sparking ................................................................................................. 63
8.5.2 Displaying the relative standard deviation (RSD) ..................................................... 63
8.6 Recalibration ............................................................................................................................ 65
8.7 Grade database ....................................................................................................................... 70
8.7.1 Selecting a grade file ................................................................................................ 70
8.7.2 Creating a new grade file.......................................................................................... 72
8.7.3 Adding a grade ......................................................................................................... 73
8.7.4 Editing a grade.......................................................................................................... 74
8.8 Searching for and comparing grades ....................................................................................... 75
8.8.1 Searching for grades ................................................................................................ 75
8.8.2 Comparing grades (grade identification)................................................................... 77
8.9 Creating a pseudo element ...................................................................................................... 79
8.10 Setting up a report file .............................................................................................................. 83
8.10.1 Editing the logo ......................................................................................................... 84
8.10.2 Editing the report header .......................................................................................... 84
8.10.3 Editing the queries for the output log ........................................................................ 85
8.10.4 Editing the output of the analysis result .................................................................... 86
8.10.5 Editing the report footer ............................................................................................ 87
8.10.6 Checking the report parameters ............................................................................... 88
8.10.7 Saving and printing the report file ............................................................................. 89
9 Removal from service ........................................................................................................................... 91
© 2013 Oxford Instruments Analytical GmbH - II - Version: 1.2GB/2013-11-25

Table of contents FOUNDRY-MASTER Xline
10 Maintenance........................................................................................................................................... 93
10.1 Safety instructions for maintenance and repair........................................................................ 93
10.2 Maintenance table.................................................................................................................... 94
10.3 Disassembling and cleaning the spark stand........................................................................... 95
10.4 Cleaning the window (optical fibre) .......................................................................................... 96
10.5 Cleaning and replacing the window (direct light path).............................................................. 98
10.5.1 Cleaning the window................................................................................................. 98
10.5.2 Replacing the window............................................................................................. 100
10.6 Maintenance of the electrode................................................................................................. 101
10.6.1 Replacing the electrode .......................................................................................... 101
10.6.2 Adjusting the electrode ........................................................................................... 103
10.6.3 Cleaning the electrode with the electrode brush..................................................... 104
10.6.4 Cleaning the electrode with the file brush ............................................................... 105
10.7 Replacing filters...................................................................................................................... 106
10.8 Cleaning and filling the wash bottle........................................................................................ 106
10.9 Replacing the argon bottle(s) ................................................................................................. 107
10.10 Cleaning the instrument ......................................................................................................... 107
11 Faults .................................................................................................................................................... 109

11.1 Information regarding WINDOWS™ installation .................................................................... 109
11.2 General faults......................................................................................................................... 109
11.3 Faults of FOUNDRY-MASTER Xline ..................................................................................... 110
12 Reshipment and disposal ................................................................................................................... 111

12.1 Declaration of Decontamination ............................................................................................. 111
12.2 Disposal ................................................................................................................................. 111
13 Reference ............................................................................................................................................. 113

13.1 Information regarding reliability of analyses........................................................................... 113
13.2 Information about setting analysis parameters ...................................................................... 115
13.2.1 Parameter file ......................................................................................................... 117
13.2.2 References file........................................................................................................ 118
13.2.3 Format file............................................................................................................... 119
13.2.4 Curve file................................................................................................................. 120
13.2.5 Alloy selection......................................................................................................... 121
13.2.6 Control standard file................................................................................................ 122
13.2.7 Standards ............................................................................................................... 123
13.3 Service menu ......................................................................................................................... 124
14 Annex ................................................................................................................................................... 127

14.1 Service ................................................................................................................................... 129
14.2 Glossary ................................................................................................................................. 131
14.3 Standard accessory case, packed ......................................................................................... 133
14.4 Forms ..................................................................................................................................... 135
14.4.1 Declaration of Conformity ....................................................................................... 135
14.4.2 Declaration of Decontamination.............................................................................. 135
Version: 1.2GB/2013-11-25 - III - © 2013 Oxford Instruments Analytical GmbH

Table of figures FOUNDRY-MASTER Xline
Table of figures
4 Description of the Instrument

Fig. 4-1 Instrument components ..................................................................................................... 14
Fig. 4-2 Operating controls and ports of the instrument.................................................................. 15
5 Scope of delivery, transport, set-up and installation

Fig. 5-1 Instrument with screwed in handles ................................................................................... 18
Fig. 5-2 Workstation at the spectrometer ........................................................................................ 19
Fig. 5-3 Ports on the instrument...................................................................................................... 20
6 Putting into service

Fig. 6-1 On/off switch ...................................................................................................................... 23
Fig. 6-2 Display of the requested recalibration sample ................................................................... 23
Fig. 6-3 Instrument front.................................................................................................................. 24
7 Quick start
Fig. 7-1 Placing the sample............................................................................................................. 28
8 WASLab software
Fig. 8-1 On-screen keyboard and virtual numeric keypad .............................................................. 35
Fig. 8-2 Start screen........................................................................................................................ 36
Fig. 8-3 "Utilities" window ................................................................................................................ 37
Fig. 8-4 "Password dialog" window ................................................................................................. 38
Fig. 8-5 "Options" window ............................................................................................................... 39
Fig. 8-6 "Edit passwords" window ................................................................................................... 41
Fig. 8-7 "Delete files" window.......................................................................................................... 42
Fig. 8-8 "Select analysis program" window ..................................................................................... 43
Fig. 8-9 "Dsp status report" window ................................................................................................ 43
Fig. 8-10 "Readout mode / settings grade identification" window ..................................................... 45
Fig. 8-11 "Select analysis" window.................................................................................................... 46
Fig. 8-12 "Repeat" window ................................................................................................................ 46
Fig. 8-13 "Grade options" window ..................................................................................................... 47
Fig. 8-14 "Print/store options" window............................................................................................... 48
Fig. 8-16 "Analysis" window .............................................................................................................. 50
Fig. 8-17 "Analysis" window (horizontal) ........................................................................................... 51
Fig. 8-18 "Start (F10)" function button............................................................................................... 52
Fig. 8-19 Analysis result (example) ................................................................................................... 52
Fig. 8-20 "New (F2)" function button ................................................................................................. 53
Fig. 8-21 "Sample ID" entry............................................................................................................... 53
Fig. 8-22 "Dialog" window ................................................................................................................. 53
Fig. 8-23 "Print (F4)" function button ................................................................................................. 54
Fig. 8-24 "Del (Del)" function button.................................................................................................. 54
Fig. 8-25 Deleting a column .............................................................................................................. 54
Fig. 8-26 "Store (F5)" function button................................................................................................ 55
Fig. 8-27 "Recal. (F6)" function button .............................................................................................. 55
Fig. 8-28 "Mode (F7)" function button ............................................................................................... 56
Fig. 8-30 "Load (F8)" function button ................................................................................................ 56
Fig. 8-31 "Change (F9)" function button............................................................................................ 57
Fig. 8-32 "Change alloy" window....................................................................................................... 57
Fig. 8-33 "RSD (Alt+R)" function button ............................................................................................ 58
Version: 1.2GB/2013-11-25 -V- © 2013 Oxford Instruments Analytical GmbH

FOUNDRY-MASTER Xline Table of figures
Fig. 8-34 "Analysis" window with indication of RSD .......................................................................... 58

Fig. 8-35 "Analysis horizontal" window with indication of RSD (example) ........................................ 58
Fig. 8-36 "Exit (Alt+Q)" function button ............................................................................................. 59
Fig. 8-37 Exit dialog .......................................................................................................................... 59
Fig. 8-38 Start screen........................................................................................................................ 60
Fig. 8-40 "Analysis" window .............................................................................................................. 61
Fig. 8-42 "Analysis" window with result ............................................................................................. 62
Fig. 8-43 "Analysis" window with indication of RSD .......................................................................... 63
Fig. 8-44 Clicking "Recal."................................................................................................................. 65
Fig. 8-45 "Recalibration method" selection window .......................................................................... 66
Fig. 8-46 Display of the requested recalibration sample ................................................................... 66
Fig. 8-47 Result of the 1st measurement for recalibration (example) ............................................... 67
Fig. 8-48 "Recalibration successful" information ............................................................................... 68
Fig. 8-49 Error message ................................................................................................................... 68
Fig. 8-50 Warning.............................................................................................................................. 68
Fig. 8-51 Result of recalibration ........................................................................................................ 69
Fig. 8-52 "Change alloy" window....................................................................................................... 70
Fig. 8-53 "Grade file selection" window............................................................................................. 70
Fig. 8-54 "Grade selection" window .................................................................................................. 71
Fig. 8-55 Result of grade search in the "Analysis" window ............................................................... 76
Fig. 8-56 Result of the comparison ................................................................................................... 77
Fig. 8-57 Selection of the analysis program...................................................................................... 79
Fig. 8-58 "Calculation file" input ........................................................................................................ 79
Fig. 8-59 "Calculation file" window .................................................................................................... 80
Fig. 8-60 Entered calculation formula ............................................................................................... 81
Fig. 8-61 "Analysis" window with pseudo element CE (section) ....................................................... 81
Fig. 8-62 Calculated pseudo element ............................................................................................... 82
Fig. 8-63 "Report file" input ............................................................................................................... 83
Fig. 8-64 "Report file" window — logo............................................................................................... 84
Fig. 8-65 "Report file" window — head.............................................................................................. 84
Fig. 8-66 "Report file" window — queries.......................................................................................... 85
Fig. 8-67 "Edit questions" window ..................................................................................................... 85
Fig. 8-68 "Report file" window — analysis......................................................................................... 86
Fig. 8-69 "Report file" window — foot................................................................................................ 87
Fig. 8-70 "Report file" window — buttons.......................................................................................... 88
Fig. 8-71 Preview window (example) ................................................................................................ 88
Fig. 8-73 "Print/store options" window............................................................................................... 89
Fig. 8-75 "Print (F4)" function button ................................................................................................. 90
© 2013 Oxford Instruments Analytical GmbH - VI - Version: 1.2GB/2013-11-25

Table of figures FOUNDRY-MASTER Xline
10 Maintenance
Fig. 10-1 Reminder to clean the spark stand .................................................................................... 95
Fig. 10-2 Opening the spark stand plate ........................................................................................... 95
Fig. 10-3 Window in front of the optical fibre ..................................................................................... 96
Fig. 10-4 Opening the spark stand.................................................................................................... 96
Fig. 10-5 Screwing out the sleeve..................................................................................................... 97
Fig. 10-6 Sleeve with window, brass nut and installation aid FOC window ...................................... 97
Fig. 10-7 Opening the cover.............................................................................................................. 98
Fig. 10-8 Shutting the ball valve ........................................................................................................ 98
Fig. 10-9 Removing window brackets ............................................................................................... 99
Fig. 10-10 Removing the window from the window brackets .............................................................. 99
Fig. 10-11 Inserting the window brackets into the light path ............................................................. 100
Fig. 10-12 Screwing out the spacer .................................................................................................. 101
Fig. 10-13 Installing the electrode ..................................................................................................... 102
Fig. 10-14 Screwing out the spacer .................................................................................................. 103
Fig. 10-15 Installing the electrode ..................................................................................................... 103
Fig. 10-16 Spark stand...................................................................................................................... 104
Fig. 10-17 Opening the spark stand.................................................................................................. 105
Fig. 10-18 Wash bottles .................................................................................................................... 106
13 Reference
Fig. 13-1 "Change (F9)" function button.......................................................................................... 115
Fig. 13-2 "Change alloy" window..................................................................................................... 116
Fig. 13-3 "Parameter file" window — settings ................................................................................. 117
Fig. 13-4 "Edit references" window ................................................................................................. 118
Fig. 13-5 "Format" window .............................................................................................................. 119
Fig. 13-6 Input window and virtual numeric keypad ........................................................................ 119
Fig. 13-7 "Curves" window .............................................................................................................. 120
Fig. 13-8 Input window and virtual numeric keypad ........................................................................ 120
Fig. 13-9 "Alloy selection" window................................................................................................... 121
Fig. 13-10 "Alloy selection" window (Control standard file) ............................................................... 122
Fig. 13-11 "Standards" window ......................................................................................................... 123
Fig. 13-12 "Create diagnostic data" query......................................................................................... 124
Fig. 13-13 2. Prompt for "Create diagnostic data"............................................................................. 124
Fig. 13-14 Analysis window for "Create diagnostic data" .................................................................. 124
Fig. 13-15 "Dialog" window for "Create diagnostic data"................................................................... 125
Fig. 13-16 Confirmation for the created diagnosis ............................................................................ 125
Fig. 13-17 "Scan utility" window ........................................................................................................ 126
Fig. 13-18 „Foundry Master controls“ window ................................................................................... 126
Version: 1.2GB/2013-11-25 - VII - © 2013 Oxford Instruments Analytical GmbH

1 Notes regarding the use of these operating instructions FOUNDRY-MASTER Xline
1 Notes regarding the use of these operating instructions
This chapter contains information regarding these operating instructions as well as

general safety instructions for handling the instrument.
Note! Due to the customer-specific configuration of all spectrometers, the matrices and/or
grades displayed on your screen can deviate from the illustrations and descriptions in
this manual.
If not indicated otherwise, we assume that the user has already started the
WINDOWS™ operating system. Basic knowledge as to handling software under
WINDOWS™ is assumed as given.
1.1 Validity of the operating instructions
These operating instructions are valid for FOUNDRY-MASTER Xline stationary optical
emission spectrometers.
Observe these operating instructions for all work. If the instrument is not used according
to these operating instructions, your safety as well as the instrument function can be
affected.
To maintain product reliability, enhance the life cycle and avoid downtimes, do in any
case observe the instructions herein.
Furthermore observe the current valid regulations for accident prevention and
environmental protection as well as the recognised technical rules for safe working
according to good professional practice.
Version: 1.2GB/2013-11-25 -1- © 2013 Oxford Instruments Analytical GmbH

FOUNDRY-MASTER Xline 1 Notes regarding the use of these operating instructions
1.2 Pictograms and signal words
Important information in these operating instructions and on the instrument is marked

with the following pictograms.
1.2.1 Hazard symbols
Danger!
This sign indicates an immediate risk of death or injury.
Danger!
Hazardous electric current!
This sign indicates hazardous electric current.
Warning!
Crush hazard!
This sign indicates hazardous situations with limb crush hazard.
Warning!
Hot surfaces!
This sign indicates hot surfaces of the instrument.
1.2.2 Symbols for personal protective equipment
Wear eye protection!
Wear ear protection!
Wear protective gloves!
1.2.3 Information symbol
Note! Tips and information are marked with the word "Note!" in bold print.
© 2013 Oxford Instruments Analytical GmbH -2- Version: 1.2GB/2013-11-25

2 Intended use and misuse FOUNDRY-MASTER Xline
2 Intended use and misuse
The stationary optical emission spectrometer (OES) is exclusively intended for

qualitative and quantitative element analysis of alloys.
The instrument may only be used in dry rooms.
The instrument may only be operated with the protective covers installed.
The intended use also includes

• the observance of all information and regulations in these operating instructions;
• the observance of the technical data;
• the adherence to the periods for inspection and maintenance work prescribed
or contained in these operating instructions.
The instrument is exclusively intended for operation in an industrial environment. For

operation in other environments, electromagnetic compatibility may not be guaranteed
due to radiated and line-bound disturbance variables.
Misuse The use in hazardous areas is not permitted.
The employment of insufficiently qualified personnel is regarded as misuse.
Measurements without correctly positioned samples is regarded as misuse.
Unauthorised structural modifications, attachments to or conversions of the instrument

as well as modifications of and interference with the instrument program are prohibited.
The manufacturer is not liable for damage resulting from misuse.
The instrument may only be transported if previously agreed with Oxford Instruments
Analytical GmbH.

3 General safety instructions FOUNDRY-MASTER Xline
3 General safety instructions
Observe the following safety instructions for the operation of the instrument:
• Only operate the instrument if free from defects and under observance of these
operating instructions.
• Prior to starting work, read these operating instructions. This applies particularly
to personnel who only occasionally work with the instrument, such as
maintenance personnel.
• Observe all safety and information signs on the instrument and maintain legible.
• Check the instrument for external visible damage. Report any visible damage
and only put the instrument into service after remediation of damage.
• Protect the instrument from influences which can cause corrosion or affect the
function of components.
• Do not place any liquids on top of the instrument.
• No not excessively load the hood of the instrument (>10 kg).
• Internal or external safety devices of the instrument shall in no case be made
inoperative. This applies particularly to the pressure relief valve of the lid on the
vacuum tank!
• Maintenance and repair may only be carried out by qualified specialised
personnel.
• In the event of malfunctions, remove the instrument from service. Have faults
immediately remedied by an electrically skilled person.
• Never open the housing! There are no user-relevant elements inside the
housing.
• Have defective parts of the instrument immediately replaced.
• Spare parts must comply with the technical requirements specified by Oxford
Instruments Analytical GmbH. This is always the case if you use original spare
parts.
• For inspection or repair work, attach a warning sign against restart to the
external de-energizing device.
• The safety instructions must be supplemented with national accident prevention
regulations.
• During measurement, electromagnetic waves may disturb other devices.
Please observe the information in chapter 5.3, page 19.
• In the event of an emergency, press the stop switch on the front to abort
measurement.
• Always use the sample clamp (hold-down device). The hold-down device
establishes the electrical connection between sample and electrode. When the
hold-down device is positioned next to the spark stand plate, measurement is
not possible.
• The sample weight shall not exceed the admissible load of the spark stand (see
chapter 4.3, page 16).
• The instrument must not be exposed to the following:
• extreme temperatures or temperature changes;
• heavy shock or vibration (particularly when the transport lock has been
removed);
• moisture and condensing humidity;
• metal dust and large quantities of dust in general.

FOUNDRY-MASTER Xline 3 General safety instructions
Danger!
During work with the spectrometer, hazards may arise from electric current / volt-
age. Observe the following safety instructions to avoid the risk of an electric
shock:
• If you touch the instrument and electrically conducting parts, such as machines
or devices, simultaneously, voltage can be generated from possible potential
differences which is perceptible but non-hazardous.
• Never spark wet or moist surfaces, since there is a risk of a short circuit!
• Never spark without a clamped sample!
• When the excitation source is switched on, avoid any contact with the spark
electrode!
• When working at the spark stand, e.g. for changing the electrode, do in any case
switch off the excitation source.
• Do not touch the sample during measurement!
• During sparking, do not, under any circumstances, introduce a conducting
object into the proximity of the spark stand hole!
• During sparking, do not, under any circumstances, remove a conducting
object from the spark stand hole!
• With the spark stand hole open during sparking, do not, under any
circumstances, bring a part of your body into its immediate vicinity!
Warning! Hot surface!

Small and/or thin samples can become hot during sparking. During measurement of
small or thin samples, wear protective gloves!
Warning!
During the analysis of samples that do not cover the hole in the spark stand plate (e.g.
wires), spark light can emerge. Your eyes can be blinded by the light and the high-
energy UV radiation can damage your eyes. Never look into the arc! Wear suitable eye
protection during work.
Warning!
wires), the sound generated upon sparking (measuring) exits through the gap. Wear ear
protection when sparking samples that do not cover the hole.
Danger!
When measuring hazardous substances, there is a hazard from escaping gases or
vapours.
• The operator must know what substances he is working with.
• The operating company must provide for suitable protective measures (e.g.
exhaustion). (Metal dusts are primarily released. Those are usually washed in
the washing bottle and do not escape.)

3.1 Safety instructions for work on the electrical system
Observe the following safety instructions for work on the electrical system:
• Only electrically skilled persons may carry out work on the electrical system.
• Do not carry out any work at live parts of the electrical system.
Observe the following safety rules when working on the electrical system:
1.De-energise.
2.Secure against restart.
3.Verify de-energised state.
4.Shield live parts.
5.Earth and short-circuit.
• In the event of faults of the electrical energy supply, immediately switch off the
instrument.
• An interruption in the energy supply of > 20 ms requires restarting the software.
• In the event of a short circuit, there is a risk of spark generation or the break-out
of a fire. Only use original fuses with specified amperage and tripping
characteristic! When a fuse must be replaced, first identify the corresponding
cause and remedy the error before you replace the fuse.
• If work on live parts is required, only use insulated tools.

FOUNDRY-MASTER Xline 3 General safety instructions
3.2 Personnel qualification
All persons entrusted with work at the instrument commit themselves to the following
before starting work:
• to observing the basic regulations related to occupational safety and accident
prevention;
• to reading the safety instructions and warnings in these operating instructions
and to confirming with their signature that they have understood them;
• to wearing or using personal protective clothing and accessories or workstation-
related personal protective clothing and accessories serving occupational
safety as required for reasons of safety during work.
Only personnel who have read and understood these operating instructions may work
with the instrument.
Personnel to be trained or instructed or personnel in training shall only work with the
instrument under constant supervision of an experienced person.
Only personnel who are at least 18 years of age may be entrusted with independent
work with the instrument.
The individual activities at the instrument require different personnel qualifications listed
in table 3-1, page 9.
The various qualifications comprise the following abilities and knowledge:
• Instructed persons must be able to operate the instrument and identify possible
damage and hazards related to the instrument.
• Electrically skilled persons must be able to read and understand electric circuit
diagrams, to put electrical machines/devices into service, to maintain them, to
wire control cabinets, to install control software, to ensure the functionality of
electrical components and to identify possible hazards from handling electrical
and electronic systems.
• Trained pneumatic specialists must be able to read and understand pneumatic
circuit diagrams, to put pneumatic systems into service and to maintain them, to
remove and install pneumatic hoses, to ensure the functionality of pneumatic
components, to evaluate the work on the pneumatic system they have been
entrusted with and to identify possible hazards.

Table 3-1 Overview of minimum required personnel qualifications
Skilled workersb with

Instructed the qualification of an Electrically
Pneumatic
Activities "industrial mechanic" skilled per-
personsa specialists
or "mechatronics sons
engineer"
Transport X
Putting into service, operation,
X
removal from service
Cleaning X
Mechanical work:
troubleshooting, repair and X X
maintenance
Work on the electrical system:
troubleshooting, repair and X
maintenance
Work on the pneumatic system:
troubleshooting, repair and X
maintenance
Disposal X
a. Instructed persons are persons trained in handling the instrument by Oxford Instruments
Analytical GmbH. For instruments delivered with a PC user interface, PC knowledge is required.
b. A skilled worker is who, due to his professional training, his knowledge and experience as well
as due to his knowledge of relevant regulations, is able to judge the work assigned to him as
well as to identify possible hazards.

4 Description of the Instrument FOUNDRY-MASTER Xline
4 Description of the Instrument
4.1 Function
FOUNDRY-MASTER Xline is a laboratory spectrometer for qualitative and quantitative

analysis of metal grades.
The metal sample to be analysed is positioned at the spark stand and clamped with a
hold-down device. The sample is sparked with an electrically generated arc at the
surface. Upon discharging, an area of the sample surface is melted and evaporated by
the spark. From the high energy in the spark, a plasma results. This plasma emits light
which is spectrally analysed and measured by means of CCDs (charge coupled devices,
light-sensitive semiconductor chips). A certain area of the measured spectrum can be
assigned to every element.
The instrument is operated via control keys using a supplied software which displays the
analysis result on the screen of the connected PC. The analysis result can be stored in
the internal database or exported. Through comparison with stored grade data it can be
determined immediately whether or with what deviations the analysed grade fulfils the
required specifications. Certificates can be easily designed and printed.
Note! Reliability of the analysis directly depends on the quality of sample preparation.
How precise a spectrometer measures can be determined by means of comparison with
certified reference material (CRM) whose precise composition is known. Two statistic
relations are to be accurately distinguished:
1. The precision of measurements.

This serves to determine the standard deviation in a series of consecutive
measurements of the same sample. If it is related to the average value, the
relative standard deviation results.
2. The accuracy of measurements.
It serves to determine whether the average value related to the stated contents
is correct.
Generally, measurements with a functioning spark spectrometer are very precise.

However, that does not mean that the analysis is at the same time accurate.
Spectrometry is a comparative process, which means that the composition of an
unknown sample is determined through comparison with data of known samples. If any
errors occur in this comparison ("systematic errors"), the instrument precisely applies
those deviations to the sample.
The certificate of analysis supplied with every certified sample indicates the element
concentrations incl. the deviation (standard deviation) between the analyses of different
laboratories.
Version: 1.2GB/2013-11-25 - 11 - © 2013 Oxford Instruments Analytical GmbH

FOUNDRY-MASTER Xline 4 Description of the Instrument
For certification, the samples of up to 15 renowned, certified national and international

laboratories are analysed. Every laboratory uses its best available analysis options (e.g.
wet chemistry, combustion, XRF, AES-ICP and spark atomic emission spectrometers).
The standard deviation resulting from the comparison of those analyses (1 sigma) does
not correspond to the standard deviations of the individual analytical measuring
instruments, but is the standard deviation of the average values from the individual
laboratories.
The average value of all measurements from the individual laboratories is considered
as the best approximation to the "real" content of an element in the sample and used as
the set value for calibration. So when CRM samples are used for calibration, despite all
care, there is always a certain deviation of the set values from the actual values
calculated from the calibration curves.
That means, there is a systematic deviation between the analysis of the spectrometer
and the certified value.
However, given today's state of analysis technology, those deviations are small and
allow a simplified procedure to determine whether a spectrometer measures sufficiently
accurately:
To estimate the deviation to expect in the analysis value from the standard deviation
of an element indicated in the certificate using an optical emission spectrometer, ac-
cording to experience, the value given in the certificate can be multiplied by 3 (re-
garding statistics: approx. 99.7 % of the values are in a 3-sigma interval). That is to
ensure that the range of all laboratory average values is covered and outliers are not
considered.
Example Indication in the certificate: average value 1.082 %, standard deviation 0.008 % of
the laboratory mean values.
==> The concentration indicated as the average value of at least 3 valid measure-
ments with an optical emission spectrometer should be in the range from 1.082 % -
0.024 % = 1.058 % to 1.082 % + 0.024 % = 1.106 %.
Note! The calibration of the spectrometer can be optimised for the customer application by
including customer-specific reference samples regarding their accuracy. In contrast,
CRM materials synthetic alloys and are designed to cover a large range of contents with
as few samples as possible.
© 2013 Oxford Instruments Analytical GmbH - 12 - Version: 1.2GB/2013-11-25

4.2 Components and operating controls
The instrument consists of three important assemblies:
Excitation Source A digitally controlled excitation source generates a strong electric discharge between
sample and electrode in the argon-purged spark stand melting a small part of the sample
material out of the surface, evaporating it and exciting it to glow in a plasma. The argon
atmosphere avoids oxidation on the sample surface and changes the discharge
conditions insofar as practically all discharge energy is converted at the sample
connected as a cathode. The characteristic blue light (common in ferrous metal)
contains the spectral information about the elements and their contents in the sample.
Optics The light generated in the spark stand is mapped on a diffraction grating and spread out
into its spectral components. Light with longer wavelengths is deflected ("diffracted")
stronger than light with shorter wavelengths. This produces an emission spectrum of the
sample which can be evaluated using light-sensitive detectors. FOUNDRY-
MASTER Xline uses the latest generation of CCD line sensors featuring high sensitivity
and long life. The complete optical system operates inside a vacuum so that emission
wavelengths shorter than approx. 200 nm are not absorbed by air.
FOUNDRY-MASTER Xline has two light paths through which the light reaches the
optical system. One path leads through an argon-purged tube ("direct light path"), while
the other leads over a short optical fibre ("indirect light path"). The advantage of this
design is the optimisation of the corresponding path for specific elements and
applications. Due to the small light losses and a specific dazzle, the direct light path is
particularly suitable for analysing low element contents, while the indirect path is
preferably used for measuring higher contents.
Readout system Recording a complete spectrum requires a fast readout system to process large
amounts of data fast. Light intensities obtained from the emission spectrum are
converted to contents using the calibration curves stored in the instrument.
The contents are displayed on the screen and further processed (quality detection,
monitoring of limit values for process control, etc.). FOUNDRY-MASTER Xline uses a
special processor which allows the simultaneous evaluation of up to 18 individual CCD
sensors. That permits very precise analysis by means of DIA (Dynamic Integration
Algorithm).

4.2.1 Spectrometer components
FOUNDRY-MASTER Xline consists of the following components (see fig. 4-1):

• cover (1) for window maintenance (direct light path)
• hold-down device (2)
• spark stand (3) with removable spark stand plate
• housing (4)
• fans (5)
• handles (6)
• vacuum pump with oil trap and air filter (no picture)
• washing bottle to clean off-gases from the spark stand (no picture)
• PC with monitor and mouse (no picture).
1 2 3 4 4 5
Fig. 4-1 Instrument components

4.2.2 Operating controls, displays and ports of the spectrometer
There are the following operating controls, display elements and ports on FOUNDRY-
MASTER Xline (see fig. 4-2):
• hold-down device (1) for sample
• rotary knob (2) to switch on the excitation source
• stop button (3)
• start button (4)
• USB port (5) to connect the PC
• port (6) for vacuum hose
• port (7) for argon
• exhaust hose for washing bottle (8)
• on/off switch (9)
• socket (10) for power plug
• fuses (11)
• PC monitor (no picture)
• PC keyboard (no picture)
• PC mouse (no picture).
1 2 3 4
5 6 7 8 9 10 11
Fig. 4-2 Operating controls and ports of the instrument

4.3 Technical data
Table 4-1 Technical data of FOUNDRY-MASTER Xline
Parameter Value
Designation FOUNDRY-MASTER Xline
Dimensions height x width x depth 380 mm x 740 mm x 880 mm
Weights Instrument without PC and vacuum approx. 100 kg

pump
max. sample weight 10 kg
Electrical system voltage 90-250 VAC, 50–60 Hz
fuse 2 x 6 A slow, 5 x 20 mm
max. power consumption (without 600 VA

PC and vacuum pump)
power consumption in idle state 110 VA; source switched on
(without PC and vacuum pump)
70 VA; source switched off
protection class IP21
optical system multi-CCD optics with Paschen-Runge mounting
focal length 350 mm and 125 mm
number of grid lines 3000/mm and 1500/mm
wavelength range 130–780 nm
Excitation source sparking high-energy pre-spark (HEPS)

parameters
frequency 80–500 Hz
voltage 200-500 V
Ambient conditions temperature 40 °C max.
air humidity 10–90 %, non-condensing
Noise emission
System requirements for Microsoft® Windows™ 7/8, with latest service packs (32/64-bit
external PC editions)
Intel® Pentium® 4, AMD Athlon™ 64 or better
1 GB RAM or more
100 MB available space
mouse
screen resolution: 1024 x 768
1 x free USB 2.0 port
DVD drive
Options wire adapter set
sample preparation devices
accessories set
consumables set

5 Scope of delivery, transport, set-up and installation FOUNDRY-MASTER Xline
5 Scope of delivery, transport, set-up and installation
5.1 Scope of delivery
The following objects are included in the scope of delivery:

• FXL basic instrument incl. optical system
• set of recalibration samples
• tungsten electrode with cleaning brush
• standard accessory case, packed (see chapter 14, page 127)
• vacuum hose
• copper tube for argon connection
• washing bottle for off-gases incl. off-gas hose
• vacuum pump
• pressure reducer
Unpack the instrument and check the delivered contents for completeness.
Should any parts be missing or damaged, please immediately contact our local Oxford
Instruments Analytical GmbH partner.

FOUNDRY-MASTER Xline 5 Scope of delivery, transport, set-up and installation
5.2 Transport
5.2.1 Transport lock
Upon delivery, there are two transport locks installed inside the instrument to protect the
optical system from damage.
• Those transport locks may only be installed and removed by a person
authorised by Oxford Instruments Analytical GmbH.
• To prevent damages during transport, consult your service partner from Oxford
Instruments Analytical GmbH or call the service centre (contact details are
provided in chapter 14.1, page 129) before each transport.
• Have transport locks reinstalled by a person authorised by Oxford Instruments
Analytical GmbH to transport the device.
5.2.2 Transport
Note! Observe the following for transport:

• In general, the instrument must be lifted and transported with greatest care.
• During transport, make sure the instrument is in horizontal position!
• Completely screw the handles (1, fig. 5-1) on both sides of the instrument into
the provided threads.
For short-distance transport (e.g. within the same room), the instrument can be lifted and
transported by several persons.
Fig. 5-1 Instrument with screwed in handles

5.3 Set-up
Warning!
When the instrument is placed on the working surface, there is a crush hazard between
the handles and the surface the instrument is placed on.
Make sure the surface is horizontal and level.
Check if the feet of the instrument are sufficiently screwed out.
Wear protective gloves.
• Place the instrument on a horizontal, level and sufficiently stable working

surface at ergonomically suitable height (workbench or work table).
Indications regarding the instrument weight are given in the technical data in
chapter 4.3, page 16.
• Make sure there is sufficient distance to the wall (> 15 cm) on the rear side so
that power cord, Ar line, vacuum hose to the vacuum pump and exhaust hose
to the washing bottle are not kinked.
• Straightly align the instrument. For improved accessibility for larger samples,
the spark stand should protrude.
• Set up the instrument so that the operator can operate the instrument on the
front (1, fig. 5-2) without restrictions to his freedom of movement. The
instrument is operated at the PC screen, at the spark stand (3) and at the
buttons (2) on the front.
Fig. 5-2 Workstation at the spectrometer

FOUNDRY-MASTER Xline 5 Scope of delivery, transport, set-up and installation
Note! In spark mode, the instrument emits electromagnetic waves. This radiation can cause
radio interference. To minimise emitted interference, the instrument must be set up and
operated as specified in this manual. In the event of electromagnetic incompatibility, the
operating company may have to take additional measures.
The following procedures may contribute to minimising interference:
• enlarging the distance to the "receivers" (power and signal/telecommunications
lines as well as radio receivers);
• specific coordination with respect to other systems;
• additional filtering for the power supply;
• low-inductive earthing of the sample to be analysed;
• and in special cases shielding of the entire instrument.
5.4 Installation
Transport locks Upon initial installation, the transport locks for the optical system must be removed from
the device. This is carried out by a person authorised by Oxford Instruments Analytical
GmbH. If somebody else opens the device, the customer's warranty claims are voided
in all forms.
The initial installation by a person authorised by Oxford Instruments Analytical GmbH
includes a complete functional test of the instrument as well as operator training.
Vacuum pump Observe the supplied operating instructions of the vacuum pump for installation and
operation of the vacuum pump.
Note! The spectrometer may only be installed by a person authorised by Oxford Instruments
Analytical GmbH.
If you connect the mains voltage, the PC and the argon to the device yourself, proceed
as follows:
1. Connect the PC to the instrument (1, fig. 5-3) using the supplied USB cable. Do
not use a USB cable longer than 2 m.
Should the original USB cable be replaced, provide the new cable with a type
"Würth 742 727 33" ferrite.
2. Connect keyboard, mouse and printer to the PC.
3. Connect the power cable to the PC.
4. Insert the exhaust hose (4) into the water-filled washing bottle.
5. Connect the power cable to the spectrometer (5).
The instrument may only be operated on mains with protective conductors.
6. Use the supplied copper pipe to connect the device's argon connection (3) to
the argon container or supply.
1 2 3 4 5
Fig. 5-3 Ports on the instrument

Note! Only use argon suitable for spectrometry (99.998 % – 99.999 % Ar)!
Other gases in the argon (e.g. nitrogen) can affect precision.
7. Ensure that the supply pressure is always in the region 3.0 bar ±0.1 bar.
Note! If the vacuum pump must be switched off, the valve to the tank must first be closed.
To avoid condensation inside the instrument, prior to putting it into service, leave the
instrument to acclimatise to the ambient temperature.

6 Putting into service FOUNDRY-MASTER Xline
6 Putting into service
Initial putting into service of the instrument is carried out by customer service
representatives of Oxford Instruments Analytical GmbH and includes a complete
functional test of the instrument as well as operator training.
Should you put the instrument into service yourself, proceed as follows:
Note! The following description of putting into service assumes that you are familiar with
operating the software and the instrument.
Prerequisite • The instrument has been installed as described in chapter 5.4, page 20.
• A known (analysed or certified) sample of similar chemical composition as the
probe you want to analyse is available.
Recalibration 1. Switch on the PC and wait until WINDOWS™ has been completely started up.
2. Open the WASLab spectrometer software double-clicking the WASLab icon
. The start screen is displayed.
3. Switch on the spectrometer at the on/off switch (1, fig. 6-1).
Fig. 6-1 On/off switch
4. In the start screen, select "Analysis" mode.

5. Select a matrix and analysis program and confirm your selection with "OK". The
analysis screen is displayed.
6. Click "Recal." to recalibrate the instrument. The selection window for the
recalibration method is displayed.
7. Select the "Full" option. The name of the first recalibration sample (e.g. RE12)
is displayed in the centre of the screen.
Fig. 6-2 Display of the requested recalibration sample

FOUNDRY-MASTER Xline 6 Putting into service
8. Place the known sample (2, fig. 6-3) on the spark stand and fix it with the hold-
down device (1).
9. Switch on the excitation source at the rotary knob (3) on the front of the
instrument.
1 2 3 4
Fig. 6-3 Instrument front
10. Spark this well prepared (freshly ground, fat-free) sample at least 3 times by
pressing the start button (4) or clicking the "Start" button in the analysis screen.
Note! Avoid sparking the same point twice. The RSD value in the right column (RSD: Relative
Standard Deviation) is displayed after the third sparking and should be less than or
equal to 10 %.
• If that is the case, carry out further sparkings.
• The results of sparking with the greatest deviations from the average value
are deleted (average value display in the right column). To delete individual
sparkings, highlight the column by double-clicking and click the "Delete"
button. Caution: Deletion cannot be undone!
11. Clean the electrode tip.

12. In the upper left of the screen click "Next" to spark the next recalibration sample.
Note! For the other samples, the RSD value in the right column should be less than or equal
to 3 %.

6 Putting into service FOUNDRY-MASTER Xline
Checking the results After recalibration is completed ("Recalibration successful" note), proceed as follows to
check the recalibration factors:
1. From the "Mode" menu bar and, in the following window, from the picklist, select
"Recalibration factors".
2. Confirm your selection with "OK". The analysis window with the recalibration
factors is displayed. All values in the "Factor" column should range between 0.5
and 2.0, ideally near 1.
3. The "offset.dat" file is in the program directory. Open the file (e.g. with the
editor).
With an ambient temperature of about 20 °C, the values in the last line should
range between -10 and +10.
Values marked with an asterisk (*) can be ignored.
Note! If factors and/or offset values are outside these ranges, please contact our local Oxford
Instruments Analytical GmbH service partner.
After putting into service and recalibration, back up the whole "Master" program
directory so that all relevant data can be recovered if required.
The customer is responsible for regular data backup. Oxford Instruments Analytical
GmbH cannot be called to account in the event of data loss. Data loss can be caused
by a failed hard disk, computer viruses, etc.

7 Quick start FOUNDRY-MASTER Xline
7 Quick start
7.1 Analysing in spark mode (argon)
Argon quality If the instrument has not been used during a prolonged period of time, the argon system
must be sufficiently purged with argon to avoid contamination. Used argon must contain
less than 5 ppm of O2 and H2O (argon for spectral analysis 99.998 % – 99.999 %).
Analysis of some elements such as nitrogen or carbon is heavily affected by impurified
argon. With an argon quality of 4.6 (99.996 %), analysis may not be possible any more.
Further information on nitrogen analysis is provided in chapter 11.4, page 113.
During measurement breaks, the spark stand hole should always be covered with a
sample.
Sample preparation The most critical part of spark analysis is the preparation of the sample.
The importance of sample preparation is often underestimated, although quality and
reliability of the analysis directly depend on it.
Since the spark discharge only evaporates material on the sample surface and does not
penetrate deep into the material, you also measure all impurities on the surface.
Dirt, oils, oxides and even fingerprints can disturb analysis and even prevent the
formation of plasma. In that case, you obtain a poor burn spot with very low luminous
efficacy ("white focal spot"). The result is a faulty analysis, that means the analysed
sample composition does not correspond to the actual composition.
Note! Observe the following information before analysing the sample:

• Freshly ground and clean sample surfaces are a basic requirement for precise
analyses!
• Replace the abrasive paper as soon as you change the matrix (e.g. from Cu to
Fe) or as soon as the paper does not grind very well any more.
In general, one set of recalibration samples can be prepared with the same
abrasive disk, always starting with the pure sample which is the sample with the
smallest number in the stamped designation (e.g. "RA10" for Al matrix).
• Do not use silicon carbide paper (SiC), since the silicon and carbon content
adulterates the analysis of those elements. Oxford Instruments Analytical
GmbH recommends the use of aluminium oxide paper (corundum) or zirconium
oxide paper.
• The spark stand must be cleaned after 300 sparkings at the latest (chapter 10.3,
page 97).
• The electrode must be cleaned upon every change of sample using a steel
brush (brass handle; chapter 10.6.3, page 106).

FOUNDRY-MASTER Xline 7 Quick start
• When you change the matrix (e.g. from iron to aluminium), replace the electrode
and brush (see chapter 10.6, page 103). Otherwise, analysis can be adulterated
by a contamination on the electrode or brush. Therefore, there are a separate
tungsten electrode and brush for every matrix.
• The spacing between electrode tip and sample surface must be set to 3.2 mm
using the spacer (chapter 10.6.2, page 105).
Prerequisites for • The instrument has been put into service as described in chapter 6, page 23.
analysis • The sample to be analysed has been prepared.
• All other required settings have been made (see chapter 8.3, page 45).
1. To spark a sample (1, fig. 7-1), place it on the spark stand (2) with the prepared
side down which is as even as possible so that the hole (3) in the spark stand
plate above the electrode is completely covered, if possible.
To facilitate sample adjustment, you can install an optional prism (5) on the
spark stand.
4 5
1
3
2
2
Fig. 7-1 Placing the sample
Note! Choose the point of support of the hold-down device on the sample so that the sample
closes the spark stand hole as tightly as possible. This is mainly the case if the point of
support is in the centre above the electrode.
2. Press on the sample using the rotatable and height-adjustable hold-down

device (4) attached to the left of the spark stand.
Note! If the sample is not placed correctly, there is a gap between sample and spark stand
plate so that air from outside can enter the argon-purged analysis volume (between
electrode and sample) and adulterate analysis. At the same time, the sound generated
during sparking (measurement) exits through the gap more easily. A sparking noise as
low as possible is therefore a good criterion for an optimally placed sample.
Warning!

Warning!
Danger!
Risk of electric shock!
During sparking, do not, under any circumstances, introduce a conducting object into
the proximity of the spark stand hole!
During sparking, do not, under any circumstances, remove a conducting object from
the spark stand hole!
With the spark stand hole open during sparking, do not, under any circumstances,
bring a part of your body into its immediate vicinity!
Note! Prior to starting sparking, make sure the hold-down device presses down the sample at
the correct position.
3. In the start screen of the WASLab program, select "Analysis".

4. In the "Select analytical program" window, select the subprogram and confirm
your selection with "OK".
5. Switch on the excitation source at the rotary knob on the front of the instrument.
6. Start analysis of the placed sample by clicking "Start" or pressing the green start
button on the front of the instrument.
The flowcharts in the following chapter illustrate the sequence of analysis and
recalibration.

7.2 Flowcharts for analysis and recalibration
7.2.1 Start and sequence of a check measurement in spark mode
Start and sequence of a check

measurement
setting argon supply to 3 bar chapter 5.4, page 20
Connect power supply
switching on computer
waiting until WINDOWS™ has

completely started up
switching on spectrometer
starting spectrometer software
Select "Analysis" and subprogram
Select "Mode" menu item;

Click "Argon purging" button;
purge for 1 minute, click button
again to complete purging
Measure control sample
not OK Recalibration: Select recalibration

Check result
method "FULL" or "TYPE"
chapter 7.2.2, page 31

OK
or
Continue with "Analysing"

7.2.2 Recalibrating "Full"
Recalibrate "Full"
Select "Recal" in analysis window
Select "Full" option
Should one sparking

deviate excessively:
remove by double- Spark shown sample
clicking the column 3 to 4 times minimum
and clicking (avoid sparking the same burn
"Delete". spot)
not
RSD within the OK Check samples
specification?
OK
Continue, until all

recalibration samples
for that matrix have
been sparked.
Continue with "Next".
all sparked,
"Recalibration successful" message


7.2.3 Recalibrating "Type"
Recalibrate "Type"
Select "Recal" in analysis window
Select "Type" option
Should one sparking

remove by double- Spark desired sample
"Delete". spot)
Check results
OK
Confirm result

7.2.4 Performing an analysis
Analyse
Select "New" in analysis window
Enter sample name/number
Should one sparking

remove by double- Spark desired sample
"Delete". spot)
Verify analysis
OK
If 3 values are
consistent Continue with
next sample
Select "Store",
"Print"?
Complete analysis

8 WASLab software FOUNDRY-MASTER Xline
8 WASLab software
This chapter contains a description of the different software windows.
Starting the software Start the WASLab software by double-clicking the icon .
If passwords have been assigned, the corresponding user must enter his password
when starting the WASLab software, see fig. 8-4, page 38. The program only starts after
the correct password has been entered.
Note! User levels 1 to 3 are restricted. Some of the options described in this chapter may not
be available to you. Should you want to change any settings, please contact your
superior.
Entering data To enter data, use an external keyboard or the screen editor (on-screen keyboard)
integrated in the WASLab software or the virtual numeric keypad, respectively.
The screen editor / virtual numeric keypad opens by double-clicking the corresponding
box and is operated with the mouse. For easier orientation in the software, the editor
(keyboard) is object-related. The current reference is indicated to the left of the input
box, here "Sample ID" (fig. 8-1).
Fig. 8-1 On-screen keyboard and virtual numeric keypad

FOUNDRY-MASTER Xline 8 WASLab software
8.1 Start screen
After starting the software, the following screen is displayed:
6 2
5 3
Fig. 8-2 Start screen
Table 8-1 Elements in the start screen
Item Element / button / input box Function

1 Company logo -
2 "Utilities" button (settings) Opens the "Utilities" menu (chapter 8.2, page 37).
3 current user level Indicates the current user level.
4 "Exit" button Terminates the program and returns to the Windows interface.
5 "Analysis" button Opens the analytical program (chapter 8.4, page 49).
6 instrument name indication of the spectrometer in use

8.2 Utilities
By clicking "Utilities" in the start screen, the "Utilities" menu opens. The options shown
depend on the set user level and can be edited by an administrator in the "Passwords"
menu item (see chapter 8.2.3, page 41).
The following illustration shows the "Utilities" menu of user level 4.
Should you see a restricted menu, you are on a lower user level.
1
2
4
5
6
7
Fig. 8-3 "Utilities" window
Table 8-2 Elements in the "Utilities" window
Item Button / input box Function

1 Return to main menu Closes this menu and returns to the start screen (chapter 8.1, page 36).
2 Password entry Opens a window for password entry (chapter 8.2.1, page 38).
3 Options Opens the "Options" menu (chapter 8.2.2, page 39).
4 Passwords Opens a menu for password assignment and setting up access rights
(chapter 8.2.3, page 41).
5 Delete file Opens a window to select a file to be deleted (chapter 8.2.4, page 42).
6 Create/change alloy Opens the window to create/edit analytical programs (chapter 8.2.5, page 43).
7 Firmware status Opens the "Dsp status report" window (chapter 8.2.6, page 43).
8 Service This menu item allows access to a program area where instrument data are
collected with the support of Oxford Instruments Analytical GmbH which can be
useful in the diagnosis and troubleshooting of problems (chapter 8.2.7,
page 44).

8.2.1 Enter password
When password protection is enabled, the "Password dialog" window opens when the
program is started (fig. 8-4).
Enter the password and confirm with "OK".
Information about password management is provided in chapter 8.2.3, page 41.
Fig. 8-4 "Password dialog" window

8.2.2 Options
The "Options" window is only available on user level 4. In this window, you define the
general options for the program's behaviour and displays.
After you have set all options, confirm your changes by clicking "OK". An information
window prompting you to restart the program is displayed. Confirm the message by
clicking "OK" and restart the program.
2 5
6
3
4
8
Fig. 8-5 "Options" window
Table 8-3 Elements in the "Options" window

1 Automatic start with analysis program When this option is enabled, the WASLab software automatically opens the
analysis program selected from the dropdown list on the right when it is started.
When this option is not enabled, a default start screen opens instead.
Further information on the use of the analytical program is provided in
chapter 8.4, page 49.
Automatic start with sorting program Only for mobile instruments:
When this option is enabled, the WASLab software automatically opens the
sorting program selected from the dropdown list on the right when it is started.
When this option is not enabled, a default start screen opens instead.
2 Display analysis horizontally line-by-line display of the analysis results in mass percent of chemical elements
(chapter 8.4.3, page 51)
Automatic average Enabled: The average value of the analysis results is automatically displayed
(only in "Percent analysis" mode).
Disabled: The average value display can be enabled and disabled with the
corresponding button in the menu bar.
Allow average editing The average value of measurements can be manually overwritten. Manipulated
data are displayed in italics.

Table 8-3 Elements in the "Options" window

3 No "Hold Trigger" message Only for mobile instruments:
Displays the No "Hold Trigger" message on the screen when the toggle switch
of the test probe is in "Start" position.
Reset = store analysis Only for mobile instruments:
Stores the analysis result if the toggle switch of the test probe is in "0" position.
Reset = print analysis Only for mobile instruments:
Prints the analysis result on the default printer if the toggle switch of the test
probe is in "0" position.
Reset = next sample Only for mobile instruments:
Changes to the next sample if the toggle switch of the test probe is in "0"
position.
Print in colour If a colour printer is connected, the report file is printed in colour.
4 Error color Error settings for bad samples, colour display assignment
Warning color
The colour of the error information window can be individually set. The error
window is displayed as soon as a sparked sample infringes the defined
specifications / limit values.
The warning window is displayed if the analysis of the sparked sample is just
within the specified limit values.
The colour of the warning can be adapted to the environment during operation.
That means, if the environment is light, an intensive colour can be chosen.
Any colour can be assigned to the word "Error". Click the "Foreground" button to
open the colour properties window. Set a colour and confirm with "OK".
Repeat this for the "Background" and the warning window.

5 Minimum sparkings during recalibration in Enter the minimum number of sparkings during recalibration in spark mode here
spark mode (chapter 8.6, page 65).
Minimum sparkings during recalibration in arc Only for mobile instruments:
mode Enter the minimum number of sparkings during recalibration in arc mode here.
6 External programs Select the programs to be executed after measurement/saving here. Enable the
- execute after measurement checkbox and enter the complete path to the desired program in the input box.
- execute after saving
7 Language Select a language.
8 Cleaning reminder Enter the number of sparkings after which the reminder for cleaning the spark
stand shall be displayed here (chapter 10.3, page 97).
9 Argon flow reduction After the set time has elapsed (after the last analysis), the argon flow in the
spark stand is reduced.

8.2.3 Passwords
2 1
Fig. 8-6 "Edit passwords" window
Assigning passwords Passwords can only be assigned in user level 4. Therefore, the access to user level 4
should be protected by a separate password.
If passwords have been assigned, the corresponding user must enter his password
when starting the WASLab software, see fig. 8-4, page 38. The program only starts after
the correct password has been entered.
Note! You cannot access the software without the password!

Passwords may consist of letters, numbers and symbols.
• In the "Edit passwords" window, click the "Level x" input box (1, fig. 8-6) and
enter the password for that user level.
Setting access rights We recommend to protect all settings against inadvertent changes.
Define the access rights for the individual user levels by adjusting the RED or GREEN
bars and assigning a password to the corresponding user.
• Click the corresponding bar (2, fig. 8-6) to change the colour and thus access
authorisation.
A red bar means that the user does not have access to the setting.
Note! Oxford Instruments Analytical GmbH cannot be called to account for damage resulting
from operational errors. Do in any case restrict access to the WASLab software.
Close the window by clicking "OK" (3, fig. 8-6).

• To enable the changed settings, restart the WASLab software. To do that, click
"Return to main menu" in the "Utilities" menu and then click "Exit" in the start
menu. Restart the WASLab software by double-clicking.

8.2.4 Delete files
The WASLab software has a central window which is the "Delete files" window. In that
window, files of all types you have created with WASLab can be deleted.
Note! Only delete files you do not need any more. Deleted files are permanently removed
and not transferred to the Windows™ recycle bin. They cannot be restored.
1 2
Fig. 8-7 "Delete files" window
All available file groups are indicated in a dropdown list (1, fig. 8-7). By selecting a file
group, the corresponding files are illustrated in the window on the right.
1. Open the dropdown list.

2. Select a group to display the corresponding files in the list on the right (2).
3. From the list on the right, select the file to be deleted.
The "Delete" button is enabled.
4. Remove the file by clicking "Delete" (3).
A confirmation window is displayed.
5. To permanently delete the selected file, close the "Confirmation" window by
clicking "Yes". -> The file is deleted.
By clicking "No", you return to the previous window.
6. Exit the "Delete files" window by clicking "Close" to return to the "Utilities"
window.

8.2.5 Select analysis program
In the "Select analysis program" menu, you can create an analysis program or open or
edit an already existing program. More information about creating and setting up an
analytical program is provided in chapter 13.2, page 123.
Fig. 8-8 "Select analysis program" window
8.2.6 Firmware status
In the "Dsp status report" window, the current firmware status for the spectrometer is
displayed.
1 3
Fig. 8-9 "Dsp status report" window
Table 8-4 Elements in the "Dsp status report" window

1 Refresh Refreshes the display.
2 Print Prints the status on the connected printer.
3 Close Closes the window.

8.2.7 Service
This menu item allows accessing a program area where instrument data are collected
— with the support of Oxford Instruments Analytical GmbH — which can be useful in the
diagnosis and troubleshooting of problems.
Only execute these functions under the instruction of a service representative!
Further information is provided in the reference section in chapter 13.3, page 132.

8.3 Readout mode / settings grade identification
In the "Readout mode / settings grade identification" window, you can make the settings
for analysis, grades and printing/saving.
1. Open the "Readout mode / settings grade identification" window clicking the
"Mode (F7)" button in the "Analysis" window (see chapter 8.4.4, page 52).
1 6
2
3 7
4 8
5
9
10
11
12
Fig. 8-10 "Readout mode / settings grade identification" window
Table 8-5 Elements in the "Readout mode / settings grade identification" window
Item Element Function
1 Recall stored analysis Opens a selection window to recall stored analyses.
2 Repeated measuring Defines the number of measurements to be automatically executed for the same sample.
3 Stand cleaned Resets the counter for the automatic spark stand cleaning reminder to zero.
4 Argon purge After a prolonged standstill, an increased argon flow helps to quickly purge the spark stand with
argon.
5 Disable alignment The software uses profiling to compare the measured results to the saved
reference lines. With profiling switched off, you can measure samples of another matrix as
the selected matrix (e.g. Cu instead of Fe). The measured result may be falsified
in this case because the assignment to reference line data is missing.
6 Mode Selection of analysis results display. The following display modes are available:
Percent analysis The analysis results are automatically displayed as percent analysis (default setting).
Channel concentrations The analysis results are displayed as the concentration of every individual element channel
(analytical line).
Corrected int. ratio The analysis results are displayed as corrected intensity ratio.
Recalibrated int. ratio The analysis results are displayed as recalibrated intensity ratio.
Intensity ratio The analysis results are displayed as intensity ratio related to the reference line.
Intensity The analysis results are displayed as intensity (light quantity).
Recalibration factor summary of the last recalibration
7 Grade set selection of the grade file for the "Search grade" button
8 Search grade Searches for the grade entered in the "Grade file" box in the database.
9 Grade selection selection of the grade for the "Compare grade" button
10 Compare grade definition of a set grade from the grade database
11 Grade options Opens the "Grade options" window.
12 Print/store options Opens the "Print/store options" window.

8.3.1 Recall stored analysis
Clicking the "Recall stored analysis" button opens the "Select analysis" window where
you can select, delete, import, open or save the selected analysis.
Fig. 8-11 "Select analysis" window
8.3.2 Repeated measuring
When you change the matrix, the first analyses of the new matrix may be affected by
residual condensate in the spark stand (contamination) of the last sparkings of the old
matrix.
This setting is used to "burn off" any contamination in repeated sparkings. The following
dialog window opens by clicking the "Repeated measuring" button:
Fig. 8-12 "Repeat" window
Enter the number of repetitions and confirm with "OK".

8.3.3 Grade options
The following window opens by clicking the "Grade options" button:
1
2
3
4
5
6
7
8
9
10
11
Fig. 8-13 "Grade options" window
Table 8-6 Elements in the "Grade options" window

1 No auto search/compare No automatic search is executed in the grade database when this checkbox is
enabled.
2 Auto search When this option is enabled, the software automatically searches the grade database.
3 Auto search on last burn Compares the result with the result of the last measurement, not with the average
value.
4 Large grade display Disabled:
The result of the automatic grade search is shown below the analysis window.
Enabled:
The result of the grade search is displayed full-screen.
5 Auto compare and After burns One box requires the other. Automatic grade identification depends on the value
entered in the "After sparkings" box. The number of sparkings should be at least 3.
6 Strict grade limits Tolerances are not considered for grade search.
7 Stop at first grade found Only the first matching grade found is shown. The database is further searched.
8 Show best match The grade which best matches with the searched grade is shown.
9 Automatic new sample When this option is enabled, a new window to enter a further sample is automatically
opened.
10 Grade compare, show all limits When this option is enabled, upper and lower limits for the elements of the analysed
grade are shown in the analysis result.
11 Apply grade settings for all alloys When this option is enabled and confirmed with "OK", all options in this menu are
applied to all subprograms of this matrix.
Multiple choice is possible.

8.3.4 Print/store options
The following window opens by clicking the "Print/store options" button:
1
2
3
4
5
6
7
8
9
10
11
Fig. 8-14 "Print/store options" window
Table 8-7 Elements in the "Print/store options" window

1 Print single burns Enabled: By selecting "Print" in the analysis window, individual sparkings are printed.
2 No report printing Enabled: Prints the individual measurement in the format selected in the "Report file" box.
This option can only be enabled after a report file has been selected.
3 Auto print on edit / new sample Enabled: The analysis result is automatically printed when "New" or "Exit" is selected.
4 Report file selection of a report file (see chapter 8.10, page 83)
5 Format file Selection of a format file. The file can be set by the Oxford customer service (see
chapter 13.2.3, page 127).
6 Printer options Opens the WINDOWS™ dialog to set the printer options.
7 Store single burns Enabled: By selecting "Store" in the analysis window, individual sparkings are stored.
8 In text file Enabled: Saves the analysis result in a text file.
9 In Excel CSV file Enabled: Saves the analysis result in a CSV file.
10 In database Enabled: Saves the analysis result in a WASLab database.
11 Auto store on exit / new sample Enabled: The analysis result is automatically saved when "New" or "Exit" is selected.
Multiple choice is possible.

8.4 Description of the analysis screens
This chapter contains a description of the screens to perform analysis on user level 4.
Note! Depending on the selected user level (password level), certain functions are disabled.
From that result different menu structures for the different user levels.
All functions of user levels 1–3 are available on user level 4.
8.4.1 Select analysis program
By selecting "Analysis" in the start screen (see chapter 8.1, page 36), the "Select
analytical program" window opens.
1 3
Table 8-8 Elements in the "Select analysis program" window

1 matrix selection (basis for By clicking the button, the available analysis programs for the selected
analysis) grade are displayed in the window above.
Depending on the configuration of the instrument, the number and
selection of matrices can vary so that the number of buttons may
deviate from the illustration.
2 selection of the analysis Select the required program.
program
3 OK Confirms the selection and displays the analysis window
(chapter 8.4.2, page 50).
4 Cancel Cancels the selection and returns to the start screen

8.4.2 Analysis window (vertical)
The "Analysis" window is displayed after selecting the analysis program.
1
2
5
3
6
7 8 9 10 11
Fig. 8-16 "Analysis" window
Table 8-9 Elements in the "Analysis" window

1 function buttons (the assigned key is given in brackets), see chapter 8.4.4, page 52
Start (F10) Enables an analysis sequence.
New (F2) Entry of a new sample name. The results of previous analyses in the display are deleted.
Average Display of the average value of current sparkings (chapter 8.4.3, page 51).
(not illustrated) This option is only available when the corresponding option is selected in the options menu.
Print (F4) Printout of the current analysis results indicating:
name of the alloy, name of the sample, date, ...
Del (Del) Selected, highlighted data (sparking) are deleted.
Store (F5) option to save data (analysis results etc.)
Recal. (F6) program to perform recalibration in the enabled analytical program
Mode (F7) selection of the display mode for analysis results
Load (F8) Opens the "Select analysis program" window.
Change (F9) change of parameters of the enabled analysis program
RSD (Alt+R) display of the relative standard deviation of at least 3 sparkings
Exit (Alt+Q) Closes the analysis window and returns to the start screen.
2 Name (ID) of the sample indication of the used sample (sample ID)
3 "Element" column all elements selected for the workpiece to be analysed
4 "Sparking x" column Number of sparkings which can be displayed simultaneously on the screen. The number depends
on the set screen resolution of your PC.
5 "Average" column Display of the average value of sparkings
6 information bar The information bar contains important additional information regarding the currently displayed
analysis mode.

Table 8-9 Elements in the "Analysis" window

7 display mode Indication of the used display mode with the following options:
PA percent analysis (mass %)
CC channel concentrations
IC corrected intensity ratio
IS recalibrated intensity ratio
IR intensity ratio
I intensity
F recalibration factor
8 analysis program abbreviation of the used analysis program
9 Mode mode of measurement, e.g. sample analysis or recalibration
10 grade Indicates the grade matching the analysis, e.g. for enabled grade search.
11 number of sparkings Indicates the total number of sparkings since the counter was last reset. Only an authorised service
partner of Oxford Instruments Analytical GmbH is allowed to reset the counter.
8.4.3 Analysis window (horizontal)
When the "Display analysis horizontally" option, see chapter 8.2.2, page 39, fig. 8-3, is
enabled and the "Automatic average" option is not enabled, the "Average" button (1,
fig. 8-17) is added to the function bar. Click the "Average" button to display the average
value (2) above the analysis results.
Fig. 8-17 "Analysis" window (horizontal)

8.4.4 Short description of the function buttons
Start (F10)
F10
Fig. 8-18 "Start (F10)" function button
By clicking "Start", sample analysis is initiated. It is an automatic process. The individual

steps are shown on the screen.
After the analysis, the result is displayed (fig. 8-19).
Alternatively, you can start analysis pressing the green start button (see chapter 4.2.2,
page 15).
Fig. 8-19 Analysis result (example)

New (F2)
F2
Fig. 8-20 "New (F2)" function button
Click "New (F2)" to analyse a new sample. The on-screen keyboard opens.
Fig. 8-21 "Sample ID" entry
Enter the sample ID and confirm with "OK". The entered name of the sample is
displayed below the function buttons on the screen.
Note! When a report file is assigned to the selected analytical program, at first, the "Dialog"
window is opened to enter data in the report file.
Fig. 8-22 "Dialog" window
Further information about the report file is provided in chapter 8.10, page 83.

Print (F4)
F4
Fig. 8-23 "Print (F4)" function button
Click the "Print (F4)" button to generate a printout of the current analysis indicating the
names of alloy and sample, date, etc.
The results are output on the installed WINDOWS™ default printer. If no printer is
connected, the print job is added to the queue and can be printed later.
The layout of the printed file can be designed individually (see chapter 8.10, page 83).
Del (Del)
Del
Fig. 8-24 "Del (Del)" function button
To delete a sparking not required any more, highlight the corresponding column on the
screen (fig. 8-25) by double-clicking that column. Then click the "Del" button.
This button is only enabled when the column is highlighted.
Fig. 8-25 Deleting a column

Store (F5)
F5
Fig. 8-26 "Store (F5)" function button
Depending on the set options, this button can be disabled.

After a sparking has been completed, you can manually save the analysis result by
selecting this button.
Successful saving is indicated by a message on the screen.
When automatic saving is enabled, the results are automatically saved to the defined
destination file (see chapter 13.2, page 123).
Recal. (F6)
F6
Fig. 8-27 "Recal. (F6)" function button
Click the "Recal. (F6)" function button to recalibrate the spectrometer.

Three recalibration methods are available in the WASLab software:
• "Type" recalibration
The current grade type (a single sample) is recalibrated.
• Analysis program
One group of alloys is recalibrated (e.g. CrNi steel).
• "Full" recalibration
A complete matrix (e.g. Cu) is recalibrated.
Further information about recalibration is provided in chapter 8.6, page 65.

Mode (F7)
F7
Fig. 8-28 "Mode (F7)" function button
By clicking the "Mode (F7)" button, the "Readout mode / settings grade identification"
window opens where you can select a mode (display of analysis results; 1, fig. 8-29).
Further information about the modes is provided in chapter 13.2, page 123.
Load (F8)
F8
Fig. 8-30 "Load (F8)" function button
By clicking the "Load (F8)" button, the "Select analytical program" window opens (fig. 8-
15, page 49). The window displays all available analysis programs. Select a program
and confirm with "OK". The selected program is loaded and indicated in the information
bar.
Note! When the matrix is changed, you must clean the complete spark stand (see
When the electrode is replaced, set the spacing between electrode and workpiece to
3.2 mm.

Change (F9)
F9
Fig. 8-31 "Change (F9)" function button
Clicking "Change (F9)" opens the "Change alloy" window for the enabled analytical
program (fig. 8-32) where you can edit the program parameters.
1
2
3 13
4 14
5
6 15
7
8
9
10
11
12 16
Fig. 8-32 "Change alloy" window
Table 8-10 Elements in the "Change alloy" window

1 Description Shall not be edited by the operator. Further information is provided in the reference section
2 Matrix element (chapter 13, page 121).
3 Parameter file
4 References file
5 Format file
6 Curve file
7 Alloy selection
8 Type recal. file data of individual samples for "Type" recalibration
9 Calculation file set-up and selection of calculation files or pseudo elements (chapter 8.9, page 79)
10 Report file set-up and selection of the report file (chapter 8.10, page 83)
11 Control standard file Enter the parameters for an individual control sample (chapter 13.2.6, page 130).
12 Storage file Define the destination folder for analysis data here.
13 Standards Shall not be edited by the operator. Further information is provided in the reference section
(chapter 13, page 121).
14 Grades Opens a window to enter grades. This is usually done by the user as required (chapter 8.7,
page 70).
15 Edit recal. Shall not be edited by the operator. Further information is provided in the reference section
(chapter 13, page 121).
16 Browse Opens the WINDOWS™ dialog to save a file.

RSD (Alt+R)
Alt+R
Fig. 8-33 "RSD (Alt+R)" function button
After at least 3 sparkings, you can display the relative standard deviation (RSD) by
clicking the "RSD" button. The result is displayed in a separate column (1, fig. 8-34) or
line (1, fig. 8-35).
Fig. 8-34 "Analysis" window with indication of RSD
Fig. 8-35 "Analysis horizontal" window with indication of RSD (example)

Exit (Alt+Q)
Alt+Q
Fig. 8-36 "Exit (Alt+Q)" function button
By clicking "Exit", the analysis window is closed. The program returns to the start screen
after confirmation (fig. 8-37), see fig. 8-2, page 36.
Fig. 8-37 Exit dialog

8.5 Analysing samples
Note! Depending on the selected user/password level, some software functions are not
available. From that result different menu structures for the different password levels.
This chapter contains a description of the analysis of a sample on password level 4

where all individual main menus can be accessed and which also contains instructions
for password levels 1 to 3.
Prerequisites for • The instrument has been put into service as described in chapter 6, page 23.
analysis
• The sample to be analysed has been prepared.
• The parameters for analysis have been set (see chapter 8.3, page 45).
1. Start the WASLab software by double-clicking the icon .

• The start screen is displayed.
Fig. 8-38 Start screen
2. Open the matrix selection by clicking "Analysis".

3. In the "Select analysis program" window, select the matrix and a subprogram
you want to analyse and confirm with "OK".
• The "Analysis" window is displayed.

Fig. 8-40 "Analysis" window
4. In the function bar, click the "New" button and enter the sample ID.
If you have assigned a report file to the analysis, fill in the "Dialog" window.
Warning!

Warning!
Danger!
Risk of electric shock!
During sparking, do not, under any circumstances, introduce a conducting object into
the proximity of the spark stand hole!
During sparking, do not, under any circumstances, remove a conducting object from
the spark stand hole!
With the spark stand hole open during sparking, do not, under any circumstances,
bring a part of your body into its immediate vicinity!
5. Place the prepared sample on the spark stand and fix it with the hold-down
device.
6. Switch on the excitation source at the rotary knob on the front of the instrument.
7. Start analysis of the placed sample by clicking "Start" or pressing the green start
button on the front of the instrument.
• Analysis is an automatic process.
• The individual steps of analysis (purging, pre-sparking, measuring) are
shown on the screen.
• After completing automatic analysis, the result is displayed in the 1st column
(Sparking 1).
8. Repeat the sequence (point 7.) for further sparkings.
Fig. 8-42 "Analysis" window with result
9. After all sparkings have been completed, you can delete, save or print the result
as described in chapter 8.4.4, page 52.

8.5.1 Disabling a sparking
By double-clicking the head of a column, you can temporarily hide a specific sparking.
The column is disabled and shown in grey font. That means, that measurement is not
included in the calculation of the average value.
That way you can easily determine the impact of every individual measurement on the
overall result.
To re-enable a hidden sparking, click the head of the column again.
8.5.2 Displaying the relative standard deviation (RSD)
The RSD display is only available after at least three sparkings have been performed or
three sparkings are active on the screen, respectively. Disabled measurements may
have to be re-enabled.
1. To display the relative standard deviation, click the "RSD" button.

• The window indicating the relative standard deviation is displayed.
Fig. 8-43 "Analysis" window with indication of RSD
Table 8-11 Columns in the "Analysis" window with indication of RSD
Column Indication of
SD absolute standard deviation
RSD Relative standard deviation: standard deviation related to the average value
Minimum minimum concentration for x sparkings
Maximum maximum concentration for x sparkings
Average average value of all current sparkings
2. Click the "RSD" button again to display the individual results of the sparkings.

Note! The (relative) standard deviation strongly depends on homogeneity and proper sample
preparation. The concentration range the indication relates to also plays an important
role for the relative standard deviation. An SD of 0.01 % at a content of 1 %, for example,
results in an RSD of 1 %. However, at a content of 0.03 %, it results in an RSD of 33 %!
For that reason, a binding indication of standard deviations is hardly possible or,
respectively, can only be determined under precisely defined measurement conditions.

8.6 Recalibration
Recalibration is a reset of the spectrometer with known samples. Recalibration is

required to compensate for changes in the spectral sensitivity due to contamination or
ageing of components so that the original calibration remains applicable during the
entire life of the instrument.
You can
• only recalibrate a single alloy ("Type" recalibration)
• recalibrate a certain group of alloys ("Analysis program", e.g. low-alloy steels
within the Fe matrix) or
• recalibrate a complete matrix ("Full").
This chapter contains a description of the "Full" recalibration of a matrix.

The procedure for the other recalibration methods is the same — only the number of
samples to be measured may be smaller.
Note! During recalibration, the recalibration samples are automatically requested by the
software one by one.
Those samples are included in the scope of delivery and are supplied in the accessory
case. A loss of the samples leads to complex adaptations to a new set of samples!
Individual samples can only be exchanged for samples of the same type and charge
number!

3. In the "Select analytical program" window, select the matrix and a subprogram
you want to recalibrate and confirm with "OK" (see chapter 8.4.1, page 49).
4. Start recalibration clicking "Recal." in the "Analysis" window (1, fig. 8-44).
Fig. 8-44 Clicking "Recal."

• The "Recalibration method" selection window is displayed.
2 3 4
Fig. 8-45 "Recalibration method" selection window
Table 8-12 Elements in the "Recalibration method" selection window

1 Type recal sample selection of a recalibration sample
2 Type Recalibration is only performed with the selected sample.
3 Use type enabling of "Type" recalibration
4 Undo type disabling of "Type" recalibration
5 Analysis program Only the specific alloy type (i.e. the selected subprogram, e.g.
FE_500) is recalibrated.
6 Full The complete matrix (e.g. FE) is recalibrated, all subprograms are
updated.
7 Cancel Cancels the selection and returns to the "Analysis" window.
5. Click "Full" to perform recalibration.

• In the analysis window, the designation of the recalibration sample to be
sparked is displayed.
Fig. 8-46 Display of the requested recalibration sample
6. Place the prepared sample on the spark stand and fix it with the hold-down
device.

7. Start recalibration by clicking "Start" or pressing the green start button on the
front of the spectrometer.
• The automatic process can be followed on the screen.
• After sparking has been completed, the result is displayed in the "Sparking
1" column.
Fig. 8-47 Result of the 1st measurement for recalibration (example)
Note! The numeric values (light intensities) should approximately correspond to the values
indicated in the left column behind the designations for the element channels.
Note! For recalibration, we recommend to perform at least three sparkings per sample. For
checking a pure sample (e.g. high-purity iron, sample designation starting with "RE12"),
the sample should be sparked approximately 10 times, since the initial sparking results
are often unusable due to the "memory effect". The pure sample is always the first of a
set to be requested for the recalibration of a matrix.
The minimum number of sparkings during recalibration is defined in the "Options" menu
(see chapter 8.2.2, page 39, fig. 8-5).
8. After at least three sparkings of each recalibration sample and checking the
displayed RSD values, click "Next".
• The designation of the next recalibration sample is displayed on the screen.

9. Repeat these steps until all recalibration samples of the enabled analysis
program or matrix have been sparked and the "Recalibration successful"
information is displayed.
Fig. 8-48 "Recalibration successful" information
10. Confirm that window by clicking "OK" to return to the analysis window.
Note! Observe the following:

• If you click "Next" before the recalibration sample has been sparked sufficiently
often, you are prompted to perform the missing sparkings.
• Click "OK" to continue with the remaining sparkings.
Fig. 8-49 Error message
• If recalibration is interrupted, the "Warning" window is displayed (fig. 8-50).

• If, in that case, sparking of a specific recalibration sample is not required,
click the "Skip recalibration sample" button in the "Warning" window. The
software then requests the next recalibration sample.
• If you want to permanently cancel recalibration, click "Next". The "Warning"
window is displayed.
• Click "Abort recalibration".
• To continue recalibration, click "Spark recalibration sample".
Fig. 8-50 Warning

After all recalibration samples have been sparked, the results of recalibration are
automatically saved and available for checking.
1. To check recalibration data, click the "Mode" button in the analysis window.
• The "Readout mode / settings grade identification" window opens.
2. From the "Mode" dropdown list, select the "Recalibration factor" option and
confirm with "OK".
• The window closes and the result of recalibration is displayed in the
"Analysis" window.
Fig. 8-51 Result of recalibration
Note! Regularly generate a printout of recalibration data and store it together with the
instrument documentation.
3. Terminate recalibration clicking the "Mode" button in the function bar and
selecting "Percent analysis" from the "Mode" dropdown list in the following
"Readout mode / settings grade identification" window. Confirm with "OK".
• The "Analysis" window is displayed again.

8.7 Grade database
This chapter contains a description of the editing and set-up of individual grade
databases. You can
• select the grade file or create a new one
• edit the existing grades in the grade file
• or add new grades.
Note! The grades already listed in the grade database upon delivery of the instrument are to
be understood as examples only.
Oxford Instruments Analytical GmbH assumes no responsibility or liability for the use of
these already listed grades.
The sole responsibility for entering grades and maintaining the grade database lies with
the operating company.
8.7.1 Selecting a grade file
1. Open the "Change alloy" window and click the "Grade Sets" button (1, fig. 8-52).
• The "Grade file selection" window opens.
Fig. 8-53 "Grade file selection" window
2. From the list, select an existing grade file and confirm with "OK".

• The "Grade selection" window of the selected grade file is displayed.
6 7 8 9
1 10
2 11
3
4
12
Fig. 8-54 "Grade selection" window
Table 8-13 Elements in the "Grade selection" window

1 Add grade Opens the on-screen keyboard to enter the new grade.
Grade designation with 40 characters maximum. The designation may consist of letters
and numbers.
2 Delete grade Deletes the selected grade.
3 Copy grade The selected grade is copied to the same grade file with all parameters.
Important! Rename the new grade prior to changing parameters!
4 list of grades Displays the grades contained in the grade file.
5 Arrow keys Shifts the selected grade in the list.
6 Alphanumeric sort. The list is searched for matching grades by alphanumeric order.
7 Sort by concentration The list is searched for matching grades depending on the concentration.
8 Excel in The list of grades is imported as a CSV (Excel) file.
9 Excel out The list of grades is exported as a CSV (Excel) file.
10 Grade name display of the selected grade
11 Formula input boxes for grade formulas for grades not contained in the list of grades
12 list of elements Input boxes for the limit values of the corresponding elements.
In addition to the lower and upper limits in mass % of the respective alloy elements, the
tolerance can also be entered in %.

8.7.2 Creating a new grade file
1. Access the "Change alloy" window (fig. 8-52, page 70) and click the "Grade
Sets" button.
The "Grade file selection" window opens.
2. Double-click the "Name" input box.
The on-screen keyboard is displayed.
3. Enter the new file name and confirm with "OK".
The new name is entered in the "Name" input box.
4. In the "Grade file selection" window, click "OK".
The "Grade selection" window opens.
Note! When a new grade file is created, the "Grade selection" menu is empty. All grade
parameters are entered in that window.
5. To define a new grade, click the "Add grade" button.

6. Proceed as described in chapter 8.7.3, page 73.

8.7.3 Adding a grade
1. To add a new grade to the selected database, click the "Add grade" button.
The on-screen keyboard is displayed.
2. Enter the new grade designation and confirm with "OK".
The new name is added to the list of grades.
3. Select the new grade from the list.
The name is indicated in the window and you can enter the values for the
individual elements of the grade.
4. For that, double-click the corresponding line of the element.
The "Edit limits" window for the selected element opens.
5. Enter the values at the connected keyboard or the virtual numeric keypad.
Confirm the entry with "OK".
6. Repeat step 5 for all alloy elements of the grade for which you want to set limit
values and tolerances.
Exemplary entries for Cr element (chromium):

For 316 L grade type, the concentration range for Cr is between:
a. lower limit 16.5 %
b. upper limit 18.5 %
Enter those numbers.
Depending on the sorting, you can enter an additional value for tolerance.
Note! There is no obligation to enter a tolerance value.
Function of the tolerance value, illustrated by an example:

The admissible range for Cr is 2 % (16.5 % – 18.5 %).
If a tolerance value of 25 % is entered, the new tolerance range is increased by ±0.5 %
(= 25 % of 2 %) so that the following results:
• new lower limit 16.0 % (16.5 – 0.5)
• new upper limit 19.0 % (18.5 + 0.5)
If the analysis result is within that increased interval, the grade is displayed with a yellow
background.

8.7.4 Editing a grade
1. Select the grade from the list.

The name is indicated in the window and you can enter the values for the
individual elements of the grade.
2. For that, double-click the corresponding line of the element.
The "Edit limits" window for the selected element opens.
3. Enter the values at the connected keyboard or the virtual numeric keypad.
Confirm the entry with "OK".
4. Repeat step 5 for all alloy elements of the grade for which you want to set limit
values and tolerances.

8.8 Searching for and comparing grades
This chapter contains a description of the function of grade search and grade
identification by comparing a sample of unknown composition with stored grade
qualities in the database.
8.8.1 Searching for grades
The following example illustrates how the grade search function can be used to compare
a sample of which you only know that it is an aluminium alloy to qualities stored in the
database.
Note! • The basic settings for grade search are made in the "Grade options" window
(see chapter 8.3.3, page 47).
• The instrument configuration is customer-specific. Therefore, the illustrations in
this chapter can deviate from what you see on your screen. The procedure is
the same for all grades in all matrices.

3. In the "Select analytical program" window, select matrix FE and subprogram
"FE Orientation". Confirm your selection with "OK".
4. Position the sample and start analysis by clicking "Start" or pressing the green
start button on the front of the housing.
• The result is displayed in the first free column on the left of the window.
5. Click "Mode" to open the "Readout mode / settings grade identification" window.
Grade search The aim is to identify an unknown grade by comparing it to stored data.
6. From the list of grade files, select the matching grade group (FE_GRADE in this
example).
7. For parameter entry, open the "Grade options" menu clicking the "Grade
options" buttons.
• In the "Grade options" window, enter the search criteria and confirm with
"OK".
8. Exit the "Readout mode / settings grade identification" window clicking "OK".
The analysis window is displayed again.

The selected grade group is now searched for matches with stored grade data after
every analysis performed. Depending on your settings, the result is displayed in the line
below the numeric values (fig. 8-55) or full-screen.
1 2 3 4 5
Fig. 8-55 Result of grade search in the "Analysis" window
The following information is indicated in the search result:
Table 8-14 Result of grade search

1 "Grade" button Opens a window with the found matches.
In that window, double-click a grade to enable it.
2 grade information bar Green: compliance of concentrations of all elements of the identified grade stored in the
database
Yellow: At least 1 element is outside the stored lower/upper limits, but within the defined
tolerance range.
Red: At least 1 element is outside the stored lower/upper limits and outside the defined
tolerance range.
Double-clicking the information bar opens a window with the elements and the corresponding
limit values.
3 priority Display of the priority of the identified grade, the highest degree of compliance is the highest
priority.
4 number display of the number of grades coming into question for the sparked sample
5 Grade name Display of found or set grade; the correspondingly displayed grade designation is according
to the operator entry in the grade database. Company-specific abbreviations can also be
used. The meaning of colours is explained further up.

8.8.2 Comparing grades (grade identification)
The grade is chosen from the database by the operator and after sparking the unknown
sample, the current analysis is compared to that of the chosen grade.
In the following example, we compare an unknown sample with stored grade ST52.0S
(1.0421).

3. In the "Select analytical program" window, select matrix and subprogram.
Because ST52.0S (1.0421) is an iron alloy, select the "FE" matrix and confirm
the selection with "OK".
4. Position the sample and start analysis by clicking "Start" or pressing the green
start button on the front of the housing.
• The result is displayed in the first free column on the left of the window.
5. Click "Mode" to open the "Readout mode / settings grade identification" window.
6. To perform the comparison,
• select "Percent analysis" mode;
• select the Fe_GRADE file from the "Grade file" dropdown list,
• select a set grade from the dropdown list, in this example that is ST52.0S
(1.0421).
7. Open the "Grade options" window, select the required options and confirm with
"OK".
8. Exit the "Readout mode / settings grade identification" window clicking
"Compare grade".
• The comparison is performed and the result displayed in the analysis
window.
Fig. 8-56 Result of the comparison
Note! • A red background of the result of the comparison indicates a considerable

deviation.
• Deviations are calculated related to the average value.

9. After the grade comparison is completed, you can display all modes. For that,
click the "Mode" button again and select a mode. Confirm your selection with
"OK".
• The result of the mode is displayed.
To analyse further samples in grade mode, select "New" and enter the name of a new
sample using the virtual keyboard and confirm the input window for the report file.

8.9 Creating a pseudo element
This chapter contains a description of the entry of individual pseudo elements.

In total, up to ten pseudo elements can be created which are to be defined by any
formula each.
The procedure for creating a calculation formula is the same for all programs.
The following description indicates an example of a formula common for the calculation
of the CE value (carbon equivalent) in steel applications.

2. Open the "Utilities" menu and in that menu open the "Create/change alloy" item.
3. In the following window, select the analysis program, in this example FE_300 —
Cr, Cr/Ni, Ni steel. Confirm your selection with "OK".
Fig. 8-57 Selection of the analysis program
4. In the next window, the "Change alloy" window, double-click the "Calculation
file" box.
• The virtual keyboard opens.
5. Enter a file name and confirm with "OK".
• The name is displayed in the "Calculation file" box and the "Edit" button is
enabled.
Fig. 8-58 "Calculation file" input

6. Click "Edit" to create the calculation formula.

• The "Calculation file" window is displayed.
Note! In this menu, you can enter up to 10 different pseudo elements. All defined pseudo
elements are automatically displayed in the analysis screen.
Fig. 8-59 "Calculation file" window
Table 8-15 Elements in the "Calculation file" window

1 Calculation Input box for the calculation formula; the virtual keyboard opens by
double-clicking the box.
2 Digits Input box for the number of decimals to be displayed; double-clicking
the box opens the virtual numeric keypad.
3 Manual element # input box for additional elements determined in other measuring
methods and to be included into calculation
4 Digits input box for decimal places for the corresponding element

7. Enter the calculation formula for the pseudo element in the first "Calculation"
input box and confirm with "OK".
For example, for CE (carbon equivalent) with the following formula:
CE = C + (Mn+Si)/6 + (Cr+Mo+V)/5 + (Ni+Cu)/15
Note! Notation of the formula must be adapted to the software. The software identifies the
individual concentrations of each element by means of the preceding percent sign. That
term must be put in brackets additionally.
The above example looks as follows for the formula to be entered:
CE=(%C)+((%MN)+(%SI))/6+((%CR)+(%MO)+(%V))/5+((%NI)+(%CU))/15
Fig. 8-60 Entered calculation formula
8. Close the "Calculation file" window by clicking "OK".

9. Close the "Change alloy" window by clicking "OK".
10. Return to the start screen and click "Analysis".
11. In the "Select analysis program" window, click "FE" and subprogram "FE_300".
Confirm your selection with "OK".
• Pseudo element CE (1, fig. 8-61) is now automatically displayed in the
analysis screen.
Fig. 8-61 "Analysis" window with pseudo element CE (section)

After you have performed three sparkings, the pseudo element is automatically
calculated (fig. 8-62).
Fig. 8-62 Calculated pseudo element
Note! The displayed CE value would be too high for practical purposes. This example shall just
serve to illustrate the entry of complex formulas.
(CE values are mainly calculated for C steels. Typical values are <0.5.)

8.10 Setting up a report file
The WASLab software provides a report file with an individual layout.

That layout can be adapted to company-specific requirements.
Note! The designation of the provided report file is WASDEMO.rep. The file is in the "Master"
directory. Create a copy of the report file before changing it!
To set up a report file, proceed as follows:

2. Open the "Utilities" menu and in that menu open the "Create/change alloy" item.
3. In the next window, select the analytical program for which you want to set up a
report file. Confirm your selection with "OK".
4. In the next window, the "Change alloy" window, double-click the "Report file"
box.
• The virtual keyboard opens.
5. Enter a file name and confirm with "OK".
• The name is displayed in the "Report file" box and the "Edit" button is
enabled.
Fig. 8-63 "Report file" input
6. Click "Edit" to create the report file.

• The "Report file" window is displayed.
In the "Report file" window, you can set the following:

• the logo in the report
• the header of the report
• the queries
• the layout of analysis data
• and the footer of the report.
You can also show a report preview and print the report. The individual settings are
described in the following chapters.
Note! All position data (XY-coordinates) are freely selectable and relate to an A4 sheet. The
X-position defines the left edge distance, while the Y-position defines the top edge
distance of the object, both in millimetres.

8.10.1 Editing the logo
A logo of your choice in bmp file format (bitmap) can be inserted in the report.
1 2 3
Fig. 8-64 "Report file" window — logo
Table 8-16 Elements in the "Report file" window — logo

1 Xpos Defines the left edge distance in mm.
2 Ypos Defines the top edge distance in mm.
3 Logo Opens a WINDOWS™ window to select the bitmap file.
8.10.2 Editing the report header
1 2 3 4
Fig. 8-65 "Report file" window — head
Table 8-17 Elements in the "Report file" window — head

3 Font Opens a WINDOWS™ window to select the font.
4 input box for the head By double-clicking the text box, a window to edit the head opens.
There are ten editable lines provided for the design of the report
header.

8.10.3 Editing the queries for the output log
Additional information, such as the number of the sample, the number of the melt, the
customer name, etc., can be input into the queries window.
The respective data are queried by the user prior to the start of an analysis, provided
that a report file had been assigned to the analytical program.
1 2
Fig. 8-66 "Report file" window — queries
Table 8-18 Elements in the "Report file" window — queries

2 input box for queries By double-clicking the text box, a window to edit the queries opens. There are 20 text lines
provided to enter questions, see fig. 8-67.
Click one of the white text boxes to edit or change data.
1 2
Fig. 8-67 "Edit questions" window
Table 8-19 Columns in the "Edit questions" window
Column Function
Question Click the respective line to enter text.
Type Further options are displayed if you repeatedly double-click the box:
Normal The entry is printed as entered.
Time The time is added to the entry (Windows™ default time).
Date The date is added to the entry (Windows™ default date).
Grade Grade data are taken from the enabled analysis/sorting program.
Program The designation of the enabled analysis/sorting program is entered here.
QX Defines the X-position of the question.
QY Defines the Y-position of the question.
AX Defines the X-position of the answer.
AY Defines the Y-position of the answer.

8.10.4 Editing the output of the analysis result
1 2 3 4 5 6 7 8 9 10 11
Fig. 8-68 "Report file" window — analysis
Table 8-20 Elements in the "Report file" window — analysis

3 Print single analyses one analysis per printed page
4 Print grade limits The entered lower and upper limits for element concentrations are printed.
5 Print average The average values are printed in the report.
7 Elements per line specification of the number of elements in a line of the output
8 Element width specification of the width of element representation
9 Analyses/page number of analysis results printed per page
10 Next to value position of the element designation (abbreviation)
11 Above value position of the element designation (abbreviation)

8.10.5 Editing the report footer
1 2 3 4
Fig. 8-69 "Report file" window — foot
Table 8-21 Elements in the "Report file" window — foot

4 input box for the head By double-clicking the text box, a window to edit the foot opens. There
are ten editable lines provided for the design of the report footer.

8.10.6 Checking the report parameters
Fig. 8-70 "Report file" window — buttons
• To print the report file, click "Print". The file is printed on the WINDOWS™
default printer.
• Click "Preview" to check if all entries and changes have been taken over.
The preview window of the report file is displayed.
Fig. 8-71 Preview window (example)
Note! All boxes in fig. 8-71 marked "########" are wildcards for answers. Those are entered
by the user (in analysis mode of the instrument).
The above illustrated results only serve as an example.
When you are satisfied with the preview, close the window and accept the changes in
the "Report file" clicking "OK".
The "Change alloy" window is displayed again.

8.10.7 Saving and printing the report file
Prerequisites The WASLab software has been started and you have selected an analysis program.
To print a report file, proceed as follows:
1. Open the "Readout mode / settings grade identification" window clicking the
"Mode (F7)" button in the "Analysis" window (see chapter 8.4.4, page 52).
2. Open the "Print/store options" window by clicking the respective button (1, fig. 8-
72).
1
2
Fig. 8-73 "Print/store options" window
3. Select a report file (1, fig. 8-73) and the corresponding program (2).
Note! Information about the other settings is provided in chapter 8.3.4, page 48.

4. Confirm the settings by clicking "OK".

5. Close the "Readout mode / settings grade identification" window clicking "OK".
The "Analysis" window is displayed again.
6. Click "New" to start analysis.
Since a report file is now assigned to the selected analytical program, the
"Dialog" window is opened first.
Note! The number of questions in the "Dialog" window depends on your entries in the "Edit
questions" window, see chapter 8.10.3, page 85.
7. Enter the data and confirm the entries with "OK" to start analysis.
Note! If you do not enter any data and click "Cancel", the performed analysis can be printed,
but the text boxes remain empty.
8. Start analysis by clicking "Start".

9. Perform the required number of sparkings.
10. To print the analysis result, click the "Print" button in the analysis window.
F4
Fig. 8-75 "Print (F4)" function button
The report file is printed with the previously defined settings on the installed printer.

9 Removal from service FOUNDRY-MASTER Xline
9 Removal from service
Proceed as follows to remove the instrument from service:
1. Switch off the excitation source at the rotary knob on the front.
2. Terminate the WASLab software (Alt+Q) and switch off the PC.
3. Switch off the instrument at the on/off switch on the rear.
4. Shut off argon supply at the pressure regulating valve of the bottle.
5. Close the ball valve between vacuum pump and vacuum tank and switch off the
vacuum pump to rule out the risk of a back-diffusion of the pump's oil vapours.

10 Maintenance FOUNDRY-MASTER Xline
10 Maintenance
10.1 Safety instructions for maintenance and repair
Maintenance and repair may only be carried out by qualified specialised personnel.
Switching off the Prior to beginning maintenance or repair work, switch off the instrument:
instrument • Switch off the excitation source at the rotary knob.
• Terminate the WASLab software.
• Switch off the instrument at the on/off switch on the rear.
• Secure the instrument against restart and attach a warning "Caution —
Maintenance!".
Warning!
There is a crush hazard when closing the holding clamps on the flap of the spark stand.
Close the holding clamps from above.
Since the software is subject to continuous further development, Oxford Instruments

Analytical GmbH recommends regular maintenance. This is to ensure the use of the
respective current version for the device and to allow the customer to benefit from the
enhanced scope of functions.

FOUNDRY-MASTER Xline 10 Maintenance
10.2 Maintenance table
In the following table,
the abbreviation means that the maintenance activity must be

performed
OH .............................................after x operating hours
m ...............................................after x months
y.................................................after x years
.
Table 10-1 Maintenance intervals FOUNDRY-MASTER Xline
Maintenance interval
Assembly Maintenance activity Further information
m y OH
entire instrument replacement of all loaded parts and analytical
1 to be performed by customer service
check of the instrument
check of filters and replacement, if required 3 chapter 10.7, page 108
cleaning of instrument 1 chapter 10.9, page 109
when dirty or filled to a low

Clean and fill wash bottle chapter 10.8, page 106
level
Replace argon bottle as necessary chapter 10.9, page 107
Optics
cleaning of window (optical fibre) after 3,000 measurements
chapter 10.4, page 98
replacement of window (optical fibre) after 9,000 measurements
cleaning of window (direct light path) after 3,000 measurements chapter 10.5.1, page 100
replacement of window (direct light path) after 9,000 measurements chapter 10.5.2, page 102
spark stand
replacement of electrode at every change of matrix chapter 10.6.1, page 103
after every change of

adjustment of the electrode chapter 10.6.2, page 105
electrode
after every measurement and
cleaning of electrode with brush at every change of the chapter 10.6.3, page 106
sample
after 300 sparkings each and
cleaning of spark stand chapter 10.3, page 97
at message
vacuum pump Information about the tasks is
check of oil level 1
provided in the operating
instructions of the vacuum pump
oil change 3000
check and cleaning of inlet filter 1
check and cleaning of gas ballast control 1
cleaning of oil inspection glass 1
cleaning of fan cover and housing 1
cleaning and overhaul of pump 15,000
installation of new slides 30,000
check of motor condition 15,000

10.3 Disassembling and cleaning the spark stand
When the spark stand must be cleaned, the following message is displayed on the
screen:
Fig. 10-1 Reminder to clean the spark stand
Note! We recommend the immediate cleaning of the spark stand when this message is
displayed.
You could skip the message clicking "Remind later", however, that is not recommended.
The cleaning interval can be set in the "Options" window (chapter 8.2.2, page 39).
Proceed as follows:
1. Switch off the instrument as described in chapter 10.1, page 93.

Opening the spark 2. Loosen the 4 holding clamps (1, fig. 10-2) on the spark stand plate (2).
stand
3. Lift the front of the spark stand plate about 45° and take it out toward the front.
Fig. 10-2 Opening the spark stand plate
Note! Make sure not to brush the dust against the window in front of the optical fibre.
Cleaning the spark 4. Brush the condensate off the surface below the spark stand plate and around
stand the electrode using the brush from the accessory case.
Warning!
There is a crush hazard when closing the holding clamps on the spark stand plate.
5. Replace the spark stand plate on the spark stand and close the holding clamps.

10.4 Cleaning the window (optical fibre)
In case of an indirect light path, there is a small window (1, fig. 10-3) in front of the optical
fibre held by a sleeve.
Fig. 10-3 Window in front of the optical fibre
Since contamination results from sparking the samples, that window must be cleaned at
certain intervals.
Remove the window for cleaning or replacement according to the intervals in the
maintenance table. If low-melting grades, such as Zn grades, are to be measured, the
intervals for cleaning and replacing the window should be shortened.
To remove the window, proceed as follows:

stand 3. Lift the front of the spark stand plate about 45° and take it out toward the front.
Fig. 10-4 Opening the spark stand

4. Use the supplied installation aid FOC window to carefully screw off the sleeve
with the window and remove the sleeve from the spark stand.
Fig. 10-5 Screwing out the sleeve
Note! When removing the window with the tweezers, make sure you do not scratch the
window!
5. Unscrew the brass nut (3) from the sleeve (1) using the hex section of the
installation aid FOC window (4, fig. 10-6) and remove the window (2).
2
3
Fig. 10-6 Sleeve with window, brass nut and installation aid FOC window
6. Clean the window with a soft, acetone-soaked cloth.

7. After cleaning the window, re-assemble all parts.
8. Screw the sleeve back on to the optical fibre using the installation aid FOC
window. Only fasten the sleeve hand-tight.
Warning!

10.5 Cleaning and replacing the window (direct light path)
10.5.1 Cleaning the window
Proceed as follows to clean the window (direct light path):

2. Loosen the screws (1, fig. 10-7) on the maintenance cover.
3. Remove the maintenance cover and place it next to the housing.
Note! The cover is connected to an earth cable. The earth cable must not be disconnected!
Fig. 10-7 Opening the cover
4. Shut the ball valve (1, fig. 10-8) so that it is positioned crosswise to the light
path.
Note! When opening the union nut, make sure the optical fibre is not damaged!
5. Loosen the union nut (2, fig. 10-8) and open it.
Fig. 10-8 Shutting the ball valve

6. Remove the window brackets (1, fig. 10-9).
Fig. 10-9 Removing window brackets
7. Loosen the screwing (1, fig. 10-10) with a screwdriver and remove O-rings (2)
and window (3). If required, press the window from the rear with a clean, soft
object.
Fig. 10-10 Removing the window from the window brackets
Note! Observe the safety regulations for handling acetone!
8. Clean the window with a soft, acetone-soaked cloth.

9. Reinsert the window and the O-rings. The O-rings must be correctly placed in
the grooves. They must be clean and intact.
10. Fasten the screwing hand-tight using the screwdriver.

11. Reinsert the window brackets into the light path.
Fig. 10-11 Inserting the window brackets into the light path
12. Retighten the union nut finger-tightly.
Note! When opening the ball valve, the spark stand opening must be open. When the opening
is covered and the window is not tightly installed, there is a risk that water is sucked from
the washing bottle into the spark stand.
When opening the ball valve, pay attention to any unusual noise.
13. Open the ball valve.

14. Replace the maintenance cover and screw it back on to the housing.
Note! When placing a sample, observe the exhaust hose and washing bottles. Immediately
remove the sample if water is drawn in.
Activate argon purging for about 5 minutes.
10.5.2 Replacing the window
To replace the window, proceed as described in chapter 10.5.1, page 98.

Replace the window instead of cleaning it.

10.6 Maintenance of the electrode
10.6.1 Replacing the electrode
When you change the matrix (e.g. from iron to aluminium), electrode and brush should
be replaced. Otherwise, analysis can be adulterated by contamination of the electrode
or brush.
There are a separate electrode and brush for every matrix.
To replace the electrode, proceed as follows:

2. Screw out the spacer (1, fig. 10-12) on the right side of the spark stand.
3. Loosen the inner grub screw (2) on the electrode clamp using a 2 mm Allen key
(3).
The electrode (4) is pushed out of the spark stand toward the top by a spring.
Fig. 10-12 Screwing out the spacer
4. Completely remove the electrode and replace it with a new one.

5. Insert the new electrode from above.

6. Completely press down the electrode with the head (1, fig. 10-13) of the spacer
to adjust the correct distance to the sample. Simultaneously fasten the grub
screw to the electrode clamp.
Fig. 10-13 Installing the electrode
7. Screw the spacer back into the side of the spark stand finger-tightly.

10.6.2 Adjusting the electrode
The spacing between electrode and sample is adjusted on the side of the spark stand
using the spacer. Proceed as follows:

2. Screw out the spacer (1, fig. 10-14) on the right side of the spark stand.
3. Loosen the inner grub screw (2) on the electrode clamp using a 2 mm Allen key
(3).
The electrode (4) is pushed out of the spark stand toward the top by a spring.
Fig. 10-14 Screwing out the spacer
4. Completely press down the electrode with the head (1, fig. 10-15) of the spacer
to adjust the correct distance to the sample. Simultaneously fasten the grub
screw to the electrode clamp again.
Fig. 10-15 Installing the electrode
5. Screw the spacer back into the side of the spark stand finger-tightly.

10.6.3 Cleaning the electrode with the electrode brush
Note! Too much combustion residue on the electrode can result in a short circuit between
electrode tip and sample.
The short circuit is detected by the instrument and indicated with an error message.
Strongly varying measurements can also indicate that there is too much combustion
residue on the electrode.
Therefore, the electrode must be regularly cleaned with an electrode brush or, in the
event of persistent contamination, with the file brush (chapter 10.6.4, page 105).
To clean the electrode using the electrode brush (brass handle), proceed as follows:
1. Switch off the excitation source at the rotary knob on the front of the instrument.
2. Brush the tungsten electrode through the hole (1, fig. 10-16) in the spark stand
plate using the electrode brush from the accessory case.
3. Switch the excitation source back on.
Fig. 10-16 Spark stand

10.6.4 Cleaning the electrode with the file brush
In the event of persistent contamination of the electrode, you must clean the electrode
using the file brush.
To clean the electrode using the file brush, proceed as follows:

stand
3. Lift the front of the spark stand plate about 45° and take it out toward the front.
Fig. 10-17 Opening the spark stand
4. Clean the tungsten electrode (3) using the file brush from the accessory case.
Warning!

10.7 Replacing filters
Check the filter mats in the fan and in the outlet filter on the rear of the housing for
contamination. Replace the filter mats if required.
10.8 Cleaning and filling the wash bottle
The washing bottle filled with tap water serves to collect the off-gases from sparking so
that they are not released into the air.
From time to time, check the wash bottle is correctly filled. Clean and fill it if the fill level
is not correct or cannot be easily seen.
1 3
2
4
max. 60 mm
min. 40 mm
Fig. 10-18 Wash bottles
Note! The empty bottle (1, fig. 10-18) prevents water being sucked into the exhaust hose. For
that reason, no water should be filled into the empty bottle (1)!
To clean and fill the wash bottle (3), proceed as follows:

• Unscrew the lid of the wash bottle.
• Empty the wash bottle.
• Rinse any dirt out with tap water.
• Fill up the wash bottle with tap water.
• The wash bottle's tube (4) must be below the water level.
• The fill level in the wash bottle must not exceed 60 mm high and should be
at least 40 mm high.
• Screw the lid back onto the wash bottle. Make sure that the lid is well positioned.

10.9 Replacing the argon bottle(s)
When replacing the Ar bottle(s), air might enter part of the Ar supply segment.
There are three possible ways to then remove it from the system again:
• One possibility is to purge the Ar system after replacement. For that, activate purging
under "Mode", "Argon purging". That method is quite time-consuming, since it may
take several hours until the supply lines have been purged sufficiently so as to
ensure the analysis is not affected any more.
• A more effective, but also more expensive possibility is the use of purchasable
fittings, with a purging device on the delivery side. That is the safest method.
• As a third possibility, the following procedure can be performed:
1. Regulate the control valve from 3 bar to 0. By that, the section from the pressure
regulator / manometer to the spectrometer is isolated.
2. Close the bottle valve.
3. Screw the pressure regulator / manometer off the bottle.
4. Replace the bottle.
5. Screw the pressure regulator / manometer on to the new bottle using a new
seal.
6. Open the bottle valve and immediately close it. The primary manometer should
now indicate the bottle pressure (usually 200 bar).
7. Loosen the union nut to the extent that the pressure between bottle and
pressure regulator / manometer can drop to 0.
8. Repeat steps 6 and 7 four to five times.
9. Adjust the control valve to 3 bar.
10. Let purging go on for about 2 min.
10.10 Cleaning the instrument
Use a soft, dry or slightly damp cloth to clean the spectrometer on the outside. DO NOT
use any solvents!
No water may penetrate into the instrument!

11 Faults FOUNDRY-MASTER Xline
11 Faults
11.1 Information regarding WINDOWS™ installation
WINDOWS™ CD-ROM WINDOWS™ CD data are provided on the hard disk in the C:\Windows directory
Installing the printer Printer drivers are provided on the WINDOWS™ CD-ROM as well as on the CD-ROM
of the printer. You can also download current printer drivers from the Internet.
11.2 General faults
You can recognise any instrument faults e.g. from error messages displayed on the
screen. Try to remedy the error using the following table and the indications in the
"WASLab software" chapter (chapter 8, page 35ff.).
Should you have any problems remedying the error, feel free to contact our customer
service for support.
Our contact data are provided under "Service" (chapter 14.1, page 129).

FOUNDRY-MASTER Xline 11 Faults
11.3 Faults of FOUNDRY-MASTER Xline
Table 11-1 Possible faults and remedies (FOUNDRY-MASTER Xline)
Fault Information Remedy/explanation

no communication between PC and Error message: Follow the instructions in the error message.
instrument No spectrometer connected! Possible reasons: ...
Measurement cannot be started. Red bar at the bottom of the analysis window of
the instrument:
1. Switch on the excitation source on the
1. No source instrument.
2. No sample 2. Place the hold-down device prior to
3. No argon D measurement.
3. Is argon pressure 3 bar?
Instrument cannot be switched on. no visible reaction at the instrument 1. Mains voltage? yes/no
2. Check fuses at the power input.
measurements extremely loud loud measurement 1. Position the sample correctly.
2. Connect the off-gas hose to the washing
bottle.
3. Check the water level in the washing
bottle.
Intensity in the direct light path Error message: 1. Clean window.
decreases or has completely ceased. Reference limits exceeded. 2. Is the ball valve possibly closed?
3. Was the wrong analysis program
selected?
4. Poor burn spot?
Intensity in the indirect light path Error message: 1. Clean window.
decreases or has completely ceased. Reference limits exceeded. 2. Was the wrong analysis program
selected?
3. Poor burn spot?
Measuring results deviate from usual (See fault) 1. Check the electrode spacing and
values, precision decreases, spark- readjust, if required.
overs in the spark stand. 2. Clean the spark stand.
Message: Message: Wrong analysis program selected — start in
e.g. Cr > 6 % Admissible calibration range exceeded. orientation program.
Message: Message: The content of the corresponding element in
e.g. C < 0.001 Detection limits fallen below of. the measured sample is too low.
Note! If none of the above named faults can be identified or the fault cannot be remedied
applying the methods indicated under "Remedy", please contact the service (see

12 Reshipment and disposal FOUNDRY-MASTER Xline
12 Reshipment and disposal
12.1 Declaration of Decontamination
Due to legal regulations and to ensure safety of our employees, Oxford Instruments
Analytical GmbH requires a signed Declaration of Decontamination prior to processing
your reshipment.
Enclose this form signed with the shipping documents and attach it on the outside of the
packaging. Reshipments that have been exposed to hazardous substances and which
have not been decontaminated according to good professional practice, are not
processed and returned at your expense.
Note! The instrument must not be shipped without the transport lock installed. Previous to that,
contact our customer service.
The Declaration of Decontamination as well as the contact information are provided in

the Annex.
12.2 Disposal
The PC includes a battery containing contaminants. That must not be disposed of with
the domestic waste.
After the life has expired, disposal may only be executed through the customer service
of Oxford Instruments Analytical GmbH or a suitable collection point.
The operating company is obliged to dispose of the instrument after the completion of
its use at his/her own expense according to the legal requirements and to exempt us
from the take-back obligation and related claims of third parties.
Disassemble the instrument for disposal into the individual material groups:
• plastics
• non-ferrous metals (e.g. copper scrap)
• aluminium
• electronic scrap
• steel.
Dispose of the materials according to national legislation!

13 Reference FOUNDRY-MASTER Xline
13 Reference
13.1 Information regarding reliability of analyses
Reliability of the analysis directly depends on the quality of sample preparation.

How precise a spectrometer measures can be determined by means of comparison with
certified reference material (CRM) whose precise composition is known. Two statistic
relations are to be accurately distinguished:
1. The precision of measurements.

This serves to determine the standard deviation in a series of consecutive
measurements of the same sample. If it is related to the average value, the
relative standard deviation results.
2. The accuracy of measurements.
It serves to determine whether the average value related to the stated contents
is correct.
Generally, measurements with a functioning spark spectrometer are very precise.

However, that does not mean that the analysis is at the same time accurate.
Spectrometry is a comparative process, which means that the composition of an
unknown sample is determined through comparison with data of known samples. If any
errors occur in this comparison ("systematic errors"), the instrument precisely applies
those deviations to the sample.
The certificate of analysis supplied with every certified sample indicates the element
concentrations incl. the deviation (standard deviation) between the analyses of different
laboratories.
For certification, the samples of up to 15 renowned, certified national and international

laboratories are analysed. Every laboratory uses its best available analysis options (e.g.
wet chemistry, combustion, XRF, AES-ICP and spark atomic emission spectrometers).
The standard deviation resulting from the comparison of those analyses (1 sigma) does
not correspond to the standard deviations of the individual analytical measuring
instruments, but is the standard deviation of the average values from the individual
laboratories.
The average value of all measurements from the individual laboratories is considered
as the best approximation to the "real" content of an element in the sample and used as
the set value for calibration. So when CRM samples are used for calibration, despite all
care, there is always a certain deviation of the set values from the actual values
calculated from the calibration curves.
That means, there is a systematic deviation between the analysis of the spectrometer
and the certified value.

FOUNDRY-MASTER Xline 13 Reference
However, given today's state of analysis technology, those deviations are small and
allow a simplified procedure to determine whether a spectrometer measures sufficiently
accurately:
To estimate the deviation to expect in the analysis value from the standard deviation
of an element indicated in the certificate using an optical emission spectrometer,
according to experience, the value given in the certificate can be multiplied by 3
(regarding statistics: approx. 99.7 % of the values are in a 3-sigma interval). That is
to ensure that the range of all laboratory average values is covered and outliers are
not considered.
Example Indication in the certificate: average value 1.082 %, standard deviation 0.008 % of
the laboratory mean values.
==> The concentration indicated as the average value of at least 3 valid
measurements with an optical emission spectrometer should be in the range from
1.082 % - 0.024 % = 1.058 % to 1.082 % + 0.024 % = 1.106 %.
Note! The calibration of the spectrometer can be optimised for the customer application by
including customer-specific reference samples regarding their accuracy. In contrast,
CRM materials synthetic alloys and are designed to cover a large range of contents with
as few samples as possible.

13.2 Information about setting analysis parameters
This chapter contains information about editing analysis parameters.
Note! Prior to setting parameters, observe the following:

• Information in this chapter only serves as a reference. Contact the Oxford
customer service before changing settings in the program.
• The functions described in this chapter allow to change important data and
settings. Only do that if you are accordingly authorised and have sufficient
experience with the instrument.
• Every change to that respect influences the analytical performance of the
instrument and can cause inaccurate results or damage the instrument.
• Subprograms of the matrices can have different parameter settings. All changes
to active programs are only valid for those programs. Other subprograms
remain unchanged.
• Settings confirmed with "OK" are saved and are available when restarting a
subprogram. Every change of the excitation parameters requires a complete
recalibration of the spectrometer!
• Oxford Instruments Analytical GmbH cannot be held liable for malfunctions or
damage resulting from changes to or interference with hardware and/or
software by authorised or unauthorised persons.
To set analysis parameters, click the "Change" button in the analysis window or press
the F9 key (1, fig. 13-1).
Fig. 13-1 "Change (F9)" function button

The "Change alloy" window opens.
Note! If no keyboard is connected to the PC, the "Edit" button is enabled by double-clicking the
respective box.
Click the "Edit" button next to the input box to open the respective window.
1
2
3 9
4
5
6 10
7
The following options are available:
Table 13-1 Elements in the "Change alloy" window

1 Description name of the enabled program
2 Matrix element selection of individual element lines for a matrix
3 Parameter file setting of software-controlled excitation parameters (chapter 13.2.1, page 117)
4 References file assignment of specific references to element lines (chapter 13.2.2, page 118)
5 Format file change of screen display and print settings (chapter 13.2.3, page 119)
6 Curve file change of calibration curves of individual lines (chapter 13.2.4, page 120)
7 Alloy selection automatic change from the global program to a suitable subprogram within a matrix
(chapter 13.2.5, page 121)
8 Control standard file Enter the parameters for an individual control sample (chapter 13.2.6, page 122).
9 Standards Define values for the proportion of the individual elements (chapter 13.2.7, page 123).
10 Edit recal Access to recalibration data.

13.2.1 Parameter file
Note! All excitation parameters are preset and should only be changed by an Oxford service
technician!
1 5
6
4 7
Fig. 13-3 "Parameter file" window — settings
The following settings can be made:
Table 13-2 Elements in the "Parameter file" window

1 Argon saver When argon saver is activated, argon continues to flow after the measurement. This is
recommended when multiple measurements are carried out successively.
When argon saver is deactivated, the argon flow is stopped directly after measurement.
2 Wire analysis number of sparkings for wire analysis
3 Preburn Settings of time period and frequency to remelt the sample surface prior to the actual
measurement; the pre-sparking time should not exceed 30 seconds to avoid excessive
heating of the sample.
4 Profiling Opens a window to specify the duration and number of repeat adjustments of the optical
system to environmental conditions, such as temperature or air pressure:.
5 Purging Setting the purging period.
In the example, the purging period is 2 seconds prior to starting sparking. That period can
be edited by double-clicking the box and entering a new value.
6 Total profiling time Displays the complete profiling time (automatically calculated)
7 Profiling time Specifies when the profiling is carried out.
8 Expose Opens the window to change the measurement parameters.

13.2.2 References file
In the "Edit references" window, assign the reference lines to the analytical lines.
Note! If another reference is assigned to an analytical line, this can have a serious impact on
the analysis result!
Any change should only be made by our local Oxford partner or using their written
instructions.
Fig. 13-4 "Edit references" window
Note! Reference monitoring:

One reference should always be monitored to be able to detect faulty measurements
and contaminations of the window. Usually, one reference and one threshold value are
input. A "Reference outside tolerance" warning is displayed when the value is reached.
The reasons for such warning can be:
• wrong matrix (e.g. Ni sample measured in the Fe program)
• poor burn spot (too low luminous efficacy)
• window dirty.

13.2.3 Format file
In the "Format" window, you define how the analysis result is to be represented on the
screen and on the printout for the individual elements.
1
2
Fig. 13-5 "Format" window
Table 13-3 Elements in the "Format" window

1 Default values Resets all values to the default values.
2 Add Adds further chemical elements.
3 Delete Deletes individual elements from the list. The elements can be
inserted at another point in the list.
By double-clicking the respective input box, a window and the virtual numeric keypad
open by means of which you can change the value.
Fig. 13-6 Input window and virtual numeric keypad

13.2.4 Curve file
In the "Curves" window, you can change the calibration curves for individual element
lines.
Note! Any change to curve data can fundamentally impact the analytical performance of the
spectrometer!
Any change should only be made by our local Oxford partner or using their written
instructions.
Fig. 13-7 "Curves" window
Table 13-4 Elements in the "Curves" window

1 Spark recalibration sample Resets all values to the default values.
2 Edit curves Selection of the element whose curve you want to edit.
After the selection, the curve window opens.
3 Delete curves Deletes the calibration curves of individual element lines.
4 Print all curves Prints all curves or inter-element correction curves.
open by means of which you can change the limit values.
Fig. 13-8 Input window and virtual numeric keypad

13.2.5 Alloy selection
In the "Alloy selection" window, you define the lower and upper limits for the
percentaged concentration of the individual elements for a selected subprogram.
Fig. 13-9 "Alloy selection" window
Table 13-5 Elements in the "Alloy selection" window

1 Add selection Opens a window where you can input a new program.
2 "alloy selection" picklist Selection of the subprogram whose elements you want to edit.
The elements and values of the subprogram are displayed in
the list.
3 Arrow keys Shifts the selected subprogram in the list.
open by means of which you can change the limit values.

13.2.6 Control standard file
In the "Control standard file" window, you define the parameters for an individual control
sample and specify the lower and upper limits for the proportion of individual elements.
1
2
3
4 6
Fig. 13-10 "Alloy selection" window (Control standard file)
Table 13-6 Elements in the "Alloy selection" window (Control standard file)

1 Save as Specifies the file path where the measurement is saved.
2 Store single burns Saves each single burn separately during a check
measurement.
3 Store element limits Saves the limit value for elements during a check
measurement.
4 Add standard Opens a window where you can specify a name for your own
check measurement.
5 Delete standard Deletes the selected check measurement from the list.
6 Lower and upper limits Input boxes for the lower and upper limits of the individual
elements of your check measurement.
Double clicking in the corresponding input box opens a virtual keyboard or the virtual
numeric keypad so that you can edit the values.

13.2.7 Standards
In the "Standards" window, you define the percentaged concentration of the individual
elements of a selected recalibration sample.
2 3
Fig. 13-11 "Standards" window
Table 13-7 Elements in the "Standards" window

1 Standard selection of a recalibration sample
2 Make input box for the manufacturer of the recalibration sample
3 picklist Selection of the element whose curve you want to edit. After
the selection, the curve window opens.

13.3 Service menu
By clicking "Service" in the "Utilities" menu, a submenu with the following options opens:
• Create diagnostic data
• CCD scan
• Test controls
Create diagnostic data By clicking "Create diagnostic data", a confirmation window opens:
Fig. 13-12 "Create diagnostic data" query
By clicking "No", the query is closed and the "Utilities" menu is displayed again.
1. Confirm the query with "Yes".

• The "Dialog" window and another query as to whether the spectrometer shall
perform test measurements opens:
Fig. 13-13 2. Prompt for "Create diagnostic data"
By clicking "No", the query is closed and the "Dialog" window to create data is displayed
(fig. 13-15, page 13-125).
2. If test measurements shall be performed by the spectrometer, confirm this query

by clicking "Yes". -> An analysis window opens.
Fig. 13-14 Analysis window for "Create diagnostic data"
3. Perform measurement at least 3 times.

4. Then click "Next" to spark another sample or "Exit" to complete measurement.

Note! Detailed information on the performance of an analysis is provided in chapter 8.5,

page 60.
• The "Dialog" window is displayed.
Fig. 13-15 "Dialog" window for "Create diagnostic data"
5. In the "Dialog" window, click the "Create diagnosis" button to create the
diagnosis files.
• The diagnosis files are created and packed. A message with path and file
name of the packed file is displayed.
Fig. 13-16 Confirmation for the created diagnosis
6. Confirm the message with "OK" and send the created file to the indicated e-mail
address.

CCD scan By clicking "CCD scan" in the "Service" menu, the "Scan utility" program opens in a new
window:
Fig. 13-17 "Scan utility" window
The required support to operate the program is provided by our service team (see
Test controls Clicking "Test controls" in the "Service" menu opens the "Foundry Master controls"
program in a new window:
Fig. 13-18 „Foundry Master controls“ window
The required support to operate the program is provided by our service team (see

14 Annex FOUNDRY-MASTER Xline
14 Annex
This chapter contains

• service address
• glossary
• parts list for probe accessory case
• Declaration of Conformity

14.1 Service
If you need any help handling this product, please contact your service partner of Oxford
Instruments Analytical GmbH or call us at the Service Centre:
Oxford Instruments Analytical GmbH

Abt. Service
Wellesweg 31
47589 Uedem
Germany
Phone: +49 (0)2825 9383-303

Fax: +49 (0)2825 9383-100
E-mail: [email protected]

14.2 Glossary
AES Short for Atomic Emission Spectrometry:
Arc mode here: Using an arc probe or a combined probe with the arc adapter. The sparking occurs
in an air atmosphere without argon. Thus, the measurement is less precise but can be
carried out faster and is less complicated.
CCD Short for Charge Coupled Device.

CCDs are light-sensitive semiconductor chips used to measure the wavelength of a
source. In a spectrometer, the source is the plasma generated during sparking.
CE value Carbon equivalent value:
CRM Short for Certified Reference Material:

designation for samples whose precise composition is known. Used for spectrometer
recalibration.
DIA short for Dynamic Integration Algorithm.
Spark mode In spark mode, the sparking occurs in argon atmospheres in the spark adapter of the
combined probe or in the head of the UVPro probe and the spark probe.
ICP short for Inductively Coupled Plasma
PMI short for "Positive Material Identification"
plasma A plasma is a material state in which so far neutral atoms or molecules of the material
are split into their charged fragments (ions and electrons) at very high temperatures.
Those fragments emit rays of a specific wavelength. That wavelength is measured in the
spectrometer and assigned to the corresponding element in the software.
Recalibration periodic remeasuring of a measuring/test device (here spectrometer and recalibration

sample) to monitor its accuracy
standard deviation The standard deviation is a measure for the deviation of measured values around their
average value. A distinction is made between relative standard deviation (RSD) and
absolute standard deviation (SD).
white burn spot Poor burn spot with very low luminous efficacy. It results from contamination on the
sparked surface.
XRF short for X-ray fluorescence analysis

14.3 Standard accessory case, packed
Table 14-1 Standard accessory case, packed
Quan-
Part number Designation Unit
tity
0000000357 tool box with organiser, 16 in 1 pc.
0000000869 electrode cleaning brush 100 mm x 25 mm Spark 1 pc.
0000002103 assembly extraction tool ceramic insert 1 pc.
0000001468 tweezers 1 pc.
0000002209 FS FM cleaning brush; short brush, straight bristles 1 pc.
4000000218 installation aid window LWL (FOC) spark stand 1 pc.
0000001996 hexagon screwdriver with T-handle SW 2; 1 pc.
WIHA 334/SW2.0 x 100
0000001325 fuse 6.3 A, 20 mm T 10 pc.
0000000028 tungsten electrode 6.15 mm x 56 mm 5 pc.
0000002045 Swagelok union nut, 6 mm 2 pc.
0000002046 locking ring set (front + rear), 6 mm 3 pc.
0000001272 DIN913 M4x4 galvanised Allen set screw 5 pc.
0000000029 compression spring 0.50 x 5; 10 x 25.00 x 8.00; compression spring for 5 pc.
probe
0000000714 window quartz d = 5-0.1 mm; t = 1 mm 2 pc.
0000000543 window quartz d = 10.0-0.1 mm; t = 1 mm 2 pc.
4000000227 locking screw window brackets LWL (FOC) without seals 2 pc.
0000000521 O-ring 8x1 mm Viton/FKM Shore 80 DIN3771 10 pc.
0000000736 O-Ring 8x2 mm Viton Shore 80 5 pc.
0000000337 Allen key SW 2.5 x 100 1 pc.
7000000162 angle Allen key SW 2.0 mm 1 pc.
0000003102 Rittal spare filter mat for filter fan SK 3321 2 pc.
0000001809 FM/FMC/TMP spark ceramic insert 1 pc.
0000001807 FM spark stand plate version 2 1 pc.
0000003836 FM spacer with rubber seal 3.3 mm 1 pc.
0000003589 FM/FMC rubber bump stop h = 6 mm; d = 10 mm; M4x10 AG 3 pc.
GP-BA-010x006-M4x10 NR55 light grey (for spacer 3836)
0000000595 O-ring 18 x 1.5 mm Viton/FKM Shore 80 DIN3771 4 pc.
0000000596 O-ring 20 x 1 mm Viton Shore 80 1 pc.
0000000287 electrode cleaning brush round 20 pc.
0000002117 assembly FM/FMC insulation body, ver.5 1 pc.
0000002039 oil for rotary vane pump 1 litre DV 1 pc.
1200000017 activated aluminium oxide particle size 2-5 mm 1 pc.
4000000227 locking screw window brackets LWL (FOC) without seals 2 pc.
4000000226 window brackets LWL (FOC) FS without seals 1 pc.

14.4 Forms
14.4.1 Declaration of Conformity
14.4.2 Declaration of Decontamination

Declaration of Conformity (translation of the original)
Under the Low Voltage Directive 2006/95/EC, Annex III, Section B
We herewith declare that the instruments designated in the following comply with all regulations of Low Voltage
Directive 2006/95/EC.
Description of electrical FOUNDRY-MASTER Xline

equipment:
Year of construction: 2013
Relevant EC directives: Low Voltage Directive 2006/95/EC as of 12 December 2006

Directive 2004/108/EC on electromagnetic compatibility as of 15 December
2004
Applied harmonised EN 61326-1:2006 Electrical equipment for measurement, control and laboratory use — EMC
standards: requirements — Part 1: General requirements IEC 61326-1:2005
EN 55011:2009 Industrial, scientific and medical equipment — Radio-frequency disturbance

characteristics — Limits and methods of measurement CISPR 11:2009 (modified)
EN 61000-3-2:2006 Electromagnetic compatibility (EMC) — Part 3-2: Limits — Limits for harmonic
current emissions (equipment input current <= 16 A per phase)
IEC 61000-3-2:2005
EN 61000-3-3:2008 Electromagnetic compatibility (EMC) — Part 3-3: Limits — Limitation of
voltage changes, voltage fluctuations and flicker in public low-voltage supply systems, for
equipment with rated current <=16 A per phase and not subject to conditional connection IEC
61000-3-3:2008
Further applied technical Accident prevention regulation Elektromagnetische Felder BGV B11: 04/2002 (electromagnetic
standards and specifications: fields)
Manufacturer: Oxford Instruments Analytical GmbH

Wellesweg 31
DE-47589 Uedem
Name of authorised Oxford Instruments Analytical GmbH

representative of the Wellesweg 31
technical documentation: DE-47589 Uedem
Place, date Signature
Managing Director
Declaration of Decontamination
Dekontaminationserklärung
Because of legal regulations and for the safety of our employees Oxford Instruments Analytical GmbH needs a signed
“declaration of decontamination” before your return can be handled.
This signed declaration must be included with the shipping documents on the outside of the packaging. Any returns which were
exposed to hazardous substances and were not professionally decontaminated are not accepted and will be sent back on your
cost.
Aufgrund gesetzlicher Bestimmungen und um die Sicherheit unserer Mitarbeiter zu gewährleisten benötigt die Oxford
Instruments Analytical GmbH eine unterschriebene Dekontaminationserklärung, bevor Ihre Rücksendung bearbeitet werden
kann. Legen Sie dieses unterschriebene Formular den Versandpapieren bei und bringen Sie es außen an der Verpackung an.
Rücksendungen, welche gefährlichen Stoffen ausgesetzt waren und nicht fachgerecht dekontaminiert wurden, werden nicht
bearbeitet und auf Ihre Kosten zurückgeschickt.
Name / Name Address / Adresse
Serial number / Seriennummer
Order number / Auftragsnummer Phone / Telefon Email / E-Mail
Notes / Bemerkungen
1. Equipment has been in contact with hazardous substances.

Das Gerät ist mit gefährlichen Stoffen in Berührung gekommen.
No / Nein Yes / Ja = Please list the hazardous substances. / Bitte benennen Sie die gefährlichen Stoffe.
Substance / Stoff Danger Class / Gefahrenklasse Safety precautions / Sicherheitsvorkehrungen

1
2. Equipment has been decontaminated professionally. / Das Gerät wurde fachgerecht dekontaminiert.
No / Nein Yes / Ja = Cleaning agent / Reinigungsmittel:
-------------------------------------------------------------------------------------
3. Legally binding declaration / Rechtsverbindliche Erklärung

Herewith I confirm that the returned instruments were cleaned and decontaminated according to the industry standards and all
appropriate regulations. The instruments are free of hazardous substances.
Hiermit bestätige ich, dass die zurückgesendeten Geräte nach industriellen und gesetzlichen Bestimmungen gereinigt und
dekontaminiert sind. Die Geräte sind frei von gefährlichen Stoffen.
------------------------------------------ ---------------------------------------------------------------------------------------
Location / Ort Company stamp and legally binding signature
Firmenstempel und rechtsverbindliche Unterschrift
------------------------------------------ ---------------------------------------------------------------------------------------
Date / Datum Name of signatory in block letters
Name des Unterzeichnenden in Druckbuchstaben

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Translation of the Original Instructions

Oxford Instruments Analytical GmbH

Right to technical changes reserved.

© 2013 Oxford Instruments Analytical GmbH

To ensure smooth operation, we have drawn up these practical operating instructions.

These operating instructions are protected by copyright.

Uedem, November 2013

Version: 1.2GB/2013-11-25 © 2013 Oxford Instruments Analytical GmbH

1 Notes regarding the use of these operating instructions.................................................................... 1

2 Intended use and misuse ....................................................................................................................... 3

3 General safety instructions .................................................................................................................... 5

4 Description of the Instrument .............................................................................................................. 11

5 Scope of delivery, transport, set-up and installation......................................................................... 17

6 Putting into service ............................................................................................................................... 23

Version: 1.2GB/2013-11-25 -I- © 2013 Oxford Instruments Analytical GmbH

8 WASLab software .................................................................................................................................. 35

9 Removal from service ........................................................................................................................... 91

© 2013 Oxford Instruments Analytical GmbH - II - Version: 1.2GB/2013-11-25

11 Faults .................................................................................................................................................... 109

12 Reshipment and disposal ................................................................................................................... 111

13 Reference ............................................................................................................................................. 113

14 Annex ................................................................................................................................................... 127

Version: 1.2GB/2013-11-25 - III - © 2013 Oxford Instruments Analytical GmbH

4 Description of the Instrument

5 Scope of delivery, transport, set-up and installation

6 Putting into service

Version: 1.2GB/2013-11-25 -V- © 2013 Oxford Instruments Analytical GmbH

Fig. 8-34 "Analysis" window with indication of RSD .......................................................................... 58

© 2013 Oxford Instruments Analytical GmbH - VI - Version: 1.2GB/2013-11-25

Version: 1.2GB/2013-11-25 - VII - © 2013 Oxford Instruments Analytical GmbH

1 Notes regarding the use of these operating instructions

This chapter contains information regarding these operating instructions as well as

1.1 Validity of the operating instructions

Version: 1.2GB/2013-11-25 -1- © 2013 Oxford Instruments Analytical GmbH

1.2 Pictograms and signal words

Important information in these operating instructions and on the instrument is marked

1.2.1 Hazard symbols

1.2.2 Symbols for personal protective equipment

Wear eye protection!

Wear ear protection!

Wear protective gloves!

1.2.3 Information symbol

© 2013 Oxford Instruments Analytical GmbH -2- Version: 1.2GB/2013-11-25

2 Intended use and misuse

The stationary optical emission spectrometer (OES) is exclusively intended for

The instrument may only be used in dry rooms.

The intended use also includes

The instrument is exclusively intended for operation in an industrial environment. For

Misuse The use in hazardous areas is not permitted.

The employment of insufficiently qualified personnel is regarded as misuse.

Measurements without correctly positioned samples is regarded as misuse.

Unauthorised structural modifications, attachments to or conversions of the instrument

The manufacturer is not liable for damage resulting from misuse.

Version: 1.2GB/2013-11-25 -3- © 2013 Oxford Instruments Analytical GmbH

3 General safety instructions

Version: 1.2GB/2013-11-25 -5- © 2013 Oxford Instruments Analytical GmbH

Warning! Hot surface!

© 2013 Oxford Instruments Analytical GmbH -6- Version: 1.2GB/2013-11-25

3.1 Safety instructions for work on the electrical system

Version: 1.2GB/2013-11-25 -7- © 2013 Oxford Instruments Analytical GmbH