SA-250P MiniFID

Operator’s Manual
204 Technology Park Lane
Fuquay-Varina, NC 27526 USA
Tel: (919) 557-7300
Web: www.apexinst.com
SA-250P MiniFID

204 Technology Park Lane

Fuquay-Varina, NC 27526
www.apexinst.com
(919) 557-7300
(800) 882-3214

For Support or Service contact:

Technical Services Group

[email protected]
(919)346-5754

SA-250P MiniFID Operator’s Manual - Version 0.2 Revision Date: 2020.08.13

Apex Instruments, Inc.
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SA-250P MiniFID

Disclaimer
Apex Instruments Inc. makes no representations or warranties with respect to this manual and, to the maximum extent
permitted by law, expressly limits its liability for breach of any warranty that may be implied to the replacement of this
manual with another. Furthermore, Apex Instruments reserves the right to revise this publication at any time without
incurring an obligation to notify any person of the revision.

The information provided in this documentation contains general descriptions and/or technical characteristics of the
performance of the products contained herein. This documentation is not intended as a substitute for and is not to be
used for determining suitability or reliability of these products for specific user applications. The user or integrator is
responsible for performing the appropriate and complete risk analysis, evaluation and testing of the products with respect
to the relevant specific application or use thereof. Neither Apex Instruments nor any of its affiliates or subsidiaries shall be
responsible or liable for misuse of the information that is contained herein. If you have any suggestions for improvements
or amendments or have found errors in this publication, please notify us.

All pertinent state, regional, and local safety regulations must be observed when installing and using this product. For
reasons of safety and to help ensure compliance with documented system data, only the manufacturer shall perform
repairs to components.

Failure to observe this information can result in injury or equipment damage.

Copyright © 2020 by Apex Instruments, Inc.

All rights reserved. No part of this publication may be reproduced, distributed, or transmitted in any form or by any means,
including photocopying, recording, or other electronic or mechanical methods, without the prior written permission of the
publisher.

Retaining Instructions
Read and understand this manual and its safety instructions before using this product. Failure to do so can result in
serious injury or improper execution of sampling procedures.

Follow all relevant instructions to avoid fire, explosions, electric shocks or other hazards that may result in damage to
property and/or severe or fatal injuries.

The product shall only be used by persons who have fully read and understood the contents of this user manual.

Ensure that each person who uses the product has read these warnings and instructions and follows them.

Keep all safety information and instructions for future reference and pass them on to subsequent users of the product.

The manufacturer is not liable for cases of material damage or personal injury caused by incorrect handling or non-
compliance with the safety instructions. In such cases, the warranty will be voided.

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Warranty Policy
Product Limited Warranty Policy
Apex Instruments, Inc. warrants products to be free from defects in materials and workmanship for a period of one year
from date of delivery. During the warranty period, we will repair or replace, at our option, any component that fails due to a
defect in materials or workmanship under normal use excluding installation. Items not manufactured by Apex Instruments
are subject to original manufacturer’s warranty. All returns must be shipped freight prepaid at the purchaser’s expense.

Repair Services Limited Warranty Policy

Apex Instruments, Inc. warrants repairs to be free from defects in materials for a period of one year and workmanship for
a period of 90 days from date of delivery. During the warranty period, we will repair any item Apex Instruments repaired or
replaced that fails due to a defect in materials or workmanship under normal use.

What is Not Covered

Accidents, misuse, abuse and modifications. All forms of corrosion or other environmental conditions including lightning,
natural disasters, improper installation and installation of an incorrect part. Normal wear and tear, used or salvage parts
installed and shipping damage.

Contamination
Customer is responsible for decontamination of all equipment returned to Apex Instruments. Apex Instruments reserves
the right to return or decontaminate any equipment deemed unsafe or contaminated at the customer's expense.

Additional Important Information

This limited warranty does not cover labor cost or incidental, indirect, special or consequential damages such as, but not
limited to, physical injuries or property damage, loss of time, loss of use of the component, inconvenience, rental equip -
ment charges, or accommodations resulting from a defect in or failure of the component. You must be the original pur-
chaser of the component, warranty is not transferable.

This limited warranty represents the exclusive remedy for any component defect or failure and the total liability of Apex
Instruments for any component it warrants.

Apex Instruments makes no other warranties, express or implied, including any warranties of merchantability, condition of
any kind or fitness for a particular purpose.

Some states do not allow disclaimers of implied warranties. Therefore, all implied warranties that may apply to the compo-
nent are limited to the duration of this written warranty. Some states also do not allow limitations on how long an implied
warranty lasts or the exclusion or limitation of incidental, special or consequential damages, so the above information
may not apply. This warranty provides specific rights and other rights which may vary from state to state. Apex
Instruments, Inc does not authorize any entity to vary the terms, conditions or exclusions of this warranty. If any provision
of the warranty should become invalid or unenforceable because of any laws, the remaining terms and provisions of the
warranty shall remain in full force and effect. To the extent allowed under local law, the remedies provided in this Limited
Warranty Policy are the purchaser’s sole and exclusive remedies. Apex Instruments, Inc., 204 Technology Park Lane,
Fuquay-Varina, NC 27526. Visit us on the web at www.apexinst.com.

Acceptance of Terms and Conditions

Apex Instruments, Inc. manufactures and sells its products under the foregoing terms and conditions and will not be bound to
terms and conditions stated by any purchaser in any offer, acceptance or other contractual document. Placing an order or
accepting delivery of products constitutes acceptance of terms and conditions.

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Document History
While we believe that the information and guidance given in this manual is correct, all
parties must rely upon their own skill and judgment when making use of it. Apex Instruments,
Inc. will not assume any liability to anyone for any loss or damage caused by any error or
omission in the manual, whether such error or omission is the result of negligence or
any other cause. Any and all such liability is disclaimed.

What’s In The Box

SA-250P MiniFID portable THC analyzer.
SA-250P operating manual.
2 x Carry strap.
Sample filter replacement tool.

Options
Selected fuel option bottle, either H2 or H2He.
Selected calibration bottle; Propane or Methane.
Data logger software and USB cable.
HSLJ-6- -SFAH4 5m/10m heated sample line.
PC6- S-H3 probe
ICF-XR2C-H4 temperature controller

Explanation of safety warnings

! DANGER
“DANGER” indicates a hazard with a high level of risk which, if not avoided, will result in
death or serious injury.

! WARNING
“WARNING” indicates a hazard with a medium level of risk which, if not avoided, could
result in death or serious injury.

! CAUTION
“CAUTION” indicates a hazard with a low level of risk which, if not avoided, could result
in minor or moderate injury.

NOTICE
“NOTICE” Indicates information considered important, but not hazard-related.

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Quick Start
Full instructions for operation of the SA-250P MiniFID are in section 4 of this Manual.
Instructions for routine maintenance of the SA-250P MiniFID are in section 5 of this Manual.
Simple Quick Start instructions are attached to the analyzer and are repeated here and
on the following two pages:

UNITS LEDs SPAN CAL

LCD DISPLAY
GAS PATH SELECT
SWITCH AND
SAMPLE LED
STANDBY/
IGNITION SWITCH

ZERO CAL
FLAME LIT LED
DISPLAY
SELECT
SWITCH FLOWMETER

RANGE SWITCH
FLOWMETER
NEEDLE VALVE

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Setting the Fuji Temperature Controllers

C1
C1
Set Value
C2
AL1 Setting C2
AL1
C2
AL1
AL2 AL2 AL2

SEL AMBIENT CURRENT

SEL SET VALUE NEW SET
SEL VALUE
SV °C SV °C SV °C

22 2 1
C1 C1 C1
C2 C2 C2
AL1 AL1 AL1
AL2 AL2 AL2

SEL SEL SEL

PRESS PRESS PRESS

To change the set value (SV) press SEL
SEL once. The current value is displayed and SV is lit.

Press the to increase or decrease the set value.

After the new set value is entered press SEL

SEL
to lock in the value and return to C1 (control 1)
display.

Repeat procedure to check value if necessary.

Sampling Train
Dual-Station Temperature Controller, Probe and Sample Line must be purchased separately.

PC6-3S-H3
Probe

SA-250P
120 Volt System Shown

HSLJ-6-15-SFAH4
Heated Sample Line

ICF-XR2C-H4
Dual-Station Temperature Controller

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SA-250P MiniFID

SA-250P MiniFID Start - Up Procedure

1. Prior to use, inspect the gas bottles and their connecting pipes and fittings, and the
heated line.
! WARNING Do not use if damage is evident.
2. Connect the Heated Line electrical and pneumatic connections to the MiniFID, and
to the sample source.
! WARNING Do not operate the Heated Line when coiled as it may overheat.
Connect the fuel and calibration bottles to the MiniFID, and open their on/off valves
only one full turn only. Check the mains supply is the correct voltage, 1000VA
minimum continuous. Plug the MiniFID in. Set the GAS PATH SELECT switch to
ZERO.

3. Switch on using the mains breaker switch to the rear of the MiniFID. Do not
connect or disconnect the Heated Line’s electrical connection when the power is on.
4. When the Oven and Heated Line have both warmed up above 130°C, flick the
STBY/IGN Switch to IGN briefly and the pump will start. Adjust the air flow using
the front panel flowmeter for a flow of 600 ml/min.
5. Press and hold the STBY/IGN switch to its IGN position whilst slowly reducing the
front panel air flow. Ignition is indicated by a ‘popping’ sound and a rise in the
analyser reading. Also the FLAME-LIT LED will illuminate continuously. When the
MiniFID is lit, slowly increase the front panel air flow to 600ml/min.
6. Allow the MiniFID to stabilise for a further 10 to 15 minutes (full accuracy after 1
hour). Set the GAS PATH SELECT switch to ZERO, and adjust ZERO CAL for a
reading of zero. Set the switch to SPAN, and adjust SPAN CAL for a reading to
match the value of the calibration bottle (select the appropriate RANGE for this).
7. Set the GAS PATH SELECT switch to SAMPLE, the SAMPLE LED will light
continuously, and the MiniFID will measure the total hydrocarbon content of your
sample. Select appropriate RANGE.
8. To shut down the MiniFID, remove the Heated Line from the sample gas source
and with the GAS PATH SELECT switch in the SAMPLE position, allow the Heated
Line to purge with ambient air for at least 15 minutes. Switch the GAS PATH
SELECT switch to ZERO for at least 2 minutes to purge the MiniFID. Move the
STBY/IGN switch to STBY (standby), then switch the mains breaker switch to off,
and close the gas bottles’ on/off valves.

! WARNING Do not coil the Heated Line until it has cooled down.

! CAUTION CAUTION: SOME PARTS MAY STILL BE HOT

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Contents
1 Introduction.........................................................................................11
1.1 SA-250P MiniFID........................................................................11
1.2 Applications.................................................................................11

2 Technical Description.........................................................................12
2.1 The Principle of Flame Ionization...............................................12
2.2 Sample System...........................................................................12
2.3 Fuel System................................................................................12
2.4 Flow Schematic..........................................................................13
2.5 Major Component Location ........................................................14
2.6 Analyzer Controls.......................................................................15

3 Installation..........................................................................................16
3.1 Carrying Options ........................................................................16
3.2 Analyzer Location .......................................................................16
3.3 Mains Power Connections .........................................................16
3.4 Gas Connections........................................................................16
3.5 Fuel ............................................................................................17
3.6 Span Calibration Gas.................................................................18
3.7 Zero Calibration Gas..................................................................18
3.8 Sample.......................................................................................18
3.9 FID Exhaust ...............................................................................18
3.10 Hot Air Dump..............................................................................19
3.11 Chart Connections.....................................................................19
3.12 Data Logging Configuration (optional).......................................19
3.12.1 Starting the Logger........................................................20
3.12.2 Downloading Data.........................................................21

4 Operation ...........................................................................................22
4.1 Introduction................................................................................22
4.2 Start -up and Temperature Monitoring.......................................22
4.3 Ignition........................................................................................22
4.4 Calibration..................................................................................23
4.5 Sample Measurement................................................................23
4.6 Standby ......................................................................................23
4.7 Shut -down..................................................................................23

5 Routine Maintenance .........................................................................24

5.1 Sample Filter Replacement .......................................................24
5.2 Replacing the Carbon Scrubber (optional) ................................25
5.3 Empty Gas Bottles .....................................................................26

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6 Routine Servicing ....................................................................... 27

6.1 Policy ................................................................................... 27

7 Specifications ............................................................................. 28
7.1 Detector ............................................................................... 28
7.2 Ranges (methane or propane equivalence) ....................... 28
7.3 Linearity ............................................................................... 28
7.4 Stability ................................................................................ 28
7.5 Noise ................................................................................... 28
7.6 Carbon Number Correlation ................................................ 28
7.7 Catalytic Air Purifier............................................................. 28
7.8 Oxygen Synergism .............................................................. 28
7.9 Sample System ................................................................... 28
7.10 Sample Flow Rate ............................................................... 28
7.11 Sample Flow Sensitivity ...................................................... 28
7.12 Response Time ................................................................... 29
7.13 Heated line .......................................................................... 29
7.14 Probe................................................................................... 29
7.15 Temperature Controllers...................................................... 29
7.16 Gas Supplies ....................................................................... 29
7.17 Pneumatic Connections ...................................................... 29
7.18 Inlet Pressures .................................................................... 29
7.19 Zero Air................................................................................ 29
7.20 Ignition ................................................................................. 29
7.21 Safety Interlocks.................................................................. 29
7.22 Display................................................................................. 30
7.23 Outputs ................................................................................ 30
7.24 Options ................................................................................ 30
7.25 Power .................................................................................. 30
7.26 Environment ........................................................................ 30
7.27 Dimensions.......................................................................... 30
7.28 Maintenance and Spare Parts.............................................31

Figures
Figure 1 Flow Schematic..................................................................... 13
Figure 2 Tube Fitting Assembly...........................................................17
Figure 3 Fuel Supply Configuration ....................................................17
Figure 4 Chart recorder pin -out connections..................................... 19
Figure 5 Launch Window..................................................................... 20
Figure 6 View - Table of Readings......................................................21
Figure 7 File – Export all cells............................................................. 21

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1 Introduction
1.1 SA-250P MiniFID
The SA-250P MiniFID uses the well established principle of Flame Ionization to detect
volatile organic compounds (VOCs) in a gas stream. It incorporates all the knowledge and
experience of five generations of product development.

NOTICE
Please read this manual thoroughly before operating the SA-250P MiniFID.

Features include:
• Improved heated sample conditioning module with built-in sample pump.
• Field-replaceable carbon scrubber cartridge to provide hydrocarbon-free
burner and zero air. Improved heated air cleaner available on request.
• Integral heated line, temperature controlled by the SA-250P MiniFID
Temperature controller required, integrated
• Lightweight for easy portability.
• Simple controls. Non-specialist personnel can operate with minimal training.
• Optional onboard data logging for analysis of collected measurements.

The analyzer will have been configured at the factory for either H 2 or H 2 He fuel and
calibrated for Propane or Methane equivalence.

1.2 Applications
The main applications for this analyzer are in automobile combustion research, mobile
emissions compliance monitoring, HSE and emission consultancies, and gas
manufacturers. The prime benefit for these users comes from the heated detector and
sample system. Raw gas can be measured with great accuracy and sensitivity, and
with very low interference from other emission components normally found in the
combustion gas sample. The SA-250P MiniFID is 300mm high, self -contained, and fully
portable. It is equally convenient for use on the laboratory bench or as a portable on -
site measurement tool.

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2 Technical Description

2.1 The Principle of Flame Ionization

This detector ionizes carbon atoms in a hydrogen flame. Normally a hydrogen flame
produces very few ions. Any carbon-hydrogen bonded molecules carried into the flame
results in the formation of carbon ions. The detector can measure most compounds
with a carbon-hydrogen bond provided that they are in gaseous form.
Because the detector responds to carbon ions, a mixture of hydrocarbon compounds
result in an output closely proportional to the carbon count. 10ppm CH 4 mixed with
10ppm C3H8 results in an output of approximately 40ppm Methane equivalence or
13.33ppm Propane equivalence. These are two of the ways that the hydrocarbon
concentration can be expressed. The Methane equivalence is mainly used in ambient
air monitoring where a comparison against background Methane is required. Propane
equivalence is used in most other industries.

2.2 Sample System

Combustion exhaust gases normally contain some hydrocarbons that are liquid at
ambient temperatures. The unit includes a 191°C heated sample handling module which
houses the FID, a sample particulate filter, a sample selection solenoid, a sample
capillary, and connections to the zero and span selection valves.
The sample module allows the connection of a heated sample line directly to the heated
sample inlet, preventing cold spots where sample condensation may occur. It uses a
make-up air bypass system to prevent sample condensation problems at the back-
pressure regulator. Make-up air is added to the sample path from the bypass air supply
at a point down-stream of the sample extraction point. This creates a constant flow at
the sample dump port. The sample is never in contact with the pressure control
components.
An internal, dual-headed pump provides sample flow and bypass air.
A portion of the bypass air is passed through a disposable Carbon Scrubber to provide
very low hydrocarbon FID combustion and zero air.
Sample gas cannot be selected until the oven and heated line are above 130°C and the
flame is lit.

2.3 Fuel System

The instrument has been designed so that no possibility of hydrogen gas build-up can
occur inside the enclosure. A flame-out sensor shuts off the fuel whenever the FID flame
extinguishes. The shut-off valve is mounted on the rear panel so that any possibility of
leaks upstream of the valve will occur on the outside of the instrument where it will be
diluted and ventilated.

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2.4 Flow Schematic

AIR INLET

EXHAUST

FUEL

SPAN

0 .7 5

SAMPLE HOT AIR

DUMP

HEATED MANIFOLD AT 1 9 1 °C

Figure 1

NOTICE

The SA-250P MiniFID has a bypass flow system which uses the air pumped by the cold
head to compensate for variations in the sample flowrate. The Hot Air Dump flowrate of
3.2 l/min is maintained mostly by the sample flow, and made up to 3.2 l/min by the make
up air, supplied at constant pressure by the pump cold head, and the back pressure
regulator. The constant 3.2 l/min Hot Air Dump causes a constant back pressure in the
bypass system. The small detector sample is taken through a capillary to the detector
from the bypass. The constant back pressure in the bypass system maintains a
constant flow to the detector. Any variation in the sample flow to the analyzer is made
up to 3.2 l/min Hot Air Dump by the Make-up Air. The sample flow to the analyzer must
never exceed the Hot Air Dump flow else the compensation system will go out of
control, allowing sample gas to be vented into the analyzer through the BPR. Also the
sample flow must never fall below 0.4 l/min else the Make-up Air may backstream
through the bypass system to the sample capillary, and dilute the sample. The system
has the benefit of maintaining accurate control through large variations in sample
bypass flowrate (0.4 to 3.0 l/min), without the necessity of having a mechanical pressure
regulator in the sample gas stream.

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2.5 Major Component Location

The location of the SA-250P MiniFID major components is illustrated in the diagram below:
SPAN AND FUEL
CHART
GAS QUICK
RECORDER
CONNECTS CARRYING
OUTPUT
HANDLE
SOCKET
MAINS ON/OFF
BREAKER
SWITCH

DISPOSABLE
OPTIONAL DATA LOGGER CARBON SCRUBBER
(VAPOUR
ADSORPTION UNIT)

FID AIR CLEANER

EXHAUST READY LIGHT

VENTILATION
AIR INLET

FRONT
PANEL !
CAUTION
HEATED LINE 115V 800W
MAX.

HOT

EXHAUST

HEATED LINE
ELECTRICAL
DUMP

SAMPLE/FILTER

CONNECTION
FLOWMETER
VENTILATION
FLOWMETER FAN OUTLET
NEEDLE VALVE
HOT AIR DUMP SAMPLE INLET
AND SAMPLE
FILTER HOLDER

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2.6 Analyzer Controls

The SA-250P MiniFID controls are illustrated, and their function(s) detailed in the diagram
below.
SPAN CALIBRATION
Scales reading to
UNITS LEDS calibrate analyzer to
LCD DISPLAY Appropriate LED will known concentration
Indicates analyzer reading in illuminate to show which when span gas is
ppm or % as shown by units apply to current LCD selected. Pot gives 10:1
illuminated units LEDs. Will display, e.g. ppm, % or gain change allowing
also indicate oven or heated °C. Led will flash if calibration for CH4 or C3H8
line temperature depending on display is over range. equivalence.
position of display select switch.
GAS SELECT &
SAMPLE LED
Selects zero or span
FLAME LIT LED gas for calibration or
Illuminated when sample gas for
FID flame measurement. Sample
successfully lit is inhibited if oven or
heated line are not at
temperature, or FID
flame not lit.
Sample led is
illuminated when
sample is measured.
STANDBY/IGNITION SWITCH
Use centre position for start up: ZERO CALIBRATION
oven and line will warm up and Sets zero point of
when at temperature, pump will analyzer. Use when
start. Set air flow and depress
zero gas is selected.
switch (momentarily) for ignition.
Once ignited re-adjust air flow.
In STBY position, heaters are DISPLAY SELECTION
maintained but pump and fuel are Selects temperature or
turned off. hydrocarbon level for
display.

RANGE SWITCH FLOWMETER

Selects the analyzer range Indicates FID air flow.
1 - most sensitive Set to ~250 ml/min for
4 - least sensitive ignition and 600 ml/min
for normal operation.

FLOWMETER
NEEDLE VALVE
Sets FID air flow

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3 Installation
! CAUTION

THIS INSTRUMENT REQUIRES A SAFETY EARTH CONNECTION

Sample inlet and bypass output ports
WILL BE HOT
while the analyser is ON, and for some time after switching off
TAKE PRECAUTIONS AGAINST BURNS BY USING GLOVES

3.1 Carrying Options

The entire instrument (and bottle rack) may be carried either by the carrying handle or the
strap. The bottle rack may be detached and carried by its own strap.
On no account should the bottle rack strap be used to carry the entire instrument.

3.2 Analyzer Location

The analyzer should be mounted on a flat surface, and should be placed in a dry and
sheltered location out of direct sunlight, avoiding drafts, and protected from water
ingress.
Observe the environmental limitations listed in the specification section.
The analyzer relies on ventilation through the sides. Do not obstruct these areas.

3.3 Mains Power Connections

110V - The analyzer is supplied with a 2m long mains lead with a BS4343 plug for
connection to a 110Vac 50/60Hz supply. This will normally be provided by a safety
isolation transformer of 1000VA continuous rating minimum.
230V - The analyzer is supplied with a 2m long mains lead with a IEC-EN60309-2 plug
for connection to a 230Vac 50/60Hz 1000VA supply. To provide maximum safety, the
circuit should be protected with a RCD residual current or earth leakage breaker.
This instrument requires a safety Earth and must not be used without one.

3.4 Gas Connections

If your sample contains toxic gases, as defined by your local legislation, the analyzer
exhaust and (hot air) dump must be routed to a safe area that complies with your local
safety regulations. Condensate will form as the exhaust gas cools and for this reason
any external pipework must run downwards. Take care as the exhaust and dump will be
hot if the analyzer has been switched on.
The analyzer is a very sensitive detector of hydrocarbons. It is very important that all
gas and sample tubing is clean and free from contaminants, and does not retain volatile
organic compounds which may be released later. PTFE tube is suitable for most
applications. Contaminated PTFE tubing can be cleaned by heating it in an oven at
200 C while passing clean air through it.

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The Sample and Hot Air Dump gas

connections have the same assembly
method. Cut the tubing to length ensuring
that the ends are cut square. Slide the nut
and ferrule over the tube. Insert the tube
into the end of the fitting and hold it firmly
against the internal shoulder. Slide the nut
and ferrule to the fitting and tighten the nut
until it is “finger tight”. Tighten the nut a
further 1¼ turns with a suitable spanner.
When connections are remade, it is only
necessary to tighten the nut slightly with the
Figure 2 Tube Fitting Assembly spanner after making it “finger tight”.

3.5 Fuel
The analyzer fuel supply must contain either H 2 or a 40% / 60% mixture of H2 He. The
bottle should include a single stage pressure reducer, flow limiter, ON/OFF valve
coiled connecting tube and quick fit connector for easy connection to the analyzer
fuel inlet. The analyzer will have been configured at the factory for either H 2 or H2 He
fuel. Check the test certificate shipped with the analyzer to confirm which type
you require. You may connect an alternate source of the fuel gas to the fuel inlet if the
supply is regulated within the limits described in the specification section of this manual.
Ensure that the regulator and piping are clean and not contaminated. If they have been
used with high concentrations of volatile organic compounds they should be purged with
clean air for at least 24 hours.

Figure 3 Fuel Supply Configuration

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3.6 Span Calibration Gas

The analyzer must be calibrated with a calibration gas containing 1000ppm Propane or
500ppm Methane in air (Alternate concentrations can be supplied. Contact your local
supplier). The calibration gas bottle should utilize a single stage pressure reducer, flow
limiter, ON/OFF valve, coiled connecting tube and quick - fit connector for easy
connection to the analyzer span inlet. Total Hydrocarbon measurements are normally
made in Propane or Methane equivalence, and you should use an appropriate
calibration gas accordingly. The actual concentration should be similar to the expected
range of results for best accuracy. You may connect an alternate source of the
calibration gas to the span inlet if the supply is regulated within the limits described in
the specification section of this manual. Ensure that the regulator and piping are clean
and not contaminated. If they have been used with high concentrations of volatile
organic compounds they should be purged with clean air for at least 24 hours.

3.7 Zero Calibration Gas

This is internally generated from room air via a field-replaceable carbon scrubber
cartridge. If there is a high hydrocarbon local ambient background, the carbon scrubber
cartridge will require regular replacement, or you may require an external source of
hydrocarbon free air to connect to the air inlet of the analyzer.
If the MiniFID PURE option has been selected, the internal Zero Calibration Gas is
cleaned by a heated catalytic air purifier (AS90). A light on the side of the analyzer will
come on to indicate that the AS90 is up to temperature. So as to avoid any background
interference, you should wait until the AS90 is up to temperature before taking
measurements.
3.8 Sample
Depending on your application, the source of sample gas may be at an elevated
temperature. The analyzer sample system is heated to 191°C in order to prevent
condensation of sample contents which can lead to inaccurate concentration readings
and blockages in the sample path. It is normal in many applications for the sample to be
routed to the analyzer using a heated line, and the SA-250P MiniFID is supplied as
standard with a 5 meter heated line. There is an optional 10 meter heated line available.
Both are powered and temperature controlled by the analyzer.
Connect the heated line to the port labeled SAMPLE/FILTER.

3.9 NOTICE The nut only requires to be “nipped” tight with a spanner and
excessive force should be avoided.
! CAUTION This port will be hot if the analyzer has been switched on.
Connect the heated line’s electrical plug to the MiniFID’s heated line electrical socket.
! WARNING Do not connect or disconnect the heated line electrical
connection to the analyzer when the analyzer is switched on.
3.9 NOTICE Do not operate the heated line when coilded as it may overheat.

3.9 FID Exhaust

The FID produces a small quantity of waste gas as a by-product. This is normally
vented to the local ambient. If the sample contains toxic gases as defined by your
legislation, this outlet must be vented to a safe area or in a manner as described by the
local legislation. The exhaust gas contains water vapor which as it cools, condenses.
This condensate may be corrosive.
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SA-250P MiniFID

The detector is very sensitive to the back pressure on this port. In particular, variations
due to an external pump used to force flow in the safe vent area can cause excessive
detector noise.
Only if necessary, connect the exhaust to a safe vent area using the largest possible
tubing. This tubing must run downwards due to the condensate.

3.10 Hot Air Dump

Unused sample gas and make-up air leave the analyzer at the DUMP port. This is
normally vented to the local ambient. If the sample contains toxic gases as defined by
your legislation, this outlet must be vented to a safe area or in a manner as described by
the local legislation. As it cools, condensate may form, which may be corrosive.
Only if necessary, connect the exhaust to a safe vent area using the largest possible
tubing. This tubing must run downwards due to the condensate.

3.11 Chart Connections

Figure 4 shows the CHART socket pin-out connections, viewed from above.

Figure 4 Chart recorder pin-out connections

Pins 1 and 9 provide a 0-10V output where Full Scale Deflection (FSD) corresponds to
the slelected range full scale. Note this signal is not iolated: the return is internally
connected to Earth.
Pins 5 and 13 provide a 4 - 20mA output where FSD corresponds to the selected range
full scale. This signal is isolated from ground to ensure trouble-free current loop
performance.
Pins 2 and 10, 3, 11 & 4 provide volt-free contact closures to indicate range. COM
connects to each of the RANGE pins corresponding to the selected range. Observe the
electrical ratings of these contacts listed in the Specifications, 7.21 Outputs, page 27.

3.12 Data Logging Configuration (optional)

The data Logger will record the 0-10v output of the currently selected range as per pins
1 and 9 of the chart recorder connector described in 3.11 Chart Connections.
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3.12.1 Starting the Logger

Before starting the onboard data logger, make sure all previous data has been
downloaded and backed up (see section 3.12.2 Downloading Data); restarting the
logger for a new session erases the data currently stored.
Because of the start options, it is necessary to set the logger up on the day of testing
(using the smallest logging interval available, the logger will have a measuring time of
just over 18 hours and the logger starts logging from the moment it is launched.).
1. Connect the data logger to a PC or laptop which has the TinyTag Explorer installed
(program on CD and USB cable supplied with the 3010MF).
2. Open TinyTag Explorer and click on the Launch button in the menu bar.
3. Make sure the advance settings are shown as below (Figure 5), if not click the
‘Advanced Settings>>’ button. Expand each option in turn and make the following
selections:

Figure 5 Launch Window

a. Description – Add a title for the session,

b. Logging Interval – Select how often the logger will record measurements
(recording capacity will be reached in 18 hours at 1 measurement per second),
c. Start Options – A relative start time of 00:00:00 for immediate start is
recommended, however, if you know the rough time of testing, an absolute
date and time can be entered.
d. Measurements – Select ‘Measured at the end of each interval’,
e. Stop Options – Select ‘Stop when full’,

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f. Alarms – Low and high alarms can be selected, but it is advised not to select
latched alarms since they can only be reset by connecting to a PC/Laptop and
restarting the logger. If the alarms are triggered, the red LED on the Data
logger module will light:
i. Low alarm – flashes twice every 4 seconds
ii. High alarm – flashes once every 4 seconds
4. After selecting the desired options, click ‘Launch’. As soon as logging commences
the green LED on the Data Logger will flash for each interval recorded.

3.12.2 Downloading Data

To retrieve the data on the Data Logger open TinyTag Explorer and click
‘Get Data’ in the menu bar.
TinyTag Explorer will ask to stop the logger, click ‘Yes’, the logger will be stopped and
the data downloaded, after a short moment a graph of the results will appear. The
results can be saved for later use as a .ttd file by clicking ‘Save As’ in the File menu.
Any data not saved to the PC/Laptop will be lost the next time the logger is started
(launching the logger erases all data currently in memory).
To save the measurements for use in a data management package such as Excel,
select ‘Table of Readings’ in the View menu (Figure 6). With the ‘Table of Readings’
window active, select ‘Export – All cells’ from the file menu (Figure 7), and save the data
file to the required format.

Figure 6 View – Table of Readings Figure 7 File – Export all cells

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4 Operation
4.1 Introduction
Analyzer operation is controlled directly by the operator from the front panel.
This section explains in detail how to operate the analyzer using the front panel controls.

4.2 Start-up and Temperature Monitoring

Before using the instrument, inspect the gas bottles and their connection tubing and the
heated line.
! WARNING Do not use the instrument if any damage is evident.
Connect the heated line electrical lead to the socket on the right hand - side before
applying mains to the instrument. This is to avoid unnecessary arcing and connection or
disconnection of the heated line should be avoided while mains power is on.
! CAUTION Do not operate the heated line when coiled as it may overheat.
Connect the heated line gas connection to the sample inlet.
The nut only requires to be ‘nipped’ tight with a spanner and
3.9 NOTICE excessive force should be avoided.
Connect to a suitable power source and switch the instrument ON.
The oven and heated line will now heat up to the set temperature of 190°C. Their temperatures
can be monitored by use of the display selection switch and integrated temperature controller.
Ignition is inhibited until the oven and heated line have reached approximately 130°C to
prevent water condensation within the FID.
If the AS90 heated air cleaner has been fitted, the green ready LED will light when the
cleaner is near to optimum temperature. Ignition is not inhibited during this warm up
time, however, it is recommended to wait for the light to come on before starting to take
measurements.
4.3 Ignition
1. Open the gas bottle valves by turning anti -clockwise. A single, full turn is sufficient.
2. Select zero gas using the gas select switch.
3. Depress momentarily the ignition switch. This starts the pump and turns on the fuel.
The front panel flowmeter should be adjusted for a flow of 600ml/min.
The FLAME LIT LED will flash to indicate that the flame-out sensor has been over-
ridden and a flame lit condition has not yet been sensed. The override period is set
at approximately 2 mins to give time for the flame to be sensed. If the flame is not
sensed within this time, the pump and fuel are turned off.
4. Depress and hold the ignition switch whilst slowly reducing the front panel air flow.
This operation energizes the igniter and provides the fuel enrichment necessary for
ignition.

Ignition is indicated by a ‘popping’ sound and the display reading will rise. Also, the
FLAME LIT LED will light continuously when the flame has been detected.
Upon successful ignition, the front panel air flow should be slowly increased to
600ml/min and then the ignition switch released.
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4.4 Calibration
Upon successful ignition, the instrument should be allowed to stabilize for 15 minutes.
Select zero gas using the gas select switch and adjust the ZERO CALIBRATION control
to achieve a zero reading. The most sensitive range, 1, is normally selected for this
operation. Make sure the DISPLAY SELECT switch is in its center position, otherwise
temperature will be displayed.
Select span gas using the gas select switch and adjust the SPAN CALIBRATION control
to achieve a reading to match the calibration gas. The appropriate range will need to be
selected for this operation.

4.5 Sample Measurement

Select the center position of the gas select switch to measure the hydrocarbon level of
the sample gas entering via the heated line. The SAMPLE LED will light.
Select appropriate range. The units LED, ppm or %, will flash to indicate over-range.
As part of the instrument’s safety philosophy, sample selection is only allowed if the
flame is lit and the heaters are above 130°C. The SAMPLE LED flashes to indicate that
sample has been selected, but has been internally inhibited and the instrument defaults
internally to zero gas.

4.6 Standby
Selecting STANDBY with the IGNITION switch will immediately stop the pump and shut
off all gas valves: the flame will extinguish. The oven and heated line temperatures are
maintained ready for a subsequent ignition sequence.

4.7 Shut -down

To prevent hydrocarbons condensing as the instrument cools down, it is important to
purge the system, as follows:
1. Remove the heated line from the sample source and with sample gas selected,
purge the line with ambient air for at least 15 minutes.
2. Select zero gas and purge the analyser for at least 2 minutes.
3. Select STANDBY with the IGNITION switch. The pump will stop and all gas valves
will shut off: the flame will extinguish.
4. Switch off the mains breaker switch and shut off the gas bottle valves.

NOTICE Do not coil the heated line until it has cooled.

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5 Routine Maintenance

5.1 Sample Filter Replacement

! CAUTION
CAUTION
If the analyzer has been switched on, the filter housing will be too hot to touch.
The filter replacement tool provides a method for changing hot filter elements.
Dry filters may contain corrosive compounds. Use gloves.

Apex Instruments, Inc. recommend and supply PTFE filters. Replacements can be ordered
under part number SG-FILT/023.
Disconnect the sample gas line. The sample
filter and filter retainer are removed using the
filter replacement tool supplied with the MiniFID

Locate the filter Locate the filter

replacement replacement
tool against the tool against the
filter retainer filter retainer

Reverse the Pull out the filter

tool and screw retainer and
the thread onto sample filter.
the end of the Replace or
filter retainer clean the filter.
pipe fitting

Push filter and

Reverse the filter retainer
tool again and into the
locate it on the MINIFID with
filter retainer the T-bar
with a vertical, then
replacement or rotate the tool
cleaned filter 90 degrees
fitted clockwise to
lock the filter
retainer in
position
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5.2 Replacing the Carbon Scrubber (optional)

The lifetime of the carbon scrubber depends entirely on the hydrocarbon level of the
local ambient air. Replacement will be necessary when an elevated zero is evident.
Replacement scrubbers can be ordered under part number SG-3010/342120.
Ensure the analyzer is either switched off, or that the STANDBY/IGNITION Switch is at
STBY. Follow the six steps below:

Push the clip Pull free

on the end of
bottom fitting scrubber
to release clear of
the carbon recess
scrubber,
and push
the scrubber
upwards

Push a
replacement
scrubber
into the top
fitting. Note
carefully the
Push clip on correct
the top fitting orientation
and pull the
scrubber free

The analyzer
is now ready
Insert for use
scrubber into
recess, and
push into
bottom fitting

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5.3 Empty Gas Bottles

Spare bottles may be purchased through your local supplier.
The bottle thread is 5/8” BSP LH, BS341 No.7.

! WARNING

Apex Instruments, Inc. does not recommend the filling of bottles unless trained
to do so.
Apex Instruments, Inc. is not liable for any damage, loss or accident caused by
the refilling of gas bottles.
Please contact your gas supplier for refill advice.

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6 Routine Servicing

6.1 Policy
Full Service Manuals are only issued to approved distributors and agents. All warranties
will cease if any unauthorized person carries or attempts to carry out his own servicing
during the warranty period, unless special arrangements have been made in writing.

If you wish to carry out your own servicing, contact Apex Instruments, Inc. or your
approved local distributor or agent.

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7 Specifications
7.1 Detector
Heated Flame Ionization Detector (FID)

7.2 Ranges (methane or propane equivalence)

0-10 ppm, 0-100 ppm, 0-1,000 ppm, 0-10,000 ppm (1%) OR
0-100 ppm, 0-1,000 ppm, 0-10,000 ppm (1%), 0-100,000ppm (10%)

7.3 Linearity
Better than ±2% of point or ±0.5% FSD on all ranges down to 10% of range. If 0-
100,000 ppm range option selected, this may be expected to be non-linear, and
readings should be corrected for actual analyzer response.

7.4 Stability
Zero drift less than ±0.2ppm or ±2% of range, whichever is greater

7.5 Noise
Less than ±0.1ppm or ±1% of range, whichever is greater

7.6 Carbon Number Correlation

Less than 5% difference in carbon count between toluene, hexane, propylene and
propane when using H2He fuel

7.7 Catalytic Air Purifier

Will remove more than 95% of 500 ppm Methane in Air.

7.8 Oxygen Synergism

100ppm C3H8 in air, changed to 100ppm C3H8 in N2 has less than 2% effect when using
H2He fuel

7.9 Sample System

Type 316 stainless steel
Internal 191°C oven
Internal heated sample pump
0.4 micron PTFE sample filter, field replaceable

7.10 Sample Flow Rate

0.4 - 2.5 litres per min

7.11 Sample Flow Sensitivity

Less than 4% change in reading from 1 to 2.5 l/min into ambient pressure exhaust

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7.12 Response Time

From 2 seconds (5%-95%) at 2 l/min flow rate, dependant on range

7.13 Heated line

The heavy-duty non-regulated heated sample line. The heated core is insulated with
braided carbon fiber. The bundle is protected by a tough high-temperature silicone
coated fiberglass sleeving. The sample line can be attached with swage lock style
compression fittings or quick connects. The maximum length is 30 feet.

7.14 Probe
Heated Probe. 6.4-mm (1⁄4 -in.) OD stainless steel tubing with a heating system capable
of maintaining a gas temperature at the exit end of at least 129 °C (265 °F). The probe
is equipped with a temperature sensor at the exit end to monitor the gas temperature.

7.15 Temperature Controllers

Integrated, panel-mounted customizable temperature controllers; 1/32 DIN temperature
controller with self-tuning, a large LED display, and an easy-to-use 3-button keypad for
temperature input.

7.16 Gas Supplies

Detachable bottle rack, with separate carrying strap, to hold fuel and calibration gas
bottles

7.17 Pneumatic Connections

1
/4” compression fittings, stainless steel

7.18 Inlet Pressures

CALIBRATION: 1.5 to 4.0 bar maximum. Flow internally regulated
FUEL: 1.5 to 4.0 bar maximum. Flow internally regulated

7.19 Zero Air

Internally generated from room air via field-replaceable carbon scrubber cartridge. If
there is a high hydrocarbon local ambient background, the carbon scrubber cartridge will
require regular replacement, or you may require an external source of hydrocarbon free
air to connect to the air inlet. 4.5 l/min typical requirement.

7.20 Ignition
Simple quick start instructions allow use with the minimum of instruction and training.
Fuel enrichment for ignition is achieved via a front-panel needle valve and flow meter,
with a momentary action switch activating the flame igniter.

7.21 Safety Interlocks

Fuel shut-off if flame fails
Sample inhibit until oven and heated line at temperature, and FID flame lit

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7.22 Display
3 1/2 digit LCD display with backlight
• 19mm (0.75”) digit height
• Automatic decimal point placement
Switch selectable readout of oven and heated line temperatures
LED indication of LCD display units (ppm, % or °C)
• Flashing ppm or % LED to indicate over-range
LED indication of FID flame status
LED indication of Sample gas path selection
• Flashing LED to indicate sample inhibit
7.23 Outputs
0-10V FSD into load resistance of greater than 5kΩ. Non-isolated from earth
4-20mA FSD into load resistance of less than 350Ω total. Isolated from earth
Volt -free contacts for analyzer range indication. Rating 24Vdc 20mA

7.24 Options
H2 fuel for applications where the oxygen content of the sample is constant, e.g. ambient
monitoring
H2He fuel for applications where the oxygen content of the sample varies, e.g.
automotive emissions or variable rate burner monitoring
Internal heated catalytic air purifier
Onboard data logger

7.25 Power
110V - 115Vac ±15% via BS4343 industrial mains plug
220V - 230 Vac ±15% via IEC-EN60309-2 industrial mains plug
350VA + 400VA for 5m heated line (maximum power during warm-up)
350VA + 800VA for 10m heated line (maximum power during warm-up)

7.26 Environment
Ambient temperature 5°C to 40°C, relative humidity up to 95%, non-condensing

7.27 Dimensions
Less bottle rack: 210mm (W) x 300mm (H) x 240mm (D), 7kg weight
With bottle rack: 210mm (W) x 300mm (H) x 353mm (D), 12kg weight

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7.28 Maintenance and Spare Parts

SG-3010/342120..........Absorption Filter Assembly
SG-FILT/023................Hydrocarbon Filter
PK-3010-QC................Quick Fit Connector for Regulator Hose

NOTICE

DUE TO A POLICY OF CONTINUOUS DEVELOPMENT, THESE SPECIFICATIONS

MAY CHANGE WITHOUT NOTICE

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