DATA SHEET OF CLEAN WATER TESTING

ENVIRONMENT LABORATORY OF PT.SUCOFINDO

No. Lab : ###
Tgl. Terima :
Tgl. Selesai : 04/06/2013
Acuan :

WWTP Final Effluent Aeration Basin Total WWTP Influent

No. Lab
Pengujian Simplo Duplo Simplo Duplo Simplo Duplo
BOD 5 days, mg/L
DO0
Titran contoh (mL) 4.6 4.6 3.7 3.7 2.3 2.3
Normalitas Na2S2O8 0.0246 0.0246 0.0246 0.0246 0.0246 0.0246
Volume Botol winkler 300 300 300 300 300 300
Volume Contoh 296 296 296 296 296 296
Volume Pemipetan 100 100 100 100
Pengenceran 15 15 20 20 1 1
DO0 137.627 137.627 147.600 147.600 1.529 1.529
DO5
Titran contoh (mL) 4.0 4.0 3.2 3.2 2.0 2.0
Normalitas Na2S2O8 0.0246 0.0246 0.0246 0.0246 #REF! #REF!
Volume Botol winkler 300 300 300 300 302 302
Volume Contoh 296 296 296 296 298 298
Volume Pemipetan 100 100 100 100
Pengenceran 15 15 20 20 1 1
DO5 119.676 119.676 127.654 127.654 #REF! #REF!
BOD 17.951 17.951 19.946 19.946 #REF! #REF!
Rata-rata 18.0 127.7 #REF!
% RPD 0.0% 0.0% #REF!
Hasil Akhir 18.0 19.9 #REF!
COD, mg/L
Titran contoh (mL) 21.80 21.8 21.3 21.3 37.6 37.6
Titran Blanko (mL) 23.7 23.7 23.7 23.7 47.4 47.4
Normalitas FAS 0.1055 0.1055 0.1055 0.1055 0.1055 0.1055
Volume Contoh 25 25 25 25 5 5
Pengenceran 1 1 1 1 1 1
Kadar COD 64.144 64.144 81.024 81.024 1654.240 1654.240
Rata-rata 64.1 81.0 1654.2
% RPD 0.0% 0.0% 0.0%
Hasil Akhir 64.1 81.0 1654.24
Soluble BOD 5 days, mg/L
DO0
Titran contoh (mL) 3.6 3.6 3.3 3.3 2.3 2.3
Normalitas Na2S2O8 0.0252 0.0252 0.0257 0.0257 0.0257 0.0257
Volume Botol winkler 300 300 300 300 300 300
Volume Contoh 296 296 296 296 296 296
Volume Pemipetan 100 100 100 100
Pengenceran 6 6 12 12 1 1
DO0 44.134 44.134 82.518 82.518 1.598 1.598
DO5
Titran contoh (mL) 3.0 3.0 2.8 2.8 2.0 2.0
Normalitas Na2S2O8 0.0252 0.0252 0.0257 0.0257 #REF! #REF!
Volume Botol winkler 300 300 300 300 302 302
Volume Contoh 296 296 296 296 298 298
Volume Pemipetan 100 100 100 100
Pengenceran 6 6 12 12 1 1
DO5 36.778 36.778 70.015 70.015 #REF! #REF!
BOD 7.356 7.356 12.503 12.503 #REF! #REF!
Rata-rata 7.4 70.0 #REF!
% RPD 0.0% 0.0% #REF!
Hasil Akhir 7.4 12.5 #REF!
Soluble COD, mg/L
Titran contoh (mL) 22.70 22.7 22.15 22.15 37.6 37.6
Titran Blanko (mL) 23.7 23.7 23.7 23.7 47.4 47.4
Normalitas FAS 0.1055 0.1055 0.1055 0.1055 0.1055 0.1055
Volume Contoh 25 25 25 25 5 5
Pengenceran 1 1 1 1 1 1
Kadar COD 33.760 33.760 52.328 52.328 1654.240 1654.240
Rata-rata 33.8 52.3 1654.2
% RPD 0.0% 0.0% 0.0%
Hasil Akhir 33.8 52.3 1654.24
TSS, mg/L
Bobot Kosong ( gram ) 0.0779 0.0737 0.0737 0.0744 0.0743 0.0745
Bobot Isi ( gram ) 0.0786 0.0743 0.0745 0.0752 0.085 0.0754
Selisih bobot ( gram ) 0.0007 0.0006 0.0008 0.0008 0.0107 0.0009
Volume Contoh 50 50 50 50 50 50
Kadar TSS 14 12 16.0 16.0 214 18
Rata-rata 13.0 16.0 116
% RPD 15.4% 0.0% 5.0%
Hasil Akhir 13.0 16.0 116.0
VSS, mg/L
Bobot Kosong ( gram ) 21.0113 20.3641 20.9368 21.5916 20.7124 26.1522
Bobot Isi ( gram ) 21.0122 20.3650 20.938 21.5928 20.7167 26.1565
Selisih bobot ( gram ) 0.0009 0.0009 0.0012 0.0012 0.0043 0.0043
Volume Contoh 100 100 100 100 100 100
Kadar TSS 9 9 12.0 12.0 43 43
Rata-rata 9.0 12.0 43
% RPD 0.0% 0.0% 0.0%
Hasil Akhir 9.0 12.0 43
 WWTP Final Effluent Aeration Basin Total WWTP Influent
No. Lab
TDS, mg/L
Bobot Kosong ( gram ) 62.8528 62.4815 47.6349 63.2541 2.5254 2.5161
Bobot Isi ( gram ) 62.8929 62.5192 47.7231 63.3423 2.5256 2.5256
Selisih bobot ( gram ) 0.0401 0.0377 0.0882 0.0882 0.0002 0.0095
Volume Contoh 50 50 50 50 50 50
Kadar TDS 802 754 1764 1764 4 190
Rata-rata 778 1764 97
% RPD 6.2% 0.0% 191.8%
Hasil Akhir 778.0 1,764 97
Phosphate, mg/L
Absorbansi 0.037 0.037 0.137 0.136 0.044 0.044
Intercept 0.00111 0.00111 0.00111 0.00111 0.00111 0.00111
Slope 0.0549 0.0549 0.0549 0.0549 0.0549 0.0549
Pengenceran 1 1 1 1 1 1
Kadar Phospate 0.7 0.7 2.473 2.455 0.781 0.781
Rata-rata 0.65 2.46 0.78
% RPD 0.0% 0.7% 0.0%
Hasil Akhir 0.7 2.5 0.78
M.O Alkalinity, mg/L
Titran Sample ( ml ) 0 0 0.0 0.0 0.3 0.3
Normalitas HCl 0.1 0.1 0.1 0.1 0.1 0.1
Konstanta ( BM CaCO3) 50 50 50 50 50 50
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 1 1 1 1 1 1
Kadar MO Alkalinity 0 0 0 0 30 30
Rata-rata 0.00 0.00 30.00
% RPD 0.0% 0.0% 0.0%
Hasil Akhir < 2.0 < 2.0 30.0

Analyzed by: Approved by :

 DATA SHEET OF CLEAN WATER TESTING
ENVIRONMENT LABORATORY OF PT.SUCOFINDO
No. Lab : ###
Tgl. Terima :
Tgl. Selesai : 04/06/2013
Acuan :

IPT A Cooling Tower Production waste oil & grease Aeraton Basin
No. Lab
Blowdown & boiler Blowdown separator from Anna Liquid 19/8/2013
Pengujian Simplo Duplo Simplo Duplo Simplo Duplo
BOD 5 days, mg/L
DO0
Titran contoh (mL) 4.0 4.0 3.6 3.6 2.3 2.3
Normalitas Na2S2O8 0.0246 0.0246 0.0257 0.0257 0.0257 0.0257
Volume Botol winkler 300 300 300 300 300 300
Volume Contoh 296 296 296 296 296 296
Volume Pemipetan 100 100 100 100
Pengenceran 25 25 20 20 1 1
DO0 199.459 199.459 150.032 150.032 1.598 1.598
DO5
Titran contoh (mL) 3.4 3.4 3.1 3.1 2.0 2.0
Normalitas Na2S2O8 0.0246 0.0246 0.0257 0.0257 #REF! #REF!
Volume Botol winkler 300 300 300 300 302 302
Volume Contoh 296 296 296 296 298 298
Volume Pemipetan 100 100 100 100
Pengenceran 25 25 20 20 1 1
DO5 169.541 169.541 129.195 129.195 #REF! #REF!
BOD 29.919 29.919 20.838 20.838 #REF! #REF!
Rata-rata 29.9 129.2 #REF!
% RPD 0.0% 0.0% #REF!
Hasil Akhir 29.9 20.8 #REF!
COD, mg/L
Titran contoh (mL) 20.55 20.55 10.7 10.7 37.6 37.6
Titran Blanko (mL) 23.7 23.7 23.7 23.7 47.4 47.4
Normalitas FAS 0.1055 0.1055 0.1055 0.1055 0.1055 0.1055
Volume Contoh 25 25 10 10 5 5
Pengenceran 1 1 1 1 1 1
Kadar COD 106.344 106.344 1097.200 1097.200 1654.240 1654.240
Rata-rata 106.3 1097.2 1654.2
% RPD 0.0% 0.0% 0.0%
Hasil Akhir 106.3 1097.2 1654.24
Soluble BOD 5 days, mg/L
DO0
Titran contoh (mL) 3.5 3.5 3.4 3.4 2.3 2.3
Normalitas Na2S2O8 0.0246 0.0246 0.0257 0.0257 0.0257 0.0257
Volume Botol winkler 300 300 300 300 300 300
Volume Contoh 296 296 296 296 296 296
Volume Pemipetan 100 100 100 100
Pengenceran 20 20 20 20 1 1
DO0 139.622 139.622 141.697 141.697 1.598 1.598
DO5
Titran contoh (mL) 3.0 3.0 3.0 3.0 2.0 2.0
Normalitas Na2S2O8 0.0246 0.0246 0.0257 0.0257 #REF! #REF!
Volume Botol winkler 300 300 300 300 302 302
Volume Contoh 296 296 296 296 298 298
Volume Pemipetan 100 100 100 100
Pengenceran 20 20 20 20 1 1
DO5 119.676 119.676 125.027 125.027 #REF! #REF!
BOD 19.946 19.946 16.670 16.670 #REF! #REF!
Rata-rata 19.9 125.0 #REF!
% RPD 0.0% 0.0% #REF!
Hasil Akhir 19.9 16.7 #REF!
Soluble COD, mg/L
Titran contoh (mL) 22.05 22.05 20.4 20.4 37.6 37.6
Titran Blanko (mL) 23.7 23.7 23.7 23.7 47.4 47.4
Normalitas FAS 0.1055 0.1055 0.1055 0.1055 0.1055 0.1055
Volume Contoh 25 25 25 25 5 5
Pengenceran 1 1 1 1 1 1
Kadar COD 55.704 55.704 111.408 111.408 1654.240 1654.240
Rata-rata 55.7 111.4 1654.2
% RPD 0.0% 0.0% 0.0%
Hasil Akhir 55.7 111.4 1654.24
TSS, mg/L
Bobot Kosong ( gram ) 0.0744 0.0746 0.0776 0.0778 0.0752 0.0753
Bobot Isi ( gram ) 0.0756 0.0757 0.0835 0.0829 0.0853 0.0854
Selisih bobot ( gram ) 0.0012 0.0011 0.0059 0.0051 0.0101 0.0101
Volume Contoh 50 50 20 20 50 50
Kadar TSS 24 22 295.0 255.0 202 202
Rata-rata 23.0 275.0 202
% RPD 8.7% 8.2% 0.0%
Hasil Akhir 23.0 275.0 202
VSS, mg/L
Bobot Kosong ( gram ) 20.8214 20.6451 18.7135 22.5581 22.4049 20.9211
Bobot Isi ( gram ) 20.8231 20.6468 18.7261 22.5707 22.4093 20.9255
Selisih bobot ( gram ) 0.0017 0.0017 0.0126 0.0126 0.0044 0.0044
Volume Contoh 100 100 100 100 100 100
Kadar TSS 17 17 126.0 126.0 44 44
Rata-rata 17.0 126.0 44
% RPD 0.0% 0.0% 0.0%
Hasil Akhir 17.0 126.0 44
 IPT A Cooling Tower Production waste oil & grease Aeraton Basin
No. Lab
Blowdown & boiler Blowdown separator from Anna Liquid 19/8/2013
TDS, mg/L
Bobot Kosong ( gram ) 62.2413 60.5244 62.8775 62.3276 2.5254 2.5161
Bobot Isi ( gram ) 62.3151 60.5982 62.9195 62.3683 2.5256 2.5256
Selisih bobot ( gram ) 0.0738 0.0738 0.0420 0.0407 0.0002 0.0095
Volume Contoh 50 50 30 30 50 50
Kadar TDS 1476 1476 1400 1357 4 190
Rata-rata 1476 1378 97
% RPD 0.0% 3.1% 191.8%
Hasil Akhir 1,476.0 1,378 97
Phosphate, mg/L
Absorbansi 0.176 0.176 0.014 0.014 0.044 0.044
Intercept 0.00111 0.00111 0.00111 0.00111 0.00111 0.00111
Slope 0.0549 0.0549 0.0549 0.0549 0.0549 0.0549
Pengenceran 1 1 1 1 1 1
Kadar Phospate 3.2 3.2 0.235 0.235 0.781 0.781
Rata-rata 3.18 0.23 0.78
% RPD 0.0% 0.0% 0.0%
Hasil Akhir 3.2 0.2 0.78
M.O Alkalinity, mg/L
Titran Sample ( ml ) 0 0 0.0 0.0 0.3 0.3
Normalitas HCl 0.1 0.1 0.1 0.1 0.1 0.1
Konstanta ( BM CaCO3) 50 50 50 50 50 50
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 1 1 1 1 1 1
Kadar MO Alkalinity 0 0 0 0 30 30
Rata-rata 0.00 0.00 30.00
% RPD 0.0% 0.0% 0.0%
Hasil Akhir < 2.0 < 2.0 30.0

Analyzed by: Approved by :

 DATA SHEET OF CLEAN WATER TESTING
ENVIRONMENTAL LABORATORY SERVICES SURABAYA AREA

No. Lab. : ###

Date Received : ###
Date of Testing : 04/06/2013
Reffernce : 0

Test Result
Parameter Unit WWTP Final Aeration Total WWTP IPT A Cooling Tower Production waste oil & grease
Effluent Basin Influent Blowdown & boiler Blowdown Separator from Anna Liquit

On site measurement

Date

Time

Temp °C

pH -

DO mg/L

On Lab Measurement
. Date 21-8-2013 21-8-2013 21-8-2013 21-8-2013
. pH 7.85 8.53 8.62 8.02
·         BOD, days 20°C mg/L 18.0 19.9 29.9
·         COD by K2Cr2O7 mg/L 64.1 81.0 106.3
·         Soluble BOD, days 20°C mg/L 7.4 12.5 19.9
·         Soluble COD by K2Cr2O7 mg/L 33.8 52.3 55.7
·        Total Suspended Solid mg/L 13.0 16.0 116.0 23.0
Test Methods *)

2550 B

4500-H+-B

4500 - O G

4500-H+-B
5210 B
5220 B
5210 B
5220 B
2540 D