Methods For Determining Moisture Content

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What is Water Content of Soil?

The water content of soil is the ratio of mass of water to mass of soil which is expressed
in percentage. Oven Dry Method and Pycnometer Method are commonly used to
determine the water content of soil in laboratory.

1. Water Content of Soil by Oven Dry Method


The oven dry method is widely used laboratory method determine the water content or
moisture content of given soil sample. It gives very accurate results.

Apparatus Required for Oven Dry Method


To determine water content by oven dry method following equipment is required.

 Hot Air Oven

 Non-corrodible air tight containers ( 3 no’s)

 Digital Weight Machine (accuracy of 0.04% of mass of sample)

 Desiccator

 Tongs
Minimum Soil Sample Quantity
The soil sample collected from the field should be of required quantity to find the water
content. The quantity of soil required is depends upon the maximum particle size and
gradation of soil sample. Below table shows the soil quantity required for test based on
the sieve analysis.

Table 1: Minimum Quantity of Soil Required for Water Content Determination

Size of particles more than 90% of passing Minimum Quantity ( grams)

425 micron sieve 25

2 mm sieve 50
4.25 mm sieve 200

10 mm sieve 300

20 mm sieve 500

40 mm sieve 1000

Fig 1: Wet Soil Sample

Test Procedure of Oven Dry Method


The test procedure of Oven Dry method to find the moisture content of soil consists
following steps.

 In first step, clean and dry the containers and weigh them and note down the mass of each
container (M1). Also note down the number of each container along with its weight.
 Collect the soil sample from field. Remove the top layer of soil and collect the wet soil from
bottom layers.

 Fill the containers with required quantity of soil sample and weigh the each container and
note down its mass (M2).
Fig 2: Placing Containers in Oven

 Place the containers in hot air oven, arrange temperature to 110 o ± 5o C and allow them to dry
for 24 hours.
 After 24 hours turn off the oven and take out the containers using tongs.

 Cool down the containers in desiccator for one hour.

 After that weigh containers and note down the mass (m 3) of each container.
Observations and Calculations of Oven Dry Method
The data collected during the test is noted in below data sheet. From this data the water
content of given soil sample is calculated by the below shown formula

Where     M1= Mass of empty container with lid,

M2= Mass of the container with wet soil and lid,

M3= Mass of the container with dry soil and lid.

Table 2: Observations and Calculations of Oven Dry Method


Determination No.
Sl. No. Observations and Calculations
1 2 3

Observation

1 Container No.

2 Mass of empty container (M1)

3 Mass of container + soil (M2)

4 Mass of container + dry soil (M3)

Calculations

5 Mass of water Mw= M2 – M3

6 Mass of solids, Ms= M3 – M1

7 Water content= (5)/(6)x100

Result of Oven Dry Method


Water content of the given soil sample = ______%.

2. Water Content of Soil by Pycnometer Method


Pycnometer method is also useful to determine water content. But this is used when the
specific gravity of the given soil sample is already known. However, Specific gravity can
also be determined using pycnometer.

Apparatus Required for Pycnometer Method


Apparatus used in pycnometer method are

 Pycnometer

 Weighing balance with an accuracy of 1.0g

 Glass rod
 Vacuum pump

Fig 3: Pycnometer Bottle

Test Procedure of Pycnometer Method


Test procedure of pycnometer method is as follows

 Wash, clean and dry the pycnometer and note down its mass (M 1) along with brass cap and
washer using weighing balance with an accuracy of 1.0 g.
 Now place a sample of wet soil about 200 to 400 g in pycnometer and note down its mass
(M2).
 Then add water to the soil in the pycnometer to make it about half full.

 Stir the soil using glass rod to remove air voids of the soil sample. If available connect the
vacuum pump to the soil specimen to remove entrapped air.

 Add some more water and after eliminating the entrapped air stop stirring and fix the brass
cap. More water is added through hole in brass cap until the water is flush with the hole.

 Now take the mass of pycnometer (M 3).


 Now empty and wash the pycnometer. Then fill it with only water and take its mass (M 4).
Observations and Calculations of Pycnometer Method
The water content (w) of the soil sample using pycnometer method is calculated from the
below formula

Where   M =mass of empty Pycnometer,


1

M = mass of the Pycnometer with wet soil


2

M = mass of the Pycnometer and soil, filled with water,


3

M  = mass of Pycnometer filled with water only.


4

G= Specific gravity of solids.

Table 2: Observations and Calculations of Pycnometer Method

Determination No.
Sl.
Observations and Calculations
No.
1 2 3

Observation

1 Mass of empty pycnometer (M1)

2 Mass of pycnometer + wet soil (M2)

Mass of Pycnometer soil filled with


3
water (M3)

Mass of Pycnometer filled with water


4
only (M4)

Calculations

5 M2 – M1

6 M3 – M4

7 (G – 1) / G
8 w (using above formula)

Result of Pycnometer Method


Water content of the given soil sample = _______%.

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