Instrument:ISQD1702517_1 Sequence:0430 Carrier Oil Page 1 of 3

KROMATOGRAM GCMS
LABORATORIUM PENELITIAN DAN PENGUJIAN TERPADU
UNIVERSITAS GADJAH MADA

No. Ret.Time Hit# 1 Chemical Formula

Mol. Weight
SI Hit#1 Hit# 2 Chemical Formula
Mol. WeightSI Hit#2 Hit# 3 Chemical Formula Mol. Weight SI Hit#3 Rel.Area Area
min min min counts*min counts*min % counts*min
1 6.74 Bicyclo[3.1.0]hex-2-ene, 4-methyl-1-(1-methylethyl)- C10H16 136 755 a-Pinene C10H16 136 752 Bicyclo[3.1.0]hex-2-ene, 2-methyl-5-(1-methylethyl)-
C10H16 136 746 0.02 105827.089
2 6.91 a-Pinene C10H16 136 919 3-Carene C10H16 136 905 Bicyclo[3.1.1]hept-2-ene, 3,6,6-trimethyl-
C10H16 136 898 0.19 865305.947
3 8.00 Z,Z,Z-1,4,6,9-Nonadecatetraene C19H32 260 690 Z,Z,Z-4,6,9-Nonadecatriene C19H34 262 685 Spiro[2.2]pentane-1-carboxylic
C10H14O2
acid, 2-cyclopropyl-2-methyl-
166 655 0.01 30619.169
4 8.08 ß-Pinene C10H16 136 760 Bicyclo[3.1.1]heptane, 6,6-dimethyl-2-methylene-,
C10H16 136 (1S)-750 Cyclohexane, 1-methylene-4-(1-methylethenyl)-
C10H16 136 748 0.02 98899.434
5 8.52 (R)-lavandulyl acetate C12H20O2 196 691 Spiro[2.2]pentane-1-carboxylicC10H14O2
acid, 2-cyclopropyl-2-methyl-
166 684 Z,Z,Z-4,6,9-NonadecatrieneC19H34 262 674 0.02 73815.432
6 8.74 trisiloxane, 1,1,1,5,5,5-hexamethyl-3-[(trimethylsilyl)oxy]- C9H28O3Si4 296 769 Cyclotetrasiloxane, octamethyl-
C8H24O4Si4 296 739 2,6-Dihydroxyacetophenone,
C14H24O3Si2
2TMS derivative 296 700 0.01 64481.478
7 8.88 Z,Z,Z-1,4,6,9-Nonadecatetraene C19H32 260 640 Z,Z,Z-4,6,9-Nonadecatriene C19H34 262 638 6,9,12-Octadecatrienoic acid,C25H36O2
phenylmethyl ester,
368(Z,Z,Z)- 617 0.01 61333.701
8 9.24 Cyclohexene, 1-methyl-4-(1-methylethylidene)- C10H16 136 921 1,3-Cyclohexadiene, 1-methyl-4-(1-methylethyl)-
C10H16 136 901 Cyclohexene, 4-methyl-3-(1-methylethylidene)-
C10H16 136 892 0.21 967105.814
9 9.48 o-Cymene C10H14 134 896 1,3,5-Cycloheptatriene, 3,7,7-trimethyl-
C10H14 134 867 Benzene, 1-methyl-3-(1-methylethyl)-
C10H14 134 862 0.13 617529.459
10 9.60 Cyclohexene, 1-methyl-5-(1-methylethenyl)-, (R)- C10H16 136 792 Cyclohexane, 1-methylene-4-(1-methylethenyl)-
C10H16 136 788 Bicyclo[2.2.1]heptane, 2,2-dimethyl-3-methylene-,
C10H16 136 (1R)- 770 0.05 215501.503
11 9.65 Eucalyptol C10H18O 154 878 Trifluoroacetyl-a-terpineol C12H17F3O2 250 829 5-Isopropyl-2-methylbicyclo[3.1.0]hexan-2-ol
C10H18O #154 782 0.11 507166.434
12 10.48 ?-Terpinene C10H16 136 936 3-Carene C10H16 136 883 Bicyclo[3.1.0]hex-2-ene, 2-methyl-5-(1-methylethyl)-
C10H16 136 869 0.81 3732185.602
13 11.34 Cyclohexene, 1-methyl-4-(1-methylethylidene)- C10H16 136 894 Cyclohexene, 3-methyl-6-(1-methylethylidene)-
C10H16 136 876 Cyclohexene, 4-methyl-3-(1-methylethylidene)-
C10H16 136 870 0.10 458765.853
14 13.32 Cyclopentasiloxane, decamethyl- C10H30O5Si5 370 854 2,6-Dihydroxybenzoic acid, 3TMS
C16H30O4Si3
derivative370 737 3,4-Dihydroxymandelic acid,C19H36O5Si3
ethyl ester, tri-TMS
428 724 0.07 307444.772
15 14.00 3-Cyclohexen-1-ol, 4-methyl-1-(1-methylethyl)-, (R)- C10H18O 154 913 Terpinen-4-ol C10H18O 154 911 5-Isopropyl-2-methylbicyclo[3.1.0]hexan-2-ol
C10H18O #154 826 1.53 7068856.508
16 14.43 a-Terpineol C10H18O 154 828 Terpineol C10H18O 154 817 exo-2,7,7-trimethylbicyclo[2.2.1]heptan-2-ol
C10H18O 154 776 0.15 712153.432
17 18.11 Cyclohexasiloxane, dodecamethyl- C12H36O6Si6 444 878 Cyclononasiloxane, octadecamethyl-
C18H54O9Si9666 590 Oxazepam, 2TMS derivativeC21H27ClN2O2Si2 430 568 0.14 640591.822
18 19.03 2,5-Dimethylhexane-2,5-dihydroperoxide C8H18O4 178 736 Hexane, 2,5-dimethoxy-2,5-dimethyl-
C10H22O2 174 646 2-Methyl-3-decanol C11H24O 172 640 0.16 742316.084
19 20.30 Patchoulene C15H24 204 729 ß-Guaiene C15H24 204 728 ß-copaene C15H24 204 727 0.02 73342.844
20 20.56 Bicyclo[7.2.0]undec-4-ene, 4,11,11-trimethyl-8-methylene-,[1R-(1R*,4Z,9S*)]-
C15H24 204 729 Bicyclo[7.2.0]undec-4-ene, 4,11,11-trimethyl-8-methylene-
C15H24 204 729 cis-a-Bisabolene C15H24 204 727 0.02 93786.355
21 21.06 Aromandendrene C15H24 204 808 (1R,9R,E)-4,11,11-Trimethyl-8-methylenebicyclo[7.2.0]undec-4-ene
C15H24 204 807 1H-Cycloprop[e]azulene, decahydro-1,1,7-trimethyl-4-methylene-
C15H24 204 804 0.05 235413.988
22 21.61 (1R,9R,E)-4,11,11-Trimethyl-8-methylenebicyclo[7.2.0]undec-4-ene
C15H24 204 758 Alloaromadendrene C15H24 204 758 Aromandendrene C15H24 204 758 0.02 104751.322
23 21.91 ß-copaene C15H24 204 702 ß-Guaiene C15H24 204 691 Cyclohexene, 6-ethenyl-6-methyl-1-(1-methylethyl)-3-(1-methylethylidene)-,
C15H24 204 680 (S)-0.01 62710.039
24 22.49 Cycloheptasiloxane, tetradecamethyl- C14H42O7Si7 518 723 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trimethylsiloxy)tetrasiloxane
C18H52O7Si7576 670 3-Butoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trimethylsiloxy)tetrasiloxane
C19H54O7Si7 590 657 0.16 718453.702
25 22.57 7-epi-cis-sesquisabinene hydrate C15H26O 222 668 a-ylangene C15H24 204 666 ß-copaene C15H24 204 666 0.01 38230.530
26 23.13 1-Isopropyl-4,7-dimethyl-1,2,3,5,6,8a-hexahydronaphthalene C15H24 204 818 Naphthalene, 1,2,3,5,6,8a-hexahydro-4,7-dimethyl-1-(1-methylethyl)-,
C15H24 204 803 .alfa.-Copaene
(1S-cis)- C15H24 204 784 0.08 353648.563
Chromeleon (c) Dionex
Screening - 3/Chromatogram Version 7.2.10.24543
Instrument:ISQD1702517_1 Sequence:0430 Carrier Oil Page 2 of 3

27 23.36 Naphthalene, 1,2,3,4,4a,7-hexahydro-1,6-dimethyl-4-(1-methylethyl)-

C15H24 204 661 a-ylangene C15H24 204 656 10,13-Octadecadiynoic acid, C19H30O2
methyl ester 290 651 0.01 47598.110
28 24.65 6,9,12,15-Docosatetraenoic acid, methyl ester C23H38O2 346 707 2H-Pyran, 2-(7-heptadecynyloxy)tetrahydro-
C22H40O2 336 704 1-Heptatriacotanol C37H76O 536 699 0.02 86264.444
29 24.86 10-Heptadecen-8-ynoic acid, methyl ester, (E)- C18H30O2 278 669 Ethyl iso-allocholate C26H44O5 436 657 2H-Pyran, 2-(7-heptadecynyloxy)tetrahydro-
C22H40O2 336 651 0.02 77747.190
30 25.63 7-epi-cis-sesquisabinene hydrate C15H26O 222 671 7-epi-trans-sesquisabinene hydrate
C15H26O 222 666 a-acorenol C15H26O 222 659 0.01 45938.702
31 26.44 Cyclooctasiloxane, hexadecamethyl- C16H48O8Si8 592 810 Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15-hexadecamethyl-
C16H50O7Si8578 645 2,6-Dihydroxybenzoic acid, 3TMS
C16H30O4Si3
derivative 370 632 0.06 264357.941
32 27.10 Tetradecane, 2,6,10-trimethyl- C17H36 240 648 Octadecane, 6-methyl- C19H40 268 645 2-Myristynoyl pantetheine C25H44N2O5S 484 642 0.01 48112.403
33 29.33 Tetradecane, 2,6,10-trimethyl- C17H36 240 670 Octadecane, 3-ethyl-5-(2-ethylbutyl)-
C26H54 366 665 Octadecane, 6-methyl- C19H40 268 664 0.02 75855.971
34 29.44 Tetradecane, 2,6,10-trimethyl- C17H36 240 735 Heptadecane, 2,6,10,15-tetramethyl-
C21H44 296 714 Octadecane, 6-methyl- C19H40 268 705 0.03 151156.597
35 29.86 Cyclononasiloxane, octadecamethyl- C18H54O9Si9 666 797 Tetracosamethyl-cyclododecasiloxane
C24H72O12Si12
888 672 Cyclohexasiloxane, dodecamethyl-
C12H36O6Si6 444 671 0.04 189434.373
36 30.96 5,6,6-Trimethyl-5-(3-oxobut-1-enyl)-1-oxaspiro[2.5]octan-4-one
C14H20O3 236 667 E,E,Z-1,3,12-Nonadecatriene-5,14-diol
C19H34O2 294 662 Ethanol, 2-(9,12-octadecadienyloxy)-,
C20H38O2(Z,Z)- 310 662 0.04 173362.188
37 31.08 Ethyl iso-allocholate C26H44O5 436 647 9,12,15-Octadecatrienoic acid, 2,3-dihydroxypropyl
C21H36O4 352 ester,
640(Z,Z,Z)-
E,E,Z-1,3,12-Nonadecatriene-5,14-diol
C19H34O2 294 639 0.02 83656.260
38 31.38 17.alfa.,21ß-28,30-Bisnorhopane C28H48 384 656 Ethyl iso-allocholate C26H44O5 436 655 Cyclopropaneoctanoic acid,C22H38O2
2-[[2-[(2-ethylcyclopropyl)methyl]cyclopropyl]methyl]-,
334 631 0.01 methyl ester
38274.454
39 31.47 7-Methyl-Z-tetradecen-1-ol acetate C17H32O2 268 670 Octadecane, 3-ethyl-5-(2-ethylbutyl)-
C26H54 366 662 2-Myristynoyl pantetheine C25H44N2O5S 484 656 0.03 116166.047
40 31.61 E-11-Methyl-12-tetradecen-1-ol acetate C17H32O2 268 717 Z-8-Methyl-9-tetradecen-1-ol C17H32O2
acetate 268 701 Spiro[4.5]decan-7-one, 1,8-dimethyl-8,9-epoxy-4-isopropyl-
C15H24O2 236 694 0.03 142329.735
41 32.04 1b,4a-Epoxy-2H-cyclopenta[3,4]cyclopropa[8,9]cycloundec[1,2-b]oxiren-5(1aH)-one,
C28H38O11 550 2,7,9,10-tetrakis(acetyloxy)decahydro-3,6,8,8,10a-pentamethyl-
639 Ethyl iso-allocholate C26H44O5 436 638 12-Methyl-E,E-2,13-octadecadien-1-ol
C19H36O 280 625 0.01 63210.227
42 32.28 17.alfa.,21ß-28,30-Bisnorhopane C28H48 384 656 Ethanol, 2-(9,12-octadecadienyloxy)-,
C20H38O2 (Z,Z)-310 636 Linolenic acid, 2-hydroxy-1-(hydroxymethyl)ethyl
C21H36O4 352 ester (Z,Z,Z)- 629 0.02 90788.768
43 32.36 17.alfa.,21ß-28,30-Bisnorhopane C28H48 384 660 2,2,4-Trimethyl-3-(3,8,12,16-tetramethyl-heptadeca-3,7,11,15-tetraenyl)-cyclohexanol
C30H52O 428 643 2-Methyl-E,E-3,13-octadecadien-1-ol
C19H36O 280 636 0.01 64420.708
44 32.74 E-11-Hexadecenoic acid, ethyl ester C18H34O2 282 845 Ethyl 9-hexadecenoate C18H34O2 282 821 Palmitoleic acid C16H30O2 254 802 0.19 900252.006
45 32.91 Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15-hexadecamethyl- C16H50O7Si8 578 674 Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tetradecamethyl-
C14H44O6Si7504 661 Hexasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11-dodecamethyl-
C12H38O5Si6 430 645 0.05 246972.497
46 33.16 Hexadecanoic acid, ethyl ester C18H36O2 284 792 Nonadecanoic acid, ethyl esterC21H42O2 326 736 Heptadecanoic acid, ethyl ester
C19H38O2 298 735 0.28 1311305.835
47 34.41 Ethyl iso-allocholate C26H44O5 436 659 Cucurbitacin b, 25-desacetoxy-C30H44O6 500 627 Tricyclo[20.8.0.0(7,16)]triacontane,
C30H52O21(22),7(16)-diepoxy-
444 624 0.02 70211.324
48 35.09 Octadecane, 3-ethyl-5-(2-ethylbutyl)- C26H54 366 654 Ethyl iso-allocholate C26H44O5 436 644 Tetradecane, 2,6,10-trimethyl-
C17H36 240 629 0.03 142631.536
49 35.72 Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15-hexadecamethyl- C16H50O7Si8 578 681 Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tetradecamethyl-
C14H44O6Si7504 677 Hexasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11-dodecamethyl-
C12H38O5Si6 430 615 0.03 127168.016
50 36.23 9,12,15-Octadecatrienoic acid, 2,3-dihydroxypropyl ester, (Z,Z,Z)-
C21H36O4 352 692 Linoleic acid ethyl ester C20H36O2 308 686 Ethyl iso-allocholate C26H44O5 436 682 0.04 165464.534
51 36.34 (E)-9-Octadecenoic acid ethyl ester C20H38O2 310 795 n-Propyl 11-octadecenoate C21H40O2 324 777 cis-Vaccenic acid C18H34O2 282 777 0.19 860257.400
52 36.44 trans-9-Octadecenoic acid, pentyl ester C23H44O2 352 715 (E)-9-Octadecenoic acid ethylC20H38O2
ester 310 712 cis-Vaccenic acid C18H34O2 282 709 0.09 432933.091
53 36.80 Ethyl iso-allocholate C26H44O5 436 630 Ergosta-5,22-dien-3-ol, acetate,
C30H48O2
(3ß,22E)- 440 608 9,10-Secocholesta-5,7,10(19)-triene-3,24,25-triol,
C27H44O3 416
(3ß,5Z,7E)- 600 0.01 31763.711
54 36.88 Ethyl iso-allocholate C26H44O5 436 671 Cholestan-3-one, cyclic 1,2-ethanediyl
C29H50O2aetal,430
(5ß)- 654 9,10-Secocholesta-5,7,10(19)-triene-3,24,25-triol,
C27H44O3 416
(3ß,5Z,7E)- 633 0.02 76400.059
55 37.25 Stigmastane C29H52 400 671 Ethyl iso-allocholate C26H44O5 436 630 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 587 0.06 diacetate 293813.669
56 37.35 Ethyl iso-allocholate C26H44O5 436 671 Stigmastane C29H52 400 661 1-Heptatriacotanol C37H76O 536 622 0.06 275564.807
57 37.45 Ethyl iso-allocholate C26H44O5 436 683 Oleic acid, 3-(octadecyloxy)propyl
C39H76O3
ester 592 652 Octadecane, 3-ethyl-5-(2-ethylbutyl)-
C26H54 366 641 0.09 410286.777
58 38.14 Ethyl iso-allocholate C26H44O5 436 637 Spirost-8-en-11-one, 3-hydroxy-,
C27H40O4
(3ß,5a,14ß,20ß,22ß,25R)-
428 630 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 615 0.01diacetate 52017.193
59 38.28 Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15-hexadecamethyl- C16H50O7Si8 578 661 Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tetradecamethyl-
C14H44O6Si7504 643 Propanoic acid, 2-(3-acetoxy-4,4,14-trimethylandrost-8-en-17-yl)-
C27H42O4 430 616 0.05 234530.519
60 38.58 Octadecane, 3-ethyl-5-(2-ethylbutyl)- C26H54 366 708 Ethanol, 2-(octadecyloxy)- C20H42O2 314 691 Z-5-Methyl-6-heneicosen-11-one
C22H42O 322 685 0.13 601632.070
61 39.14 Ethyl iso-allocholate C26H44O5 436 675 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 643 Spirost-8-en-11-one, 3-hydroxy-,
diacetate
C27H40O4
(3ß,5a,14ß,20ß,22ß,25R)-
428 641 0.06 256329.127
62 40.00 Ethyl iso-allocholate C26H44O5 436 628 8,14-Seco-3,19-epoxyandrostane-8,14-dione,
C24H36O6 420 17-acetoxy-3ß-methoxy-4,4-dimethyl-
599 Spirost-8-en-11-one, 3-hydroxy-,
C27H40O4
(3ß,5a,14ß,20ß,22ß,25R)-
428 597 0.01 66747.976
63 40.22 Cholestan-3-one, cyclic 1,2-ethanediyl aetal, (5ß)- C29H50O2 430 642 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 634 Stearic acid, 3-(octadecyloxy)propyl
diacetate
C39H78O3 ester 594 621 0.04 177426.763
64 40.67 Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15-hexadecamethyl- C16H50O7Si8 578 674 Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tetradecamethyl-
C14H44O6Si7504 653 Hexasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11-dodecamethyl-
C12H38O5Si6 430 641 0.02 88956.618
65 40.76 Ethyl iso-allocholate C26H44O5 436 631 Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15-hexadecamethyl-
C16H50O7Si8578 589 3-Pyridinecarboxylic acid, 2,7,10-tris(acetyloxy)-1,1a,2,3,4,6,7,10,11,11a-decahydro-1,1,3,6,9-pentamethyl-4-oxo-4a,7a-epoxy-5H-cyclopenta[a]cyclopropa[f]cy
C32H39NO10 597 587 0.03 140156.007
66 41.53 Ethyl iso-allocholate C26H44O5 436 646 Acetic acid, 17-acetoxy-4,4,10,13-tetramethyl-7-oxo-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl
C25H36O5 416 614 Spirost-8-en-11-one, 3-hydroxy-,C27H40O4
(3ß,5a,14ß,20ß,22ß,25R)-
428 607 (ester) 0.02 108253.550
67 41.61 Glycidyl oleate C21H38O3 338 708 Ethyl iso-allocholate C26H44O5 436 694 9-Octadecenoic acid, (2-phenyl-1,3-dioxolan-4-yl)methyl
C28H44O4 444 ester, cis-643 0.16 721013.073
68 42.03 Oleic acid, 3-(octadecyloxy)propyl ester C39H76O3 592 665 Octadecane, 3-ethyl-5-(2-ethylbutyl)-
C26H54 366 663 Octadecane, 1,1'-[(1-methyl-1,2-ethanediyl)bis(oxy)]bis-
C39H80O2 580 659 0.18 834429.934
69 43.05 Ethyl iso-allocholate C26H44O5 436 607 Methyl glycocholate, 3TMS derivative
C36H69NO6Si3
695 583 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 571 0.10diacetate 480870.094
70 43.57 Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,15-hexadecamethyl- C16H50O7Si8 578 636 Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tetradecamethyl-
C14H44O6Si7504 625 Hexasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11-dodecamethyl-
C12H38O5Si6 430 612 0.03 132305.885
71 43.98 8,14-Seco-3,19-epoxyandrostane-8,14-dione, 17-acetoxy-3ß-methoxy-4,4-dimethyl-
C24H36O6 420 639 Spirost-8-en-11-one, 3-hydroxy-,
C27H40O4
(3ß,5a,14ß,20ß,22ß,25R)-
428 613 Cholestan-3-one, cyclic 1,2-ethanediyl
C29H50O2aetal, (5ß)-
430 612 0.10 441138.717
72 44.29 Ethyl iso-allocholate C26H44O5 436 642 Methyl glycocholate, 3TMS derivative
C36H69NO6Si3
695 612 7,8-Epoxylanostan-11-ol, 3-acetoxy-
C32H54O4 502 610 0.03 121332.963
73 44.66 Ethyl iso-allocholate C26H44O5 436 643 Methyl glycocholate, 3TMS derivative
C36H69NO6Si3
695 628 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 625 0.05diacetate 211799.177
74 45.19 Oleic acid, 3-(octadecyloxy)propyl ester C39H76O3 592 626 Cholestan-3-one, cyclic 1,2-ethanediyl
C29H50O2aetal,430
(5ß)- 617 17-Pentatriacontene C35H70 490 617 0.09 414747.397
75 45.55 17-Pentatriacontene C35H70 490 655 Oleic acid, 3-(octadecyloxy)propyl
C39H76O3
ester 592 651 Tetrapentacontane, 1,54-dibromo-
C54H108Br2 914 641 0.14 630958.449
76 45.90 Squalane C30H62 422 894 Pentadecane, 2,6,10,14-tetramethyl-
C19H40 268 845 Tetracosane C24H50 338 837 90.13 417508530.672
77 46.33 Tetrapentacontane, 1,54-dibromo- C54H108Br2 914 715 Octadecane, 3-ethyl-5-(2-ethylbutyl)-
C26H54 366 707 Triacontane, 1-bromo- C30H61Br 500 695 0.09 424374.457
78 46.37 Octadecane, 3-ethyl-5-(2-ethylbutyl)- C26H54 366 701 17-Pentatriacontene C35H70 490 695 Tetrapentacontane, 1,54-dibromo-
C54H108Br2 914 692 0.01 27708.239
79 46.52 17-Pentatriacontene C35H70 490 718 Tetrapentacontane, 1,54-dibromo-
C54H108Br2 914 716 Octatriacontyl pentafluoropropionate
C41H77F5O2 696 714 0.32 1487148.905
80 46.85 Tetrapentacontane, 1,54-dibromo- C54H108Br2 914 666 17-Pentatriacontene C35H70 490 655 Oleic acid, 3-(octadecyloxy)propyl
C39H76O3
ester 592 647 0.09 431479.204
81 47.13 Tetrapentacontane, 1,54-dibromo- C54H108Br2 914 662 17-Pentatriacontene C35H70 490 646 Oleic acid, 3-(octadecyloxy)propyl
C39H76O3
ester 592 641 0.06 290623.151
82 47.34 Tetrapentacontane, 1,54-dibromo- C54H108Br2 914 659 17-Pentatriacontene C35H70 490 659 Oleic acid, 3-(octadecyloxy)propyl
C39H76O3
ester 592 654 0.11 505083.882
83 48.18 17-Pentatriacontene C35H70 490 712 Tetrapentacontane, 1,54-dibromo-
C54H108Br2 914 704 Octatriacontyl pentafluoropropionate
C41H77F5O2 696 702 0.45 2096418.588
84 48.26 Tetrapentacontane, 1,54-dibromo- C54H108Br2 914 719 17-Pentatriacontene C35H70 490 713 Pentyl triacontyl ether C35H72O 508 704 1.39 6452702.800

Chromeleon (c) Dionex

Screening - 3/Chromatogram Version 7.2.10.24543
Instrument:ISQD1702517_1 Sequence:0430 Carrier Oil Page 3 of 3

85 49.46 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,

C28H43NO6 489 diacetate
632 Cholestan-3-one, cyclic 1,2-ethanediyl
C29H50O2aetal,430
(5ß)- 629 Oleic acid, 3-(octadecyloxy)propyl
C39H76O3
ester 592 620 0.15 700813.859
86 50.36 Ethyl iso-allocholate C26H44O5 436 610 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 610 7,8-Epoxylanostan-11-ol,
diacetate
3-acetoxy-
C32H54O4 502 605 0.04 171627.850
87 51.35 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 diacetate
624 Spirost-8-en-11-one, 3-hydroxy-,
C27H40O4
(3ß,5a,14ß,20ß,22ß,25R)-
428 594 Cholestan-3-one, cyclic 1,2-ethanediyl
C29H50O2aetal, (5ß)-
430 589 0.16 723349.614
88 51.97 Ethyl iso-allocholate C26H44O5 436 640 (5ß)Pregnane-3,20ß-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4-diyl)]-,
C28H43NO6 489 618 Spirost-8-en-11-one, 3-hydroxy-,
diacetate
C27H40O4
(3ß,5a,14ß,20ß,22ß,25R)-
428 617 0.14 662441.451
Total: 463250884.445

Chromeleon (c) Dionex

Screening - 3/Chromatogram Version 7.2.10.24543