International Journal of Pure and Applied Mathematic s

Volume 119 No. 15 2018, 2063-2078

ISSN: 1314-3395 (on-line version)
url: http://www.acadpubl.eu/hub/
Special Issue
http://www.acadpubl.eu/hub/

ENHANCEMENT OF MECHANICAL PROPERTIES OF ALUMINIUM 6061 METAL MATRIX COMPOSITE

1 Ajith kumar.R , 2 Chandan singh M, 3 Nagasaravanan A and Thiruchitrambaam M 4

1,2,3,4Department of Mechanical engineering, VEL TECH MULTITECH, Chennai 62,India

email id: [email protected] , [email protected],

[email protected]

Abstract—The mechanical properties of aluminium alloys were studied and analyzed. In this research, we have
prepared aluminium metal matrix composites in which aluminium is the base metal and graphite powder and
titanium dioxide powder are the reinforcement materials. The aluminium metal matrix composites were
manufactured by using stir casting method. The cast aluminium metal matrix composites were machined to the
required dimensions for testing. After that, mechanical tests were conducted on the composites prepared. The
tests carried out are tensile test, hardness test and optical microscopy. The test results were studied and
analyzed. The changes in the mechanical properties of the prepared composites were briefly discussed in this
paper. Finally, we have concluded that aluminium metal matrix composites can replace aluminium alloys in
many applications. There is a great scope and opportunity for research in the area of prediction on tribological
and mechanical properties of the aluminium alloys by reinforcing with different material reinforcements.

Keywords—Aluminium alloys, metal matrix composites, base metal, reinforcement materials, stir casting, mechanical
testing

I.INTRODUCTION

Normally, conventional alloy materials have some problems in achieving a good combination of
mechanical properties such as strength, hardness, toughness, stiffness, density and other inevitable
mechanical properties. To overcome this limitation, composite materials are developed. A composite
material is a combination of two or more materials and the composite materials exhibit the properties
of both the materials.

A metal matrix composite otherwise called as MMC is also a composite material with two or more
constituent parts. One must be a metal necessarily and the other one may be a different metal or
another material. If more than two materials present in a composite, then it is known as a hybrid

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composite. This research is an attempt to test and analyze the mechanical properties of 6061 Aluminium
alloy reinforced with 3%, 8%, 13% of TiO2 and 2% of Graphite weight particles respectively.

Aluminium 6061 alloy is an alloy which is precipitation- hardened. It contains magnesium and
silicon as its important alloying constituents. It has comparatively good mechanical properties and
exhibits good machinability and it is one of the most common alloys of aluminium for general purpose
use. The aluminium alloy which can be easily worked is aluminium 6061 and it also remains resistant to
corrosion even when the surface is abraded.

Initially, the material on which the metal matrix composites are going to be prepared is selected. The
identified material is aluminium 6061 alloy. After this step, the reinforcement materials and their
compositions are decided. Graphite powder and Titanium dioxide powder are the reinforcement
materials selected to improve the mechanical properties of a normal aluminium 6061 alloy. The
different compositions of those reinforcement materials give slight differences in their mechanical
properties. Here, aluminium 6061 alloy is the base metal or metal matrix wherein the reinforcements
are going to be made.

The metal matrix composites were prepared using stir casting method. The reinforcement materials are
mixed up with molten aluminium alloy and stirred well for complete mixing. Then the molten mixture is
poured into the mould cavity and allowed to solidify to get the aluminium metal matrix composite.

After the preparation of those aluminium metal matrix composites, mechanical tests are done on those
samples to ensure the improvement in its mechanical properties and their results are discussed in this
research.

II LITRATURE SURVEY

In the review [1] by B.Balamugundan et al ., the authors compared the mechanical properties before
and after heat treatment of various aluminium alloys

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A survey by G.Sivakaruna and Dr. P.Suresh Babu[2] have written a review on the effects of
reinforcement on Aluminium metal matrix composites and observed that as the % of reinforcement
increased the mechanical properties improved and also wear resistance improved.

Gowrishankar T P, and co authors[3] reviewed the manufacturing methods and mechanical properties
of various aluminium matrix composites. By selecting suitable values of process parameters such as
stirring speed, pouring temperature, etc. good quality composites can be made. By using graphite,
friction can be reduced and also the machinability can be improved.

Ganesh Khandoori, et al [4] reorted that by adding TiO2 the wear resistance can be improved
significantly during sliding wear. The wear rate at high normal loads decreased to large extent in
comparison to base aluminium alloy. G.Baskaran et al [5] observed that by increasing TiO2 and TiC
content hardness, and wear rate increased. Maninder Singh, et al [6] fabricated composite using
aluminium 6061 and silicon oxide/titanium oxide . The composites were better than the base alloy in all
aspects. Niranjan K N [7] reported about the preparation and characterization of Al 6061 hybrid
composite. The decrease in hardness of Al 6061 hybrid composite is likely because of poor wetting
characteristics of Al 6061 on graphite. It was observed by them ,that the compressive strength increased
as the SiC and graphite content increased.

G.S. Kataiah[8] concluded that in the case of cast Al 6061 alloy/ TiO 2 particulate composites the
mechanical properties improved significantly. It was found that by increasing TiO2 the hardness, tensile
strength and Impact strength can be improved.

Padmavathi.K.R and Ramakrishnan[9] fabricated Al6061 based composites by reinforcing with micro
TiO2 and nano TiO2 by stir casting method. Al6061 - nano TiO2 composites exhibited superior wear
properties in comparison to Al6061-micro TiO2 composites.

Himanshu Kala et al [10] have written a review on the tribological aspects and mechanical properties of
Al matrix composites made by stir casting method. They found that by adding graphite the tensile
properties improved but the hardness decreased.

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III METHODOLOGY

The methodology which has been followed in our research is represented in this flow chart.

Material Identification

Selection of reinforcement materials

Collection of raw materials

Fabrication of composite material

Mechanical testing

Results and discussion

IV. PREPARATION OF Al 6061 MMC BY STIR CASTING

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The stir casting setup was prepared initially. The Aluminium 6061 alloy + 2% graphite powder with 3%,
8%, 13% TiO2 powder respectively were prepared by stir casting technique wherein aluminium is the
matrix and graphite powder + TiO2 powder is the reinforcement.

Step 1: Melting of base metal Al 6061in furnace

First of all, Al 6061 was melted in a crucible placed inside the pit furnace as shown in the figure below.
Aluminium starts melting at around 650˚C.

Step 2: Addition of graphite powder and TiO2 powder into molten Al

Into the molten matrix, 2% (by weight) graphite powder was added. 3%, 8%, 13% TiO2 powder were also
added and three different compositions of molten metal were prepared.

Step 3: Stirring of the Al + graphite + TiO2 mixture

First of all, a stirrer was made out of 100mm length and 25mm diameter for stirring. External threading
was done on the stirrer and an internally threaded 3 feet long stainless steel rod was fitted over this
stirrer. The mixture was mechanically stirred using a motor of around 300 rpm for 10 minutes before
pouring into the mould.

Step 4: Pouring of molten metal mixture into the mould and solidifying

Melting of base metal Al

6061in furnace

Addition of graphite powder and

TiO2 powder into molten Al

Stirring of Al + graphite + TiO 2 mixture

Pouring of molten metal mixture

into the mould and solidifying

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The mixture was poured into the mould and allowed to solidify for some time. The final cast specimens
were taken out and allowed to cool.

Fig.1 Sand mould

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V CHARACTERIZATION OF ALUMINIUM 6061 MMCs

The tests conducted on the metal composites are:

 Tensile test
 Hardness test
 Microstructure test

A.TENSILE TEST:

The tensile test specimens should be prepared initially from the cast aluminium metal matrix
composites. The test pieces were prepared as per universal standards. The standard test method which
is being commonly used for tensile testing of aluminium alloys is ASTM B557M.

B.BRINELL HARDNESS TEST:

Initially, the surface of the specimen to be tested is cleaned and polished. The specimen is fitted in the
sample holder. Once the sample is fitted, the ball indenter is forced to penetrate the surface MMC
specimen. The diameter of the ball indentation is measured and the mean of the three readings are
taken into consideration. The Brinell hardness number is calculated using the diameter of indenter and
diameter indentation as follows:

BHN = F/ 𝝅𝝅 ∗ √(D2-(Di)2)

where, F - Applied force or load = 250 kg D - Indenter diameter = 5 mm

D1 - Indentation diameter

C. MICROSTRUCTURAL TEST

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Scanning Electron Microscopes (SEMs) are used for higher magnifications and they are utilized for highly
detailed micro structural study. The surface of the specimen should be cleaned and polished well before
doing micro structural analysis. First, polish the surface of the specimen where the micro structural
images were taken. Hydrofluoric acid (HF) was used as an etchant in this process.

VI RESULTS AND DISCUSSION

Table 1 - Tensile test results

Observed values

Test
parameter Al Al 6061 Al 6061 Al 6061 Al 6061
6061 +2% +2% +2% +2%
Graphite Graphite+ Graphite Graphite+
3%TiO2 +8%TiO2 13%TiO2

Yield 48 52 80 79 83
strength
(N/mm2 or
MPa)

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Ultimate 93 93 115 115 119

Tensile
strength
(MPa)

% 11.0 8.5 4.50 3.50 3.50

Elongation
in 50mm
GL

Figure 2 - Brinell hardness test results

Observed values

Test Al6061 Al6061 Al6061

+2% +2% +2%
Obs
Al Al 6061 Graphite Graphite Graphite
6061 +2% + + +
Graphite 3% TiO2 8%TiO2 13%TiO2

BHN 1 37.1 38.1 53.8 54.8 55.3

(5 mm
Ball / 2 35.8 37.1 54.8 55.8 55.8

250 kg
3 36.5 37.7 54.8 54.8 53.8
load)

While comparing aluminium 6061 and aluminium 6061+2% graphite, there is an increase in the yield
strength of graphite added composite but the ultimate tensile strength does not have much variation in
its value. It is clearly seen from the above results that the yield strength of metal matrix composite
increases initially with the addition of 3% TiO2 and then decreases slightly and again increasing with
higher weight percentage of TiO2, while graphite reinforcement remains the same 2% by weight. Yield
strength of this composite material is greater when compared to the aluminium alloy Al 6061, with yield

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strength of 48 MPa. Similarly, Ultimate Tensile Strength (UTS) of the prepared metal composite is
greater than that of Al 6061 whose ultimate tensile strength is 93 MPa and it is also steadily increasing
with increase in percentage composition. The percentage of elongation at break is decreasing with
increase in the percentage reinforcement.

Initially, aluminium 6061 and aluminium 6061+2% graphite were tested and compared. While adding
graphite, hardness value of the composite material is increasing clearly. Then, three observations were
made for each composition of Al+graphite+TiO2. It is clearly seen that the hardness value of the

Fig.2 Tensile test samples

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Fig.3 Brinell hardness test samples

composite is steadily increasing as 53.8 BHN for first composition, 54.8 BHN for second composition and
55.8 for the third composition. The BHN for Al 6061 is 36.5 BHN but the composite material prepared
has higher hardness value.

MICROSTRUCTURAL IMAGES

Fig.4 Micro structural view of Al 6061

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Fig.5 Micro structural view of Al 6061+2% Graphite

Fig.6 Micro structural view of Al 6061+2% Graphite+3%TiO2

Fig.7 Micro structural view of Al 6061+2% Graphite+8%TiO2

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Fig.8 Micro structural view of Al 6061+2% Graphite+13%TiO2

The microstructure images for four different compositions of composite material are taken with
100x and 500x magnification. It is clearly known from the above images that there is an
improvement in its structure and reinforcement causes close bonding of grains within the structure.
The uniform distribution of graphite and TiO2 particles can also be seen in this microstructural view.
This shows that mechanical property increases with the increase in percentage of reinforcement.
Hence, these composite materials can replace Al 6061 aluminium alloy in many applications.

VII CONCLUSION

Aluminium metal matrix composites with reinforcements such as graphite and TiO2 with
different compositions were prepared and tested successfully. The test results were analyzed and
discussed. They show enhanced mechanical properties than that of the Al 6061 aluminium
alloy.The yield strength of aluminium 6061 was found as 48 MPa while testing. When 2% graphite
was added, its yield strength was increased by 8.33% that is 52 MPa. When 3% TiO2 is added
along with Al 6061+2% graphite, its yield strength was increased by 66.67% that is 80 MPa. With
8% TiO2, its yield strength was increased by 64.60% that is 79 MPa and with 13% TiO2, its yield
strength was increased by 72.92% that is 83 MPa.

The Ultimate tensile strength of base metal was found to be 93 MPa while testing. Addition of 2%
graphite has not shown any significant change in the ultimate tensile strength. But when 3% TiO2
was reinforced with Al 6061+2% graphite, its ultimate tensile strength was increased by 23.65%
that is 115 MPa and with 8% TiO2, it has shown the same result. When 13% TiO2 was added, its
tensile strength was increased by 27.96% that is 119 MPa.

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The hardness value of aluminium 6061 was obtained as 36.5 BHN while testing. Its hardness value
was increased by 3.01% that is 37.6 BHN when 2% graphite was reinforced with it. Its hardness value
was increased by 49.32% that is 54.5 BHN when 3% TiO2 was added with Al 6061+2% graphite. With
8% TiO2, its hardness value was increased by 50.96% that is 55.1 BHN and with 13% TiO2, its
hardness value was increased by 51.51% that is 55.3 BHN.

Microstructural images were also clearly analysed and the effects of reinforcements such as
graphite and TiO2 were also discussed.

REFERENCES

[1] G.Sivakaruna and Dr. P.Suresh Babu, “A survey on effects of reinforcement on

Aluminium metal matrix composites”, International Journal of Mechanical Engineering
and Technology (IJMET), volume no.8, pp.112–131, 2017.

[2] B.Balamugundan, L.Karthikeyan, K.Karthik, C.Keerthi, “Enhancement of mechanical

properties on aluminium alloys – A review”, IOSR Journal of Mechanical and Civil
Engineering (IOSR-JMCE), pp.2320–3340, 2017.

[3] Gowrishankar T P, Manjunath L, Jegadeeswaran N “The Properties of an Aluminium

Metal Matrix Composite - A review”, International Journal of Advances in Scientific
Research and Engineering (IJASRE), volume no.3, 2017.

[4] Ganesh Khandoori, Dr. K.K.S Mer and Chandraveer Singh, “Sliding behaviour of
Aluminium metal matrix composite reinforced with Titanium oxide” International
Journal of Recent Scientific Research, volume no.6, pp.4197-4203, 2015.

[5] G.Baskaran, I.Daniel Lawrence, C.Ramesh Kannan, B.Stalin, “Characterization of

Aluminium Based Metal Matrix Composite Reinforced with TiC and TiO2” International
Journal of Applied Engineering Research, volume no.10, pp.51, 2015.

[6] Maninder Singh, Khushdeep Goyal, Deepak Kumar Goyal, “Fabrication and
Performance of Aluminium Based Metal Matrix Composites with SiO2 and TiO2 as
Reinforced Particles”, Universal Journal of Mechanical Engineering, pp.142-146, 2015.

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[7] Niranjan K N, Shivaraj B N, Sunil kumar M, Deepak A R, “Study of Mechanical

Properties on Aluminium 6061 hybrid composite by stir casting method” International
Research Journal of Engineering and Technology (IRJET), volume no.4, 2017.

[8]G.S. Kataiah, Dr.D.P.Girish “The mechanical properties of aluminium 6061 - TiO2

composites” International Journal of Innovative Research and Development (Special
Issue) volume no.5, 2016.
[9] Padmavathi.K.R,Dr.R.Ramakrishnan, “Tribological behaviour of Aluminium Hybrid Metal
Matrix Composite”, Elsevier publications, pp.660-667, 2014.
[10] Himanshu Kala, K.K.S Mer, Sandeep Kumar, “A Review on Mechanical and Tribological
Behaviors of Stir Cast Aluminium Matrix Composites”, Science direct, pp.1951-1960, 2014.

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