OREAS 603 DataPack

Table 1.
Abbreviations used for OREAS 603
Abbreviation
Std.Dev.
Rel.Std.Dev.
PDM3
NR
<
Method Codes:
4A*AAS
4A*MS
4A*OES
4A*OES/AAS
4A*OES/MS
AD*AAS
AR*AAS
AR*MS
AR*OES
AR*OES/AAS
AR*OES/MS
FA*AAS
FA*GRAV
FA*OES
INAA
IRC
PF*MS
PF*OES
Legend:-
Individual
Batch & Limits

Table 1. Abbreviations used for OREAS 603
Explanation
one sigma standard deviation

one sigma relative standard deviation
percent deviation of lab mean from corrected mean of means
not reported
‘less than’
4-acid (HF-HNO3-HClO4-HCl) digest with AAS finish

4-acid (HF-HNO3-HClO4-HCl) digest with ICP-MS finish
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-OES finish
4-acid (HF-HNO3-HClO4-HCl) digest with either AAS or ICP-OES finish as appropriate
4-acid (HF-HNO3-HClO4-HCl) digest with ICP-OES or ICP-MS finish as appropriate
acid digest (non-specific) with AAS finish
aqua regia digest with AAS finish
aqua regia digest with ICP-MS finish
aqua regia digest with ICP-OES finish
ore grade aqua regia digest with either AAS or ICP-OES finish as appropriate
aqua regia digest with ICP-OES or ICP-MS finish as appropriate
fire assay with AAS finish
fire assay with gravimetric finish
fire assay with ICP-OES finish
INAA using a charge weight as deemed appropriate
infrared combustion furnace
sodium peroxide fusion with ICP-MS finish
sodium peroxide fusion with ICP-OES finish
(for Method Group Tabulated Results omitted in the determination of Certified Values)
- Outlying individual values
- Outlying laboratory batch data sets and superfluous limit values

NB. Formatted area for below table ends at row 46 inclusive, allowing for 40 maximum potential laboratories
Table 5. Participating Laboratory List used for OREAS 603
Lab Slot
1.21
1.23
2.01
1.20
1.06
1.05
1.03
1.08
1.04
1.07
1.24
1.27
1.25
1.26
1.11
1.12
1.02
1.14
1.09
1.15
1.22
1.01
1.16
1.18
1.19
1.17
1.13
1.10
tted area for below table ends at row 46 inclusive, allowing for 40 maximum potential laboratories.
Table 5. Participating Laboratory List used for OREAS 603
Laboratory Name and Location
Accurassay, Thunder Bay, Ontario, Canada

Acme (BV), Santiago, Chile
Actlabs, Ancaster, Ontario, Canada
AH Knight, Spartanburg, SC, USA
ALS, Johannesburg, South Africa
ALS, Lima, Peru
ALS, Reno, Nevada, USA
ALS, Townsville, QLD, Australia
ALS, Val-d'or, Quebec, Canada
ALS, Vancouver, BC, Canada
Bureau Veritas Geoanalytical, Adelaide, SA, Australia
Bureau Veritas Geoanalytical, Kalgoorlie, WA, Australia
Bureau Veritas Geoanalytical, Perth, WA, Australia
Bureau Veritas Kalassay, Kalgoorlie, WA, Australia
Inspectorate (BV), Lima, Peru
Inspectorate (BV), Sparks, Nevada, USA
Intertek Genalysis, Adelaide, SA, Australia
Intertek Genalysis, Perth, WA, Australia
Intertek Testing Services, Cupang, Muntinlupa, Philippines
Intertek Testing Services, Shunyi, Beijing, China
MINTEK Analytical Services, Randburg, South Africa
PT Geoservices Ltd, Cikarang, Jakarta Raya, Indonesia
SGS de Mexico, Durango, Mexico
SGS Geosol Laboratorios Ltda, Vespasiano, Minas Gerais, Brazil
SGS Lakefield Research Ltd, Lakefield, Ontario, Canada
SGS South Africa Pty Ltd, Booysens, Gauteng, South Africa
Shiva Analyticals Ltd, Bangalore North, Karnataka, India
SRL, Perth, WA, Australia
Table 2. Certified Values, SD's, 95% Confidence and Tolerance Limits for OREAS 603
Certified 95% Confidence Limits
Constituent SD
Value Low
Pb Fire Assay
Ag, Silver (ppm) 284 16 275
Au, Gold (ppm) 5.18 0.151 5.12
4-Acid Digestion
Al, Aluminium (wt.%) 3.98 0.156 3.90
As, Arsenic (ppm) 1801 119 1743
Be, Beryllium (ppm) 0.71 0.08 0.67
Bi, Bismuth (ppm) 149 13 143
Ca, Calcium (wt.%) 0.318 0.015 0.312
Cd, Cadmium (ppm) 54 3.3 52
Ce, Cerium (ppm) 25.7 3.7 22.2
Co, Cobalt (ppm) 15.3 0.96 14.9
Cr, Chromium (ppm) 30.2 5.3 27.8
Cs, Cesium (ppm) 1.66 0.071 1.61
Cu, Copper (wt.%) 1.00 0.034 0.99
Dy, Dysprosium (ppm) 1.21 0.072 1.15
Er, Erbium (ppm) 0.59 0.024 0.58
Eu, Europium (ppm) <1 IND IND
Fe, Iron (wt.%) 2.92 0.135 2.86
Ga, Gallium (ppm) 22.2 1.96 21.1
Gd, Gadolinium (ppm) 1.77 0.107 1.69
Hf, Hafnium (ppm) 2.53 0.167 2.42
Ho, Holmium (ppm) 0.21 0.020 0.19
In, Indium (ppm) 11.2 0.96 10.7
K, Potassium (wt.%) 0.623 0.019 0.614
La, Lanthanum (ppm) 11.9 2.3 10.5
Li, Lithium (ppm) 18.9 1.30 18.2
Lu, Lutetium (ppm) 0.099 0.012 0.088
Mg, Magnesium (ppm) 828 45 809
Mn, Manganese (ppm) 133 11 127
Mo, Molybdenum (ppm) 6.05 0.516 5.83
Na, Sodium (wt.%) 0.428 0.015 0.421
Nb, Niobium (ppm) 7.09 0.74 6.55
Nd, Neodymium (ppm) 11.4 1.1 10.1
Ni, Nickel (ppm) 112 5 110
P, Phosphorus (ppm) 534 31 523
Pb, Lead (ppm) 1908 125 1852
Pr, Praseodymium (ppm) 3.23 0.190 3.01
Rb, Rubidium (ppm) 23.6 1.91 22.3
S, Sulphur (wt.%) 3.71 0.161 3.62
Sb, Antimony (ppm) 205 18 196
Sc, Scandium (ppm) 4.04 0.50 3.81
Se, Selenium (ppm) 60 9 55
Sm, Samarium (ppm) 2.14 0.134 2.00
Sn, Tin (ppm) 12.9 0.98 12.3
Sr, Strontium (ppm) 459 77 422
Ta, Tantalum (ppm) <1 IND IND
Tb, Terbium (ppm) 0.23 0.023 0.21
Te, Tellurium (ppm) 56 7 49
Th, Thorium (ppm) 5.90 0.85 5.28
Ti, Titanium (wt.%) 0.191 0.018 0.182
Tl, Thallium (ppm) 4.18 0.174 4.07
U, Uranium (ppm) 2.71 0.144 2.60
V, Vanadium (ppm) 32.0 2.22 31.0
W, Tungsten (ppm) 14.0 2.6 12.6
Y, Yttrium (ppm) 5.64 0.431 5.43
Yb, Ytterbium (ppm) 0.61 0.09 0.53
Zn, Zinc (wt.%) 0.920 0.031 0.906
Zr, Zirconium (ppm) 78 6.0 75
Aqua Regia Digestion
Al, Aluminium (wt.%) 0.580 0.092 0.537
As, Arsenic (ppm) 1766 91 1722
Au, Gold (ppm) 5.08 0.179 4.96
B, Boron (ppm) < 10 IND IND
Be, Beryllium (ppm) < 0.5 IND IND
Bi, Bismuth (ppm) 151 14 144
Ca, Calcium (wt.%) 0.237 0.017 0.229
Cd, Cadmium (ppm) 55 3.6 53
Ce, Cerium (ppm) 13.0 2.4 11.2
Co, Cobalt (ppm) 15.2 0.79 14.8
Cr, Chromium (ppm) 29.2 2.47 28.2
Cs, Cesium (ppm) 0.74 0.12 0.65
Cu, Copper (wt.%) 1.01 0.026 1.00
Dy, Dysprosium (ppm) 0.56 0.06 0.49
Er, Erbium (ppm) 0.22 0.03 0.19
Eu, Europium (ppm) 0.25 0.05 0.18
Fe, Iron (wt.%) 2.85 0.155 2.78
Ga, Gallium (ppm) 6.58 0.84 6.08
Gd, Gadolinium (ppm) 0.86 0.12 0.74
Hf, Hafnium (ppm) 0.46 0.07 0.40
Hg, Mercury (ppm) <4 IND IND
Ho, Holmium (ppm) 0.096 0.013 0.082
In, Indium (ppm) 11.7 1.15 10.9
K, Potassium (wt.%) 0.093 0.015 0.086
La, Lanthanum (ppm) < 10 IND IND
Li, Lithium (ppm) 4.62 0.82 4.10
Lu, Lutetium (ppb) 26 5 22
Mg, Magnesium (ppm) 517 61 490
Mn, Manganese (ppm) 130 6 127
Mo, Molybdenum (ppm) 6.10 0.564 5.82
Na, Sodium (ppm) 275 58 247
Nb, Niobium (ppm) < 0.5 IND IND
Nd, Neodymium (ppm) 5.90 0.71 5.11
Ni, Nickel (ppm) 113 3 111
P, Phosphorus (ppm) 172 27 159
Pb, Lead (ppm) 1691 36 1674
Pr, Praseodymium (ppm) 1.57 0.25 1.28
Rb, Rubidium (ppm) 4.89 0.88 4.20
S, Sulphur (wt.%) 3.46 0.185 3.36
Sb, Antimony (ppm) 160 24 148
Sc, Scandium (ppm) 1.06 0.16 0.98
Se, Selenium (ppm) 59 8 54
Sm, Samarium (ppm) 1.12 0.13 0.98
Sn, Tin (ppm) 12.0 1.11 11.3
Sr, Strontium (ppm) 46.4 6.1 43.0
Tb, Terbium (ppm) 0.11 0.02 0.10
Te, Tellurium (ppm) 57 2.8 55
Th, Thorium (ppm) 2.30 0.29 2.05
Ti, Titanium (ppm) 98 13 87
Tl, Thallium (ppm) 4.07 0.60 3.62
U, Uranium (ppm) 0.89 0.10 0.81
V, Vanadium (ppm) 10.0 1.1 9.5
W, Tungsten (ppm) 3.88 0.78 3.20
Y, Yttrium (ppm) 2.28 0.35 2.04
Yb, Ytterbium (ppm) 0.17 0.02 0.16
Zn, Zinc (wt.%) 0.911 0.034 0.895
Zr, Zirconium (ppm) 16.0 1.6 15.0
Infrared Combustion
S, Sulphur (wt.%) 3.97 0.161 3.88
olerance Limits for OREAS 603
95% Confidence Limits 95% Tolerance Limits
High Low High
294 278 291

5.23 5.14 5.21
301 292 303

4.06 3.89 4.08
1858 1760 1842
0.75 0.66 0.76
155 144 155
0.324 0.307 0.329
55 52 55
29.2 24.0 27.5
15.7 14.8 15.8
32.7 27.4 33.0
1.72 1.56 1.76
1.02 0.99 1.02
1.27 1.13 1.29
0.61 0.54 0.65
IND IND IND
2.98 2.85 2.99
23.3 21.6 22.9
1.85 1.54 2.00
2.63 2.37 2.68
0.23 0.17 0.25
11.7 10.8 11.6
0.632 0.606 0.639
13.3 11.1 12.7
19.7 18.3 19.6
0.109 IND IND
848 806 851
138 129 136
6.27 5.73 6.38
0.436 0.414 0.442
7.64 6.81 7.38
12.7 10.8 11.9
114 108 116
545 510 558
1964 1851 1965
3.44 3.04 3.41
25.0 22.7 24.5
3.79 3.60 3.82
214 197 213
4.27 3.73 4.35
66 57 63
2.27 2.00 2.27
13.5 12.1 13.6
497 441 478
IND IND IND
0.25 0.21 0.25
63 54 59
6.52 5.54 6.27
0.200 0.185 0.197
4.29 4.02 4.35
2.81 2.59 2.82
33.0 31.0 33.0
15.4 13.3 14.7
5.85 5.42 5.86
0.69 0.57 0.65
0.934 0.906 0.934
81 75 81
300 289 297

0.624 0.565 0.595
1810 1732 1801
5.19 5.03 5.12
IND IND IND
IND IND IND
158 147 154
0.245 0.227 0.247
57 54 56
14.7 12.4 13.5
15.5 14.7 15.7
30.2 26.9 31.6
0.83 0.70 0.77
1.02 0.99 1.03
0.63 0.53 0.58
0.25 IND IND
0.32 0.23 0.27
2.92 2.79 2.91
7.09 6.32 6.85
0.98 0.81 0.92
0.52 0.43 0.49
IND IND IND
0.111 IND IND
12.5 11.3 12.0
0.100 0.091 0.095
IND IND IND
5.14 4.47 4.78
31 IND IND
543 IND IND
133 126 133
6.39 5.81 6.40
302 IND IND
IND IND IND
6.69 5.66 6.14
114 110 116
186 162 183
1707 1666 1715
1.85 1.47 1.66
5.59 4.65 5.14
3.56 3.38 3.53
172 157 164
1.15 1.03 1.10
64 57 61
1.25 1.06 1.18
12.7 11.7 12.3
49.8 44.7 48.0
0.13 0.10 0.12
60 56 59
2.55 2.21 2.39
108 IND IND
4.52 3.89 4.25
0.96 0.84 0.93
10.6 9.4 10.7
4.57 3.66 4.11
2.52 2.21 2.35
0.19 IND IND
0.926 0.895 0.927
17.0 15.5 16.6
4.06 3.91 4.03

Table 3. Indicative Values for OREAS 603
Constituent Unit Value Constituent Unit Value Constituent
Pb Fire Assay
Pd ppb 754 Pt ppb 144
4-Acid Digestion
B ppm < 20 Ge ppm 5.05 Re
Ba ppm 2504 Hg ppm <1 Tm
Ba ppm 686 Pt ppb 132 Ta
Ge ppm 1.35 Re ppb 1 Tm
Pd ppb 734 Ru ppb <2
Infrared Combustion
C wt.% 0.068
Unit Value
ppb 4
ppm 0.088
ppm < 0.01

ppm 0.028
Table 3. Indicative Values for OREAS 603
Constituent Unit Value Constituent Unit Value Constituent
Laser Ablation ICP-MS

Ag ppm 282 Ho ppm 0.23 Sn
As ppm 1715 In ppm 10.1 Sr
Ba ppm 11550 La ppm 18.1 Ta
Be ppm 0.60 Lu ppm 0.095 Tb
Bi ppm 145 Mn wt.% 0.014 Te
Cd ppm 53 Mo ppm 6.30 Th
Ce ppm 30.7 Nb ppm 7.79 Ti
Co ppm 16.5 Nd ppm 11.5 Tl
Cr ppm 39.0 Ni ppm 110 Tm
Cs ppm 1.51 Pb ppm 1945 U
Cu ppm 9830 Pr ppm 3.58 V
Dy ppm 1.20 Rb ppm 23.3 W
Er ppm 0.69 Re ppm 0.013 Y
Eu ppm 0.31 Sb ppm 184 Yb
Ga ppm 24.1 Sc ppm 4.35 Zn
Gd ppm 1.66 Se ppm <5 Zr
Hf ppm 3.64 Sm ppm 2.04
Borate Fusion XRF
Al2O3 wt.% 7.80 Fe2O3 wt.% 4.19 Pb
As ppm 1780 K2O wt.% 0.773 SiO2
Ba ppm 11400 MgO wt.% 0.180 Sn
CaO wt.% 0.455 MnO wt.% 0.020 SO3
Co ppm 25.0 Na2O wt.% 0.550 TiO2
Cr ppm 35.0 Ni ppm 95 U
Cu ppm 10100 P2O5 wt.% 0.129 Zn
Thermogravimetry
LOI1000 wt.% 5.42
Unit Value
ppm 13.0
ppm 571
ppm 0.71
ppm 0.20
ppm 60
ppm 6.98
wt.% 0.198
ppm 4.20
ppm 0.10
ppm 2.73
ppm 32.4
ppm 14.8
ppm 6.28
ppm 0.68
ppm 8530
ppm 122
ppm 2015
wt.% 75.29
ppm 12.5
wt.% 9.50
wt.% 0.335
ppm < 10
ppm 8800
Table 4. Pooled-Lab Performance Gates for OREAS 603
Certified Absolute Standard Deviations Relative Standard Deviat

Constituent
Value 1SD 2SD Low 2SD High 3SD Low 3SD High 1RSD
Pb Fire Assay
Ag, ppm 284 16 253 316 237 332 5.59%
Au, ppm 5.18 0.151 4.87 5.48 4.72 5.63 2.91%
4-Acid Digestion
Ag, ppm 298 8 281 314 273 322 2.73%
Al, wt.% 3.98 0.156 3.67 4.29 3.51 4.45 3.91%
As, ppm 1801 119 1563 2039 1443 2158 6.61%
Be, ppm 0.71 0.08 0.55 0.87 0.47 0.95 11.38%
Bi, ppm 149 13 123 176 109 189 8.88%
Ca, wt.% 0.318 0.015 0.289 0.347 0.274 0.362 4.59%
Cd, ppm 54 3.3 47 60 44 63 6.09%
Ce, ppm 25.7 3.7 18.3 33.1 14.7 36.8 14.35%
Co, ppm 15.3 0.96 13.4 17.2 12.4 18.2 6.26%
Cr, ppm 30.2 5.3 19.7 40.8 14.4 46.1 17.47%
Cs, ppm 1.66 0.071 1.52 1.80 1.45 1.88 4.29%
Cu, wt.% 1.00 0.034 0.94 1.07 0.90 1.10 3.37%
Dy, ppm 1.21 0.072 1.07 1.36 1.00 1.43 5.94%
Er, ppm 0.59 0.024 0.55 0.64 0.52 0.67 4.05%
Eu, ppm <1 IND IND IND IND IND IND
Fe, wt.% 2.92 0.135 2.65 3.19 2.52 3.33 4.60%
Ga, ppm 22.2 1.96 18.3 26.1 16.3 28.1 8.81%
Gd, ppm 1.77 0.107 1.56 1.99 1.45 2.09 6.04%
Hf, ppm 2.53 0.167 2.19 2.86 2.02 3.03 6.63%
Ho, ppm 0.21 0.020 0.17 0.25 0.15 0.27 9.35%
In, ppm 11.2 0.96 9.3 13.1 8.3 14.1 8.61%
K, wt.% 0.623 0.019 0.584 0.662 0.565 0.681 3.11%
La, ppm 11.9 2.3 7.3 16.6 5.0 18.9 19.45%
Li, ppm 18.9 1.30 16.3 21.5 15.1 22.8 6.85%
Lu, ppm 0.099 0.012 0.074 0.124 0.061 0.136 12.62%
Mg, ppm 828 45 738 919 692 965 5.48%
Mn, ppm 133 11 111 154 100 165 8.16%
Mo, ppm 6.05 0.516 5.02 7.08 4.51 7.60 8.52%
Na, wt.% 0.428 0.015 0.398 0.459 0.383 0.474 3.56%
Nb, ppm 7.09 0.74 5.62 8.57 4.88 9.31 10.42%
Nd, ppm 11.4 1.1 9.1 13.7 8.0 14.8 10.03%
Ni, ppm 112 5 102 121 98 126 4.25%
P, ppm 534 31 472 597 440 628 5.86%
Pb, ppm 1908 125 1658 2158 1534 2282 6.54%
Pr, ppm 3.23 0.190 2.85 3.61 2.65 3.80 5.90%
Rb, ppm 23.6 1.91 19.8 27.5 17.9 29.4 8.09%
S, wt.% 3.71 0.161 3.39 4.03 3.23 4.19 4.34%
Sb, ppm 205 18 170 240 152 258 8.61%
Sc, ppm 4.04 0.50 3.04 5.04 2.54 5.54 12.37%
Se, ppm 60 9 42 78 33 87 14.92%
Sm, ppm 2.14 0.134 1.87 2.40 1.73 2.54 6.27%
Sn, ppm 12.9 0.98 10.9 14.8 9.9 15.8 7.63%
Sr, ppm 459 77 306 613 229 689 16.71%
Ta, ppm <1 IND IND IND IND IND IND
Tb, ppm 0.23 0.023 0.19 0.28 0.16 0.30 9.87%
Te, ppm 56 7 42 71 35 78 12.66%
Th, ppm 5.90 0.85 4.20 7.60 3.35 8.45 14.42%
Ti, wt.% 0.191 0.018 0.156 0.226 0.138 0.244 9.25%
Tl, ppm 4.18 0.174 3.83 4.53 3.66 4.71 4.17%
U, ppm 2.71 0.144 2.42 2.99 2.27 3.14 5.33%
V, ppm 32.0 2.22 27.5 36.4 25.3 38.6 6.94%
W, ppm 14.0 2.6 8.8 19.2 6.2 21.8 18.47%
Y, ppm 5.64 0.431 4.78 6.50 4.35 6.93 7.64%
Yb, ppm 0.61 0.09 0.44 0.78 0.35 0.87 14.24%
Zn, wt.% 0.920 0.031 0.857 0.982 0.826 1.013 3.39%
Zr, ppm 78 6.0 66 90 60 96 7.70%
Ag, ppm 293 13 267 319 254 332 4.40%
Al, wt.% 0.580 0.092 0.396 0.765 0.303 0.857 15.91%
As, ppm 1766 91 1584 1949 1493 2040 5.16%
Au, ppm 5.08 0.179 4.72 5.43 4.54 5.61 3.53%
B, ppm < 10 IND IND IND IND IND IND
Be, ppm < 0.5 IND IND IND IND IND IND
Bi, ppm 151 14 123 179 109 193 9.25%
Ca, wt.% 0.237 0.017 0.202 0.271 0.185 0.289 7.27%
Cd, ppm 55 3.6 48 62 44 66 6.53%
Ce, ppm 13.0 2.4 8.1 17.8 5.7 20.2 18.73%
Co, ppm 15.2 0.79 13.6 16.7 12.8 17.5 5.19%
Cr, ppm 29.2 2.47 24.3 34.1 21.8 36.6 8.46%
Cs, ppm 0.74 0.12 0.50 0.97 0.39 1.09 15.76%
Cu, wt.% 1.01 0.026 0.96 1.06 0.93 1.08 2.56%
Dy, ppm 0.56 0.06 0.43 0.68 0.36 0.75 11.54%
Er, ppm 0.22 0.03 0.17 0.27 0.14 0.30 11.87%
Eu, ppm 0.25 0.05 0.15 0.35 0.10 0.40 19.92%
Fe, wt.% 2.85 0.155 2.54 3.16 2.38 3.31 5.44%
Ga, ppm 6.58 0.84 4.91 8.26 4.08 9.09 12.69%
Gd, ppm 0.86 0.12 0.63 1.10 0.51 1.21 13.54%
Hf, ppm 0.46 0.07 0.32 0.60 0.25 0.67 15.00%
Hg, ppm <4 IND IND IND IND IND IND
Ho, ppm 0.096 0.013 0.071 0.122 0.058 0.135 13.44%
In, ppm 11.7 1.15 9.4 14.0 8.2 15.1 9.83%
K, wt.% 0.093 0.015 0.062 0.124 0.047 0.139 16.44%
La, ppm < 10 IND IND IND IND IND IND
Li, ppm 4.62 0.82 2.99 6.26 2.17 7.08 17.71%
Lu, ppb 26 5 17 36 12 41 18.27%
Mg, ppm 517 61 395 639 334 700 11.82%
Mn, ppm 130 6 117 142 110 149 4.99%
Mo, ppm 6.10 0.564 4.98 7.23 4.41 7.80 9.23%
Na, ppm 275 58 160 390 102 447 20.96%
Nb, ppm < 0.5 IND IND IND IND IND IND
Nd, ppm 5.90 0.71 4.47 7.33 3.75 8.04 12.12%
Ni, ppm 113 3 106 119 103 122 2.84%
P, ppm 172 27 117 227 90 255 15.94%
Pb, ppm 1691 36 1618 1763 1582 1799 2.15%
Pr, ppm 1.57 0.25 1.06 2.07 0.81 2.32 16.08%
Rb, ppm 4.89 0.88 3.13 6.65 2.25 7.54 17.98%
S, wt.% 3.46 0.185 3.09 3.83 2.91 4.01 5.34%
Sb, ppm 160 24 111 209 87 233 15.27%
Sc, ppm 1.06 0.16 0.74 1.39 0.57 1.55 15.39%
Se, ppm 59 8 43 75 35 84 13.82%
Sm, ppm 1.12 0.13 0.86 1.37 0.73 1.50 11.51%
Sn, ppm 12.0 1.11 9.8 14.2 8.7 15.3 9.25%
Sr, ppm 46.4 6.1 34.2 58.6 28.1 64.7 13.16%
Tb, ppm 0.11 0.02 0.08 0.15 0.06 0.17 17.02%
Te, ppm 57 2.8 52 63 49 66 4.97%
Th, ppm 2.30 0.29 1.72 2.88 1.43 3.17 12.59%
Ti, ppm 98 13 71 124 58 138 13.67%
Tl, ppm 4.07 0.60 2.87 5.27 2.27 5.87 14.77%
U, ppm 0.89 0.10 0.69 1.08 0.59 1.18 11.00%
V, ppm 10.0 1.1 7.8 12.3 6.7 13.4 11.14%
W, ppm 3.88 0.78 2.32 5.45 1.54 6.23 20.15%
Y, ppm 2.28 0.35 1.58 2.98 1.23 3.33 15.33%
Yb, ppm 0.17 0.02 0.14 0.21 0.12 0.23 11.11%
Zn, wt.% 0.911 0.034 0.843 0.979 0.809 1.013 3.72%
Zr, ppm 16.0 1.6 12.8 19.3 11.2 20.9 10.10%
Infrared Combustion
S, wt.% 3.97 0.161 3.65 4.29 3.49 4.45 4.06%
r OREAS 603
Relative Standard Deviations 5% window
2RSD 3RSD Low High
11.18% 16.76% 270 299

5.83% 8.74% 4.92 5.43
5.47% 8.20% 283 312

7.82% 11.73% 3.78 4.18
13.23% 19.84% 1711 1891
22.76% 34.14% 0.67 0.75
17.76% 26.64% 142 157
9.18% 13.77% 0.302 0.334
12.18% 18.26% 51 56
28.69% 43.04% 24.4 27.0
12.53% 18.79% 14.5 16.1
34.93% 52.40% 28.7 31.7
8.57% 12.86% 1.58 1.75
6.75% 10.12% 0.95 1.05
11.89% 17.83% 1.15 1.27
8.09% 12.14% 0.57 0.62
IND IND IND IND
9.21% 13.81% 2.78 3.07
17.63% 26.44% 21.1 23.3
12.08% 18.13% 1.68 1.86
13.26% 19.90% 2.40 2.65
18.71% 28.06% 0.20 0.22
17.22% 25.83% 10.6 11.8
6.21% 9.32% 0.592 0.654
38.90% 58.34% 11.3 12.5
13.70% 20.55% 18.0 19.9
25.24% 37.86% 0.094 0.104
10.95% 16.43% 787 870
16.32% 24.49% 126 139
17.05% 25.57% 5.75 6.36
7.13% 10.69% 0.407 0.450
20.83% 31.25% 6.74 7.45
20.06% 30.10% 10.8 12.0
8.49% 12.74% 106 117
11.72% 17.57% 507 561
13.08% 19.62% 1813 2003
11.81% 17.71% 3.06 3.39
16.18% 24.28% 22.4 24.8
8.67% 13.01% 3.52 3.89
17.23% 25.84% 195 215
24.73% 37.10% 3.84 4.24
29.85% 44.77% 57 63
12.55% 18.82% 2.03 2.24
15.25% 22.88% 12.2 13.5
33.43% 50.14% 436 482
IND IND IND IND
19.74% 29.61% 0.22 0.24
25.31% 37.97% 53 59
28.85% 43.27% 5.61 6.20
18.51% 27.76% 0.182 0.201
8.33% 12.50% 3.97 4.39
10.67% 16.00% 2.57 2.84
13.88% 20.82% 30.4 33.6
36.94% 55.41% 13.3 14.7
15.27% 22.91% 5.36 5.92
28.48% 42.71% 0.58 0.64
6.77% 10.16% 0.874 0.966
15.39% 23.09% 74 82
8.80% 13.20% 278 308

31.82% 47.74% 0.551 0.609
10.33% 15.49% 1678 1855
7.07% 10.60% 4.82 5.33
IND IND IND IND
IND IND IND IND
18.50% 27.75% 143 158
14.54% 21.81% 0.225 0.249
13.06% 19.59% 52 58
37.45% 56.18% 12.3 13.6
10.38% 15.57% 14.4 15.9
16.92% 25.38% 27.7 30.7
31.53% 47.29% 0.70 0.77
5.11% 7.67% 0.96 1.06
23.07% 34.61% 0.53 0.58
23.74% 35.61% 0.21 0.23
39.84% 59.76% 0.24 0.26
10.88% 16.32% 2.71 2.99
25.38% 38.07% 6.26 6.91
27.08% 40.61% 0.82 0.91
30.00% 45.00% 0.44 0.48
IND IND IND IND
26.88% 40.32% 0.092 0.101
19.66% 29.50% 11.1 12.3
32.87% 49.31% 0.088 0.098
IND IND IND IND
35.42% 53.13% 4.39 4.85
36.54% 54.81% 25 28
23.64% 35.46% 491 543
9.99% 14.98% 123 136
18.47% 27.70% 5.80 6.41
41.91% 62.87% 261 288
IND IND IND IND
24.23% 36.35% 5.60 6.19
5.67% 8.51% 107 118
31.89% 47.83% 164 181
4.29% 6.44% 1606 1775
32.15% 48.23% 1.49 1.64
35.96% 53.94% 4.65 5.14
10.67% 16.01% 3.29 3.63
30.53% 45.80% 152 168
30.78% 46.16% 1.01 1.12
27.64% 41.46% 56 62
23.02% 34.53% 1.06 1.17
18.50% 27.76% 11.4 12.6
26.32% 39.47% 44.1 48.7
34.05% 51.07% 0.11 0.12
9.93% 14.90% 54 60
25.17% 37.76% 2.19 2.42
27.34% 41.01% 93 103
29.53% 44.30% 3.86 4.27
21.99% 32.99% 0.84 0.93
22.28% 33.42% 9.5 10.5
40.30% 60.45% 3.69 4.08
30.67% 46.00% 2.17 2.39
22.23% 33.34% 0.17 0.18
7.44% 11.17% 0.865 0.956
20.20% 30.30% 15.2 16.8
8.12% 12.19% 3.77 4.17

Analytical results for Ag in OREAS 603 (Certified Value 284 ppm)
Ag Round Replicate Lab Lab Lab Lab
No No 01 03 05 07
FA*GRAV FA*GRAV FA*GRAV FA*GRAV
40g 30g 30g 30g
1 1 270 274 301 280
1 2 262 277 353 279
1 3 239 277 290 274
1 4 245 272 345 281
1 5 251 279 303 274
1 6 257 275 304 279
Mean 254 276 316 278
Median 254 276 304 279
Std Dev. 11 3 26 3
Rel.Std.Dev. 4.42% 0.91% 8.28% 1.10%
PDM3 -10.68% -3.05% 11.14% -2.29%
Z-Score (Absolute) 2.02 0.51 1.15 0.36
Analytical results for Au in OREAS 603 (Certified Value 5.18 ppm)

Au Round Replicate Lab Lab Lab Lab
No No 00 01 02 03
INAA FA*AAS FA*AAS FA*OES
1.0g 40g 25g 30g
1 1 4.95 5.16 4.90 5.38
1 2 4.96 5.16 4.97 5.37
1 3 4.88 5.21 4.99 5.34
1 4 4.95 5.25 4.97 5.39
1 5 4.81 5.07 4.99 5.40
1 6 4.89 5.16 4.94 5.33
7 4.81
8 4.89
9 4.80
10 4.94
11 4.84
12 4.98
13 4.87
14 4.96
15 4.89
16 4.85
17 4.78
18 4.96
19 4.89
20 4.95
Mean 4.89 5.17 4.96 5.37
Median 4.89 5.16 4.97 5.38
Std Dev. 0.062 0.060 0.035 0.028
Rel.Std.Dev. 1.27% 1.16% 0.70% 0.52%
PDM3 -5.47% -0.17% -4.17% 3.72%
Z-Score (Absolute) NA 0.07 1.20 1.31
Analytical results for Pd in OREAS 603 (Indicative Value 754 ppb)

Pd Round Replicate Lab Lab
No No 22 25
FA*OES FA*OES
30g 40g
1 1 740
1 2 720
1 3 745
1 4 745
1 5 750 735
1 6 790 740
Mean 770 738
Median 770 740
Std Dev. 28 9
Rel.Std.Dev. 3.67% 1.27%
PDM3 2.16% -2.16%
Z-Score (Absolute) 0.67 0.67
Analytical results for Pt in OREAS 603 (Indicative Value 144 ppb)

Pt Round Replicate Lab Lab
No No 22 25
FA*OES FA*OES
30g 40g
1 1 125
1 2 120
1 3 120
1 4 120
1 5 180 125
1 6 150 130
Mean 165 123
Median 165 123
Std Dev. 21 4
Rel.Std.Dev. 12.86% 3.31%
PDM3 14.45% -14.45%
Lab Lab Lab Lab Lab Lab Lab
08 10 11 12 16 17 19
FA*GRAV FA*OES FA*GRAV FA*GRAV FA*GRAV FA*GRAV FA*GRAV
30g 30g 30g 30g 30g 30g 30g
315 292 297 273 282 268 287
319 293 295 241 284 287 291
288 292 298 277 293 286 294
277 293 295 282 286 276 295
299 292 297 286 281 273 298
300 294 294 307 282 277 298
300 293 296 278 285 278 294
300 293 296 280 283 277 295
16 1 2 22 4 7 4
5.30% 0.28% 0.52% 7.74% 1.57% 2.67% 1.45%
5.39% 2.93% 4.10% -2.32% 0.12% -2.29% 3.34%
1.16 0.67 0.91 0.37 0.00 0.36 0.76

04 05 06 07 08 09 10
FA*AAS FA*AAS FA*AAS FA*GRAV FA*AAS FA*AAS FA*GRAV
30g 30g 30g 30g 30g 30g 30g
5.07 5.12 4.72 5.29 5.04 5.12 5.12
4.88 5.18 4.95 5.23 5.19 5.09 5.04
4.96 4.98 5.19 5.32 4.90 5.10 5.13
4.92 5.17 5.30 5.30 4.60 5.16 5.13
4.98 4.99 5.12 5.27 4.98 5.10 5.14
5.04 5.11 4.98 5.20 5.12 5.28 5.01
4.98 5.09 5.04 5.27 4.97 5.14 5.10

4.97 5.12 5.05 5.28 5.01 5.11 5.13
0.071 0.087 0.205 0.045 0.209 0.074 0.055
1.44% 1.71% 4.07% 0.86% 4.20% 1.44% 1.09%
-3.88% -1.63% -2.56% 1.79% -3.94% -0.72% -1.56%
1.11 0.39 0.69 0.70 0.67 0.28 0.37
Lab
23
FA*GRAV
30g
N.A.
N.A.
N.A.
N.A.
N.A.
N.A.
NA

11 12 13 14 15 16 17
FA*AAS FA*AAS FA*AAS FA*OES FA*AAS FA*AAS FA*AAS
30g 30g 30g 25g 30g 30g 30g
5.20 5.21 5.55 5.05 5.23 5.25 5.24
5.38 5.28 5.50 4.97 5.27 5.12 5.21
5.31 5.20 5.26 5.10 5.26 5.12 5.07
5.28 5.24 5.49 5.13 5.27 5.10 4.90
5.32 5.28 5.53 5.16 5.25 5.17 5.93
5.34 5.23 5.28 5.06 5.26 5.18 5.93
5.30 5.24 5.44 5.08 5.26 5.16 5.38

5.31 5.23 5.50 5.08 5.26 5.15 5.23
0.060 0.034 0.129 0.067 0.015 0.055 0.443
1.13% 0.64% 2.38% 1.33% 0.29% 1.06% 8.23%
2.49% 1.23% 5.04% -1.88% 1.56% -0.40% 3.94%
0.92 0.52 1.73 0.47 0.62 0.00 0.31
18 19 20 21 22 23 24
FA*AAS FA*AAS FA*GRAV FA*AAS FA*OES FA*AAS FA*AAS
30g 30g 40g 30g 30g 30g 20g
5.13 5.26 5.10 4.77 5.21 5.18
5.23 5.20 5.35 4.67 5.24 5.16
5.16 4.96 5.50 4.89 5.30 5.22
5.22 5.22 5.20 4.81 5.32 5.26
5.19 5.28 5.25 4.64 4.46 5.28 5.20
5.27 5.26 5.25 4.59 4.68 5.25 5.24
5.20 5.20 5.28 4.73 4.57 5.27 5.21

5.21 5.24 5.25 4.72 4.57 5.27 5.21
0.051 0.118 0.137 0.114 0.156 0.040 0.037
0.97% 2.28% 2.60% 2.42% 3.40% 0.77% 0.72%
0.47% 0.38% 1.92% -8.64% -11.71% 1.78% 0.66%
0.28 0.53 0.74 2.63 3.61 0.69 0.34
Lab Lab Lab
25 26 27
FA*OES FA*AAS FA*AAS
40g 40g 20g
5.15 5.45 4.96
5.13 5.43 4.96
5.19 5.41 4.91
5.17 5.40 4.95
5.06 5.37 4.93
5.05 5.42 5.07
5.13 5.41 4.96

5.14 5.42 4.95
0.058 0.027 0.056
1.13% 0.50% 1.14%
-0.98% 4.59% -4.14%
0.19 1.59 1.19
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
284
7
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
5.18
8.00
Indicative
1.00
ppb
0.00
0.00
1
1
16
754
7
Indicative
1.00
ppb
0.00
0.00
1
1
16
144
7
No No 01 02 04 05
AR*OES AR*MS AR*AAS AR*OES/AAS
0.5g 40g 01g 0.5g
1 1 302 > 250 291 299
1 2 304 > 250 292 301
1 3 304 > 250 290 304
1 4 304 > 250 292 303
1 5 303 > 250 294 302
1 6 302 > 250 291 301
Mean 303 292 302
Median 303 292 302
Std Dev. 1 1 2
Rel.Std.Dev. 0.28% 0.47% 0.58%
PDM3 3.42% -0.43% 2.99%
Z-Score (Absolute) 0.77 NA 0.11 0.67
Analytical results for Al in OREAS 603 (Certified Value 0.58 wt.%)

Al Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
AR*OES AR*OES AR*OES AR*OES
0.5g 40g 01g 01g
1 1 0.823 0.766 0.590 0.550
1 2 0.803 0.768 0.600 0.550
1 3 0.817 0.734 0.600 0.550
1 4 0.823 0.746 0.600 0.530
1 5 0.815 0.736 0.610 0.540
1 6 0.825 0.731 0.590 0.550
Mean 0.818 0.747 0.598 0.545
Median 0.820 0.741 0.600 0.550
Std Dev. 0.008 0.017 0.008 0.008
Rel.Std.Dev. 1.00% 2.21% 1.26% 1.54%
PDM3 40.90% 28.68% 3.09% -6.10%
Z-Score (Absolute) 2.55 1.82 0.28 0.28
Analytical results for As in OREAS 603 (Certified Value 1766 ppm)

As Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
AR*OES AR*MS AR*OES AR*OES
0.5g 40g 01g 01g
1 1 2112 1750 1850 1890
1 2 2114 1733 1830 1870
1 3 2104 1725 1830 1850
1 4 2102 1767 1860 1810
1 5 2115 1826 1870 1840
1 6 2112 1744 1820 1880
Mean 2110 1758 1843 1857
Median 2112 1747 1840 1860
Std Dev. 5 37 20 29
Rel.Std.Dev. 0.26% 2.08% 1.07% 1.59%
PDM3 19.43% -0.51% 4.35% 5.11%
Z-Score (Absolute) 3.28 0.30 0.67 0.80
Analytical results for Au in OREAS 603 (Certified Value 5.08 ppm)

Au Round Replicate Lab Lab Lab Lab
No No 00 01 02 05
INAA AR*AAS AR*MS AR*MS
1.0g 30g 25g 25g
1 1 4.95 5.19 4.82 5.10
1 2 4.96 5.09 4.77 5.15
1 3 4.88 4.98 4.79 5.10
1 4 4.95 5.05 4.62 5.09
1 5 4.81 5.04 4.78 5.18
1 6 4.89 5.01 4.71 5.16
7 4.81
8 4.89
9 4.80
10 4.94
11 4.84
12 4.98
13 4.87
14 4.96
15 4.89
16 4.85
17 4.78
18 4.96
19 4.89
20 4.95
Mean 4.89 5.06 4.75 5.13
Median 4.89 5.04 4.78 5.13
Std Dev. 0.062 0.076 0.071 0.038
Rel.Std.Dev. 1.27% 1.51% 1.50% 0.74%
PDM3 -3.60% -0.30% -6.42% 1.08%
Z-Score (Absolute) NA 0.23 2.24 0.26
Analytical results for B in OREAS 603 (Certified Value < 10 ppm)

B Round Replicate Lab Lab Lab Lab
No No 05 06 07 08
01g 01g 01g 01g
1 1 < 10 < 10 < 10 < 10
1 2 < 10 < 10 < 10 < 10
1 3 < 10 < 10 < 10 < 10
1 4 < 10 < 10 < 10 < 10
1 5 < 10 < 10 < 10 < 10
1 6 < 10 < 10 < 10 < 10
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA NA NA NA
Analytical results for Ba in OREAS 603 (Indicative Value 686 ppm)

Ba Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 12 203 40 20
1 2 12 198 40 30
1 3 12 207 40 30
1 4 12 197 40 30
1 5 12 199 40 30
1 6 12 200 40 30
Mean 12 201 40 28
Median 12 200 40 30
Std Dev. 0 4 0 4
Rel.Std.Dev. 1.55% 1.86% 0.00% 14.41%
PDM3 -98.27% -70.75% -94.17% -95.87%
Z-Score (Absolute) 0.71 3.54 0.07 0.30
Analytical results for Be in OREAS 603 (Certified Value < 0.5 ppm)
Be Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 <1 0.21 < 0.5 < 0.5
1 2 <1 0.18 < 0.5 < 0.5
1 3 <1 0.19 < 0.5 < 0.5
1 4 <1 0.18 < 0.5 < 0.5
1 5 <1 0.18 < 0.5 < 0.5
1 6 <1 0.18 < 0.5 < 0.5
Mean 0.19
Median 0.18
Std Dev. 0.012
Rel.Std.Dev. 6.49%
PDM3
Z-Score (Absolute) NA 0.30 NA NA
Analytical results for Bi in OREAS 603 (Certified Value 151 ppm)

Bi Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 183 154 160 160
1 2 180 160 159 159
1 3 181 155 158 160
1 4 180 158 162 151
1 5 181 157 162 156
1 6 181 155 157 158
Mean 181 156 160 157
Median 181 156 160 159
Std Dev. 1 2 2 3
Rel.Std.Dev. 0.63% 1.47% 1.29% 2.19%
PDM3 19.87% 3.68% 5.87% 4.32%
Z-Score (Absolute) 2.88 0.24 0.59 0.48
Analytical results for Ca in OREAS 603 (Certified Value 0.237 wt.%)

Ca Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 0.207 0.240 0.230 0.250
1 2 0.210 0.250 0.240 0.250
1 3 0.213 0.240 0.230 0.240
1 4 0.210 0.250 0.240 0.240
1 5 0.220 0.240 0.240 0.240
1 6 0.213 0.240 0.230 0.250
Mean 0.212 0.243 0.235 0.245
Median 0.212 0.240 0.235 0.245
Std Dev. 0.005 0.005 0.005 0.005
Rel.Std.Dev. 2.15% 2.12% 2.33% 2.24%
PDM3 -10.42% 2.71% -0.80% 3.42%
Z-Score (Absolute) 1.87 0.22 0.34 0.34
Analytical results for Cd in OREAS 603 (Certified Value 55 ppm)

Cd Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 73 52 56 58
1 2 73 49 56 58
1 3 74 51 56 58
1 4 74 51 57 56
1 5 74 54 57 57
1 6 75 52 56 57
Mean 74 52 56 57
Median 74 52 56 57
Std Dev. 0.8 1.4 0.5 0.9
Rel.Std.Dev. 1.11% 2.75% 0.96% 1.56%
PDM3 33.94% -6.63% 1.53% 3.71%
Z-Score (Absolute) 4.20 1.04 0.02 0.30
Analytical results for Ce in OREAS 603 (Certified Value 13 ppm)

Ce Round Replicate Lab Lab Lab Lab
No No 02 09 11 13
AR*MS AR*OES/MS AR*OES AR*MS
40g 20g 0.15g 01g
1 1 13.7 15.3 14.0 9.6
1 2 14.0 15.4 14.0 10.5
1 3 13.2 15.4 15.0 10.3
1 4 13.8 15.3 14.0 10.5
1 5 13.3 15.7 13.0 10.5
1 6 13.4 15.4 10.0 10.3
Mean 13.6 15.4 13.3 10.3
Median 13.5 15.4 14.0 10.4
Std Dev. 0.3 0.2 1.8 0.4
Rel.Std.Dev. 2.30% 1.03% 13.13% 3.48%
PDM3 4.58% 19.04% 2.91% -20.73%
Z-Score (Absolute) 0.00 0.67 0.16 1.18
Analytical results for Co in OREAS 603 (Certified Value 15.2 ppm)

Co Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 14.5 14.5 15.0 15.0
1 2 14.3 14.8 15.0 15.0
1 3 14.5 14.3 15.0 15.0
1 4 14.5 14.0 15.0 15.0
1 5 14.5 14.3 15.0 15.0
1 6 14.5 14.0 15.0 15.0
Mean 14.5 14.3 15.0 15.0
Median 14.5 14.3 15.0 15.0
Std Dev. 0.075 0.306 0.000 0.000
Rel.Std.Dev. 0.52% 2.14% 0.00% 0.00%
PDM3 -4.63% -5.59% -1.08% -1.08%
Z-Score (Absolute) 1.13 1.39 0.20 0.20
Analytical results for Cr in OREAS 603 (Certified Value 29.2 ppm)

Cr Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 31.3 28.0 29.0 30.0
1 2 31.8 30.0 29.0 29.0
1 3 31.4 31.0 27.0 31.0
1 4 30.9 31.0 28.0 28.0
1 5 31.1 32.0 28.0 30.0
1 6 32.3 30.0 31.0 32.0
Mean 31.5 30.3 28.7 30.0
Median 31.4 30.5 28.5 30.0
Std Dev. 0.507 1.366 1.366 1.414
Rel.Std.Dev. 1.61% 4.50% 4.77% 4.71%
PDM3 7.84% 3.85% -1.85% 2.71%
Z-Score (Absolute) 0.67 0.15 0.60 0.00
Analytical results for Cs in OREAS 603 (Certified Value 0.74 ppm)

Cs Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
AR*MS AR*OES/MS AR*MS AR*MS
40g 20g 01g 0.5g
1 1 0.77 0.83 0.75 0.69
1 2 0.77 0.84 0.84 0.70
1 3 0.78 0.82 0.79 0.67
1 4 0.75 0.82 0.82 0.67
1 5 0.76 0.82 0.82 0.67
1 6 0.78 0.84 0.86 0.69
Mean 0.77 0.83 0.81 0.68
Median 0.77 0.83 0.82 0.68
Std Dev. 0.012 0.011 0.039 0.013
Rel.Std.Dev. 1.52% 1.34% 4.84% 1.95%
PDM3 4.18% 12.11% 10.35% -7.57%
Z-Score (Absolute) 0.00 0.46 0.35 0.67
Analytical results for Cu in OREAS 603 (Certified Value 1.01 wt.%)

Cu Round Replicate Lab Lab Lab Lab
No No 01 02 04 05
AR*OES AR*OES AR*AAS AR*OES/AAS
0.5g 40g 01g 0.5g
1 1 1.00 0.99 0.99 0.97
1 2 1.00 1.05 1.00 0.99
1 3 1.01 0.99 0.99 1.00
1 4 1.01 1.00 0.99 0.99
1 5 1.01 1.03 1.01 0.99
1 6 1.00 0.99 1.01 1.00
Mean 1.00 1.01 1.00 0.99
Median 1.00 1.00 1.00 0.99
Std Dev. 0.004 0.027 0.010 0.011
Rel.Std.Dev. 0.37% 2.70% 0.99% 1.15%
PDM3 -0.46% 0.21% -0.94% -1.74%
Z-Score (Absolute) 0.04 0.30 0.28 0.67
Analytical results for Dy in OREAS 603 (Certified Value 0.56 ppm)

Dy Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 0.59 0.59 0.47 0.51
1 2 0.60 0.62 0.53 0.52
1 3 0.58 0.63 0.51 0.50
1 4 0.60 0.60 0.52 0.51
1 5 0.59 0.61 0.56 0.52
1 6 0.58 0.60 0.54 0.54
Mean 0.59 0.61 0.52 0.52
Median 0.59 0.61 0.52 0.52
Std Dev. 0.009 0.014 0.031 0.014
Rel.Std.Dev. 1.52% 2.34% 5.91% 2.64%
PDM3 6.11% 9.30% -6.15% -7.08%
Z-Score (Absolute) 0.50 0.77 0.50 0.58
Analytical results for Er in OREAS 603 (Certified Value 0.22 ppm)

Er Round Replicate Lab Lab Lab Lab
No No 02 09 14 15
AR*MS AR*OES/MS AR*MS AR*OES/MS
40g 20g 0.5g 01g
1 1 0.22 0.23 0.20 0.26
1 2 0.24 0.24 0.22 0.26
1 3 0.23 0.21 0.20 0.26
1 4 0.23 0.23 0.21 0.21
1 5 0.24 0.24 0.21 0.19
1 6 0.23 0.25 0.20 0.23
Mean 0.23 0.23 0.21 0.24
Median 0.23 0.24 0.21 0.25
Std Dev. 0.008 0.012 0.008 0.030
Rel.Std.Dev. 3.25% 5.18% 3.95% 12.84%
PDM3 6.42% 7.25% -5.07% 7.95%
Z-Score (Absolute) 0.00 0.37 5.06 0.67
Analytical results for Eu in OREAS 603 (Certified Value 0.25 ppm)

Eu Round Replicate Lab Lab Lab Lab
No No 02 09 14 15
40g 20g 0.5g 01g
1 1 0.24 0.26 0.21 0.34
1 2 0.24 0.25 0.22 0.35
1 3 0.24 0.27 0.20 0.34
1 4 0.25 0.24 0.21 0.30
1 5 0.24 0.26 0.20 0.32
1 6 0.24 0.27 0.22 0.36
Mean 0.24 0.26 0.21 0.34
Median 0.24 0.26 0.21 0.34
Std Dev. 0.004 0.010 0.009 0.022
Rel.Std.Dev. 1.69% 3.73% 4.26% 6.47%
PDM3 -3.11% 4.04% -15.81% 34.30%
Z-Score (Absolute) 0.00 0.38 0.67 1.99
Analytical results for Fe in OREAS 603 (Certified Value 2.85 wt.%)

Fe Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 2.78 2.88 2.72 2.82
1 2 2.81 2.91 2.75 2.80
1 3 2.82 2.81 2.72 2.78
1 4 2.84 2.88 2.78 2.70
1 5 2.82 2.90 2.76 2.75
1 6 2.84 2.86 2.73 2.78
Mean 2.82 2.87 2.74 2.77
Median 2.82 2.88 2.74 2.78
Std Dev. 0.025 0.036 0.024 0.042
Rel.Std.Dev. 0.88% 1.24% 0.88% 1.52%
PDM3 -1.10% 0.87% -3.70% -2.70%
Z-Score (Absolute) 0.28 0.00 0.64 0.50
Analytical results for Ga in OREAS 603 (Certified Value 6.58 ppm)

Ga Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
AR*OES AR*MS AR*OES/MS AR*OES
0.5g 40g 20g 0.15g
1 1 7.13 6.14 7.20 7.00
1 2 6.80 6.24 7.53 <5
1 3 6.91 6.11 7.29 8.00
1 4 6.89 5.95 7.24 5.00
1 5 7.15 6.15 7.39 8.00
1 6 7.16 6.01 7.46 9.00
Mean 7.01 6.10 7.35 7.40
Median 7.02 6.13 7.34 8.00
Std Dev. 0.159 0.104 0.128 1.517
Rel.Std.Dev. 2.27% 1.71% 1.74% 20.49%
PDM3 6.41% -7.36% 11.63% 12.38%
Z-Score (Absolute) 0.16 0.90 0.56 0.62
Analytical results for Gd in OREAS 603 (Certified Value 0.86 ppm)

Gd Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 0.93 0.88 0.71 0.83
1 2 0.95 0.93 0.79 0.84
1 3 0.91 0.90 0.73 0.79
1 4 0.94 0.90 0.76 0.83
1 5 0.94 0.90 0.81 0.80
1 6 0.93 0.92 0.85 0.83
Mean 0.93 0.90 0.77 0.82
Median 0.94 0.90 0.77 0.83
Std Dev. 0.014 0.019 0.051 0.020
Rel.Std.Dev. 1.46% 2.08% 6.65% 2.44%
PDM3 8.07% 4.58% -10.53% -5.05%
Z-Score (Absolute) 0.60 0.35 0.75 0.35
Analytical results for Ge in OREAS 603 (Indicative Value 1.35 ppm)

Ge Round Replicate Lab Lab Lab Lab
No No 11 15 17 19
AR*OES AR*OES/MS AR*OES/MS AR*OES/MS
0.15g 01g 0.25g 0.25g
1 1 < 10 < 0.5 1.40 1.33
1 2 < 10 < 0.5 1.50 1.27
1 3 < 10 < 0.5 1.50 1.25
1 4 < 10 < 0.5 1.60 1.21
1 5 < 10 < 0.5 1.50 1.16
1 6 < 10 < 0.5 1.30 1.17
Mean 1.47 1.23
Median 1.50 1.23
Std Dev. 0.103 0.063
Rel.Std.Dev. 7.04% 5.09%
PDM3 8.78% -8.78%
Z-Score (Absolute) NA NA 0.67 0.67
Analytical results for Hf in OREAS 603 (Certified Value 0.46 ppm)

Hf Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 0.56 0.49 0.39 0.42
1 2 0.59 0.51 0.43 0.43
1 3 0.55 0.55 0.38 0.41
1 4 0.57 0.49 0.42 0.42
1 5 0.58 0.52 0.42 0.41
1 6 0.54 0.54 0.42 0.41
Mean 0.57 0.52 0.41 0.42
Median 0.57 0.52 0.42 0.42
Std Dev. 0.019 0.026 0.018 0.008
Rel.Std.Dev. 3.31% 5.00% 4.34% 1.96%
PDM3 22.59% 12.38% -11.13% -9.60%
Z-Score (Absolute) 4.97 3.33 0.45 0.20
Analytical results for Hg in OREAS 603 (Certified Value < 4 ppm)

Hg Round Replicate Lab Lab Lab Lab
No No 05 06 07 08
01g 01g 01g 01g
1 1 1.00 2.00 2.00 1.00
1 2 1.00 3.00 2.00 1.00
1 3 2.00 1.00 3.00 2.00
1 4 2.00 2.00 2.00 1.00
1 5 2.00 2.00 2.00 2.00
1 6 1.00 1.00 2.00 2.00
Mean 1.50 1.83 2.17 1.50
Median 1.50 2.00 2.00 1.50
Std Dev. 0.548 0.753 0.408 0.548
Rel.Std.Dev. 36.51% 41.06% 18.84% 36.51%
PDM3
Z-Score (Absolute) 0.59 0.90 1.65 0.59
Analytical results for Ho in OREAS 603 (Certified Value 0.096 ppm)

Ho Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 0.100 0.093 0.099 0.090
1 2 0.100 0.099 0.110 0.090
1 3 0.090 0.100 0.110 0.090
1 4 0.090 0.097 0.114 0.090
1 5 0.100 0.097 0.110 0.090
1 6 0.090 0.100 0.125 0.090
Mean 0.095 0.098 0.111 0.090
Median 0.095 0.098 0.110 0.090
Std Dev. 0.005 0.003 0.009 0.000
Rel.Std.Dev. 5.77% 2.73% 7.71% 0.00%
PDM3 -1.53% 1.19% 15.28% -6.71%
Z-Score (Absolute) 0.09 0.09 1.00 0.43
Analytical results for In in OREAS 603 (Certified Value 11.7 ppm)

In Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
0.5g 40g 20g 0.15g
1 1 10.5 11.4 11.1 13.0
1 2 10.6 11.2 11.5 14.0
1 3 11.4 11.4 11.4 13.0
1 4 10.3 11.4 11.3 13.0
1 5 10.9 11.7 11.4 13.0
1 6 11.1 11.4 11.7 14.0
Mean 10.8 11.4 11.4 13.3
Median 10.8 11.4 11.4 13.0
Std Dev. 0.397 0.162 0.180 0.516
Rel.Std.Dev. 3.67% 1.42% 1.58% 3.87%
PDM3 -7.38% -2.26% -2.46% 14.20%
Z-Score (Absolute) 0.61 0.01 0.02 1.98
Analytical results for K in OREAS 603 (Certified Value 0.093 wt.%)

K Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 0.120 0.125 0.090 0.090
1 2 0.120 0.125 0.090 0.090
1 3 0.120 0.119 0.090 0.080
1 4 0.120 0.121 0.090 0.080
1 5 0.120 0.120 0.090 0.080
1 6 0.120 0.118 0.090 0.080
Mean 0.120 0.121 0.090 0.083
Median 0.120 0.121 0.090 0.080
Std Dev. 0.000 0.003 0.000 0.005
Rel.Std.Dev. 0.00% 2.66% 0.00% 6.20%
PDM3 29.07% 30.52% -3.20% -10.37%
Z-Score (Absolute) 2.02 2.11 0.00 0.45
Analytical results for La in OREAS 603 (Certified Value < 10 ppm)

La Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 4.4 7.1 < 10 10.0
1 2 4.4 7.2 < 10 < 10
1 3 4.5 7.2 < 10 10.0
1 4 4.4 7.1 < 10 10.0
1 5 4.5 7.0 < 10 < 10
1 6 4.4 7.1 < 10 10.0
Mean 4.4 7.1 10.0
Median 4.4 7.1 10.0
Std Dev. 0.0 0.1 0.0
Rel.Std.Dev. 0.96% 0.90% 0.00%
PDM3
Z-Score (Absolute) 0.56 0.61 NA 1.86
Analytical results for Li in OREAS 603 (Certified Value 4.62 ppm)

Li Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
0.5g 40g 20g 0.15g
1 1 5.73 5.10 6.07 <5
1 2 5.82 5.20 6.18 <5
1 3 5.79 5.00 6.31 <5
1 4 5.90 4.70 6.34 <5
1 5 5.79 4.70 6.07 <5
1 6 5.80 4.80 6.35 <5
Mean 5.81 4.92 6.22
Median 5.80 4.90 6.25
Std Dev. 0.055 0.214 0.131
Rel.Std.Dev. 0.95% 4.35% 2.11%
PDM3 25.58% 6.34% 34.55%
Z-Score (Absolute) 1.48 0.42 1.97 NA
Analytical results for Lu in OREAS 603 (Certified Value 26 ppb)

Lu Round Replicate Lab Lab Lab Lab
No No 02 09 14 15
40g 20g 0.5g 01g
1 1 30 25 25 < 100
1 2 40 23 27 < 100
1 3 40 25 23 < 100
1 4 30 23 24 < 100
1 5 30 27 24 < 100
1 6 30 25 26 < 100
Mean 33 25 25
Median 30 25 25
Std Dev. 5 1 1
Rel.Std.Dev. 15.49% 6.02% 5.93%
PDM3 25.87% -6.63% -6.23%
Analytical results for Mg in OREAS 603 (Certified Value 517 ppm)

Mg Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 600 600 500 500
1 2 600 600 500 500
1 3 600 600 500 500
1 4 600 600 500 500
1 5 600 600 500 500
1 6 600 600 500 500
Mean 600 600 500 500
Median 600 600 500 500
Std Dev. 0 0 0 0
Rel.Std.Dev. 0.00% 0.00% 0.00% 0.00%
PDM3 16.11% 16.11% -3.24% -3.24%
Z-Score (Absolute) 2.02 2.02 0.00 0.00
Analytical results for Mn in OREAS 603 (Certified Value 130 ppm)

Mn Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 126 133 128 133
1 2 127 134 128 133
1 3 129 129 127 131
1 4 129 132 129 126
1 5 129 132 130 130
1 6 130 131 127 132
Mean 129 132 128 131
Median 129 132 128 132
Std Dev. 1 2 1 3
Rel.Std.Dev. 1.17% 1.31% 0.91% 2.02%
PDM3 -0.73% 1.79% -1.04% 1.02%
Z-Score (Absolute) 0.25 0.40 0.34 0.20
Analytical results for Mo in OREAS 603 (Certified Value 6.1 ppm)

Mo Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 6.26 6.10 6.00 8.00
1 2 6.46 6.00 6.00 8.00
1 3 6.63 6.30 6.00 8.00
1 4 6.50 6.20 6.00 8.00
1 5 6.42 6.30 6.00 8.00
1 6 6.38 6.10 6.00 8.00
Mean 6.44 6.17 6.00 8.00
Median 6.44 6.15 6.00 8.00
Std Dev. 0.125 0.121 0.000 0.000
Rel.Std.Dev. 1.94% 1.96% 0.00% 0.00%
PDM3 5.49% 1.02% -1.71% 31.05%
Z-Score (Absolute) 0.67 0.26 0.00 3.07
Analytical results for Na in OREAS 603 (Certified Value 275 ppm)

Na Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 233 300 100 300
1 2 200 300 100 300
1 3 233 300 100 300
1 4 233 300 100 300
1 5 233 300 100 300
1 6 233 300 100 300
Mean 228 300 100 300
Median 233 300 100 300
Std Dev. 14 0 0 0
Rel.Std.Dev. 5.97% 0.00% 0.00% 0.00%
PDM3 -17.06% 9.24% -63.59% 9.24%
Z-Score (Absolute) 0.90 0.00 2.70 0.00
Analytical results for Nb in OREAS 603 (Certified Value < 0.5 ppm)
Nb Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
0.5g 40g 20g 0.15g
1 1 <5 0.40 0.30 < 10
1 2 <5 0.42 0.29 < 10
1 3 <5 0.46 0.32 < 10
1 4 <5 0.35 0.33 < 10
1 5 <5 0.31 0.33 < 10
1 6 <5 0.44 0.33 < 10
Mean 0.40 0.32
Median 0.41 0.33
Std Dev. 0.057 0.018
Rel.Std.Dev. 14.32% 5.65%
PDM3
Z-Score (Absolute) NA 0.67 0.00 NA
Analytical results for Nd in OREAS 603 (Certified Value 5.9 ppm)

Nd Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 6.03 6.76 5.43 5.74
1 2 6.08 6.89 5.29 5.85
1 3 5.95 7.05 5.19 5.78
1 4 6.16 6.60 5.23 5.86
1 5 6.06 6.99 5.17 5.90
1 6 5.99 6.82 5.48 5.97
Mean 6.05 6.85 5.30 5.85
Median 6.05 6.85 5.26 5.86
Std Dev. 0.073 0.162 0.129 0.082
Rel.Std.Dev. 1.21% 2.37% 2.44% 1.41%
PDM3 2.50% 16.17% -10.19% -0.81%
Z-Score (Absolute) 0.11 1.00 0.72 0.11
Analytical results for Ni in OREAS 603 (Certified Value 113 ppm)

Ni Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 112 111 111 116
1 2 111 117 112 115
1 3 112 114 109 115
1 4 112 114 112 112
1 5 113 114 112 113
1 6 113 112 112 114
Mean 112 113 111 114
Median 112 114 112 115
Std Dev. 1 2 1 1
Rel.Std.Dev. 0.51% 1.78% 1.09% 1.29%
PDM3 -0.52% 0.73% -1.18% 1.34%
Z-Score (Absolute) 0.00 0.37 0.19 0.54
Analytical results for P in OREAS 603 (Certified Value 172 ppm)

P Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 180 315 160 160
1 2 183 423 160 170
1 3 183 440 160 160
1 4 186 396 170 160
1 5 187 372 170 160
1 6 187 461 160 170
Mean 184 401 163 163
Median 185 410 160 160
Std Dev. 3 53 5 5
Rel.Std.Dev. 1.58% 13.13% 3.16% 3.16%
PDM3 6.79% 132.61% -5.29% -5.29%
Z-Score (Absolute) 0.59 8.65 0.18 0.18
Analytical results for Pb in OREAS 603 (Certified Value 1691 ppm)

Pb Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 1708 1700 1680 1735
1 2 1716 1718 1690 1725
1 3 1725 1722 1680 1710
1 4 1728 1705 1710 1665
1 5 1731 1698 1700 1690
1 6 1726 1696 1680 1710
Mean 1722 1707 1690 1706
Median 1725 1703 1685 1710
Std Dev. 9 11 13 25
Rel.Std.Dev. 0.50% 0.65% 0.75% 1.48%
PDM3 1.87% 0.94% -0.04% 0.90%
Z-Score (Absolute) 0.67 0.32 0.05 0.31
Analytical results for Pd in OREAS 603 (Indicative Value 734 ppb)

Pd Round Replicate Lab Lab Lab
No No 09 14 25
AR*OES/MS AR*MS AR*MS
20g 0.5g 40g
1 1 718 751 720
1 2 710 784 710
1 3 700 747 740
1 4 711 749 740
1 5 701 752 740
1 6 703 780 760
Mean 707 761 735
Median 706 752 740
Std Dev. 7 17 18
Rel.Std.Dev. 0.99% 2.21% 2.40%
PDM3 -3.69% 3.58% 0.11%
Z-Score (Absolute) 0.74 0.67 0.00
Analytical results for Pr in OREAS 603 (Certified Value 1.57 ppm)

Pr Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 1.72 1.71 1.29 1.48
1 2 1.75 1.77 1.40 1.53
1 3 1.67 1.78 1.38 1.50
1 4 1.72 1.73 1.42 1.50
1 5 1.70 1.75 1.43 1.48
1 6 1.69 1.73 1.45 1.56
Mean 1.71 1.74 1.40 1.51
Median 1.71 1.74 1.41 1.50
Std Dev. 0.028 0.026 0.056 0.031
Rel.Std.Dev. 1.63% 1.50% 4.03% 2.07%
PDM3 9.15% 11.34% -10.73% -3.63%
Z-Score (Absolute) 0.42 0.56 0.79 0.42
Analytical results for Pt in OREAS 603 (Indicative Value 132 ppb)

Pt Round Replicate Lab Lab Lab
No No 09 14 25
20g 0.5g 40g
1 1 130 126 140
1 2 126 132 145
1 3 133 132 140
1 4 121 128 140
1 5 123 129 140
1 6 125 131 140
Mean 126 130 141
Median 126 130 140
Std Dev. 4 2 2
Rel.Std.Dev. 3.36% 1.87% 1.45%
PDM3 -4.48% -1.98% 6.46%
Z-Score (Absolute) 0.67 0.00 2.28
Analytical results for Rb in OREAS 603 (Certified Value 4.89 ppm)

Rb Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 5.91 5.71 4.47 3.97
1 2 5.71 5.83 4.84 4.08
1 3 5.53 5.59 4.81 4.00
1 4 5.50 5.65 4.74 4.09
1 5 5.55 5.95 4.62 4.01
1 6 5.56 5.93 4.99 4.09
Mean 5.63 5.78 4.75 4.04
Median 5.56 5.77 4.77 4.05
Std Dev. 0.157 0.150 0.182 0.053
Rel.Std.Dev. 2.79% 2.59% 3.83% 1.31%
PDM3 14.95% 18.01% -3.05% -17.46%
Z-Score (Absolute) 0.67 0.84 0.00 0.58
Analytical results for Re in OREAS 603 (Indicative Value 1 ppb)

Re Round Replicate Lab Lab Lab Lab
No No 02 09 11 14
40g 20g 0.15g 0.5g
1 1 2 <1 < 5000 2
1 2 2 <1 < 5000 2
1 3 2 <1 < 5000 1
1 4 2 <1 < 5000 1
1 5 2 1 < 5000 2
1 6 2 <1 < 5000 2
Mean 2 1 2
Median 2 1 2
Std Dev. 0 1
Rel.Std.Dev. 0.00% 30.98%
PDM3 42.60% -46.84% 18.83%
Analytical results for Ru in OREAS 603 (Indicative Value < 2 ppb)

Ru Round Replicate Lab
No No 14
AR*MS
0.5g
1 1 <2
1 2 <2
1 3 <2
1 4 <2
1 5 <2
1 6 <2
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Z-Score (Absolute) NA
Analytical results for S in OREAS 603 (Certified Value 3.46 wt.%)

S Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 3.70 3.26 3.55 3.54
1 2 3.70 3.11 3.54 3.55
1 3 3.76 3.24 3.55 3.51
1 4 3.75 3.40 3.61 3.42
1 5 3.78 3.45 3.59 3.49
1 6 3.81 3.28 3.54 3.53
Mean 3.75 3.29 3.56 3.51
Median 3.76 3.27 3.55 3.52
Std Dev. 0.046 0.120 0.029 0.048
Rel.Std.Dev. 1.23% 3.64% 0.83% 1.36%
PDM3 8.41% -4.92% 3.02% 1.38%
Z-Score (Absolute) 1.60 0.95 0.57 0.26
Analytical results for Sb in OREAS 603 (Certified Value 160 ppm)

Sb Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 123 154 183 154
1 2 122 150 181 154
1 3 123 156 180 153
1 4 124 151 183 152
1 5 125 154 183 152
1 6 125 149 178 154
Mean 124 152 181 153
Median 124 152 182 154
Std Dev. 1 3 2 1
Rel.Std.Dev. 1.00% 1.79% 1.14% 0.64%
PDM3 -22.65% -4.81% 13.30% -4.30%
Z-Score (Absolute) 0.95 0.09 0.79 0.06
Analytical results for Sc in OREAS 603 (Certified Value 1.06 ppm)

Sc Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 1.12 1.20 1.00 1.00
1 2 1.11 1.20 1.00 1.00
1 3 1.12 1.20 1.00 1.00
1 4 1.13 1.10 1.00 1.00
1 5 1.12 1.10 1.00 1.00
1 6 1.13 1.20 1.00 1.00
Mean 1.12 1.17 1.00 1.00
Median 1.12 1.20 1.00 1.00
Std Dev. 0.006 0.052 0.000 0.000
Rel.Std.Dev. 0.58% 4.43% 0.00% 0.00%
PDM3 5.55% 9.68% -5.99% -5.99%
Z-Score (Absolute) NA NA NA NA
Analytical results for Se in OREAS 603 (Certified Value 59 ppm)

Se Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
0.5g 40g 20g 0.15g
1 1 67 60 60 55
1 2 66 60 60 56
1 3 68 60 60 55
1 4 67 59 61 56
1 5 68 60 60 56
1 6 68 58 61 56
Mean 67 60 60 56
Median 67 60 60 56
Std Dev. 1 1 0 1
Rel.Std.Dev. 1.05% 1.41% 0.71% 0.93%
PDM3 13.67% 0.62% 2.13% -5.87%
Z-Score (Absolute) 1.02 0.02 0.10 0.54
Analytical results for Sm in OREAS 603 (Certified Value 1.12 ppm)

Sm Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 1.17 1.27 1.00 1.01
1 2 1.19 1.30 0.99 1.04
1 3 1.19 1.24 1.01 1.01
1 4 1.17 1.28 1.03 1.06
1 5 1.15 1.27 0.97 1.04
1 6 1.16 1.28 1.04 1.08
Mean 1.17 1.27 1.01 1.04
Median 1.17 1.27 1.00 1.04
Std Dev. 0.016 0.021 0.025 0.028
Rel.Std.Dev. 1.37% 1.65% 2.45% 2.65%
PDM3 4.92% 13.94% -9.90% -6.87%
Z-Score (Absolute) 0.38 0.95 0.57 0.38
Analytical results for Sn in OREAS 603 (Certified Value 12 ppm)

Sn Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
0.5g 40g 20g 0.15g
1 1 13.7 11.5 11.6 11.0
1 2 13.6 10.8 11.8 12.0
1 3 13.8 10.9 11.9 12.0
1 4 14.3 11.5 11.9 12.0
1 5 14.0 11.6 11.8 12.0
1 6 13.9 10.7 11.7 12.0
Mean 13.9 11.2 11.8 11.8
Median 13.8 11.2 11.8 12.0
Std Dev. 0.248 0.397 0.126 0.408
Rel.Std.Dev. 1.79% 3.56% 1.07% 3.45%
PDM3 15.75% -6.98% -1.68% -1.28%
Z-Score (Absolute) 1.87 0.70 0.10 0.05
Analytical results for Sr in OREAS 603 (Certified Value 46.4 ppm)

Sr Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 36.0 71.5 52.0 50.0
1 2 37.0 70.5 52.0 51.0
1 3 36.0 70.6 53.0 50.0
1 4 35.8 68.2 53.0 50.0
1 5 36.3 70.1 54.0 50.0
1 6 36.7 69.3 53.0 50.0
Mean 36.3 70.0 52.8 50.2
Median 36.2 70.3 53.0 50.0
Std Dev. 0.4 1.2 0.8 0.4
Rel.Std.Dev. 1.23% 1.65% 1.42% 0.81%
PDM3 -21.68% 51.04% 13.93% 8.18%
Z-Score (Absolute) 1.47 2.77 0.61 0.27
Analytical results for Ta in OREAS 603 (Indicative Value < 0.01 ppm)
Ta Round Replicate Lab Lab Lab Lab
No No 02 09 14 15
40g 20g 0.5g 01g
1 1 0.130 < 0.01 < 0.01 < 0.1
1 2 0.110 < 0.01 < 0.01 < 0.1
1 3 0.110 < 0.01 < 0.01 < 0.1
1 4 0.100 < 0.01 < 0.01 < 0.1
1 5 0.120 < 0.01 < 0.01 < 0.1
1 6 0.090 < 0.01 < 0.01 < 0.1
Mean 0.110
Median 0.110
Std Dev. 0.014
Rel.Std.Dev. 12.86%
PDM3
Z-Score (Absolute) 0.67 NA NA NA
Analytical results for Tb in OREAS 603 (Certified Value 0.11 ppm)

Tb Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 0.12 0.14 0.10 0.11
1 2 0.12 0.14 0.10 0.12
1 3 0.12 0.13 0.11 0.11
1 4 0.12 0.13 0.11 0.11
1 5 0.12 0.14 0.10 0.11
1 6 0.12 0.14 0.11 0.12
Mean 0.12 0.14 0.10 0.11
Median 0.12 0.14 0.10 0.11
Std Dev. 0.000 0.005 0.006 0.002
Rel.Std.Dev. 0.00% 3.63% 5.46% 2.17%
PDM3 5.19% 21.58% -9.79% -0.94%
Z-Score (Absolute) 0.62 1.63 0.30 0.25
Analytical results for Te in OREAS 603 (Certified Value 57 ppm)

Te Round Replicate Lab Lab Lab Lab
No No 02 09 11 14
40g 20g 0.15g 0.5g
1 1 61 52 56 58
1 2 60 54 55 58
1 3 62 52 53 57
1 4 62 52 51 57
1 5 62 52 55 58
1 6 63 54 55 58
Mean 62 53 54 58
Median 62 52 55 58
Std Dev. 0.8 0.7 1.8 0.4
Rel.Std.Dev. 1.29% 1.37% 3.39% 0.63%
PDM3 7.33% -8.00% -5.53% 0.41%
Z-Score (Absolute) 1.15 1.22 0.67 0.08
Analytical results for Th in OREAS 603 (Certified Value 2.3 ppm)

Th Round Replicate Lab Lab Lab Lab
No No 02 05 06 07
AR*MS AR*OES AR*OES AR*OES
40g 01g 01g 01g
1 1 2.64 < 20 < 20 < 20
1 2 2.68 < 20 < 20 < 20
1 3 2.56 < 20 < 20 < 20
1 4 2.64 < 20 < 20 < 20
1 5 2.67 < 20 < 20 < 20
1 6 2.49 < 20 < 20 < 20
Mean 2.61
Median 2.64
Std Dev. 0.074
Rel.Std.Dev. 2.82%
PDM3 13.61%
Analytical results for Ti in OREAS 603 (Certified Value 98 ppm)

Ti Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 105 92 100 100
1 2 105 92 100 100
1 3 105 88 100 100
1 4 105 90 100 100
1 5 105 90 100 100
1 6 105 92 100 100
Mean 105 91 100 100
Median 105 91 100 100
Std Dev. 0 2 0 0
Rel.Std.Dev. 0.00% 1.80% 0.00% 0.00%
PDM3 7.48% -7.19% 2.36% 2.36%
Z-Score (Absolute) 1.35 2.52 0.00 0.00
Analytical results for Tl in OREAS 603 (Certified Value 4.07 ppm)

Tl Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 <5 4.51 < 10 < 10
1 2 <5 4.47 < 10 < 10
1 3 <5 4.58 < 10 < 10
1 4 <5 4.65 < 10 < 10
1 5 <5 4.68 < 10 < 10
1 6 <5 4.49 < 10 < 10
Mean 4.56
Median 4.55
Std Dev. 0.088
Rel.Std.Dev. 1.92%
PDM3 12.17%
Z-Score (Absolute) NA 0.05 NA NA
Analytical results for Tm in OREAS 603 (Indicative Value 0.028 ppm)

Tm Round Replicate Lab Lab Lab Lab
No No 02 09 14 15
40g 20g 0.5g 01g
1 1 0.030 0.028 0.030 < 0.1
1 2 0.030 0.031 0.030 < 0.1
1 3 0.030 0.034 0.030 < 0.1
1 4 0.030 0.030 0.030 < 0.1
1 5 0.030 0.029 0.030 < 0.1
1 6 0.030 0.035 0.030 < 0.1
Mean 0.030 0.031 0.030
Median 0.030 0.030 0.030
Std Dev. 0.000 0.003 0.000
Rel.Std.Dev. 0.00% 8.08% 0.00%
PDM3 7.91% 12.24% 7.91%
Analytical results for U in OREAS 603 (Certified Value 0.89 ppm)

U Round Replicate Lab Lab Lab Lab
No No 02 05 07 08
AR*MS AR*OES AR*OES AR*OES
40g 01g 01g 01g
1 1 0.96 < 10 < 10 < 10
1 2 0.98 < 10 < 10 < 10
1 3 0.94 < 10 < 10 < 10
1 4 0.98 < 10 < 10 < 10
1 5 0.97 < 10 < 10 < 10
1 6 0.92 < 10 < 10 < 10
Mean 0.96
Median 0.97
Std Dev. 0.024
Rel.Std.Dev. 2.51%
PDM3 8.28%
Analytical results for V in OREAS 603 (Certified Value 10 ppm)

V Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 12.1 11.0 10.0 10.0
1 2 12.0 11.0 10.0 10.0
1 3 12.2 11.0 10.0 10.0
1 4 12.3 11.0 10.0 9.0
1 5 12.6 11.0 10.0 10.0
1 6 12.7 11.0 10.0 10.0
Mean 12.3 11.0 10.0 9.8
Median 12.2 11.0 10.0 10.0
Std Dev. 0.3 0.0 0.0 0.4
Rel.Std.Dev. 2.17% 0.00% 0.00% 4.15%
PDM3 22.84% 9.67% -0.30% -1.96%
Z-Score (Absolute) 2.01 0.94 0.13 0.00
Analytical results for W in OREAS 603 (Certified Value 3.88 ppm)

W Round Replicate Lab Lab Lab Lab
No No 01 02 05 07
0.5g 40g 01g 01g
1 1 <5 4.40 < 10 10.00
1 2 <5 4.47 < 10 10.00
1 3 <5 4.80 < 10 10.00
1 4 <5 4.34 < 10 10.00
1 5 <5 4.34 < 10 10.00
1 6 <5 4.80 < 10 10.00
Mean 4.53 10.00
Median 4.44 10.00
Std Dev. 0.218 0.000
Rel.Std.Dev. 4.83% 0.00%
PDM3 16.58% 157.63%
Z-Score (Absolute) NA 0.26 NA 5.78
Analytical results for Y in OREAS 603 (Certified Value 2.28 ppm)

Y Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
0.5g 40g 20g 0.15g
1 1 3.12 2.36 2.41 2.00
1 2 3.05 2.36 2.57 2.00
1 3 3.09 2.37 2.45 2.00
1 4 3.14 2.34 2.43 2.00
1 5 3.00 2.32 2.53 2.00
1 6 3.08 2.40 2.53 2.00
Mean 3.08 2.36 2.48 2.00
Median 3.09 2.36 2.49 2.00
Std Dev. 0.049 0.027 0.064 0.000
Rel.Std.Dev. 1.60% 1.15% 2.59% 0.00%
PDM3 35.07% 3.40% 8.93% -12.31%
Z-Score (Absolute) 2.75 0.46 0.86 0.67
Analytical results for Yb in OREAS 603 (Certified Value 0.17 ppm)

Yb Round Replicate Lab Lab Lab Lab
No No 02 09 13 14
40g 20g 01g 0.5g
1 1 0.20 0.17 0.17 0.17
1 2 0.19 0.20 0.17 0.18
1 3 0.19 0.19 0.18 0.18
1 4 0.19 0.19 0.19 0.17
1 5 0.19 0.18 0.19 0.18
1 6 0.19 0.19 0.19 0.18
Mean 0.19 0.19 0.18 0.18
Median 0.19 0.19 0.18 0.18
Std Dev. 0.004 0.012 0.011 0.005
Rel.Std.Dev. 2.13% 6.32% 5.88% 2.92%
PDM3 9.72% 7.38% 3.08% 1.14%
Z-Score (Absolute) 0.56 0.39 0.07 0.07
Analytical results for Zn in OREAS 603 (Certified Value 0.911 wt.%)

Zn Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
0.5g 40g 01g 01g
1 1 0.951 0.897 0.939 0.926
1 2 0.950 0.899 0.951 0.920
1 3 0.958 0.903 0.939 0.909
1 4 0.950 0.907 0.958 0.885
1 5 0.951 0.919 0.955 0.901
1 6 0.952 0.921 0.947 0.917
Mean 0.952 0.908 0.948 0.910
Median 0.951 0.905 0.949 0.913
Std Dev. 0.003 0.010 0.008 0.015
Rel.Std.Dev. 0.29% 1.13% 0.84% 1.64%
PDM3 4.53% -0.36% 4.09% -0.13%
Z-Score (Absolute) 1.38 0.06 1.27 0.12
[α]: Lab 14: Rnd 01 - AR*MS (0.5g), Rnd 01 - AR*OES (0.5g)
Analytical results for Zr in OREAS 603 (Certified Value 16 ppm)

Zr Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
0.5g 40g 20g 0.15g
1 1 18.4 16.1 18.0 13.0
1 2 18.7 16.4 18.5 15.0
1 3 19.1 16.2 18.0 13.0
1 4 19.1 15.8 18.0 14.0
1 5 19.0 16.5 18.2 14.0
1 6 19.1 15.2 18.7 13.0
Mean 18.9 16.0 18.2 13.7
Median 19.1 16.2 18.1 13.5
Std Dev. 0.3 0.5 0.3 0.8
Rel.Std.Dev. 1.54% 2.97% 1.62% 5.97%
PDM3 17.87% -0.07% 13.58% -14.82%
Z-Score (Absolute) 1.35 0.01 1.00 1.05
06 07 08 09 10 11 12
AR*OES/AAS AR*OES/AAS AR*OES/AAS AR*OES/MS AR*OES AR*AAS AR*OES
0.5g 0.5g 0.5g 20g 01g 0.5g 0.5g
287 294 304 308 284 282 > 100
290 290 305 319 272 284 > 100
302 293 305 313 282 284 > 100
299 294 306 318 288 282 > 100
303 294 305 312 290 289 > 100
303 295 304 325 284 289 > 100
297 293 305 316 283 285
301 294 305 316 284 284
7 2 1 6 6 3
2.37% 0.60% 0.25% 1.96% 2.22% 1.13%
1.51% 0.14% 4.07% 7.88% -3.27% -2.70%
0.34 0.02 0.92 1.80 0.76 0.63 NA

07 08 09 10 11 12 13
AR*OES AR*OES AR*OES/MS AR*OES AR*OES AR*OES AR*OES
01g 01g 20g 01g 0.15g 0.5g 01g
0.550 0.550 0.712 0.430 0.550 0.600 0.688
0.550 0.550 0.762 0.450 0.560 0.590 0.668
0.570 0.550 0.723 0.470 0.540 0.610 0.679
0.560 0.550 0.706 0.460 0.570 0.590 0.671
0.580 0.550 0.693 0.470 0.550 0.610 0.680
0.570 0.540 0.739 0.450 0.540 0.630 0.687
0.563 0.548 0.723 0.455 0.552 0.605 0.679
0.565 0.550 0.717 0.455 0.550 0.605 0.679
0.012 0.004 0.025 0.015 0.012 0.015 0.008
2.15% 0.74% 3.46% 3.33% 2.12% 2.51% 1.16%
-2.94% -5.52% 24.49% -21.60% -4.95% 4.24% 16.96%
0.09 0.24 1.57 1.21 0.21 0.35 1.11

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
1840 1800 1833 1730 1809 1596 2036
1840 1805 1857 1730 1871 1583 2081
1890 1770 1815 1840 1818 1638 2089
1870 1795 1801 1810 1867 1608 2043
1895 1830 1811 1850 1787 1627 2152
1885 1795 1861 1790 1794 1650 2098
1870 1799 1830 1792 1824 1617 2083
1878 1798 1824 1800 1814 1618 2085
25 19 25 52 36 26 42
1.32% 1.08% 1.37% 2.92% 1.99% 1.59% 2.02%
5.86% 1.85% 3.59% 1.43% 3.28% -8.46% 17.93%
0.93 0.24 0.54 0.17 0.49 1.54 3.02

06 07 09 14 15 18 24
AR*MS AR*MS AR*MS AR*MS AR*AAS AR*AAS AR*MS
25g 25g 25g 25g 30g 50g 40g
4.97 5.10 5.11 4.68 5.16 5.03 5.29
3.73 5.22 5.09 4.74 5.11 5.08 5.29
4.37 5.04 4.89 4.73 5.17 5.02 5.10
4.81 5.31 5.04 4.77 5.11 5.03 5.17
4.18 5.28 4.95 4.69 5.07 5.07 5.41
4.47 5.18 5.01 4.68 5.09 5.25 5.23
4.42 5.19 5.01 4.71 5.12 5.08 5.25

4.42 5.20 5.03 4.71 5.11 5.05 5.26
0.446 0.104 0.085 0.036 0.039 0.085 0.108
10.08% 2.00% 1.69% 0.76% 0.77% 1.68% 2.05%
-12.88% 2.23% -1.21% -7.11% 0.85% 0.04% 3.41%
4.73 0.67 0.56 2.67 0.18 0.35 1.10
Lab Lab Lab Lab Lab Lab

09 14 18 19 21 23
AR*OES/MS AR*OES AR*OES AR*OES/MS AR*OES AR*OES
20g 0.5g 10g 0.25g 0.25g 0.5g
< 10 <5 < 10 19.5 11.0 < 20
< 10 <5 < 10 19.4 10.0 < 20
< 10 <5 < 10 18.9 < 10 < 20
< 10 <5 < 10 18.7 < 10 < 20
< 10 <5 < 10 19.5 < 10 < 20
< 10 <5 < 10 19.1 < 10 < 20
19.2 10.5
19.3 10.5
0.3 0.7
1.75% 6.73%
NA NA NA 0.67 0.67 NA

07 08 09 11 12 13 14
01g 01g 20g 0.15g 0.5g 01g 0.5g
20 50 42 631 60 130 22
20 40 44 1606 61 128 20
10 40 43 753 52 126 22
10 40 41 1468 58 120 21
10 40 43 651 64 124 20
10 50 44 638 58 127 22
13 43 43 958 59 126 21
10 40 43 702 59 126 22
5 5 1 453 4 3 1
38.73% 11.92% 2.80% 47.28% 6.83% 2.67% 4.65%
-98.06% -93.68% -93.73% 39.63% -91.42% -81.69% -96.91%
0.67 0.00 0.01 20.56 0.35 1.85 0.50

07 08 09 11 13 14 15
AR*OES AR*OES AR*OES/MS AR*OES AR*MS AR*MS AR*OES/MS
01g 01g 20g 0.15g 01g 0.5g 01g
< 0.5 < 0.5 0.24 < 0.5 0.21 0.21 < 0.5
< 0.5 < 0.5 0.23 < 0.5 0.22 0.30 < 0.5
< 0.5 < 0.5 0.25 < 0.5 0.22 0.26 < 0.5
< 0.5 < 0.5 0.23 < 0.5 0.22 0.22 < 0.5
< 0.5 < 0.5 0.22 < 0.5 0.23 0.27 < 0.5
< 0.5 < 0.5 0.23 < 0.5 0.22 0.22 < 0.5
0.23 0.22 0.25
0.23 0.22 0.24
0.012 0.008 0.036
5.04% 3.80% 14.43%
NA NA 0.55 NA 0.30 0.80 NA

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
154 153 121 160 138 161 126
155 154 122 160 144 159 134
160 155 125 180 141 172 131
156 150 121 170 147 158 132
156 152 122 170 142 160 124
161 150 125 170 141 164 128
157 152 123 168 142 162 129
156 153 122 170 142 161 130
3 2 2 8 3 5 4
1.80% 1.36% 1.49% 4.47% 2.15% 3.18% 2.83%
4.10% 1.01% -18.56% 11.62% -5.73% 7.64% -14.26%
0.31 0.20 3.39 1.53 1.30 0.67 2.69

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
0.250 0.250 0.245 0.240 0.240 0.250 0.207
0.250 0.240 0.255 0.250 0.250 0.250 0.207
0.260 0.250 0.259 0.270 0.240 0.250 0.211
0.250 0.250 0.247 0.270 0.260 0.250 0.205
0.260 0.250 0.249 0.270 0.240 0.250 0.217
0.250 0.240 0.254 0.260 0.240 0.250 0.213
0.253 0.247 0.252 0.260 0.245 0.250 0.210
0.250 0.250 0.251 0.265 0.240 0.250 0.209
0.005 0.005 0.005 0.013 0.008 0.000 0.005
2.04% 2.09% 2.09% 4.87% 3.41% 0.00% 2.15%
6.93% 4.12% 6.17% 9.75% 3.42% 5.53% -11.37%
0.90 0.45 0.78 1.35 0.34 0.67 2.03

07 08 09 10 11 12 13
AR*OES AR*OES AR*OES/MS AR*OES AR*OES AR*OES AR*MS
01g 01g 20g 01g 0.15g 0.5g 01g
56 56 62 56 55 59 47
55 56 63 56 55 59 50
57 55 62 60 55 61 50
56 56 63 60 53 60 50
57 56 63 62 55 61 50
56 56 65 59 54 62 50
56 56 63 59 55 60 50
56 56 63 60 55 60 50
0.7 0.3 0.9 2.4 0.8 1.0 1.2
1.18% 0.58% 1.49% 4.08% 1.54% 1.68% 2.47%
1.99% 1.11% 14.57% 6.64% -1.21% 9.33% -10.12%
0.07 0.04 1.70 0.67 0.34 1.02 1.37
Lab Lab Lab Lab Lab

14 15 17 19 25
AR*OES AR*OES/MS AR*OES/MS AR*OES/MS AR*MS
0.5g 01g 0.25g 0.25g 40g
13.0 16.2 13.0 11.7 9.3
16.0 15.9 13.1 11.5 9.4
11.0 15.9 12.7 11.3 8.6
12.0 15.4 13.4 11.2 9.1
19.0 16.2 14.8 11.3 9.3
13.0 16.3 12.3 11.1 9.2
14.0 16.0 13.2 11.4 9.1
13.0 16.0 13.1 11.3 9.2
3.0 0.3 0.9 0.2 0.3
21.19% 2.04% 6.52% 1.74% 3.24%
8.06% 23.21% 2.01% -12.25% -29.53%
0.16 0.87 0.23 0.79 1.59

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
15.0 15.0 14.7 16.0 15.0 16.0 14.8
14.0 15.0 15.3 16.0 15.0 16.0 15.3
16.0 15.0 15.0 17.0 15.0 16.0 14.7
16.0 15.0 14.8 17.0 16.0 16.0 15.1
16.0 15.0 15.2 16.0 15.0 17.0 15.2
16.0 15.0 15.5 17.0 15.0 16.0 15.6
15.5 15.0 15.1 16.5 15.2 16.2 15.1
16.0 15.0 15.1 16.5 15.0 16.0 15.2
0.837 0.000 0.293 0.548 0.408 0.408 0.329
5.40% 0.00% 1.94% 3.32% 2.69% 2.53% 2.18%
2.22% -1.08% -0.45% 8.81% 0.02% 6.61% -0.33%
0.67 0.20 0.03 2.42 0.09 1.84 0.00

07 08 09 10 11 12 14
01g 01g 20g 01g 0.15g 0.5g 0.5g
31.0 30.0 33.4 24.0 31.0 30.0 28.0
28.0 34.0 29.9 26.0 33.0 29.0 30.0
32.0 31.0 28.6 25.0 31.0 31.0 29.0
31.0 32.0 30.8 27.0 31.0 29.0 31.0
32.0 31.0 30.9 28.0 33.0 31.0 28.0
29.0 28.0 33.1 27.0 31.0 30.0 30.0
30.5 31.0 31.1 26.2 31.7 30.0 29.3
31.0 31.0 30.9 26.5 31.0 30.0 29.5
1.643 2.000 1.847 1.472 1.033 0.894 1.211
5.39% 6.45% 5.94% 5.63% 3.26% 2.98% 4.13%
4.42% 6.14% 6.53% -10.41% 8.42% 2.71% 0.43%
0.22 0.45 0.50 1.72 0.75 0.00 0.30
Lab Lab Lab Lab Lab

15 17 19 24 25
AR*OES/MS AR*OES/MS AR*OES/MS AR*MS AR*MS
01g 0.25g 0.25g 40g 40g
0.93 0.75 0.64 0.60 0.60
0.95 0.82 0.62 0.60 0.60
0.93 0.77 0.61 0.60 0.58
0.96 0.86 0.61 0.60 0.60
0.90 0.67 0.62 0.70 0.58
1.01 0.74 0.62 0.60 0.60
0.95 0.77 0.62 0.62 0.59
0.94 0.76 0.62 0.60 0.60
0.037 0.066 0.012 0.041 0.010
3.93% 8.61% 1.92% 6.62% 1.74%
28.36% 4.18% -15.68% -16.38% -19.55%
1.39 0.00 1.14 1.18 1.36

06 07 08 09 10 11 12
AR*OES/AAS AR*OES/AAS AR*OES/AAS AR*OES/MS AR*OES AR*AAS AR*AAS
0.5g 0.5g 0.5g 20g 01g 0.5g 01g
1.00 1.01 1.01 1.04 0.99 1.00 1.04
1.02 0.99 1.01 1.03 0.99 1.00 1.00
1.05 1.01 1.00 1.04 1.04 1.00 1.00
1.05 1.02 1.03 1.02 1.01 1.01 1.00
1.06 1.02 1.02 1.02 1.06 1.00 1.01
1.07 1.01 1.02 1.04 0.99 1.01 1.01
1.04 1.01 1.01 1.03 1.01 1.00 1.01
1.05 1.01 1.01 1.04 1.00 1.00 1.00
0.027 0.009 0.010 0.009 0.030 0.005 0.015
2.56% 0.90% 0.97% 0.88% 2.98% 0.46% 1.50%
3.19% -0.03% 0.56% 2.63% 0.56% -0.38% 0.08%
1.78 0.17 0.47 1.49 0.47 0.00 0.07
Lab Lab
15 25
AR*OES/MS AR*MS
01g 40g
0.64 0.47
0.59 0.46
0.61 0.46
0.62 0.47
0.68 0.46
0.68 0.46
0.64 0.46
0.63 0.46
0.037 0.005
5.85% 1.11%
14.50% -16.67%
1.20 1.37
Lab
25
AR*MS
40g
0.19
0.19
0.19
0.17
0.17
0.18
0.18
0.19
0.010
5.41%
-16.55%
10.11
Lab
25
AR*MS
40g
0.20
0.20
0.21
0.19
0.20
0.18
0.20
0.20
0.010
4.96%
-21.69%
0.87

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
2.68 2.71 2.94 2.88 3.03 2.98 2.83
2.68 2.71 3.04 2.90 2.88 2.83 2.89
2.76 2.67 3.01 3.09 3.06 3.06 2.93
2.72 2.71 2.99 3.05 2.84 2.87 2.86
2.77 2.70 2.99 3.15 2.96 2.96 3.00
2.74 2.69 3.09 3.01 2.99 2.92 2.94
2.73 2.70 3.01 3.01 2.96 2.94 2.91
2.73 2.71 3.00 3.03 2.98 2.94 2.91
0.039 0.016 0.050 0.106 0.086 0.082 0.060
1.43% 0.59% 1.65% 3.53% 2.89% 2.80% 2.06%
-4.34% -5.28% 5.66% 5.78% 3.91% 3.09% 2.13%
0.73 0.86 0.67 0.69 0.43 0.31 0.18

13 14 15 17 19 23 24
AR*MS AR*MS AR*OES/MS AR*OES/MS AR*OES/MS AR*OES AR*MS
01g 0.5g 01g 0.25g 0.25g 0.5g 40g
6.43 5.75 7.48 6.80 5.41 13.00 6.90
6.56 5.90 7.63 7.30 5.32 8.00 6.60
6.64 5.68 7.54 7.10 5.27 7.00 6.90
6.39 5.79 7.39 7.40 5.20 <5 6.60
6.41 5.83 6.92 6.50 5.15 <5 8.00
6.52 5.87 7.45 6.80 5.08 10.00 6.80
6.49 5.80 7.40 6.98 5.24 9.50 6.97
6.48 5.81 7.47 6.95 5.24 9.00 6.85
0.101 0.081 0.250 0.343 0.120 2.646 0.524
1.55% 1.39% 3.37% 4.91% 2.28% 27.85% 7.52%
-1.41% -11.87% 12.40% 6.05% -20.45% 44.27% 5.80%
0.44 1.25 0.73 0.13 1.91 3.07 0.13
Lab Lab
15 25
AR*OES/MS AR*MS
01g 40g
1.15 0.76
0.91 0.73
1.04 0.71
0.88 0.74
1.15 0.71
1.06 0.70
1.03 0.72
1.05 0.72
0.115 0.022
11.19% 3.05%
19.46% -16.53%
1.43 1.18
Lab Lab Lab Lab

15 17 19 25
AR*OES/MS AR*OES/MS AR*OES/MS AR*MS
01g 0.25g 0.25g 40g
0.54 0.42 0.41 0.40
0.56 0.43 0.41 0.40
0.56 0.44 0.42 0.40
0.47 0.46 0.40 0.40
0.63 0.39 0.40 0.40
0.50 0.43 0.40 0.40
0.54 0.43 0.41 0.40
0.55 0.43 0.41 0.40
0.055 0.023 0.008 0.000
10.19% 5.41% 2.01% 0.00%
17.88% -7.07% -11.84% -13.21%
4.21 0.20 0.56 0.78

09 11 14 16 17 19 23
AR*OES/MS AR*OES AR*MS AR*OES AR*OES/MS AR*OES/MS AR*OES
20g 0.15g 0.5g 10g 0.25g 0.25g 0.5g
1.64 2.00 1.55 <5 2.83 1.65 1.00
1.66 2.00 1.62 <5 3.25 1.67 1.00
1.69 1.00 1.55 <5 3.05 1.50 1.00
1.64 1.00 1.61 <5 3.24 1.59 2.00
1.68 1.00 1.58 <5 3.09 1.55 1.00
1.68 2.00 1.68 <5 2.95 1.52 2.00
1.67 1.50 1.60 3.07 1.58 1.33
1.67 1.50 1.60 3.07 1.57 1.00
0.018 0.548 0.050 0.164 0.069 0.516
1.10% 36.51% 3.10% 5.34% 4.35% 38.73%
0.15 0.59 0.15 NA 6.42 0.24 1.33
Lab Lab
15 25
AR*OES/MS AR*MS
01g 40g
< 0.1 0.075
0.100 0.075
0.120 0.075
0.110 0.075
0.110 0.085
0.110 0.075
0.110 0.077
0.110 0.075
0.007 0.004
6.43% 5.32%
14.02% -20.53%
0.92 1.44

13 14 15 17 19 24 25
AR*MS AR*MS AR*OES/MS AR*OES/MS AR*OES/MS AR*MS AR*MS
01g 0.5g 01g 0.25g 0.25g 40g 40g
11.6 11.4 12.9 10.3 10.2 13.5 10.8
12.4 11.6 13.2 11.4 10.1 12.5 10.8
12.4 11.2 13.2 10.5 9.9 13.5 10.7
12.4 11.4 12.7 11.3 9.8 13.0 10.6
12.4 11.5 13.0 11.3 9.8 15.5 10.8
12.6 11.4 13.2 9.8 9.6 13.5 10.8
12.3 11.4 13.0 10.8 9.9 13.6 10.8
12.4 11.4 13.1 10.9 9.8 13.5 10.8
0.355 0.140 0.191 0.651 0.203 1.021 0.084
2.89% 1.22% 1.46% 6.04% 2.06% 7.51% 0.78%
5.35% -2.30% 11.59% -7.72% -15.38% 16.35% -7.92%
1.06 0.00 1.67 0.65 1.57 1.84 0.67

07 08 09 11 12 13 14
01g 01g 20g 0.15g 0.5g 01g 0.5g
0.080 0.080 0.121 0.090 0.100 0.097 0.090
0.090 0.080 0.126 0.090 0.100 0.097 0.090
0.090 0.080 0.122 0.090 0.100 0.096 0.090
0.090 0.080 0.121 0.100 0.100 0.097 0.090
0.090 0.080 0.125 0.090 0.100 0.097 0.090
0.090 0.080 0.127 0.090 0.100 0.096 0.090
0.088 0.080 0.124 0.092 0.100 0.097 0.090
0.090 0.080 0.124 0.090 0.100 0.097 0.090
0.004 0.000 0.003 0.004 0.000 0.000 0.000
4.62% 0.00% 2.07% 4.45% 0.00% 0.40% 0.00%
-4.99% -13.96% 32.97% -1.41% 7.56% 4.00% -3.20%
0.11 0.67 2.27 0.11 0.67 0.45 0.00

07 08 09 11 12 13 14
01g 01g 20g 0.15g 0.5g 01g 0.5g
< 10 10.0 7.5 7.0 6.0 4.1 4.9
10.0 10.0 7.6 6.0 6.0 4.3 5.0
< 10 10.0 7.6 7.0 6.0 4.4 5.0
< 10 10.0 7.3 6.0 5.0 4.2 5.0
< 10 10.0 7.7 6.0 6.0 4.6 4.8
< 10 10.0 7.4 6.0 6.0 4.4 5.1
10.0 10.0 7.5 6.3 5.8 4.3 5.0
10.0 10.0 7.5 6.0 6.0 4.3 5.0
0.0 0.1 0.5 0.4 0.2 0.1
0.00% 1.71% 8.15% 7.00% 4.19% 1.93%
1.86 1.86 0.79 0.27 0.13 0.59 0.32

13 14 15 16 17 18 19
AR*OES AR*MS AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS
01g 0.5g 01g 10g 0.25g 10g 0.25g
3.49 4.60 6.00 4.00 5.00 4.00 4.75
3.46 4.40 5.00 4.00 5.00 4.00 4.80
3.68 3.90 5.00 4.00 5.00 4.00 4.81
3.62 4.20 5.00 4.00 5.00 4.00 4.55
3.51 4.30 4.00 4.00 5.00 4.00 4.80
3.39 4.60 5.00 4.00 5.00 4.00 4.83
3.52 4.33 5.00 4.00 5.00 4.00 4.76
3.50 4.35 5.00 4.00 5.00 4.00 4.80
0.106 0.266 0.632 0.000 0.000 0.000 0.106
3.01% 6.13% 12.65% 0.00% 0.00% 0.00% 2.22%
-23.78% -6.28% 8.14% -13.49% 8.14% -13.49% 2.87%
1.24 0.28 0.52 0.67 0.52 0.67 0.28
Lab Lab Lab

17 19 25
AR*OES/MS AR*OES/MS AR*MS
0.25g 0.25g 40g
30 28 20
30 29 20
30 25 20
30 25 20
30 24 20
30 25 20
30 26 20
30 25 20
0 2 0
0.00% 7.69% 0.00%
13.28% -1.82% -24.48%
1.17 0.15 1.39

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
500 500 570 450 500 600 421
500 500 589 500 500 600 423
500 500 584 500 500 600 429
500 500 575 500 500 600 422
500 500 579 500 500 600 433
500 500 601 500 500 600 426
500 500 583 492 500 600 425
500 500 581 500 500 600 424
0 0 11 20 0 0 5
0.00% 0.00% 1.91% 4.15% 0.00% 0.00% 1.09%
-3.24% -3.24% 12.80% -4.85% -3.24% 16.11% -17.66%
0.00 0.00 1.68 0.17 0.00 2.02 1.51

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
125 130 134 128 119 131 127
129 125 138 129 119 129 129
130 130 136 137 117 132 132
129 129 136 135 127 128 127
132 129 137 137 119 133 134
128 123 140 133 118 136 131
129 128 137 133 120 132 130
129 129 137 134 119 132 130
2 3 2 4 4 3 3
1.80% 2.31% 1.46% 2.94% 3.00% 2.19% 2.20%
-0.53% -1.43% 5.82% 2.82% -7.48% 1.53% 0.31%
0.20 0.44 1.46 0.67 2.31 0.34 0.02

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
6.00 6.00 6.04 6.00 4.00 5.00 5.00
6.00 6.00 6.12 6.00 4.00 5.00 5.49
6.00 6.00 6.17 6.00 4.00 5.00 5.51
6.00 6.00 6.00 6.00 5.00 6.00 5.41
6.00 6.00 6.01 6.00 4.00 5.00 5.64
6.00 6.00 6.11 6.00 4.00 6.00 5.72
6.00 6.00 6.08 6.00 4.17 5.33 5.46
6.00 6.00 6.08 6.00 4.00 5.00 5.50
0.000 0.000 0.068 0.000 0.408 0.516 0.251
0.00% 0.00% 1.11% 0.00% 9.80% 9.68% 4.60%
-1.71% -1.71% -0.47% -1.71% -31.75% -12.64% -10.51%
0.00 0.00 0.12 0.00 2.81 1.02 0.68

07 08 09 11 12 13 14
01g 01g 20g 0.15g 0.5g 01g 0.5g
200 200 298 200 300 261 200
200 200 322 300 300 257 300
200 200 312 200 300 261 200
200 200 307 300 300 257 300
200 200 311 200 300 255 200
200 200 317 200 300 254 300
200 200 311 233 300 258 250
200 200 311 200 300 257 250
0 0 8 52 0 3 55
0.00% 0.00% 2.67% 22.13% 0.00% 1.21% 21.91%
-27.17% -27.17% 13.26% -15.04% 9.24% -6.21% -8.97%
1.35 1.35 0.15 0.90 0.00 0.57 0.67
Lab Lab Lab Lab Lab

14 15 17 19 25
AR*MS AR*OES/MS AR*OES/MS AR*OES/MS AR*MS
0.5g 01g 0.25g 0.25g 40g
0.31 0.59 0.25 0.46 0.20
0.28 0.58 0.26 0.43 < 0.2
0.28 0.62 0.26 0.42 < 0.2
0.30 0.66 0.27 0.40 0.20
0.30 0.68 0.30 0.53 < 0.2
0.30 0.63 0.26 0.51 < 0.2
0.30 0.63 0.27 0.46 0.20
0.30 0.63 0.26 0.44 0.20
0.012 0.039 0.018 0.050 0.000
4.15% 6.19% 6.57% 10.92% 0.00%
0.19 2.62 0.48 1.19 0.99
Lab Lab
15 25
AR*OES/MS AR*MS
01g 40g
6.76 4.94
6.61 4.83
6.10 4.81
6.14 4.84
6.86 4.75
6.66 4.76
6.52 4.82
6.64 4.82
0.323 0.069
4.95% 1.42%
10.58% -18.25%
0.63 1.24

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
116 112 116 123 109 114 99
114 114 117 147 111 113 98
118 112 114 133 108 115 98
116 114 115 133 115 110 97
119 113 117 136 109 115 97
117 112 117 130 111 116 98
117 113 116 134 111 114 98
117 113 116 133 110 115 98
2 1 1 8 3 2 1
1.50% 0.87% 1.08% 5.90% 2.27% 1.88% 0.62%
3.56% 0.15% 3.11% 18.64% -1.92% 1.04% -13.02%
1.19 0.20 1.06 5.61 0.41 0.46 3.66

07 08 09 11 12 13 14
01g 01g 20g 0.15g 0.5g 01g 0.5g
160 160 200 155 222 353 168
160 160 209 160 224 350 170
160 160 220 152 230 351 170
160 170 190 163 232 346 164
170 160 203 152 219 357 168
170 160 210 154 223 348 169
163 162 205 156 225 351 168
160 160 206 155 224 350 169
5 4 10 5 5 4 2
3.16% 2.53% 4.85% 2.90% 2.21% 1.09% 1.33%
-5.29% -6.26% 18.99% -9.54% 30.46% 103.56% -2.49%
0.18 0.24 1.37 0.45 2.11 6.79 0.00

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
1680 1680 1676 1870 1694 1668 1702
1680 1680 1686 1860 1709 1656 1729
1730 1670 1677 1970 1695 1689 1759
1720 1680 1683 1970 1742 1628 1705
1740 1680 1688 2010 1692 1698 1797
1720 1670 1688 1950 1690 1729 1751
1712 1677 1683 1938 1704 1678 1740
1720 1680 1684 1960 1695 1679 1740
26 5 5 60 20 35 36
1.50% 0.31% 0.31% 3.10% 1.17% 2.10% 2.07%
1.24% -0.83% -0.45% 14.65% 0.77% -0.75% 2.95%
0.44 0.35 0.20 5.53 0.26 0.32 1.09
Lab Lab
15 25
AR*OES/MS AR*MS
01g 40g
1.92 1.16
1.93 1.14
1.88 1.10
1.85 1.13
1.80 1.13
1.88 1.16
1.88 1.14
1.88 1.14
0.048 0.023
2.54% 1.98%
19.91% -27.37%
1.11 1.96
Lab Lab Lab Lab Lab
15 17 19 24 25
AR*OES/MS AR*OES/MS AR*OES/MS AR*MS AR*MS
01g 0.25g 0.25g 40g 40g
5.98 5.70 3.89 4.30 4.25
6.07 6.20 3.82 4.00 4.10
5.78 6.00 3.69 4.20 4.10
5.94 6.20 3.63 4.20 4.20
6.07 5.20 3.73 4.90 4.15
6.17 5.80 3.66 4.30 4.00
6.00 5.85 3.74 4.32 4.13
6.03 5.90 3.71 4.25 4.13
0.135 0.378 0.100 0.306 0.088
2.25% 6.46% 2.67% 7.09% 2.12%
22.61% 19.51% -23.66% -11.81% -15.56%
1.03 0.90 0.83 0.45 0.50
Lab
15
AR*OES/MS
01g
10
10
30
< 10
< 10
10
15
10
10
66.67%
969.49%
9.09
07 08 09 10 11 13 14
01g 01g 20g 01g 0.15g 01g 0.5g
3.38 3.51 3.79 3.62 3.45 3.56 3.35
3.39 3.52 3.79 3.62 3.45 3.55 3.46
3.47 3.48 3.66 3.83 3.53 3.54 3.29
3.43 3.52 3.73 3.78 3.41 3.50 3.38
3.49 3.51 3.79 3.88 3.44 3.57 3.44
3.44 3.50 3.74 3.73 3.48 3.54 3.48
3.43 3.51 3.75 3.74 3.46 3.54 3.40
3.44 3.51 3.76 3.76 3.45 3.55 3.41
0.043 0.015 0.053 0.108 0.041 0.024 0.073
1.26% 0.43% 1.41% 2.88% 1.18% 0.66% 2.14%
-0.74% 1.38% 8.39% 8.22% 0.03% 2.44% -1.71%
0.15 0.26 1.60 1.56 0.00 0.46 0.33

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
171 202 128 150 169 161 129
167 202 134 140 173 161 133
169 203 133 150 174 165 131
174 204 132 150 186 159 126
171 201 133 160 172 161 136
171 201 136 140 170 166 133
171 202 133 148 174 162 131
171 202 133 150 173 161 132
2 1 3 8 6 3 3
1.38% 0.58% 1.98% 5.07% 3.54% 1.67% 2.65%
6.53% 26.32% -17.16% -7.32% 8.72% 1.32% -17.97%
0.46 1.42 0.69 0.21 0.49 0.21 0.72

07 08 09 11 12 13 14
AR*OES AR*OES AR*OES/MS AR*OES AR*OES AR*MS AR*MS
01g 01g 20g 0.15g 0.5g 01g 0.5g
1.00 1.00 1.35 1.00 1.00 1.11 1.03
1.00 1.00 1.30 1.00 1.00 1.12 1.12
1.00 1.00 1.27 1.00 1.00 1.16 0.94
1.00 1.00 1.39 1.00 1.00 1.18 0.96
1.00 1.00 1.33 1.00 1.00 1.16 0.97
1.00 1.00 1.37 1.00 1.00 1.18 1.00
1.00 1.00 1.34 1.00 1.00 1.15 1.00
1.00 1.00 1.34 1.00 1.00 1.16 0.99
0.000 0.000 0.043 0.000 0.000 0.031 0.065
0.00% 0.00% 3.20% 0.00% 0.00% 2.72% 6.51%
-5.99% -5.99% 25.52% -5.99% -5.99% 8.17% -5.68%
NA NA NA NA NA NA NA

14 15 17 18 19 21 24
AR*MS AR*OES/MS AR*OES/MS AR*OES AR*OES/MS AR*OES AR*MS
0.5g 01g 0.25g 10g 0.25g 0.25g 40g
56 72 70 46 47 64 58
58 70 75 52 49 62 60
55 70 71 41 47 60 62
56 70 76 42 46 70 56
56 68 75 55 48 53 65
57 71 67 43 47 58 59
56 70 72 47 47 61 60
56 70 73 45 47 61 59
1 1 4 6 1 6 3
1.48% 1.75% 4.92% 12.37% 2.43% 9.39% 5.20%
-4.94% 18.62% 22.32% -21.37% -19.86% 3.43% 1.18%
0.47 1.41 1.71 1.78 1.71 0.20 0.02
Lab Lab
15 25
AR*OES/MS AR*MS
01g 40g
1.20 0.98
1.35 0.96
1.08 0.94
1.18 0.99
1.40 0.97
1.24 0.97
1.24 0.97
1.22 0.97
0.117 0.017
9.43% 1.78%
11.19% -13.28%
0.78 0.79

14 15 16 17 18 19 21
AR*MS AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
12.2 12.8 12.0 11.6 < 10 10.4 13.0
12.1 12.8 10.0 12.0 < 10 10.3 17.0
12.0 12.6 12.0 12.0 < 10 10.2 18.0
12.1 12.7 11.0 12.7 < 10 10.0 14.0
12.1 12.7 < 10 9.7 < 10 10.2 13.0
12.1 12.5 11.0 11.1 < 10 10.0 13.0
12.1 12.7 11.2 11.5 10.2 14.7
12.1 12.7 11.0 11.8 10.2 13.5
0.063 0.113 0.837 1.034 0.145 2.251
0.52% 0.89% 7.47% 8.98% 1.43% 15.35%
0.94% 5.70% -6.57% -3.93% -15.09% 22.35%
0.20 0.73 0.65 0.35 NA 1.61 2.61

07 08 09 11 12 13 14
01g 01g 20g 0.15g 0.5g 01g 0.5g
48.0 55.0 69.6 61.0 51.0 41.1 44.6
49.0 52.0 69.7 75.0 50.0 42.4 44.0
48.0 52.0 70.8 63.0 50.0 42.7 44.4
48.0 53.0 70.6 75.0 50.0 40.5 44.8
51.0 52.0 71.6 64.0 50.0 42.4 44.3
48.0 54.0 71.6 63.0 51.0 42.6 45.1
48.7 53.0 70.6 66.8 50.3 42.0 44.5
48.0 52.5 70.7 63.5 50.0 42.4 44.5
1.2 1.3 0.9 6.4 0.5 0.9 0.4
2.49% 2.39% 1.26% 9.58% 1.03% 2.17% 0.92%
4.94% 14.29% 52.34% 44.12% 8.54% -9.50% -3.94%
0.08 0.63 2.84 2.36 0.29 0.72 0.43
Lab Lab Lab

17 19 25
AR*OES/MS AR*OES/MS AR*MS
0.25g 0.25g 40g
0.120 < 0.05 < 0.005
0.120 < 0.05 < 0.005
0.120 < 0.05 < 0.005
0.110 < 0.05 < 0.005
0.120 < 0.05 < 0.005
0.110 < 0.05 < 0.005
0.117
0.120
0.005
4.43%
0.67 NA NA
Lab Lab Lab Lab

15 17 19 25
01g 0.25g 0.25g 40g
0.15 0.09 0.11 0.09
0.15 0.10 0.11 0.09
0.15 0.09 0.10 0.09
0.13 0.10 0.10 0.10
0.14 0.10 0.10 0.10
0.16 0.09 0.10 0.09
0.15 0.10 0.10 0.09
0.15 0.10 0.10 0.09
0.010 0.005 0.003 0.004
7.04% 5.77% 3.25% 4.52%
28.57% -16.72% -8.98% -18.91%
2.06 0.72 0.25 0.86
Lab Lab Lab Lab

15 17 19 25
AR*OES AR*OES/MS AR*OES/MS AR*MS
01g 0.25g 0.25g 40g
60 42 58 58
61 48 58 57
65 44 57 58
59 48 56 59
59 45 57 58
60 42 57 58
61 45 57 58
60 44 57 58
2.3 2.7 0.6 0.7
3.71% 6.16% 1.10% 1.16%
5.81% -22.19% -0.62% 1.01%
0.68 3.42 0.08 0.17

08 09 13 14 15 17 18
AR*OES AR*OES/MS AR*MS AR*MS AR*OES/MS AR*OES/MS AR*OES
01g 20g 01g 0.5g 01g 0.25g 10g
< 20 2.36 1.94 1.93 2.72 2.30 < 10
< 20 2.35 2.07 1.97 2.82 2.60 < 10
< 20 2.38 2.01 1.90 2.74 2.40 < 10
< 20 2.35 2.03 1.89 2.74 2.50 < 10
< 20 2.36 1.99 1.90 2.82 2.20 < 10
< 20 2.34 2.08 1.96 2.75 2.30 < 10
2.36 2.02 1.93 2.77 2.38
2.36 2.02 1.92 2.75 2.35
0.014 0.054 0.034 0.044 0.147
0.59% 2.67% 1.76% 1.58% 6.18%
2.51% -12.15% -16.31% 20.21% 3.61%
NA 0.53 0.46 0.75 1.73 0.60 NA

07 08 09 11 12 14 15
01g 01g 20g 0.15g 0.5g 0.5g 01g
100 100 113 < 100 < 100 65 100
100 100 119 < 100 < 100 65 100
100 100 116 < 100 < 100 65 100
100 100 118 < 100 < 100 67 100
100 100 118 < 100 < 100 66 100
100 100 123 < 100 < 100 66 100
100 100 118 66 100
100 100 118 66 100
0 0 3 1 0
0.00% 0.00% 2.96% 1.24% 0.00%
2.36% 2.36% 20.67% -32.78% 2.36%
0.00 0.00 4.82 NA NA 9.26 0.00

07 08 09 11 12 13 14
AR*OES AR*OES AR*OES/MS AR*OES AR*OES AR*MS AR*MS
01g 01g 20g 0.15g 0.5g 01g 0.5g
< 10 < 10 3.64 <5 < 10 2.69 4.10
10.00 10.00 3.71 <5 < 10 2.89 4.24
10.00 10.00 3.79 <5 < 10 2.91 4.03
10.00 < 10 3.63 <5 < 10 2.85 4.07
< 10 10.00 3.67 <5 < 10 2.81 4.10
< 10 < 10 3.73 <5 < 10 2.89 4.20
10.00 10.00 3.70 2.84 4.12
10.00 10.00 3.69 2.87 4.10
0.000 0.000 0.061 0.081 0.080
0.00% 0.00% 1.66% 2.84% 1.94%
145.81% 145.81% -9.14% -30.17% 1.35%
4.58 4.58 0.68 NA NA 1.37 0.32
Lab
25
AR*MS
40g
0.020
0.025
0.020
0.020
0.020
0.020
0.021
0.020
0.002
9.80%
-25.06%
11.22

09 11 13 14 15 17 18
AR*OES/MS AR*OES AR*MS AR*MS AR*OES/MS AR*OES/MS AR*OES
20g 0.15g 01g 0.5g 01g 0.25g 10g
0.89 < 10 0.72 0.84 0.96 1.01 < 10
0.89 < 10 0.74 0.84 0.97 1.08 < 10
0.90 < 10 0.78 0.79 0.98 1.02 < 10
0.89 < 10 0.73 0.79 0.98 1.06 < 10
0.93 < 10 0.75 0.80 0.97 0.87 < 10
0.90 < 10 0.78 0.81 1.01 0.97 < 10
0.90 0.75 0.81 0.98 1.00
0.90 0.74 0.81 0.98 1.02
0.015 0.026 0.023 0.017 0.075
1.65% 3.48% 2.85% 1.76% 7.51%
1.77% -15.00% -8.29% 10.54% 13.17%
0.00 NA 1.29 0.77 0.67 0.88 NA

07 08 09 11 12 13 14
01g 01g 20g 0.15g 0.5g 01g 0.5g
9.0 10.0 11.6 9.0 10.0 8.3 10.0
9.0 10.0 12.1 10.0 10.0 8.7 10.0
10.0 10.0 12.0 9.0 11.0 8.9 10.0
10.0 10.0 11.8 10.0 10.0 8.9 10.0
10.0 9.0 12.1 9.0 11.0 8.8 10.0
10.0 10.0 12.6 9.0 11.0 9.1 10.0
9.7 9.8 12.0 9.3 10.5 8.8 10.0
10.0 10.0 12.1 9.0 10.5 8.9 10.0
0.5 0.4 0.3 0.5 0.5 0.3 0.0
5.34% 4.15% 2.59% 5.53% 5.22% 3.08% 0.00%
-3.62% -1.96% 20.00% -6.95% 4.68% -12.19% -0.30%
0.13 0.00 1.78 0.40 0.54 0.83 0.13

08 09 11 13 14 15 17
AR*OES AR*OES/MS AR*OES AR*MS AR*MS AR*OES/MS AR*OES/MS
01g 20g 0.15g 01g 0.5g 01g 0.25g
< 10 3.34 < 10 2.92 3.87 4.77 3.70
10.00 3.45 < 10 3.04 3.94 4.55 4.20
< 10 3.52 < 10 2.88 3.80 4.77 3.90
< 10 3.51 < 10 2.92 3.98 4.92 4.30
10.00 3.38 < 10 3.01 3.84 4.70 4.00
10.00 3.59 < 10 3.03 3.91 4.77 3.90
10.00 3.46 2.97 3.89 4.75 4.00
10.00 3.48 2.97 3.89 4.77 3.95
0.000 0.092 0.070 0.066 0.120 0.219
0.00% 2.65% 2.36% 1.71% 2.54% 5.48%
157.63% -10.73% -23.57% 0.22% 22.29% 3.05%
5.78 0.80 NA 1.31 0.38 0.53 0.26

13 14 15 16 17 18 19
AR*MS AR*MS AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS
01g 0.5g 01g 10g 0.25g 10g 0.25g
2.42 2.45 2.00 <5 1.79 <1 2.29
2.61 2.44 2.00 <5 1.80 <1 2.23
2.58 2.37 2.00 <5 1.79 <1 2.22
2.62 2.36 2.00 <5 1.83 <1 2.20
2.61 2.42 2.00 <5 1.69 <1 2.22
2.78 2.44 2.00 <5 1.75 <1 2.19
2.60 2.41 2.00 1.78 2.23
2.61 2.43 2.00 1.79 2.22
0.114 0.039 0.000 0.049 0.035
4.37% 1.61% 0.00% 2.75% 1.58%
14.08% 5.81% -12.31% -22.17% -2.41%
1.23 0.64 0.67 NA 1.33 NA 0.00
Lab Lab Lab Lab

15 17 19 25
01g 0.25g 0.25g 40g
0.15 0.20 0.17 0.16
0.16 0.20 0.17 0.16
0.14 0.20 0.15 0.16
0.14 0.20 0.15 0.16
0.15 0.20 0.16 0.15
0.13 0.20 0.16 0.15
0.15 0.20 0.16 0.16
0.15 0.20 0.16 0.16
0.010 0.000 0.007 0.005
7.23% 0.00% 4.20% 3.30%
-16.99% 14.49% -8.50% -10.31%
1.41 0.92 0.79 0.92

07 08 09 10 11 12 13
01g 01g 20g 01g 0.15g 0.5g 01g
0.961 0.945 0.939 0.897 0.903 0.887 0.778
0.958 0.924 0.942 0.893 0.909 0.882 0.772
0.991 0.931 0.956 0.955 0.903 0.902 0.784
0.980 0.942 0.953 0.950 0.900 0.880 0.769
0.993 0.944 0.954 0.982 0.900 0.900 0.763
0.971 0.900 0.960 0.943 0.908 0.898 0.777
0.976 0.931 0.951 0.937 0.904 0.891 0.774
0.976 0.937 0.954 0.947 0.903 0.892 0.775
0.015 0.017 0.008 0.035 0.004 0.010 0.007
1.52% 1.86% 0.87% 3.73% 0.43% 1.11% 0.95%
7.11% 2.21% 4.40% 2.83% -0.77% -2.15% -15.06%
2.09 0.75 1.35 0.92 0.06 0.43 3.94

12 13 14 15 16 17 18
AR*OES AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES
0.5g 01g 0.5g 01g 10g 0.25g 10g
17.0 15.8 16.0 17.7 14.9 15.1 14.0
17.0 16.0 16.0 18.3 14.6 15.3 14.0
17.0 16.2 16.0 17.6 14.2 15.0 15.0
17.0 16.6 16.0 18.0 14.7 15.4 14.0
17.0 16.3 16.0 18.4 14.2 15.6 15.0
18.0 16.5 16.0 17.6 13.8 15.1 14.0
17.2 16.2 16.0 17.9 14.4 15.3 14.3
17.0 16.2 16.0 17.8 14.4 15.2 14.0
0.4 0.3 0.0 0.4 0.4 0.2 0.5
2.38% 1.91% 0.00% 2.00% 2.81% 1.48% 3.60%
6.99% 1.17% -0.28% 11.81% -10.25% -4.96% -10.67%
0.52 0.10 0.00 0.87 0.72 0.34 0.75
13 14 15 16 17 18 19
AR*MS AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES/MS
01g 0.5g 01g 10g 0.25g 10g 0.25g
293 > 200 294 > 100 - 260 > 100
298 > 200 306 > 100 - 263 > 100
293 > 200 295 > 100 - 265 > 100
289 > 200 304 > 100 - 261 > 100
294 > 200 297 > 100 - 272 > 100
291 > 200 305 > 100 - 275 > 100
293 300 266
293 300 264
3 6 6
1.07% 1.86% 2.31%
0.04% 2.49% -9.19%
0.00 NA 0.56 NA NA 2.12 NA

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
0.560 0.760 0.530 0.660 0.480 0.578 0.440
0.570 0.750 0.510 0.660 0.470 0.580 0.430
0.570 0.750 0.500 0.670 0.470 0.571 0.420
0.570 0.750 0.510 0.660 0.460 0.545 0.420
0.580 0.750 0.500 0.650 0.470 0.579 0.410
0.580 0.760 0.490 0.660 0.450 0.589 0.430
0.572 0.753 0.507 0.660 0.467 0.574 0.425
0.570 0.750 0.505 0.660 0.470 0.579 0.425
0.008 0.005 0.014 0.006 0.010 0.015 0.010
1.32% 0.69% 2.70% 0.96% 2.21% 2.65% 2.47%
-1.50% 29.80% -12.70% 13.72% -19.59% -1.16% -26.77%
0.00 1.88 0.67 0.92 1.09 0.08 1.52

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
1744 1958 1628 1390 1604 1697 1727
1809 1940 1644 1390 1623 1688 1716
1717 1915 1646 1430 1677 1668 1697
1763 1921 1685 1455 1632 1645 1713
1773 1925 1633 1405 1675 1631 1688
1785 1957 1593 1355 1677 1622 1700
1765 1936 1638 1404 1648 1658 1707
1768 1933 1639 1398 1654 1656 1707
32 19 30 35 32 31 14
1.82% 0.96% 1.82% 2.48% 1.96% 1.84% 0.84%
-0.07% 9.60% -7.26% -20.51% -6.71% -6.12% -3.38%
0.09 1.58 1.33 3.62 1.23 1.13 0.66
Lab Lab Lab

25 26 27
AR*MS AR*AAS AR*AAS
40g 40g 40g
5.23 5.24 5.10
5.23 5.23 5.16
5.33 5.27 4.99
5.26 5.25 5.17
5.22 5.19 5.14
5.31 5.35 5.00
5.26 5.26 5.09

5.25 5.25 5.12
0.046 0.054 0.081
0.88% 1.02% 1.60%
3.71% 3.54% 0.34%
1.20 1.14 0.00
16 17 18 21 23 25
AR*OES AR*OES/MS AR*OES AR*OES AR*OES AR*MS
10g 0.25g 10g 0.25g 0.5g 40g
104 62 98 430 13 36
90 60 104 409 12 38
104 59 101 388 12 36
123 61 96 428 12 35
107 62 96 406 13 35
124 60 109 424 13 41
109 61 101 414 13 37
106 61 100 417 13 36
13 1 5 16 1 2
11.89% 2.00% 5.09% 3.92% 4.38% 6.29%
-84.16% -91.16% -85.33% -39.63% -98.18% -94.63%
1.47 0.39 1.29 8.34 0.69 0.16
Lab Lab Lab Lab Lab

16 17 18 19 21
AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES
10g 0.25g 10g 0.25g 0.25g
< 0.5 0.20 <1 0.13 <2
< 0.5 0.20 <1 0.15 <2
< 0.5 0.10 <1 0.23 <2
< 0.5 0.20 <1 0.13 <2
< 0.5 0.10 <1 0.19 <2
< 0.5 0.10 <1 0.13 <2
0.15 0.16
0.15 0.14
0.055 0.041
36.51% 25.92%
NA 0.96 NA 1.04 NA

14 15 16 17 18 19 21
AR*MS AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
155 157 127 96 204 148 140
158 151 133 105 203 150 140
152 156 130 97 210 150 140
153 152 133 103 204 151 140
156 153 133 107 208 146 140
157 156 130 93 213 151 142
155 154 131 100 207 149 140
156 155 132 100 206 150 140
3 2 2 6 4 2 1
1.61% 1.61% 1.87% 5.67% 1.93% 1.41% 0.58%
2.89% 2.22% -13.14% -33.64% 37.25% -1.07% -6.95%
0.11 0.00 2.51 5.85 5.72 0.54 1.50

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
0.240 0.270 0.210 0.240 0.220 0.233 0.220
0.250 0.280 0.220 0.230 0.220 0.233 0.220
0.230 0.270 0.210 0.240 0.220 0.235 0.220
0.240 0.270 0.210 0.240 0.210 0.226 0.220
0.240 0.270 0.210 0.230 0.220 0.229 0.220
0.240 0.270 0.210 0.240 0.220 0.232 0.220
0.240 0.272 0.212 0.237 0.218 0.231 0.220
0.240 0.270 0.210 0.240 0.220 0.233 0.220
0.006 0.004 0.004 0.005 0.004 0.003 0.000
2.64% 1.50% 1.93% 2.18% 1.87% 1.41% 0.00%
1.31% 14.67% -10.65% -0.10% -7.84% -2.35% -7.14%
0.00 2.14 1.91 0.22 1.46 0.58 1.35

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
56 57 50 51 43 52 54
59 56 51 52 43 52 54
55 55 50 52 43 51 53
57 56 51 53 44 50 54
58 56 50 55 44 50 53
58 56 48 48 45 50 54
57 56 50 52 44 51 54
57 56 50 52 44 51 54
1.1 0.6 1.1 2.2 0.8 1.0 0.5
2.00% 1.04% 2.19% 4.28% 1.87% 1.87% 0.96%
3.44% 1.41% -9.37% -6.05% -20.85% -7.73% -2.72%
0.26 0.00 1.39 0.96 2.87 1.18 0.53

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
15.0 16.9 14.0 13.6 15.0 14.9 16.0
16.0 17.1 14.0 14.1 15.0 14.9 17.0
15.0 16.7 14.0 14.2 16.0 15.2 15.0
15.0 17.2 14.0 14.6 15.0 14.7 15.0
16.0 16.5 14.0 15.8 15.0 14.6 15.0
16.0 17.1 13.0 13.6 16.0 15.2 15.0
15.5 16.9 13.8 14.3 15.3 14.9 15.5
15.5 17.0 14.0 14.2 15.0 14.9 15.0
0.548 0.285 0.408 0.821 0.516 0.225 0.837
3.53% 1.69% 2.95% 5.73% 3.37% 1.51% 5.40%
2.22% 11.62% -8.77% -5.59% 1.12% -1.71% 2.22%
0.67 3.16 2.23 1.39 0.38 0.36 0.67

15 16 17 18 21 23 24
01g 10g 0.25g 10g 0.25g 0.5g 40g
32.0 32.0 28.0 33.0 27.0 26.0 30.0
31.0 28.0 29.0 26.0 26.0 28.0 30.0
31.0 26.0 26.0 28.0 26.0 28.0 30.0
33.0 29.0 27.0 26.0 28.0 30.0 30.0
31.0 25.0 28.0 27.0 23.0 26.0 30.0
35.0 25.0 28.0 31.0 28.0 27.0 30.0
32.2 27.5 27.7 28.5 26.3 27.5 30.0
31.5 27.0 28.0 27.5 26.5 27.5 30.0
1.602 2.739 1.033 2.881 1.862 1.517 0.000
4.98% 9.96% 3.73% 10.11% 7.07% 5.51% 0.00%
10.13% -5.85% -5.28% -2.42% -9.84% -5.85% 2.71%
0.97 1.12 1.05 0.67 1.65 1.12 0.00

13 14 15 16 17 18 19
AR*OES AR*OES AR*OES AR*OES AR*OES/MS AR*OES AR*OES
01g 0.5g 01g 10g 0.25g 10g 0.5g
0.95 0.99 1.05 0.93 1.00 0.95 1.04
0.99 > 10000 1.04 0.94 > 10000 0.95 1.04
1.00 0.98 1.02 0.93 > 10000 0.96 1.04
0.97 > 10000 1.02 0.95 > 10000 0.94 1.02
1.02 > 10000 1.01 0.95 > 10000 0.98 1.02
0.99 > 10000 1.04 0.91 > 10000 0.98 1.02
0.99 0.98 1.03 0.94 1.00 0.96 1.03
0.99 0.98 1.03 0.94 1.00 0.96 1.03
0.021 0.010 0.015 0.015 0.015 0.011
2.12% 0.98% 1.47% 1.61% 1.59% 1.10%
-2.05% -2.39% 2.13% -7.05% -0.93% -4.64% 2.45%
0.83 1.00 1.25 3.31 0.27 2.12 1.41
14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
2.79 3.08 2.65 2.84 2.61 3.15 2.62
2.89 3.07 2.68 2.92 2.60 3.07 2.62
2.77 3.03 2.65 2.89 2.63 3.06 2.59
2.85 3.04 2.69 2.87 2.54 3.06 2.61
2.85 3.02 2.71 2.74 2.62 3.12 2.57
2.88 3.06 2.59 2.87 2.62 3.08 2.61
2.84 3.05 2.66 2.86 2.60 3.09 2.60
2.85 3.05 2.67 2.87 2.62 3.08 2.61
0.048 0.024 0.042 0.062 0.033 0.038 0.020
1.70% 0.78% 1.58% 2.18% 1.25% 1.23% 0.76%
-0.36% 7.07% -6.56% 0.22% -8.61% 8.54% -8.61%
0.17 0.87 1.05 0.02 1.33 1.08 1.33
Lab
25
AR*MS
40g
5.80
5.80
5.80
5.80
5.80
5.60
5.77
5.80
0.082
1.42%
-12.43%
1.25
Lab Lab
24 25
AR*MS AR*MS
40g 40g
2.00 1.84
2.00 1.78
2.00 1.78
2.00 1.77
2.50 1.82
2.00 1.82
2.08 1.80
2.00 1.80
0.204 0.029
9.80% 1.59%
1.65 0.76
15 16 17 18 19 21 23
AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES
01g 10g 0.25g 10g 0.25g 0.25g 0.5g
0.110 0.080 0.100 0.080 0.087 0.080 0.080
0.110 0.080 0.100 0.070 0.086 0.080 0.080
0.110 0.080 0.100 0.070 0.086 0.070 0.080
0.110 0.080 0.100 0.070 0.082 0.070 0.080
0.110 0.080 0.100 0.080 0.087 0.070 0.070
0.110 0.080 0.100 0.070 0.089 0.080 0.080
0.110 0.080 0.100 0.073 0.086 0.075 0.078
0.110 0.080 0.100 0.070 0.087 0.075 0.080
0.000 0.000 0.000 0.005 0.002 0.005 0.004
0.00% 0.00% 0.00% 7.04% 2.69% 7.30% 5.21%
18.31% -13.96% 7.56% -21.13% -7.32% -19.33% -15.75%
1.35 0.67 0.67 1.12 0.26 1.01 0.79

15 16 17 18 19 23 25
AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*MS
01g 10g 0.25g 10g 0.25g 0.5g 40g
8.0 5.6 4.0 < 10 5.7 4.0 2.9
8.0 5.3 4.0 < 10 5.5 4.0 2.9
8.0 5.2 3.9 < 10 5.4 4.0 2.6
8.0 5.4 4.0 < 10 5.5 4.0 2.6
8.0 5.5 4.5 < 10 5.3 4.0 2.7
8.0 5.4 3.7 < 10 5.2 4.0 2.8
8.0 5.4 4.0 5.4 4.0 2.8
8.0 5.4 4.0 5.4 4.0 2.8
0.0 0.1 0.3 0.2 0.0 0.1
0.00% 2.62% 6.57% 3.29% 0.00% 4.94%
0.99 0.13 0.77 NA 0.13 0.74 1.28
Lab Lab
21 25
AR*OES AR*MS
0.25g 40g
4.00 4.00
4.00 3.80
4.00 3.70
4.00 4.00
4.00 3.90
4.00 3.90
4.00 3.88
4.00 3.90
0.000 0.117
0.00% 3.01%
-13.49% -16.01%
0.67 0.81

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
500 500 500 600 400 590 500
500 500 500 600 400 580 500
500 500 500 500 500 580 400
500 500 500 600 400 570 400
500 500 400 500 400 590 400
500 500 400 500 400 600 400
500 500 467 550 417 585 433
500 500 500 550 400 585 400
0 0 52 55 41 10 52
0.00% 0.00% 11.07% 9.96% 9.80% 1.79% 11.92%
-3.24% -3.24% -9.69% 6.44% -19.37% 13.21% -16.14%
0.00 0.00 0.67 1.01 1.69 1.72 1.35

14 15 16 17 18 19 21
AR*MS AR*OES AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
131 148 116 126 100 141 138
136 148 117 124 100 141 137
125 148 116 124 100 142 135
126 144 119 124 100 139 137
129 147 116 125 100 143 134
132 148 113 123 100 144 136
130 147 116 124 100 142 136
130 148 116 124 100 142 137
4 2 2 1 0 2 1
3.13% 1.14% 1.67% 0.83% 0.00% 1.28% 1.08%
0.24% 13.63% -10.31% -4.00% -22.79% 9.28% 5.13%
0.00 3.51 2.76 1.11 6.04 2.37 1.28

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
6.00 6.00 13.00 3.14 7.00 6.23 6.00
6.00 6.00 11.00 3.37 7.00 6.07 6.00
6.00 6.00 13.00 3.21 7.00 6.14 6.00
6.00 6.00 10.00 3.41 7.00 5.98 5.00
6.00 6.00 11.00 3.38 9.00 5.87 6.00
6.00 6.00 11.00 3.07 8.00 5.91 6.00
6.00 6.00 11.50 3.26 7.50 6.03 5.83
6.00 6.00 11.00 3.29 7.00 6.03 6.00
0.000 0.000 1.225 0.143 0.837 0.139 0.408
0.00% 0.00% 10.65% 4.38% 11.16% 2.31% 7.00%
-1.71% -1.71% 88.38% -46.54% 22.86% -1.14% -4.44%
0.00 0.00 8.43 4.19 1.53 0.05 0.26

15 16 17 18 19 21 23
01g 10g 0.25g 10g 0.25g 0.25g 0.5g
300 300 300 300 430 400 200
300 200 300 300 410 400 200
300 200 300 300 410 400 200
300 300 300 300 400 400 200
300 200 300 300 410 400 200
300 300 300 300 440 400 200
300 250 300 300 417 400 200
300 250 300 300 410 400 200
0 55 0 0 15 0 0
0.00% 21.91% 0.00% 0.00% 3.61% 0.00% 0.00%
9.24% -8.97% 9.24% 9.24% 51.72% 45.65% -27.17%
0.00 0.67 0.00 0.00 1.57 1.35 1.35

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
107 115 104 84 102 112 106
111 115 99 94 101 118 106
107 113 99 88 104 117 106
109 116 102 95 101 112 107
109 113 99 93 102 115 105
112 116 101 84 108 111 107
109 115 101 89 103 114 106
109 115 100 90 102 114 106
2 1 2 5 3 3 1
1.87% 1.19% 2.05% 5.45% 2.61% 2.37% 0.71%
-3.10% 1.78% -10.65% -20.63% -8.58% 1.36% -5.76%
0.75 0.67 2.96 5.88 2.62 0.55 1.53

16 17 18 19 21 23 24
AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES AR*OES
10g 0.25g 10g 0.25g 0.25g 0.5g 40g
100 180 < 100 199 258 160 220
200 170 < 100 173 241 140 180
100 160 100 222 242 140 200
100 190 100 132 279 160 180
< 100 150 100 241 261 150 200
< 100 160 100 367 249 150 200
125 168 100 222 255 150 197
100 165 100 210 254 150 200
50 15 0 80 14 9 15
40.00% 8.74% 0.00% 36.20% 5.61% 5.96% 7.66%
-27.52% -2.39% -42.02% 28.90% 47.86% -13.02% 14.04%
1.60 0.01 2.53 0.94 3.22 0.67 1.06

14 15 16 17 18 19 21
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
1682 1813 1630 1976 1510 1723 1561
1732 1795 1650 1941 1499 1748 1552
1642 1777 1630 2005 1558 1751 1537
1690 1792 1670 2032 1523 1729 1553
1696 1790 1630 1851 1552 1693 1539
1696 1802 1600 1912 1567 1745 1545
1690 1795 1635 1953 1535 1732 1548
1693 1794 1630 1959 1538 1737 1549
29 12 23 66 28 22 9
1.72% 0.67% 1.43% 3.37% 1.82% 1.26% 0.59%
-0.06% 6.16% -3.29% 15.51% -9.21% 2.43% -8.45%
0.06 2.31 1.28 5.86 3.53 0.89 3.24
15 16 17 19 23 24 25
AR*OES AR*OES AR*OES/MS AR*OES/MS AR*OES AR*OES AR*OES
01g 10g 0.25g 0.25g 0.5g 40g 40g
3.36 3.22 - 3.18 3.21 3.90 3.37
3.35 3.19 - 3.30 3.21 4.08 3.42
3.30 3.19 - 3.29 3.19 3.73 3.46
3.33 3.22 - 3.20 3.24 3.63 3.41
3.32 3.21 - 3.29 3.15 4.24 3.34
3.37 3.21 - 3.26 3.18 4.08 3.43
3.34 3.21 3.25 3.20 3.94 3.41
3.34 3.21 3.27 3.20 3.99 3.42
0.025 0.014 0.051 0.031 0.233 0.043
0.74% 0.43% 1.56% 0.96% 5.90% 1.27%
-3.50% -7.30% -5.94% -7.58% 14.00% -1.56%
0.67 1.40 NA 1.14 1.45 2.67 0.30

14 15 16 17 18 19 21
AR*MS AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES
0.5g 01g 10g 0.25g 10g 0.25g 0.25g
183 210 158 92 174 131 97
186 212 158 90 172 127 96
179 193 158 92 175 127 95
184 203 155 93 168 123 98
181 203 158 85 175 126 90
181 208 164 88 168 127 96
182 205 159 90 172 127 95
182 206 158 91 173 127 96
2 7 3 3 3 2 3
1.30% 3.24% 1.86% 3.39% 1.91% 1.90% 2.94%
13.86% 27.95% -0.97% -43.87% 7.47% -20.87% -40.43%
0.81 1.49 0.06 1.98 0.50 0.86 1.78

15 16 17 18 19 23 24
01g 10g 0.25g 10g 0.25g 0.5g 40g
1.00 0.80 1.40 <3 1.09 <5 2.00
1.00 0.70 1.30 <3 1.12 <5 2.00
1.00 0.70 1.50 <3 1.10 <5 1.00
1.00 0.70 1.50 <3 1.17 <5 1.00
1.00 0.70 1.60 <3 1.17 <5 2.00
1.00 0.70 1.50 <3 1.18 <5 2.00
1.00 0.72 1.47 1.14 1.67
1.00 0.70 1.50 1.15 2.00
0.000 0.041 0.103 0.040 0.516
0.00% 5.70% 7.04% 3.49% 30.98%
-5.99% -32.63% 37.88% 7.01% 56.68%
NA NA NA NA NA NA NA
Lab
25
AR*MS
40g
55
51
53
55
54
54
54
54
2
2.81%
-9.25%
0.81
Lab Lab
24 25
AR*MS AR*MS
40g 40g
14.0 11.9
13.0 11.9
14.0 12.0
13.0 12.0
16.0 12.0
14.0 11.9
14.0 12.0
14.0 12.0
1.095 0.055
7.82% 0.46%
16.79% -0.31%
1.61 0.05

15 16 17 18 19 21 23
AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES
01g 10g 0.25g 10g 0.25g 0.25g 0.5g
39.1 49.0 55.9 45.0 50.7 48.0 36.0
35.5 45.6 54.8 45.0 49.3 48.0 37.0
40.2 46.3 56.9 44.0 48.7 47.0 36.0
35.7 48.5 56.4 43.0 48.3 47.0 37.0
36.4 48.0 53.9 44.0 49.7 45.0 35.0
39.3 46.7 57.5 44.0 49.6 48.0 34.0
37.7 47.4 55.9 44.2 49.4 47.2 35.8
37.7 47.4 56.2 44.0 49.4 47.5 36.0
2.1 1.3 1.3 0.8 0.9 1.2 1.2
5.49% 2.84% 2.40% 1.70% 1.75% 2.48% 3.26%
-18.72% 2.10% 20.54% -4.76% 6.48% 1.71% -22.73%
1.29 0.08 0.99 0.48 0.17 0.11 1.53
Lab Lab Lab Lab
19 23 24 25
AR*OES/MS AR*OES AR*MS AR*MS
0.25g 0.5g 40g 40g
2.32 2.00 1.05 1.48
2.33 2.00 1.05 1.48
2.32 <2 1.00 1.42
2.34 2.00 1.10 1.40
2.34 <2 1.35 1.40
2.38 <2 1.20 1.42
2.34 2.00 1.13 1.43
2.33 2.00 1.08 1.42
0.022 0.000 0.129 0.037
0.94% 0.00% 11.50% 2.60%
1.58% -13.05% -51.09% -37.69%
0.46 0.53 3.10 2.19

16 17 18 19 21 23 25
AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES AR*OES
10g 0.25g 10g 0.25g 0.25g 0.5g 40g
< 100 < 100 < 100 < 100 < 100 50 < 50
< 100 < 100 < 100 < 100 < 100 50 < 50
< 100 < 100 < 100 < 100 < 100 50 < 50
< 100 < 100 < 100 < 100 < 100 50 < 50
< 100 < 100 < 100 < 100 < 100 50 < 50
< 100 < 100 < 100 < 100 < 100 50 < 50
50
50
0
0.00%
-48.82%
NA NA NA NA NA 13.49 NA

15 17 18 19 21 23 24
AR*OES/MS AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES AR*MS
01g 0.25g 10g 0.25g 0.25g 0.5g 40g
4.78 4.39 < 10 4.15 3.00 8.00 4.70
4.93 4.80 < 10 4.17 4.00 9.00 4.60
4.91 4.53 < 10 4.24 <2 11.00 4.80
4.79 4.89 < 10 4.20 <2 7.00 4.40
5.02 4.06 < 10 4.11 <2 10.00 5.40
5.03 4.38 < 10 4.15 <2 8.00 4.70
4.91 4.51 4.17 3.50 8.83 4.77
4.92 4.46 4.16 3.50 8.50 4.70
0.108 0.304 0.047 0.707 1.472 0.339
2.20% 6.75% 1.13% 20.20% 16.66% 7.10%
20.69% 10.82% 2.51% -13.97% 117.13% 17.17%
0.34 0.00 NA 0.28 0.84 3.61 0.11
Lab Lab Lab

19 24 25
0.25g 40g 40g
0.93 0.90 0.76
0.93 0.90 0.74
0.93 0.85 0.74
0.91 0.80 0.76
0.89 0.95 0.72
0.93 1.00 0.74
0.92 0.90 0.74
0.93 0.90 0.74
0.018 0.071 0.015
1.93% 7.86% 2.03%
3.87% 1.69% -16.02%
0.16 0.01 1.37

15 16 17 18 19 21 23
AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES
01g 10g 0.25g 10g 0.25g 0.25g 0.5g
10.5 10.0 14.0 9.0 11.2 9.0 9.0
10.0 9.0 14.0 9.0 11.1 9.0 8.0
10.4 11.0 14.0 9.0 11.0 9.0 9.0
11.3 10.0 14.0 9.0 10.8 9.0 9.0
11.5 9.0 14.0 9.0 10.8 9.0 8.0
10.7 9.0 14.0 9.0 11.0 9.0 8.0
10.7 9.7 14.0 9.0 11.0 9.0 8.5
10.6 9.5 14.0 9.0 11.0 9.0 8.5
0.6 0.8 0.0 0.0 0.2 0.0 0.5
5.22% 8.45% 0.00% 0.00% 1.67% 0.00% 6.44%
7.01% -3.62% 39.58% -10.27% 9.45% -10.27% -15.26%
0.73 0.13 3.37 0.67 0.93 0.67 1.08
Lab Lab Lab Lab

18 19 23 25
AR*OES AR*OES/MS AR*OES AR*MS
10g 0.25g 0.5g 40g
< 10 4.93 <2 2.50
< 10 4.87 <2 2.60
< 10 4.85 <2 2.50
< 10 4.66 <2 2.70
< 10 4.85 <2 2.60
< 10 4.66 <2 2.80
4.80 2.62
4.85 2.60
0.117 0.117
2.44% 4.47%
23.75% -32.59%
NA 0.55 NA 1.66
Lab Lab
21 25
AR*OES AR*MS
0.25g 40g
2.00 2.16
2.00 2.13
2.00 2.16
2.00 2.16
2.00 2.14
2.00 2.12
2.00 2.15
2.00 2.15
0.000 0.018
0.00% 0.82%
-12.31% -5.95%
0.67 0.21
14 15 16 17 18 19 21
Various [α] AR*OES/MS AR*OES AR*OES/MS AR*OES AR*OES/MS AR*OES/AAS
see footer 01g 10g 0.25g 10g 0.25g 02.5g
> 0.2 0.922 0.899 0.884 0.844 >1 0.860
> 0.2 0.922 0.894 0.872 0.837 >1 0.857
0.886 0.905 0.892 0.895 0.845 >1 0.886
> 0.2 0.926 0.898 0.894 0.809 >1 0.873
> 0.2 0.909 0.899 0.850 0.847 >1 0.857
> 0.2 0.932 0.874 0.878 0.853 >1 0.887
0.886 0.919 0.893 0.879 0.839 0.870
0.886 0.922 0.896 0.881 0.844 0.866
0.010 0.010 0.017 0.016 0.014
1.12% 1.07% 1.93% 1.88% 1.62%
-2.75% 0.94% -2.00% -3.51% -7.89% -4.50%
0.60 0.41 0.39 0.80 1.81 NA 1.07
Lab Lab
19 25
AR*OES/MS AR*MS
0.25g 40g
16.0 15.0
16.4 15.0
15.9 14.0
15.2 15.0
15.8 14.0
15.7 14.0
15.8 14.5
15.8 14.5
0.4 0.5
2.59% 3.78%
-1.35% -9.63%
0.08 0.67
Lab Lab Lab Lab
21 23 24 25
AR*OES AR*OES AR*OES AR*MS
0.25g 01g 40g 40g
279 288 N.A. 28
278 292 N.A. 28
275 289 N.A. 27
278 293 N.A. 27
272 286 N.A. 27
276 288 N.A. 28
276 289 27
277 289 27
2 3 0
0.81% 0.92% 1.60%
-5.72% -1.22% -90.71%
1.32 0.29 NA 20.79
Lab Lab Lab

23 24 25
AR*OES AR*OES AR*OES
0.5g 40g 40g
0.510 0.600 0.540
0.520 0.590 0.540
0.510 0.590 0.540
0.530 0.600 0.520
0.490 0.620 0.500
0.480 0.580 0.520
0.507 0.597 0.527
0.510 0.595 0.530
0.019 0.014 0.016
3.67% 2.29% 3.10%
-12.70% 2.81% -9.25%
0.67 0.26 0.47
Lab Lab Lab

23 24 25
AR*OES AR*MS AR*MS
0.5g 40g 40g
1784 1740 1770
1779 1670 1700
1766 1780 1770
1801 1660 1790
1750 1750 1760
1766 1730 1770
1774 1722 1760
1773 1735 1770
18 47 31
0.99% 2.73% 1.76%
0.45% -2.54% -0.37%
0.00 0.51 0.02
Lab Lab Lab
23 24 25
AR*OES AR*MS AR*MS
0.5g 40g 40g
142 156 150
142 157 151
141 153 152
142 146 152
139 162 150
140 160 152
141 156 151
142 157 152
1 6 1
0.90% 3.65% 0.65%
-6.51% 3.22% 0.23%
1.42 0.16 0.32
Lab Lab Lab

23 24 25
0.5g 40g 40g
0.220 0.230 0.240
0.220 0.230 0.240
0.220 0.240 0.250
0.230 0.240 0.240
0.220 0.220 0.240
0.220 0.220 0.240
0.222 0.230 0.242
0.220 0.230 0.240
0.004 0.009 0.004
1.84% 3.89% 1.69%
-6.43% -2.92% 2.01%
1.24 0.67 0.11
Lab Lab Lab

23 24 25
AR*OES AR*MS AR*MS
0.5g 40g 40g
56 64 55
56 65 53
56 69 54
57 66 54
55 79 54
56 68 54
56 69 54
56 67 54
0.6 5.6 0.7
1.08% 8.13% 1.24%
1.44% 24.40% -2.24%
0.00 2.46 0.47
Lab Lab Lab

23 24 25
AR*OES AR*MS AR*OES
0.5g 40g 40g
15.0 16.6 16.0
15.0 16.4 17.0
15.0 16.8 17.0
15.0 15.8 16.0
15.0 19.2 17.0
15.0 16.4 17.0
15.0 16.9 16.7
15.0 16.5 17.0
0.000 1.191 0.516
0.00% 7.06% 3.10%
-1.08% 11.23% 9.91%
0.20 2.24 2.71
Lab
25
AR*OES
40g
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
0.000
0.00%
-14.41%
2.25
Lab Lab Lab Lab

21 23 24 25
0.25g 01g 40g 40g
0.99 1.02 N.A. 1.02
1.00 1.04 N.A. 1.04
0.98 1.00 N.A. 1.05
0.99 1.05 N.A. 1.05
0.97 0.99 N.A. 1.05
0.98 1.01 N.A. 1.06
0.99 1.02 1.05
0.99 1.02 1.05
0.011 0.023 0.014
1.12% 2.22% 1.32%
-2.23% 0.86% 3.71%
0.92 0.62 NA 2.03
Lab Lab Lab
23 24 25
0.5g 40g 40g
2.68 3.19 2.88
2.72 3.07 2.91
2.64 3.05 2.93
2.75 3.01 2.92
2.67 3.02 2.91
2.63 3.04 2.95
2.68 3.06 2.92
2.68 3.05 2.92
0.046 0.066 0.023
1.72% 2.14% 0.80%
-5.86% 7.54% 2.39%
0.95 0.81 0.21
Lab Lab
24 25
AR*OES AR*OES
40g 40g
0.090 0.080
0.090 0.080
0.090 0.080
0.090 0.080
0.100 0.080
0.090 0.080
0.092 0.080
0.090 0.080
0.004 0.000
4.45% 0.00%
-1.41% -13.96%
0.11 0.67
Lab Lab Lab
23 24 25
0.5g 40g 40g
500 600 500
500 600 500
500 600 500
500 600 500
500 600 500
500 600 500
500 600 500
500 600 500
0 0 0
0.00% 0.00% 0.00%
-3.24% 16.11% -3.24%
0.00 2.02 0.00
Lab Lab Lab

23 24 25
0.5g 40g 40g
124 140 127
124 140 128
124 140 127
126 130 126
121 130 124
123 140 127
124 137 127
124 140 127
2 5 1
1.32% 3.78% 1.09%
-4.52% 5.52% -2.33%
1.25 1.38 0.67
Lab Lab Lab

23 24 25
AR*OES AR*MS AR*MS
0.5g 40g 40g
5.00 6.80 7.40
5.00 6.40 7.20
5.00 7.00 7.20
6.00 6.60 7.40
5.00 8.20 7.40
5.00 7.40 7.40
5.17 7.07 7.33
5.00 6.90 7.40
0.408 0.653 0.103
7.90% 9.24% 1.41%
-15.37% 15.76% 20.13%
1.28 1.29 2.04
Lab
25
AR*OES
40g
300
300
300
400
300
400
333
300
52
15.49%
21.38%
0.45
Lab Lab Lab

23 24 25
AR*OES AR*MS AR*OES
0.5g 40g 40g
111 119 110
112 113 111
111 119 112
114 113 110
109 124 108
111 125 109
111 119 110
111 119 110
2 5 1
1.47% 4.34% 1.29%
-1.18% 5.48% -2.36%
0.19 1.02 0.54
Lab
25
AR*OES
40g
160
180
160
160
160
160
163
160
8
5.00%
-5.29%
0.18
Lab Lab Lab

23 24 25
AR*OES AR*MS AR*MS
0.5g 40g 40g
1698 1670 1640
1700 1620 1630
1691 1670 1640
1717 1620 1640
1665 1660 1620
1682 1640 1650
1692 1647 1637
1695 1650 1640
18 23 10
1.04% 1.42% 0.63%
0.09% -2.60% -3.19%
0.00 1.02 1.25
Lab Lab
23 25
AR*OES AR*MS
0.5g 40g
133 179
134 174
133 170
134 175
132 174
134 179
133 175
134 175
1 3
0.61% 1.96%
-16.69% 9.45%
0.66 0.60
Lab
25
AR*MS
40g
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
0.000
0.00%
-5.99%
NA
Lab Lab
24 25
AR*MS AR*MS
40g 40g
28.0 18.7
26.0 20.7
26.0 20.3
27.0 21.5
28.0 17.8
27.0 18.7
27.0 19.6
27.0 19.5
0.9 1.4
3.31% 7.27%
-41.78% -57.70%
2.64 3.56
Lab
25
AR*MS
40g
3.70
3.70
3.70
3.70
3.70
3.70
3.70
3.70
0.000
0.00%
-9.05%
0.67
Lab
25
AR*OES
40g
10.0
8.0
10.0
10.0
8.0
10.0
9.3
10.0
1.0
11.07%
-6.95%
0.40
Lab Lab Lab
23 24 25
0.5g 40g 40g
0.915 0.898 0.894
0.923 0.906 0.895
0.910 0.923 0.905
0.936 0.881 0.892
0.903 0.893 0.883
0.902 0.890 0.897
0.915 0.899 0.894
0.912 0.896 0.895
0.013 0.015 0.007
1.43% 1.62% 0.80%
0.42% -1.36% -1.82%
0.27 0.22 0.34
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
293
67
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.580
68.000
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1766
69
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
5.08
70.00
Certified
1.00
ppm
1.00
1.00
1.0
3.0
16.0
< 10
71.0
Indicative
1.00
ppm
0.00
0.00
1
4
16
686
12
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
< 0.5
72.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
151
73
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.237
74.000
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
55
75
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
13.0
76.0
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
15.2
77.0
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
29.2
78.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.74
79.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.01
80.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.56
81.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.22
82.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.25
83.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
2.85
84.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
6.58
85.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.86
86.00
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
1.35
13.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.46
87.00
Certified
1.00
ppm
2.00
2.00
1.00
4.00
16.00
<4
88.00
Certified
1.00
ppm
3.00
3.00
1.000
#N/A
16.000
0.096
89.000
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
11.7
90.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.093
91.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
< 10
92.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
4.62
93.00
Certified
1.00
ppb
0.00
0.00
1
#N/A
16
26
94
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
517
95
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
130
96
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
6.10
97.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
275
98
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
< 0.5
99.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
5.90
100.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
113
101
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
172
102
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1691
103
Indicative
1.00
ppb
0.00
0.00
1
1
16
734
14
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
1.57
104.00
Indicative
1.00
ppb
0.00
0.00
1
1
16
132
12
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
4.89
105.00
Indicative
1.00
ppb
0.00
0.00
1
7
16
1
13
Indicative
1.00
ppb
0.00
0.00
1
8
16
<2
14
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
3.46
106.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
160
107
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
1.06
108.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
59
109
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
1.12
110.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
12.0
111.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
46.4
112.0
Indicative
1.00
ppm
3.00
3.00
1.000
6.000
16.000
< 0.01
12.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.11
113.00
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
57
114
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
2.30
115.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
98
116
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
4.07
117.00
Indicative
1.00
ppm
3.00
3.00
1.000
4.000
16.000
0.028
13.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.89
118.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
10.0
119.0
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
3.88
120.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
2.28
121.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.17
122.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.911
123.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
16.0
124.0
Analytical results for Ag in OREAS 603 (Indicative Value 282 ppm)
Ag Round Replicate Lab
No No 01
ABL*MS
1 1 283
1 2 281
Mean 282
Median 282
Std Dev. 1
Rel.Std.Dev. 0.50%
PDM3 0.00%
Analytical results for As in OREAS 603 (Indicative Value 1715 ppm)

As Round Replicate Lab
No No 01
ABL*MS
1 1 1730
1 2 1700
Mean 1715
Median 1715
Std Dev. 21
Rel.Std.Dev. 1.24%
PDM3 0.00%

Ba Round Replicate Lab
No No 01
ABL*MS
1 1 11900
1 2 11200
Mean 11550
Median 11550
Std Dev. 495
Rel.Std.Dev. 4.29%
PDM3 0.00%
Analytical results for Be in OREAS 603 (Indicative Value 0.6 ppm)

Be Round Replicate Lab
No No 01
ABL*MS
1 1 0.80
1 2 0.40
Mean 0.60
Median 0.60
Std Dev. 0.283
Rel.Std.Dev. 47.14%
PDM3 0.00%
Analytical results for Bi in OREAS 603 (Indicative Value 145 ppm)
Bi Round Replicate Lab
No No 01
ABL*MS
1 1 147
1 2 143
Mean 145
Median 145
Std Dev. 3
Rel.Std.Dev. 1.95%
PDM3 0.00%
Analytical results for Cd in OREAS 603 (Indicative Value 53 ppm)

Cd Round Replicate Lab
No No 01
ABL*MS
1 1 52
1 2 54
Mean 53
Median 53
Std Dev. 1
Rel.Std.Dev. 2.54%
PDM3 0.00%
Analytical results for Ce in OREAS 603 (Indicative Value 30.7 ppm)

Ce Round Replicate Lab
No No 01
ABL*MS
1 1 31.5
1 2 29.9
Mean 30.7
Median 30.7
Std Dev. 1.1
Rel.Std.Dev. 3.69%
PDM3 0.00%
Analytical results for Co in OREAS 603 (Indicative Value 16.5 ppm)

Co Round Replicate Lab
No No 01
ABL*MS
1 1 16.0
1 2 16.9
Mean 16.5
Median 16.5
Std Dev. 0.6
Rel.Std.Dev. 3.87%
PDM3 0.00%
Analytical results for Cr in OREAS 603 (Indicative Value 39 ppm)
Cr Round Replicate Lab
No No 01
ABL*MS
1 1 42.0
1 2 36.0
Mean 39.0
Median 39.0
Std Dev. 4.2
Rel.Std.Dev. 10.88%
PDM3 0.00%
Analytical results for Cs in OREAS 603 (Indicative Value 1.51 ppm)

Cs Round Replicate Lab
No No 01
ABL*MS
1 1 1.48
1 2 1.53
Mean 1.51
Median 1.51
Std Dev. 0.035
Rel.Std.Dev. 2.35%
PDM3 0.00%
Analytical results for Cu in OREAS 603 (Indicative Value 9830 ppm)

Cu Round Replicate Lab
No No 01
ABL*MS
1 1 10000
1 2 9660
Mean 9830
Median 9830
Std Dev. 240
Rel.Std.Dev. 2.45%
PDM3 0.00%
Analytical results for Dy in OREAS 603 (Indicative Value 1.2 ppm)

Dy Round Replicate Lab
No No 01
ABL*MS
1 1 1.28
1 2 1.11
Mean 1.20
Median 1.20
Std Dev. 0.120
Rel.Std.Dev. 10.06%
PDM3 0.00%
Analytical results for Er in OREAS 603 (Indicative Value 0.69 ppm)
Er Round Replicate Lab
No No 01
ABL*MS
1 1 0.60
1 2 0.78
Mean 0.69
Median 0.69
Std Dev. 0.127
Rel.Std.Dev. 18.45%
PDM3 0.00%
Analytical results for Eu in OREAS 603 (Indicative Value 0.31 ppm)

Eu Round Replicate Lab
No No 01
ABL*MS
1 1 0.31
1 2 0.30
Mean 0.31
Median 0.31
Std Dev. 0.007
Rel.Std.Dev. 2.32%
PDM3 0.00%
Analytical results for Ga in OREAS 603 (Indicative Value 24.1 ppm)

Ga Round Replicate Lab
No No 01
ABL*MS
1 1 25.8
1 2 22.3
Mean 24.1
Median 24.1
Std Dev. 2.5
Rel.Std.Dev. 10.29%
PDM3 0.00%
Analytical results for Gd in OREAS 603 (Indicative Value 1.66 ppm)

Gd Round Replicate Lab
No No 01
ABL*MS
1 1 1.58
1 2 1.73
Mean 1.66
Median 1.66
Std Dev. 0.106
Rel.Std.Dev. 6.41%
PDM3 0.00%
Analytical results for Hf in OREAS 603 (Indicative Value 3.64 ppm)
Hf Round Replicate Lab
No No 01
ABL*MS
1 1 3.46
1 2 3.82
Mean 3.64
Median 3.64
Std Dev. 0.255
Rel.Std.Dev. 6.99%
PDM3 0.00%
Analytical results for Ho in OREAS 603 (Indicative Value 0.23 ppm)

Ho Round Replicate Lab
No No 01
ABL*MS
1 1 0.24
1 2 0.21
Mean 0.23
Median 0.23
Std Dev. 0.021
Rel.Std.Dev. 9.43%
PDM3 0.00%
Analytical results for In in OREAS 603 (Indicative Value 10.1 ppm)

In Round Replicate Lab
No No 01
ABL*MS
1 1 10.4
1 2 9.9
Mean 10.1
Median 10.1
Std Dev. 0.4
Rel.Std.Dev. 3.84%
PDM3 0.00%
Analytical results for La in OREAS 603 (Indicative Value 18.1 ppm)

La Round Replicate Lab
No No 01
ABL*MS
1 1 18.4
1 2 17.8
Mean 18.1
Median 18.1
Std Dev. 0.4
Rel.Std.Dev. 2.34%
PDM3 0.00%
Analytical results for Lu in OREAS 603 (Indicative Value 0.095 ppm)
Lu Round Replicate Lab
No No 01
ABL*MS
1 1 0.100
1 2 0.090
Mean 0.095
Median 0.095
Std Dev. 0.007
Rel.Std.Dev. 7.44%
PDM3 0.00%
Analytical results for Mn in OREAS 603 (Indicative Value 0.014 wt.%)

Mn Round Replicate Lab
No No 01
ABL*MS
1 1 0.014
1 2 0.013
Mean 0.014
Median 0.014
Std Dev. 0.001
Rel.Std.Dev. 7.83%
PDM3 0.00%
Analytical results for Mo in OREAS 603 (Indicative Value 6.3 ppm)

Mo Round Replicate Lab
No No 01
ABL*MS
1 1 6.60
1 2 6.00
Mean 6.30
Median 6.30
Std Dev. 0.424
Rel.Std.Dev. 6.73%
PDM3 0.00%
Analytical results for Nb in OREAS 603 (Indicative Value 7.79 ppm)

Nb Round Replicate Lab
No No 01
ABL*MS
1 1 7.78
1 2 7.79
Mean 7.79
Median 7.79
Std Dev. 0.007
Rel.Std.Dev. 0.09%
PDM3 0.00%
Analytical results for Nd in OREAS 603 (Indicative Value 11.5 ppm)
Nd Round Replicate Lab
No No 01
ABL*MS
1 1 11.5
1 2 11.5
Mean 11.5
Median 11.5
Std Dev. 0.0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Ni in OREAS 603 (Indicative Value 110 ppm)

Ni Round Replicate Lab
No No 01
ABL*MS
1 1 114
1 2 106
Mean 110
Median 110
Std Dev. 6
Rel.Std.Dev. 5.14%
PDM3 0.00%
Analytical results for Pb in OREAS 603 (Indicative Value 1945 ppm)

Pb Round Replicate Lab
No No 01
ABL*MS
1 1 1980
1 2 1910
Mean 1945
Median 1945
Std Dev. 49
Rel.Std.Dev. 2.54%
PDM3 0.00%
Analytical results for Pr in OREAS 603 (Indicative Value 3.58 ppm)

Pr Round Replicate Lab
No No 01
ABL*MS
1 1 3.58
1 2 3.57
Mean 3.58
Median 3.58
Std Dev. 0.007
Rel.Std.Dev. 0.20%
PDM3 0.00%
Analytical results for Rb in OREAS 603 (Indicative Value 23.3 ppm)
Rb Round Replicate Lab
No No 01
ABL*MS
1 1 24.4
1 2 22.1
Mean 23.3
Median 23.3
Std Dev. 1.6
Rel.Std.Dev. 7.00%
PDM3 0.00%
Analytical results for Re in OREAS 603 (Indicative Value 0.013 ppm)

Re Round Replicate Lab
No No 01
ABL*MS
1 1 0.020
1 2 < 0.01
Mean 0.020
Median 0.020
Std Dev.
Rel.Std.Dev.
PDM3 60.00%
Analytical results for Sb in OREAS 603 (Indicative Value 184 ppm)

Sb Round Replicate Lab
No No 01
ABL*MS
1 1 188
1 2 179
Mean 184
Median 184
Std Dev. 6
Rel.Std.Dev. 3.47%
PDM3 0.00%
Analytical results for Sc in OREAS 603 (Indicative Value 4.35 ppm)

Sc Round Replicate Lab
No No 01
ABL*MS
1 1 4.60
1 2 4.10
Mean 4.35
Median 4.35
Std Dev. 0.354
Rel.Std.Dev. 8.13%
PDM3 0.00%
Analytical results for Se in OREAS 603 (Indicative Value < 5 ppm)
Se Round Replicate Lab
No No 01
ABL*MS
1 1 <5
1 2 <5
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Analytical results for Sm in OREAS 603 (Indicative Value 2.04 ppm)

Sm Round Replicate Lab
No No 01
ABL*MS
1 1 2.17
1 2 1.91
Mean 2.04
Median 2.04
Std Dev. 0.184
Rel.Std.Dev. 9.01%
PDM3 0.00%
Analytical results for Sn in OREAS 603 (Indicative Value 13 ppm)

Sn Round Replicate Lab
No No 01
ABL*MS
1 1 13.4
1 2 12.6
Mean 13.0
Median 13.0
Std Dev. 0.6
Rel.Std.Dev. 4.35%
PDM3 0.00%
Analytical results for Sr in OREAS 603 (Indicative Value 571 ppm)

Sr Round Replicate Lab
No No 01
ABL*MS
1 1 573
1 2 569
Mean 571
Median 571
Std Dev. 3
Rel.Std.Dev. 0.50%
PDM3 0.00%
Analytical results for Ta in OREAS 603 (Indicative Value 0.71 ppm)
Ta Round Replicate Lab
No No 01
ABL*MS
1 1 0.69
1 2 0.72
Mean 0.71
Median 0.71
Std Dev. 0.021
Rel.Std.Dev. 3.01%
PDM3 0.00%
Analytical results for Tb in OREAS 603 (Indicative Value 0.2 ppm)

Tb Round Replicate Lab
No No 01
ABL*MS
1 1 0.18
1 2 0.22
Mean 0.20
Median 0.20
Std Dev. 0.028
Rel.Std.Dev. 14.14%
PDM3 0.00%
Analytical results for Te in OREAS 603 (Indicative Value 60 ppm)

Te Round Replicate Lab
No No 01
ABL*MS
1 1 60
1 2 60
Mean 60
Median 60
Std Dev. 0
Rel.Std.Dev. 0.47%
PDM3 0.00%
Analytical results for Th in OREAS 603 (Indicative Value 6.98 ppm)

Th Round Replicate Lab
No No 01
ABL*MS
1 1 7.18
1 2 6.77
Mean 6.98
Median 6.98
Std Dev. 0.290
Rel.Std.Dev. 4.16%
PDM3 0.00%
Analytical results for Ti in OREAS 603 (Indicative Value 0.198 wt.%)
Ti Round Replicate Lab
No No 01
ABL*MS
1 1 0.203
1 2 0.192
Mean 0.198
Median 0.198
Std Dev. 0.008
Rel.Std.Dev. 3.94%
PDM3 0.00%
Analytical results for Tl in OREAS 603 (Indicative Value 4.2 ppm)

Tl Round Replicate Lab
No No 01
ABL*MS
1 1 4.40
1 2 4.00
Mean 4.20
Median 4.20
Std Dev. 0.283
Rel.Std.Dev. 6.73%
PDM3 0.00%

Tm Round Replicate Lab
No No 01
ABL*MS
1 1 0.11
1 2 0.09
Mean 0.10
Median 0.10
Std Dev. 0.014
Rel.Std.Dev. 14.14%
PDM3 0.00%
Analytical results for U in OREAS 603 (Indicative Value 2.73 ppm)

U Round Replicate Lab
No No 01
ABL*MS
1 1 2.84
1 2 2.62
Mean 2.73
Median 2.73
Std Dev. 0.156
Rel.Std.Dev. 5.70%
PDM3 0.00%
Analytical results for V in OREAS 603 (Indicative Value 32.4 ppm)
V Round Replicate Lab
No No 01
ABL*MS
1 1 33.4
1 2 31.4
Mean 32.4
Median 32.4
Std Dev. 1.4
Rel.Std.Dev. 4.36%
PDM3 0.00%
Analytical results for W in OREAS 603 (Indicative Value 14.8 ppm)

W Round Replicate Lab
No No 01
ABL*MS
1 1 14.9
1 2 14.6
Mean 14.8
Median 14.8
Std Dev. 0.2
Rel.Std.Dev. 1.44%
PDM3 0.00%
Analytical results for Y in OREAS 603 (Indicative Value 6.28 ppm)

Y Round Replicate Lab
No No 01
ABL*MS
1 1 6.74
1 2 5.82
Mean 6.28
Median 6.28
Std Dev. 0.651
Rel.Std.Dev. 10.36%
PDM3 0.00%
Analytical results for Yb in OREAS 603 (Indicative Value 0.68 ppm)

Yb Round Replicate Lab
No No 01
ABL*MS
1 1 0.70
1 2 0.65
Mean 0.68
Median 0.68
Std Dev. 0.035
Rel.Std.Dev. 5.24%
PDM3 0.00%
Analytical results for Zn in OREAS 603 (Indicative Value 8530 ppm)
Zn Round Replicate Lab
No No 01
ABL*MS
1 1 8710
1 2 8350
Mean 8530
Median 8530
Std Dev. 255
Rel.Std.Dev. 2.98%
PDM3 0.00%
Analytical results for Zr in OREAS 603 (Indicative Value 122 ppm)

Zr Round Replicate Lab
No No 01
ABL*MS
1 1 123
1 2 120
Mean 122
Median 122
Std Dev. 2
Rel.Std.Dev. 1.75%
PDM3 0.00%
Indicative
1.00
ppm
0.00
0.00
1
1
16
282
7
Indicative
1.00
ppm
0.00
0.00
1
2
16
1715
8
Indicative
1.00
ppm
0.00
0.00
1
3
16
11550
9
Indicative
1.00
ppm
2.00
2.00
1.00
4.00
16.00
0.60
10.00
Indicative
1.00
ppm
0.00
0.00
1
5
16
145
11
Indicative
1.00
ppm
0.00
0.00
1
6
16
53
12
Indicative
1.00
ppm
1.00
1.00
1.0
7.0
16.0
30.7
13.0
Indicative
1.00
ppm
1.00
1.00
1.0
8.0
16.0
16.5
14.0
Indicative
1.00
ppm
1.00
1.00
1.0
9.0
16.0
39.0
15.0
Indicative
1.00
ppm
2.00
2.00
1.00
10.00
16.00
1.51
16.00
Indicative
1.00
ppm
0.00
0.00
1
11
16
9830
17
Indicative
1.00
ppm
2.00
2.00
1.00
12.00
16.00
1.20
18.00
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
0.69
19.00
Indicative
1.00
ppm
2.00
2.00
1.00
14.00
16.00
0.31
20.00
Indicative
1.00
ppm
1.00
1.00
1.0
15.0
16.0
24.1
21.0
Indicative
1.00
ppm
2.00
2.00
1.00
16.00
16.00
1.66
22.00
Indicative
1.00
ppm
2.00
2.00
1.00
17.00
16.00
3.64
23.00
Indicative
1.00
ppm
2.00
2.00
1.00
1.00
16.00
0.23
7.00
Indicative
1.00
ppm
1.00
1.00
1.0
2.0
16.0
10.1
8.0
Indicative
1.00
ppm
1.00
1.00
1.0
3.0
16.0
18.1
9.0
Indicative
1.00
ppm
3.00
3.00
1.000
4.000
16.000
0.095
10.000
Indicative
1.00
wt.%
3.00
3.00
1.000
5.000
16.000
0.014
11.000
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
6.30
12.00
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
7.79
13.00
Indicative
1.00
ppm
1.00
1.00
1.0
8.0
16.0
11.5
14.0
Indicative
1.00
ppm
0.00
0.00
1
9
16
110
15
Indicative
1.00
ppm
0.00
0.00
1
10
16
1945
16
Indicative
1.00
ppm
2.00
2.00
1.00
11.00
16.00
3.58
17.00
Indicative
1.00
ppm
1.00
1.00
1.0
12.0
16.0
23.3
18.0
Indicative
1.00
ppm
3.00
3.00
1.000
13.000
16.000
0.013
19.000
Indicative
1.00
ppm
0.00
0.00
1
14
16
184
20
Indicative
1.00
ppm
2.00
2.00
1.00
15.00
16.00
4.35
21.00
Indicative
1.00
ppm
2.00
2.00
1.00
16.00
16.00
<5
22.00
Indicative
1.00
ppm
2.00
2.00
1.00
17.00
16.00
2.04
23.00
Indicative
1.00
ppm
1.00
1.00
1.0
1.0
16.0
13.0
7.0
Indicative
1.00
ppm
0.00
0.00
1
2
16
571
8
Indicative
1.00
ppm
2.00
2.00
1.00
3.00
16.00
0.71
9.00
Indicative
1.00
ppm
2.00
2.00
1.00
4.00
16.00
0.20
10.00
Indicative
1.00
ppm
0.00
0.00
1
5
16
60
11
Indicative
1.00
ppm
2.00
2.00
1.00
6.00
16.00
6.98
12.00
Indicative
1.00
wt.%
3.00
3.00
1.000
7.000
16.000
0.198
13.000
Indicative
1.00
ppm
2.00
2.00
1.00
8.00
16.00
4.20
14.00
Indicative
1.00
ppm
2.00
2.00
1.00
9.00
16.00
0.10
15.00
Indicative
1.00
ppm
2.00
2.00
1.00
10.00
16.00
2.73
16.00
Indicative
1.00
ppm
1.00
1.00
1.0
11.0
16.0
32.4
17.0
Indicative
1.00
ppm
1.00
1.00
1.0
12.0
16.0
14.8
18.0
Indicative
1.00
ppm
2.00
2.00
1.00
13.00
16.00
6.28
19.00
Indicative
1.00
ppm
2.00
2.00
1.00
14.00
16.00
0.68
20.00
Indicative
1.00
ppm
0.00
0.00
1
15
16
8530
21
Indicative
1.00
ppm
0.00
0.00
1
16
16
122
22
Analytical results for Al2O3 in OREAS 603 (Indicative Value 7.8 wt.%)
Al2O3 Round Replicate Lab
No No 01
BF*XRF
1 1 7.80
1 2 7.79
Mean 7.80
Median 7.80
Std Dev. 0.007
Rel.Std.Dev. 0.09%
PDM3 0.00%
Analytical results for As in OREAS 603 (Indicative Value 1780 ppm)

As Round Replicate Lab
No No 01
BF*XRF
1 1 1780
1 2 1780
Mean 1780
Median 1780
Std Dev. 0
Rel.Std.Dev. 0.00%
PDM3 0.00%

Ba Round Replicate Lab
No No 01
BF*XRF
1 1 11400
1 2 11400
Mean 11400
Median 11400
Std Dev. 0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for CaO in OREAS 603 (Indicative Value 0.455 wt.%)
CaO Round Replicate Lab
No No 01
BF*XRF
1 1 0.460
1 2 0.450
Mean 0.455
Median 0.455
Std Dev. 0.007
Rel.Std.Dev. 1.55%
PDM3 0.00%
Analytical results for Co in OREAS 603 (Indicative Value 25 ppm)
Co Round Replicate Lab
No No 01
BF*XRF
1 1 30.0
1 2 20.0
Mean 25.0
Median 25.0
Std Dev. 7.1
Rel.Std.Dev. 28.28%
PDM3 0.00%
Analytical results for Cr in OREAS 603 (Indicative Value 35 ppm)

Cr Round Replicate Lab
No No 01
BF*XRF
1 1 40.0
1 2 30.0
Mean 35.0
Median 35.0
Std Dev. 7.1
Rel.Std.Dev. 20.20%
PDM3 0.00%
Analytical results for Cu in OREAS 603 (Indicative Value 10100 ppm)

Cu Round Replicate Lab
No No 01
BF*XRF
1 1 10100
1 2 10100
Mean 10100
Median 10100
Std Dev. 0
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Fe2O3 in OREAS 603 (Indicative Value 4.19 wt.%)
Fe2O3 Round Replicate Lab
No No 01
BF*XRF
1 1 4.19
1 2 4.18
Mean 4.19
Median 4.19
Std Dev. 0.007
Rel.Std.Dev. 0.17%
PDM3 0.00%
Analytical results for K2O in OREAS 603 (Indicative Value 0.773 wt.%)
K2O Round Replicate Lab
No No 01
BF*XRF
1 1 0.775
1 2 0.771
Mean 0.773
Median 0.773
Std Dev. 0.003
Rel.Std.Dev. 0.37%
PDM3 0.00%
Analytical results for MgO in OREAS 603 (Indicative Value 0.18 wt.%)
MgO Round Replicate Lab
No No 01
BF*XRF
1 1 0.180
1 2 0.180
Mean 0.180
Median 0.180
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for MnO in OREAS 603 (Indicative Value 0.02 wt.%)
MnO Round Replicate Lab
No No 01
BF*XRF
1 1 0.020
1 2 0.020
Mean 0.020
Median 0.020
Std Dev. 0.000
Rel.Std.Dev. 0.00%
PDM3 0.00%
Analytical results for Na2O in OREAS 603 (Indicative Value 0.55 wt.%)
Na2O Round Replicate Lab
No No 01
BF*XRF
1 1 0.540
1 2 0.560
Mean 0.550
Median 0.550
Std Dev. 0.014
Rel.Std.Dev. 2.57%
PDM3 0.00%
Analytical results for Ni in OREAS 603 (Indicative Value 95 ppm)

Ni Round Replicate Lab
No No 01
BF*XRF
1 1 90
1 2 100
Mean 95
Median 95
Std Dev. 7
Rel.Std.Dev. 7.44%
PDM3 0.00%
Analytical results for P2O5 in OREAS 603 (Indicative Value 0.129 wt.%)
P2O5 Round Replicate Lab
No No 01
BF*XRF
1 1 0.128
1 2 0.130
Mean 0.129
Median 0.129
Std Dev. 0.001
Rel.Std.Dev. 1.10%
PDM3 0.00%
Analytical results for Pb in OREAS 603 (Indicative Value 2015 ppm)

Pb Round Replicate Lab
No No 01
BF*XRF
1 1 2020
1 2 2010
Mean 2015
Median 2015
Std Dev. 7
Rel.Std.Dev. 0.35%
PDM3 0.00%
Analytical results for SiO2 in OREAS 603 (Indicative Value 75.29 wt.%)
SiO2 Round Replicate Lab
No No 01
BF*XRF
1 1 75.31
1 2 75.27
Mean 75.29
Median 75.29
Std Dev. 0.028
Rel.Std.Dev. 0.04%
PDM3 0.00%
Analytical results for Sn in OREAS 603 (Indicative Value 12.5 ppm)

Sn Round Replicate Lab
No No 01
BF*XRF
1 1 20.0
1 2 < 10
Mean 20.0
Median 20.0
Std Dev.
Rel.Std.Dev.
PDM3 60.00%
Analytical results for SO3 in OREAS 603 (Indicative Value 9.5 wt.%)
SO3 Round Replicate Lab
No No 01
BF*XRF
1 1 9.49
1 2 9.51
Mean 9.50
Median 9.50
Std Dev. 0.015
Rel.Std.Dev. 0.16%
PDM3 0.00%
Analytical results for TiO2 in OREAS 603 (Indicative Value 0.335 wt.%)
TiO2 Round Replicate Lab
No No 01
BF*XRF
1 1 0.336
1 2 0.333
Mean 0.335
Median 0.335
Std Dev. 0.002
Rel.Std.Dev. 0.63%
PDM3 0.00%
Analytical results for U in OREAS 603 (Indicative Value < 10 ppm)

U Round Replicate Lab
No No 01
BF*XRF
1 1 < 10
1 2 < 10
Mean
Median
Std Dev.
Rel.Std.Dev.
PDM3
Analytical results for Zn in OREAS 603 (Indicative Value 8800 ppm)

Zn Round Replicate Lab
No No 01
BF*XRF
1 1 8760
1 2 8840
Mean 8800
Median 8800
Std Dev. 57
Rel.Std.Dev. 0.64%
PDM3 0.00%
Indicative
1.00
wt.%
2.00
2.00
1.00
19.00
16.00
7.80
25.00
Indicative
1.00
ppm
0.00
0.00
1
2
16
1780
26
Indicative
1.00
ppm
0.00
0.00
1
3
16
11400
27
Indicative
1.00
wt.%
3.00
3.00
1.000
22.000
16.000
0.455
28.000
Indicative
1.00
ppm
1.00
1.00
1.0
8.0
16.0
25.0
29.0
Indicative
1.00
ppm
1.00
1.00
1.0
9.0
16.0
35.0
30.0
Indicative
1.00
ppm
0.00
0.00
1
11
16
10100
31
Indicative
1.00
wt.%
2.00
2.00
1.00
19.00
16.00
4.19
25.00
Indicative
1.00
wt.%
3.00
3.00
1.000
20.000
16.000
0.773
26.000
Indicative
1.00
wt.%
3.00
3.00
1.000
21.000
16.000
0.180
27.000
Indicative
1.00
wt.%
3.00
3.00
1.000
22.000
16.000
0.020
28.000
Indicative
1.00
wt.%
3.00
3.00
1.000
23.000
16.000
0.550
29.000
Indicative
1.00
ppm
0.00
0.00
1
9
16
95
30
Indicative
1.00
wt.%
3.00
3.00
1.000
25.000
16.000
0.129
31.000
Indicative
1.00
ppm
0.00
0.00
1
10
16
2015
25
Indicative
1.00
wt.%
2.00
2.00
1.00
20.00
16.00
75.29
26.00
Indicative
1.00
ppm
1.00
1.00
1.0
1.0
16.0
12.5
27.0
Indicative
1.00
wt.%
2.00
2.00
1.00
22.00
16.00
9.50
28.00
Indicative
1.00
wt.%
3.00
3.00
1.000
23.000
16.000
0.335
29.000
Indicative
1.00
ppm
1.00
1.00
1.0
10.0
16.0
< 10
30.0
Indicative
1.00
ppm
0.00
0.00
1
15
16
8800
31
Analytical results for LOI1000 in OREAS 603 (Indicative Value 5.42 wt.%)
LOI1000 Round Replicate Lab
No No 01
at 1000°C
1 1 5.44
1 2 5.39
Mean 5.42
Median 5.42
Std Dev. 0.035
Rel.Std.Dev. 0.65%
PDM3 0.00%
Indicative
1.00
wt.%
2.00
2.00
1.00
27.00
16.00
5.42
33.00
No No 01 02 04 05
4A*OES 4A*OES 4A*AAS 4A*OES/AAS
1 1 303 292 289 302

1 2 304 292 291 303
1 3 303 295 286 303
1 4 302 297 289 303
1 5 300 292 287 304
1 6 301 287 290 301
Mean 302 293 289 303
Median 302 292 289 303
Std Dev. 2 3 2 1
Rel.Std.Dev. 0.54% 1.16% 0.64% 0.34%
PDM3 1.60% -1.68% -2.97% 1.74%
Z-Score (Absolute) 0.86 0.19 0.60 0.90
Analytical results for Al in OREAS 603 (Certified Value 3.98 wt.%)

Al Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
4A*OES 4A*OES 4A*OES 4A*OES
1 1 4.12 3.93 3.96 3.83

1 2 3.84 3.95 3.88 3.93
1 3 4.08 3.92 3.89 3.84
1 4 4.11 3.92 3.99 3.87
1 5 4.03 3.99 4.05 3.82
1 6 4.09 3.96 4.00 3.91
Mean 4.04 3.94 3.96 3.87
Median 4.09 3.94 3.98 3.86
Std Dev. 0.105 0.026 0.066 0.045
Rel.Std.Dev. 2.59% 0.66% 1.67% 1.16%
PDM3 1.58% -0.93% -0.49% -2.87%
Z-Score (Absolute) 0.76 0.05 0.05 0.50
Analytical results for As in OREAS 603 (Certified Value 1801 ppm)

As Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
4A*OES 4A*MS 4A*OES 4A*OES
1 1 1998 1782 1850 1870

1 2 2023 1781 1760 1915
1 3 2018 1827 1830 1845
1 4 2034 1791 1910 1885
1 5 1988 1775 1880 1845
1 6 2023 1765 1860 1900
Mean 2014 1787 1848 1877
Median 2020 1782 1855 1878
Std Dev. 18 21 51 29
Rel.Std.Dev. 0.87% 1.19% 2.77% 1.53%
PDM3 11.84% -0.78% 2.64% 4.22%
Z-Score (Absolute) 1.50 0.05 0.44 0.63
Analytical results for B in OREAS 603 (Indicative Value < 20 ppm)

B Round Replicate Lab
No No 25
PF*OES
1 1 < 20
1 2 < 20
1 3 < 20
1 4 < 20
1 5 < 20
1 6 20.0
Mean 20.0
Median 20.0
Std Dev.
Rel.Std.Dev.
PDM3

Ba Round Replicate Lab Lab Lab Lab
No No 02 05 06 07
4A*MS 4A*OES 4A*OES 4A*OES
1 1 2083 3760 40 150

1 2 2148 3240 50 130
1 3 2107 3250 40 150
1 4 2113 2710 40 170
1 5 2289 2620 40 180
1 6 2165 2780 40 170
Mean 2151 3060 42 158
Median 2130 3010 40 160
Std Dev. 74 437 4 18
Rel.Std.Dev. 3.44% 14.27% 9.80% 11.59%
PDM3 -14.11% 22.21% -98.34% -93.68%
Z-Score (Absolute) 0.44 1.10 1.02 0.94
Analytical results for Be in OREAS 603 (Certified Value 0.71 ppm)

Be Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 0.77 0.73 0.70 0.70

1 2 0.76 0.70 0.70 0.70
1 3 0.76 0.75 0.70 0.70
1 4 0.77 0.74 0.70 0.70
1 5 0.76 0.72 0.70 0.70
1 6 0.78 0.72 0.70 0.80
Mean 0.77 0.73 0.70 0.72
Median 0.77 0.73 0.70 0.70
Std Dev. 0.008 0.018 0.000 0.041
Rel.Std.Dev. 1.10% 2.41% 0.00% 5.70%
PDM3 7.74% 2.33% -1.43% 0.92%
Z-Score (Absolute) 0.50 0.11 0.16 0.01
Analytical results for Bi in OREAS 603 (Certified Value 149 ppm)

Bi Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 174 160 160 157

1 2 163 160 154 164
1 3 170 160 154 154
1 4 170 157 160 161
1 5 167 166 163 157
1 6 171 162 161 162
Mean 169 161 159 159
Median 170 160 160 159
Std Dev. 4 3 4 4
Rel.Std.Dev. 2.10% 1.88% 2.38% 2.36%
PDM3 13.34% 7.90% 6.36% 6.70%
Z-Score (Absolute) 1.30 0.62 0.52 0.56
Analytical results for Ca in OREAS 603 (Certified Value 0.318 wt.%)

Ca Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 0.430 0.317 0.320 0.330

1 2 0.380 0.317 0.310 0.330
1 3 0.455 0.314 0.320 0.330
1 4 0.415 0.316 0.330 0.330
1 5 0.390 0.322 0.330 0.320
1 6 0.410 0.319 0.330 0.330
Mean 0.413 0.318 0.323 0.328
Median 0.413 0.317 0.325 0.330
Std Dev. 0.027 0.003 0.008 0.004
Rel.Std.Dev. 6.57% 0.87% 2.53% 1.24%
PDM3 29.99% -0.12% 1.69% 3.26%
Z-Score (Absolute) 7.35 0.40 0.07 0.47
Analytical results for Cd in OREAS 603 (Certified Value 54 ppm)
Cd Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 79 53 56 58
1 2 78 52 54 59
1 3 79 52 55 57
1 4 81 51 56 58
1 5 78 52 57 56
1 6 81 53 56 58
Mean 79 52 56 58
Median 79 52 56 58
Std Dev. 1.3 0.6 1.0 1.1
Rel.Std.Dev. 1.64% 1.13% 1.82% 1.86%
PDM3 47.76% -2.60% 3.66% 7.30%
Z-Score (Absolute) 6.87 0.77 0.18 0.74
Analytical results for Ce in OREAS 603 (Certified Value 25.7 ppm)

Ce Round Replicate Lab Lab Lab Lab
No No 02 09 11 12
4A*MS 4A*OES/MS 4A*OES 4A*MS
1 1 19.5 29.3 25.0 13.7

1 2 20.4 30.0 23.0 17.3
1 3 20.5 30.3 25.0 12.5
1 4 20.0 30.3 22.0 13.0
1 5 21.9 29.2 23.0 13.6
1 6 19.7 29.8 23.0 14.5
Mean 20.3 29.8 23.5 14.1
Median 20.2 29.9 23.0 13.6
Std Dev. 0.9 0.5 1.2 1.7
Rel.Std.Dev. 4.32% 1.57% 5.21% 12.02%
PDM3 -20.95% 15.94% -8.63% -45.24%
Z-Score (Absolute) 0.70 0.67 0.24 1.69
Analytical results for Co in OREAS 603 (Certified Value 15.3 ppm)

Co Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 18.0 15.0 15.0 17.0

1 2 17.8 14.9 15.0 17.0
1 3 18.1 14.8 15.0 16.0
1 4 18.6 15.0 16.0 16.0
1 5 18.1 15.0 15.0 16.0
1 6 18.7 15.2 16.0 16.0
Mean 18.2 15.0 15.3 16.3
Median 18.1 15.0 15.0 16.0
Std Dev. 0.351 0.133 0.516 0.516
Rel.Std.Dev. 1.93% 0.89% 3.37% 3.16%
PDM3 18.95% -2.04% 0.25% 6.79%
Z-Score (Absolute) 3.57 0.23 0.18 1.37
Analytical results for Cr in OREAS 603 (Certified Value 30.2 ppm)

Cr Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 30.0 29.0 23.0 29.0

1 2 30.8 28.0 22.0 28.0
1 3 30.1 28.0 25.0 31.0
1 4 32.2 26.0 22.0 28.0
1 5 29.9 29.0 22.0 29.0
1 6 31.7 28.0 32.0 28.0
Mean 30.8 28.0 24.3 28.8
Median 30.4 28.0 22.5 28.5
Std Dev. 1.0 1.1 3.9 1.2
Rel.Std.Dev. 3.22% 3.91% 16.16% 4.05%
PDM3 1.78% -7.40% -19.53% -4.65%
Z-Score (Absolute) 0.02 0.49 1.44 0.33
Analytical results for Cs in OREAS 603 (Certified Value 1.66 ppm)

Cs Round Replicate Lab Lab Lab Lab
No No 02 09 12 13
4A*MS 4A*OES/MS 4A*MS 4A*MS
1 1 1.60 1.69 1.99 1.76

1 2 1.59 1.65 2.19 1.78
1 3 1.56 1.67 2.07 2.26
1 4 1.61 1.65 1.75 1.81
1 5 1.60 1.68 1.80 1.63
1 6 1.65 1.61 1.82 1.79
Mean 1.60 1.66 1.94 1.84
Median 1.60 1.66 1.91 1.79
Std Dev. 0.029 0.028 0.174 0.218
Rel.Std.Dev. 1.83% 1.67% 9.00% 11.83%
PDM3 -3.64% -0.19% 16.52% 10.67%
Z-Score (Absolute) 0.95 0.17 3.64 1.14
Analytical results for Cu in OREAS 603 (Certified Value 1 wt.%)

Cu Round Replicate Lab Lab Lab Lab
No No 01 02 04 05
4A*OES 4A*OES 4A*AAS 4A*OES/AAS
1 1 1.01 0.99 1.04 1.01

1 2 1.00 0.99 1.02 1.01
1 3 1.00 1.00 1.03 1.02
1 4 1.01 0.98 1.04 1.02
1 5 1.01 1.00 1.04 1.02
1 6 1.01 1.00 1.04 1.01
Mean 1.01 0.99 1.04 1.01
Median 1.01 0.99 1.04 1.01
Std Dev. 0.002 0.006 0.008 0.005
Rel.Std.Dev. 0.23% 0.63% 0.78% 0.49%
PDM3 0.31% -1.10% 3.19% 0.78%
Z-Score (Absolute) 0.07 0.36 0.93 0.21
[α]: Lab 07: Rnd 01 - 4A*OES, Rnd 01 - 4A*OES/AAS
[β]: Lab 08: Rnd 01 - 4A*OES, Rnd 01 - 4A*OES/AAS
Analytical results for Dy in OREAS 603 (Certified Value 1.21 ppm)

Dy Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 1.18 1.24 1.13 1.37

1 2 1.20 1.26 1.14 1.19
1 3 1.22 1.29 1.18 1.22
1 4 1.22 1.28 1.13 1.23
1 5 1.26 1.27 1.00 1.23
1 6 1.19 1.29 1.14 1.20
Mean 1.21 1.27 1.12 1.24
Median 1.21 1.27 1.13 1.23
Std Dev. 0.029 0.020 0.062 0.066
Rel.Std.Dev. 2.36% 1.58% 5.54% 5.30%
PDM3 0.04% 4.96% -7.46% 2.38%
Z-Score (Absolute) 0.25 0.79 1.82 0.25
Analytical results for Er in OREAS 603 (Certified Value 0.59 ppm)

Er Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 0.58 0.62 0.20 0.63

1 2 0.58 0.58 0.20 0.61
1 3 0.61 0.62 0.18 0.53
1 4 0.61 0.61 0.18 0.59
1 5 0.60 0.61 0.14 0.61
1 6 0.58 0.57 0.17 0.59
Mean 0.59 0.60 0.18 0.59
Median 0.59 0.61 0.18 0.60
Std Dev. 0.015 0.021 0.021 0.034
Rel.Std.Dev. 2.54% 3.50% 11.62% 5.81%
PDM3 -0.27% 1.08% -70.07% -0.27%
Z-Score (Absolute) 0.00 0.44 22.69 0.00
Analytical results for Eu in OREAS 603 (Certified Value < 1 ppm)

Eu Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 0.43 0.50 - 0.76

1 2 0.42 0.47 - 0.61
1 3 0.41 0.52 - 0.69
1 4 0.41 0.51 - 0.75
1 5 0.43 0.49 - 0.72
1 6 0.41 0.44 - 0.61
Mean 0.42 0.49 0.69
Median 0.42 0.49 0.71
Std Dev. 0.010 0.030 0.067
Rel.Std.Dev. 2.35% 6.06% 9.66%
PDM3
Analytical results for Fe in OREAS 603 (Certified Value 2.92 wt.%)

Fe Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 2.82 2.90 2.86 2.78

1 2 2.81 2.92 2.79 2.86
1 3 2.82 2.91 2.80 2.79
1 4 2.86 2.90 2.88 2.82
1 5 2.80 2.96 2.91 2.77
1 6 2.86 2.93 2.89 2.83
Mean 2.83 2.92 2.86 2.81
Median 2.82 2.92 2.87 2.81
Std Dev. 0.027 0.023 0.049 0.034
Rel.Std.Dev. 0.96% 0.78% 1.73% 1.22%
PDM3 -3.22% -0.09% -2.32% -3.91%
Z-Score (Absolute) 0.41 0.42 0.17 0.60
Analytical results for Ga in OREAS 603 (Certified Value 22.2 ppm)

Ga Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 25.3 22.4 20.0 20.0

1 2 25.3 22.3 20.0 20.0
1 3 25.1 22.5 20.0 20.0
1 4 25.2 22.2 30.0 20.0
1 5 25.6 22.9 30.0 20.0
1 6 25.5 22.3 20.0 20.0
Mean 25.3 22.4 23.3 20.0
Median 25.3 22.4 20.0 20.0
Std Dev. 0.203 0.230 5.164 0.000
Rel.Std.Dev. 0.80% 1.03% 22.13% 0.00%
PDM3 14.04% 1.03% 5.05% -9.96%
Z-Score (Absolute) 1.31 0.14 0.84 0.84
Analytical results for Gd in OREAS 603 (Certified Value 1.77 ppm)

Gd Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 1.68 2.31 1.67 1.87

1 2 1.67 2.24 1.75 1.72
1 3 1.75 2.37 1.67 1.79
1 4 1.76 2.35 1.64 1.82
1 5 1.77 2.28 1.74 1.85
1 6 1.65 2.33 1.72 1.83
Mean 1.71 2.31 1.70 1.81
Median 1.72 2.32 1.70 1.83
Std Dev. 0.052 0.047 0.045 0.053
Rel.Std.Dev. 3.06% 2.02% 2.63% 2.93%
PDM3 -3.27% 30.55% -4.15% 2.38%
Z-Score (Absolute) 1.04 5.69 1.21 0.08
Analytical results for Ge in OREAS 603 (Indicative Value 5.05 ppm)

Ge Round Replicate Lab Lab Lab Lab
No No 02 09 11 12
1 1 5.29 8.40 < 10 5.67

1 2 5.69 8.44 < 10 5.84
1 3 5.36 8.56 < 10 5.46
1 4 5.56 8.75 < 10 4.84
1 5 6.08 8.31 < 10 5.72
1 6 6.10 8.39 < 10 5.92
Mean 5.68 8.47 5.58
Median 5.63 8.42 5.70
Std Dev. 0.348 0.160 0.393
Rel.Std.Dev. 6.13% 1.89% 7.05%
PDM3 12.58% 67.93% 10.49%
Analytical results for Hf in OREAS 603 (Certified Value 2.53 ppm)

Hf Round Replicate Lab Lab Lab Lab
No No 02 09 12 13
1 1 2.58 2.61 2.40 2.40
1 2 2.69 2.59 2.70 2.49
1 3 2.60 2.66 2.50 2.36
1 4 2.58 2.70 2.20 2.42
1 5 2.76 2.51 2.20 2.30
1 6 2.59 2.60 2.40 2.40
Mean 2.63 2.61 2.40 2.39
Median 2.60 2.60 2.40 2.40
Std Dev. 0.075 0.064 0.190 0.062
Rel.Std.Dev. 2.84% 2.44% 7.91% 2.59%
PDM3 4.29% 3.48% -4.95% -5.18%
Z-Score (Absolute) 0.56 0.59 0.83 0.87
Analytical results for Hg in OREAS 603 (Indicative Value < 1 ppm)

Hg Round Replicate Lab
No No 11
4A*OES
1 1 <1
1 2 1.00
1 3 <1
1 4 <1
1 5 <1
1 6 <1
Mean 1.00
Median 1.00
Std Dev.
Rel.Std.Dev.
PDM3
Analytical results for Ho in OREAS 603 (Certified Value 0.21 ppm)

Ho Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 0.22 0.21 0.20 0.25

1 2 0.21 0.21 0.20 0.22
1 3 0.23 0.22 0.18 0.19
1 4 0.21 0.23 0.18 0.22
1 5 0.23 0.22 0.17 0.23
1 6 0.21 0.24 0.17 0.23
Mean 0.22 0.22 0.18 0.22
Median 0.22 0.22 0.18 0.23
Std Dev. 0.010 0.011 0.012 0.020
Rel.Std.Dev. 4.50% 4.75% 6.75% 8.80%
PDM3 4.14% 5.65% -12.68% 6.53%
Z-Score (Absolute) 0.11 0.55 4.73 0.80
Analytical results for In in OREAS 603 (Certified Value 11.2 ppm)

In Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
4A*OES 4A*MS 4A*OES/MS 4A*OES
1 1 8.3 11.1 11.5 < 10

1 2 8.3 11.2 11.6 12.0
1 3 8.2 11.3 11.9 13.0
1 4 8.4 11.1 11.4 10.0
1 5 8.2 11.2 11.5 11.0
1 6 8.5 10.9 11.4 10.0
Mean 8.3 11.1 11.5 11.2
Median 8.3 11.1 11.5 11.0
Std Dev. 0.112 0.118 0.187 1.304
Rel.Std.Dev. 1.35% 1.06% 1.62% 11.64%
PDM3 -25.94% -0.74% 3.00% -0.01%
Z-Score (Absolute) 3.38 0.24 0.15 0.15
Analytical results for K in OREAS 603 (Certified Value 0.623 wt.%)

K Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 0.630 0.633 0.600 0.640

1 2 0.585 0.625 0.590 0.640
1 3 0.620 0.645 0.600 0.640
1 4 0.620 0.636 0.610 0.640
1 5 0.625 0.639 0.620 0.630
1 6 0.620 0.629 0.610 0.640
Mean 0.617 0.635 0.605 0.638
Median 0.620 0.635 0.605 0.640
Std Dev. 0.016 0.007 0.010 0.004
Rel.Std.Dev. 2.60% 1.11% 1.73% 0.64%
PDM3 -0.99% 1.89% -2.87% 2.48%
Z-Score (Absolute) 0.09 0.49 0.99 0.67
Analytical results for La in OREAS 603 (Certified Value 11.9 ppm)

La Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 13.1 13.3 10.0 10.0

1 2 13.8 13.3 10.0 10.0
1 3 12.9 13.6 10.0 10.0
1 4 13.2 13.7 10.0 10.0
1 5 13.4 13.5 10.0 10.0
1 6 13.5 14.0 10.0 10.0
Mean 13.3 13.6 10.0 10.0
Median 13.3 13.5 10.0 10.0
Std Dev. 0.3 0.3 0.0 0.0
Rel.Std.Dev. 2.38% 1.99% 0.00% 0.00%
PDM3 11.74% 13.76% -16.08% -16.08%
Z-Score (Absolute) 0.64 0.71 0.34 0.34
Analytical results for Li in OREAS 603 (Certified Value 18.9 ppm)

Li Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
1 1 18.8 19.1 19.9 20.0

1 2 18.5 18.5 21.1 20.0
1 3 18.6 19.5 20.5 20.0
1 4 18.6 18.5 20.6 20.0
1 5 18.3 19.0 21.1 20.0
1 6 18.6 18.8 20.7 20.0
Mean 18.6 18.9 20.7 20.0
Median 18.6 18.9 20.6 20.0
Std Dev. 0.193 0.385 0.455 0.000
Rel.Std.Dev. 1.04% 2.04% 2.21% 0.00%
PDM3 -2.06% -0.23% 9.01% 5.58%
Z-Score (Absolute) 0.21 0.02 1.20 0.76
Analytical results for Lu in OREAS 603 (Certified Value 0.099 ppm)

Lu Round Replicate Lab Lab Lab Lab
No No 02 09 15 17
4A*MS 4A*OES/MS 4A*MS 4A*OES/MS
1 1 0.090 0.100 0.130 0.080

1 2 0.090 0.095 0.100 0.080
1 3 0.090 0.110 < 0.1 0.090
1 4 0.090 0.112 0.100 0.100
1 5 0.090 0.094 0.110 0.080
1 6 0.080 0.092 0.100 0.080
Mean 0.088 0.101 0.108 0.085
Median 0.090 0.098 0.100 0.080
Std Dev. 0.004 0.009 0.013 0.008
Rel.Std.Dev. 4.62% 8.85% 12.07% 9.84%
PDM3 -10.54% 1.89% 9.38% -13.91%
Z-Score (Absolute) 0.97 0.00 0.59 1.24
Analytical results for Mg in OREAS 603 (Certified Value 828 ppm)

Mg Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 750 834 800 800
1 2 754 826 800 800
1 3 817 857 800 800
1 4 861 822 800 800
1 5 841 846 800 800
1 6 861 834 800 800
Mean 814 837 800 800
Median 829 834 800 800
Std Dev. 50 13 0 0
Rel.Std.Dev. 6.19% 1.55% 0.00% 0.00%
PDM3 -1.75% 0.97% -3.44% -3.44%
Z-Score (Absolute) 0.14 0.47 0.51 0.51
Analytical results for Mn in OREAS 603 (Certified Value 133 ppm)

Mn Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 132 125 139 144

1 2 138 126 133 145
1 3 133 140 137 144
1 4 135 124 140 146
1 5 131 134 141 139
1 6 135 131 141 144
Mean 134 130 139 144
Median 134 129 140 144
Std Dev. 2 6 3 2
Rel.Std.Dev. 1.77% 4.79% 2.23% 1.69%
PDM3 1.00% -2.03% 4.37% 8.26%
Z-Score (Absolute) 0.11 0.59 0.42 1.15
Analytical results for Mo in OREAS 603 (Certified Value 6.05 ppm)

Mo Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 6.50 6.00 6.00 7.00

1 2 6.24 5.90 5.00 7.00
1 3 6.66 5.90 6.00 6.00
1 4 6.47 5.90 6.00 6.00
1 5 6.42 6.10 6.00 6.00
1 6 6.59 5.60 6.00 6.00
Mean 6.48 5.90 5.83 6.33
Median 6.48 5.90 6.00 6.00
Std Dev. 0.149 0.167 0.408 0.516
Rel.Std.Dev. 2.29% 2.84% 7.00% 8.15%
PDM3 7.05% -2.53% -3.63% 4.63%
Z-Score (Absolute) 0.85 0.38 0.67 0.50
Analytical results for Na in OREAS 603 (Certified Value 0.428 wt.%)

Na Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 0.429 0.426 0.420 0.440

1 2 0.418 0.425 0.400 0.450
1 3 0.435 0.448 0.410 0.450
1 4 0.445 0.432 0.420 0.450
1 5 0.420 0.437 0.430 0.440
1 6 0.423 0.424 0.430 0.460
Mean 0.428 0.432 0.418 0.448
Median 0.426 0.429 0.420 0.450
Std Dev. 0.010 0.010 0.012 0.008
Rel.Std.Dev. 2.37% 2.20% 2.79% 1.68%
PDM3 0.00% 0.85% -2.34% 4.67%
Z-Score (Absolute) 0.00 0.24 0.67 1.34
Analytical results for Nb in OREAS 603 (Certified Value 7.09 ppm)

Nb Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
1 1 5.61 7.05 7.47 < 10

1 2 5.63 7.14 7.54 < 10
1 3 5.93 7.06 7.41 < 10
1 4 5.83 7.06 7.56 < 10
1 5 5.73 7.41 7.41 < 10
1 6 5.81 7.01 7.39 < 10
Mean 5.76 7.12 7.47
Median 5.77 7.06 7.44
Std Dev. 0.123 0.147 0.071
Rel.Std.Dev. 2.14% 2.07% 0.95%
PDM3 -18.87% 0.39% 5.24%
Analytical results for Nd in OREAS 603 (Certified Value 11.4 ppm)

Nd Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 9.5 12.8 11.5 12.5

1 2 9.6 12.6 11.4 11.8
1 3 9.7 12.8 11.1 11.8
1 4 9.5 12.8 11.4 12.3
1 5 10.3 12.6 11.0 12.0
1 6 9.2 12.6 11.0 12.2
Mean 9.6 12.7 11.2 12.1
Median 9.5 12.7 11.3 12.1
Std Dev. 0.4 0.1 0.2 0.3
Rel.Std.Dev. 3.75% 1.00% 1.98% 2.41%
PDM3 -15.67% 11.55% -1.37% 6.06%
Z-Score (Absolute) 1.77 0.85 0.34 0.34
Analytical results for Ni in OREAS 603 (Certified Value 112 ppm)

Ni Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 118 113 112 111

1 2 115 115 108 110
1 3 115 114 111 112
1 4 118 114 115 109
1 5 115 117 116 109
1 6 117 113 120 109
Mean 116 114 114 110
Median 116 114 114 110
Std Dev. 2 2 4 1
Rel.Std.Dev. 1.48% 1.38% 3.72% 1.15%
PDM3 4.06% 2.32% 1.63% -1.65%
Z-Score (Absolute) 0.96 0.57 0.42 0.32
Analytical results for P in OREAS 603 (Certified Value 534 ppm)

P Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 525 658 520 530

1 2 526 740 510 550
1 3 524 761 510 540
1 4 531 658 530 530
1 5 532 639 530 510
1 6 532 742 540 540
Mean 528 700 523 533
Median 528 699 525 535
Std Dev. 4 54 12 14
Rel.Std.Dev. 0.71% 7.65% 2.31% 2.56%
PDM3 -1.11% 30.99% -2.02% -0.15%
Z-Score (Absolute) 0.00 8.32 0.24 0.25
Analytical results for Pb in OREAS 603 (Certified Value 1908 ppm)

Pb Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 1882 1789 2030 1990
1 2 1882 1811 1985 2060
1 3 1885 1815 1995 2010
1 4 1895 1790 2050 2020
1 5 1857 1869 2070 1970
1 6 1889 1784 2050 2030
Mean 1882 1810 2030 2013
Median 1883 1801 2040 2015
Std Dev. 13 32 34 31
Rel.Std.Dev. 0.70% 1.75% 1.66% 1.56%
PDM3 -1.39% -5.15% 6.39% 5.52%
Z-Score (Absolute) 0.34 0.96 0.75 0.63
Analytical results for Pr in OREAS 603 (Certified Value 3.23 ppm)

Pr Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 2.51 3.33 3.31 3.54

1 2 2.57 3.31 3.41 3.34
1 3 2.60 3.41 3.20 3.37
1 4 2.55 3.36 3.31 3.45
1 5 2.73 3.34 3.12 3.46
1 6 2.43 3.30 3.11 3.46
Mean 2.57 3.34 3.24 3.44
Median 2.56 3.34 3.25 3.46
Std Dev. 0.100 0.039 0.120 0.072
Rel.Std.Dev. 3.90% 1.15% 3.72% 2.09%
PDM3 -20.49% 3.58% 0.49% 6.53%
Z-Score (Absolute) 2.46 0.69 0.29 1.08
Analytical results for Rb in OREAS 603 (Certified Value 23.6 ppm)

Rb Round Replicate Lab Lab Lab Lab
No No 02 09 12 13
1 1 21.9 24.9 27.8 25.0

1 2 21.7 24.3 30.8 24.7
1 3 21.2 24.2 29.3 25.3
1 4 22.0 24.4 24.4 24.8
1 5 21.9 23.9 25.0 25.1
1 6 21.6 23.6 25.8 24.9
Mean 21.7 24.2 27.2 25.0
Median 21.8 24.3 26.8 24.9
Std Dev. 0.283 0.442 2.544 0.200
Rel.Std.Dev. 1.30% 1.83% 9.36% 0.80%
PDM3 -8.09% 2.51% 15.04% 5.62%
Z-Score (Absolute) 0.86 0.18 1.11 0.49
Analytical results for Re in OREAS 603 (Indicative Value 4 ppb)

Re Round Replicate Lab Lab Lab Lab
No No 02 09 11 12
1 1 3 <2 < 5000 4

1 2 2 <2 < 5000 4
1 3 3 3 < 5000 4
1 4 3 <2 < 5000 4
1 5 <2 2 < 5000 3
1 6 2 <2 < 5000 4
Mean 3 3 4
Median 3 3 4
Std Dev. 1 1 0
Rel.Std.Dev. 21.07% 51.39% 10.65%
PDM3 -31.98% -33.73% 0.29%

No No 01 02 05 06
1 1 4.02 3.49 3.81 3.73

1 2 4.06 3.52 3.71 3.86
1 3 4.07 3.52 3.73 3.74
1 4 4.04 3.50 3.81 3.77
1 5 4.01 3.50 3.86 3.71
1 6 4.02 3.60 3.83 3.80
Mean 4.04 3.52 3.79 3.77
Median 4.03 3.51 3.81 3.76
Std Dev. 0.025 0.040 0.059 0.055
Rel.Std.Dev. 0.61% 1.15% 1.55% 1.46%
PDM3 8.89% -5.00% 2.27% 1.64%
Z-Score (Absolute) 2.06 1.25 0.48 0.33
Analytical results for Sb in OREAS 603 (Certified Value 205 ppm)

Sb Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 204 204 218 216

1 2 200 203 218 226
1 3 201 205 213 219
1 4 205 200 223 222
1 5 194 208 223 214
1 6 200 203 221 219
Mean 201 204 219 219
Median 201 204 220 219
Std Dev. 4 3 4 4
Rel.Std.Dev. 1.83% 1.43% 1.75% 1.95%
PDM3 -1.97% -0.44% 7.04% 7.04%
Z-Score (Absolute) 0.17 0.02 0.73 0.73
Analytical results for Sc in OREAS 603 (Certified Value 4.04 ppm)

Sc Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 3.23 3.30 4.00 4.00

1 2 3.25 3.40 4.00 4.00
1 3 3.57 3.30 4.00 4.00
1 4 3.93 3.30 4.00 4.00
1 5 3.59 3.40 4.00 4.00
1 6 3.71 3.50 4.00 4.00
Mean 3.55 3.37 4.00 4.00
Median 3.58 3.35 4.00 4.00
Std Dev. 0.269 0.082 0.000 0.000
Rel.Std.Dev. 7.57% 2.43% 0.00% 0.00%
PDM3 -12.26% -16.69% -1.02% -1.02%
Z-Score (Absolute) 2.67 3.73 0.00 0.00
Analytical results for Se in OREAS 603 (Certified Value 60 ppm)

Se Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
1 1 67 58 58 45
1 2 66 59 55 47
1 3 67 61 59 45
1 4 66 59 58 46
1 5 66 60 58 47
1 6 67 56 56 46
Mean 67 59 57 46
Median 66 59 58 46
Std Dev. 0 2 2 1
Rel.Std.Dev. 0.43% 3.03% 2.72% 1.94%
PDM3 10.66% -2.51% -4.79% -23.47%
Z-Score (Absolute) 0.69 0.13 0.22 1.44
Analytical results for Sm in OREAS 603 (Certified Value 2.14 ppm)

Sm Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 2.06 2.22 1.97 2.16
1 2 2.07 2.33 2.00 2.15
1 3 2.10 2.41 2.04 2.21
1 4 2.12 2.25 2.06 2.22
1 5 2.08 2.20 1.99 2.08
1 6 1.89 2.30 1.98 2.27
Mean 2.05 2.29 2.01 2.18
Median 2.08 2.28 2.00 2.19
Std Dev. 0.083 0.080 0.036 0.066
Rel.Std.Dev. 4.04% 3.50% 1.77% 3.03%
PDM3 -3.84% 7.01% -5.93% 2.17%
Z-Score (Absolute) 0.41 1.08 0.70 0.41
Analytical results for Sn in OREAS 603 (Certified Value 12.9 ppm)

Sn Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
1 1 14.2 11.7 12.5 14.0

1 2 14.4 11.5 12.8 13.0
1 3 14.7 11.6 13.3 14.0
1 4 14.5 11.7 13.2 13.0
1 5 14.0 11.9 12.7 13.0
1 6 14.5 11.9 12.7 13.0
Mean 14.4 11.7 12.9 13.3
Median 14.5 11.7 12.8 13.0
Std Dev. 0.261 0.160 0.290 0.516
Rel.Std.Dev. 1.81% 1.37% 2.25% 3.87%
PDM3 11.92% -8.99% -0.02% 3.57%
Z-Score (Absolute) 1.29 1.58 0.35 0.14
Analytical results for Sr in OREAS 603 (Certified Value 459 ppm)

Sr Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 487 360 507 447

1 2 445 370 490 458
1 3 477 377 493 446
1 4 495 366 503 442
1 5 498 388 507 423
1 6 501 364 507 452
Mean 484 371 501 445
Median 491 368 505 447
Std Dev. 21 10 8 12
Rel.Std.Dev. 4.32% 2.79% 1.54% 2.69%
PDM3 5.39% -19.19% 9.14% -3.16%
Z-Score (Absolute) 0.22 1.03 0.32 0.22
Analytical results for Ta in OREAS 603 (Certified Value < 1 ppm)

Ta Round Replicate Lab Lab Lab Lab
No No 02 09 12 14
1 1 0.84 0.50 0.22 0.54

1 2 0.87 0.49 0.21 0.59
1 3 0.85 0.53 0.18 0.59
1 4 0.75 0.55 0.20 0.58
1 5 0.85 0.52 0.17 0.54
1 6 0.82 0.51 0.18 0.55
Mean 0.83 0.52 0.19 0.57
Median 0.85 0.51 0.19 0.57
Std Dev. 0.042 0.022 0.020 0.024
Rel.Std.Dev. 5.11% 4.20% 10.17% 4.30%
PDM3
Z-Score (Absolute) 1.51 0.00 1.48 0.22
Analytical results for Tb in OREAS 603 (Certified Value 0.23 ppm)

Tb Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 0.23 0.26 0.19 0.26

1 2 0.22 0.26 0.22 0.23
1 3 0.22 0.25 0.25 0.22
1 4 0.23 0.27 0.21 0.24
1 5 0.23 0.26 0.18 0.26
1 6 0.21 0.27 0.20 0.25
Mean 0.22 0.26 0.21 0.24
Median 0.23 0.26 0.21 0.25
Std Dev. 0.008 0.007 0.024 0.016
Rel.Std.Dev. 3.66% 2.59% 11.35% 6.71%
PDM3 -3.50% 13.41% -9.67% 5.14%
Z-Score (Absolute) 0.13 1.45 0.71 0.67
Analytical results for Te in OREAS 603 (Certified Value 56 ppm)

Te Round Replicate Lab Lab Lab Lab
No No 02 09 11 12
1 1 65 57 52 29
1 2 67 56 52 33
1 3 64 57 57 30
1 4 67 57 55 26
1 5 69 56 57 29
1 6 65 56 56 31
Mean 66 56 55 30
Median 66 56 56 29
Std Dev. 2 0 2 2
Rel.Std.Dev. 2.59% 0.86% 4.22% 7.73%
PDM3 17.28% 0.38% -2.54% -47.42%
Z-Score (Absolute) 1.07 0.16 0.00 2.43
Analytical results for Th in OREAS 603 (Certified Value 5.9 ppm)

Th Round Replicate Lab Lab Lab Lab
No No 02 05 06 07
4A*MS 4A*OES 4A*OES 4A*OES
1 1 4.40 < 20 < 20 < 20

1 2 4.72 < 20 < 20 < 20
1 3 4.54 < 20 < 20 < 20
1 4 4.52 < 20 < 20 < 20
1 5 5.12 < 20 < 20 < 20
1 6 4.52 < 20 < 20 < 20
Mean 4.64
Median 4.53
Std Dev. 0.258
Rel.Std.Dev. 5.57%
PDM3 -21.42%
Analytical results for Ti in OREAS 603 (Certified Value 0.191 wt.%)

Ti Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 0.165 0.192 0.200 0.200

1 2 0.160 0.195 0.190 0.210
1 3 0.170 0.198 0.200 0.200
1 4 0.175 0.193 0.210 0.210
1 5 0.170 0.198 0.210 0.200
1 6 0.175 0.195 0.200 0.210
Mean 0.169 0.195 0.202 0.205
Median 0.170 0.195 0.200 0.205
Std Dev. 0.006 0.002 0.008 0.005
Rel.Std.Dev. 3.46% 1.25% 3.73% 2.67%
PDM3 -11.47% 2.13% 5.54% 7.29%
Z-Score (Absolute) 1.13 0.09 0.40 0.56
Analytical results for Tl in OREAS 603 (Certified Value 4.18 ppm)

Tl Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
1 1 <5 4.35 3.95 <5
1 2 <5 4.36 3.90 <5
1 3 <5 4.29 4.05 <5
1 4 <5 4.34 4.03 <5
1 5 <5 4.39 4.05 <5
1 6 <5 4.37 4.15 <5
Mean 4.35 4.02
Median 4.36 4.04
Std Dev. 0.034 0.086
Rel.Std.Dev. 0.78% 2.14%
PDM3 3.99% -3.87%
Z-Score (Absolute) NA 0.74 0.72 NA

Tm Round Replicate Lab Lab Lab Lab
No No 02 09 15 17
4A*MS 4A*OES/MS 4A*MS 4A*OES/MS
1 1 0.090 0.089 0.120 0.070

1 2 0.080 0.086 < 0.1 0.070
1 3 0.090 0.094 < 0.1 0.070
1 4 0.080 0.093 0.110 0.080
1 5 0.090 0.082 0.120 0.070
1 6 0.080 0.087 0.100 0.070
Mean 0.085 0.089 0.113 0.072
Median 0.085 0.088 0.115 0.070
Std Dev. 0.005 0.004 0.010 0.004
Rel.Std.Dev. 6.44% 5.04% 8.51% 5.70%
PDM3 -3.61% 0.47% 27.57% -18.73%
Z-Score (Absolute) 0.67 0.00 0.58 3.17
Analytical results for U in OREAS 603 (Certified Value 2.71 ppm)

U Round Replicate Lab Lab Lab Lab
No No 02 07 08 09
4A*MS 4A*OES 4A*OES 4A*OES/MS
1 1 2.67 < 10 < 10 2.55

1 2 2.72 < 10 < 10 2.58
1 3 2.70 < 10 < 10 2.64
1 4 2.66 < 10 < 10 2.60
1 5 2.78 < 10 < 10 2.61
1 6 2.62 < 10 < 10 2.57
Mean 2.69 2.59
Median 2.69 2.59
Std Dev. 0.055 0.031
Rel.Std.Dev. 2.05% 1.18%
PDM3 -0.50% -4.14%
Z-Score (Absolute) 0.13 NA NA 0.43
Analytical results for V in OREAS 603 (Certified Value 32 ppm)

V Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 33.3 30.0 31.0 34.0

1 2 33.8 31.0 30.0 34.0
1 3 33.3 30.0 31.0 34.0
1 4 33.6 30.0 32.0 34.0
1 5 33.6 32.0 32.0 33.0
1 6 33.6 30.0 32.0 34.0
Mean 33.5 30.5 31.3 33.8
Median 33.6 30.0 31.5 34.0
Std Dev. 0.198 0.837 0.816 0.408
Rel.Std.Dev. 0.59% 2.74% 2.61% 1.21%
PDM3 4.88% -4.65% -2.05% 5.77%
Z-Score (Absolute) 0.71 0.35 0.06 0.81
Analytical results for W in OREAS 603 (Certified Value 14 ppm)

W Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 10.8 16.1 < 10 30.0

1 2 10.9 16.2 < 10 40.0
1 3 10.4 16.4 < 10 40.0
1 4 10.2 16.2 < 10 40.0
1 5 10.6 16.8 < 10 40.0
1 6 10.9 16.5 < 10 30.0
Mean 10.6 16.4 36.7
Median 10.7 16.3 40.0
Std Dev. 0.3 0.3 5.2
Rel.Std.Dev. 2.57% 1.58% 14.08%
PDM3 -24.13% 16.84% 161.75%
Analytical results for Y in OREAS 603 (Certified Value 5.64 ppm)

Y Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
1 1 5.23 5.34 5.62 6.00

1 2 5.31 5.17 5.88 5.00
1 3 5.56 5.34 5.77 6.00
1 4 5.86 5.19 5.82 5.00
1 5 5.77 5.29 5.59 6.00
1 6 5.89 5.42 5.63 6.00
Mean 5.60 5.29 5.72 5.67
Median 5.67 5.32 5.70 6.00
Std Dev. 0.283 0.096 0.119 0.516
Rel.Std.Dev. 5.05% 1.82% 2.08% 9.11%
PDM3 -0.63% -6.18% 1.41% 0.47%
Z-Score (Absolute) 0.26 1.57 0.22 0.00
Analytical results for Yb in OREAS 603 (Certified Value 0.61 ppm)

Yb Round Replicate Lab Lab Lab Lab
No No 02 09 13 15
1 1 0.62 0.62 0.43 0.63

1 2 0.63 0.57 0.45 0.64
1 3 0.62 0.65 0.46 0.73
1 4 0.61 0.63 0.45 0.66
1 5 0.64 0.58 0.46 0.63
1 6 0.61 0.59 0.43 0.64
Mean 0.62 0.61 0.45 0.66
Median 0.62 0.60 0.45 0.64
Std Dev. 0.012 0.031 0.013 0.038
Rel.Std.Dev. 1.88% 5.19% 2.84% 5.85%
PDM3 2.01% -0.62% -26.67% 7.48%
Z-Score (Absolute) 0.14 0.32 4.91 0.67
Analytical results for Zn in OREAS 603 (Certified Value 0.92 wt.%)

Zn Round Replicate Lab Lab Lab Lab
No No 01 02 05 06
1 1 0.968 0.908 0.920 0.946

1 2 0.973 0.921 0.887 0.971
1 3 0.971 0.905 0.911 0.939
1 4 0.979 0.909 0.937 0.958
1 5 0.975 0.910 0.945 0.933
1 6 0.978 0.910 0.930 0.961
Mean 0.974 0.910 0.922 0.951
Median 0.974 0.909 0.925 0.952
Std Dev. 0.004 0.005 0.021 0.014
Rel.Std.Dev. 0.42% 0.59% 2.26% 1.52%
PDM3 5.92% -1.02% 0.22% 3.44%
Z-Score (Absolute) 2.49 0.42 0.10 1.45
Analytical results for Zr in OREAS 603 (Certified Value 78 ppm)

Zr Round Replicate Lab Lab Lab Lab
No No 01 02 09 11
1 1 71 75 84 87
1 2 70 77 84 85
1 3 73 75 84 85
1 4 71 76 85 87
1 5 70 79 84 89
1 6 72 78 85 90
Mean 71 76 84 87
Median 71 76 84 87
Std Dev. 1.3 1.4 0.4 2.0
Rel.Std.Dev. 1.88% 1.89% 0.48% 2.34%
PDM3 -8.48% -1.98% 7.96% 11.74%
Z-Score (Absolute) 0.77 0.00 1.18 1.62
06 07 08 09 10 11 12
4A*OES/AAS 4A*OES/AAS 4A*OES 4A*OES/MS 4A*OES 4A*AAS 4A*MS
299 306 > 100 319 280 294 > 100

301 303 > 100 316 292 295 > 100
306 295 > 100 324 289 284 > 100
302 298 > 100 310 291 291 > 100
296 301 > 100 315 291 297 > 100
308 307 > 100 307 285 293 > 100
302 302 315 288 292
302 302 315 290 294
4 5 6 5 5
1.47% 1.54% 1.93% 1.61% 1.56%
1.51% 1.40% 5.96% -3.19% -1.74%
0.83 0.79 NA 2.05 0.67 0.03 NA

07 08 09 10 11 12 13
4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*OES
4.02 3.96 4.24 2.51 4.11 2.65 4.07

3.82 3.95 4.30 2.71 4.15 2.89 4.07
3.92 3.86 4.33 3.20 4.10 2.80 4.17
3.86 3.97 4.34 2.59 4.13 2.34 4.15
3.97 3.96 4.30 2.79 4.03 2.72 4.10
3.87 3.89 4.27 2.57 4.06 3.29 4.07
3.91 3.93 4.30 2.73 4.10 2.78 4.10
3.90 3.96 4.30 2.65 4.11 2.76 4.08
0.075 0.045 0.039 0.252 0.045 0.312 0.046
1.91% 1.15% 0.90% 9.25% 1.09% 11.22% 1.13%
-1.79% -1.24% 7.95% -31.47% 2.90% -30.13% 3.08%
0.25 0.12 1.99 7.62 0.83 6.77 0.87

07 08 09 10 11 12 14
4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*MS 4A*MS
1895 1830 1892 1770 1885 225 1957

1790 1840 1904 1760 1898 262 2015
1850 1790 1959 1750 1869 232 1884
1825 1820 1953 1730 1887 184 1944
1880 1810 1916 1750 1888 215 1934
1830 1785 1912 1760 1885 250 1938
1845 1813 1923 1753 1885 228 1945
1840 1815 1914 1755 1886 228 1941
38 22 27 14 9 27 42
2.09% 1.21% 1.41% 0.78% 0.50% 12.00% 2.17%
2.46% 0.65% 6.76% -2.63% 4.70% -87.33% 8.03%
0.42 0.22 0.92 0.16 0.68 9.86 1.06

08 09 11 12 13 14 16
4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*MS 4A*OES
2800 9488 1158 1462 2296 941 140

2810 9656 2371 1775 2379 1559 158
9440 9380 1045 1398 2228 1958 130
2130 9601 1228 1571 2305 1454 141
2160 9641 1506 1536 2280 777 179
2760 9851 1899 1772 2317 2058 179
3683 9603 1535 1586 2301 1458 155
2780 9621 1367 1554 2300 1507 150
2838 160 512 157 49 520 21
77.05% 1.67% 33.34% 9.92% 2.14% 35.66% 13.59%
47.10% 283.51% -38.72% -36.67% -8.11% -41.78% -93.83%
0.73 5.68 0.03 0.06 0.56 0.03 0.94

07 08 09 11 12 13 14
4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*MS 4A*MS
0.70 0.70 0.77 0.80 0.83 0.59 0.60

0.70 0.70 0.65 1.00 0.91 0.59 0.70
0.70 0.70 0.66 0.80 0.90 0.55 0.50
0.70 0.70 0.79 0.80 0.71 0.58 0.70
0.70 0.70 0.73 0.80 0.79 0.59 0.60
0.70 0.70 0.69 0.80 0.79 0.57 0.60
0.70 0.70 0.71 0.83 0.82 0.58 0.62
0.70 0.70 0.71 0.80 0.81 0.58 0.60
0.000 0.000 0.060 0.082 0.075 0.015 0.075
0.00% 0.00% 8.33% 9.80% 9.19% 2.65% 12.21%
-1.43% -1.43% 0.63% 17.35% 15.71% -18.56% -13.16%
0.16 0.16 0.01 0.85 1.07 1.38 1.00

07 08 09 10 11 12 13
161 151 145 140 149 167 140

154 156 145 130 139 186 134
162 157 148 120 149 180 131
159 157 148 120 151 152 140
165 153 149 150 154 156 137
164 146 148 150 149 159 138
161 153 147 135 149 167 137
162 155 148 135 149 163 137
4 4 2 14 5 14 3
2.47% 2.82% 1.26% 10.21% 3.40% 8.17% 2.51%
7.82% 2.79% -1.35% -9.50% -0.45% 11.80% -8.42%
0.69 0.13 0.34 1.25 0.09 1.13 1.13

07 08 09 10 11 12 13
0.340 0.330 0.311 0.220 0.330 0.350 0.304

0.320 0.330 0.306 0.240 0.340 0.370 0.313
0.330 0.330 0.310 0.260 0.330 0.430 0.313
0.330 0.330 0.311 0.220 0.320 0.300 0.315
0.330 0.330 0.314 0.250 0.320 0.320 0.313
0.330 0.320 0.315 0.230 0.320 0.310 0.309
0.330 0.328 0.311 0.237 0.327 0.347 0.311
0.330 0.330 0.311 0.235 0.325 0.335 0.313
0.006 0.004 0.003 0.016 0.008 0.048 0.004
1.92% 1.24% 0.99% 6.90% 2.50% 13.97% 1.24%
3.78% 3.26% -2.12% -25.57% 2.73% 9.02% -2.19%
0.61 0.47 0.91 6.95 0.34 0.61 0.93
07 08 09 10 11 12 13
58 58 56 54 54 66 50
55 58 56 53 53 73 49
57 59 56 52 55 77 48
56 57 56 52 54 60 51
57 57 56 52 55 63 49
56 56 56 53 55 64 51
57 57 56 53 54 67 50
57 57 56 53 55 65 50
1.2 0.8 0.3 0.8 0.8 6.4 1.2
2.08% 1.35% 0.51% 1.55% 1.50% 9.49% 2.33%
5.49% 6.89% 4.15% -1.84% 1.27% 25.08% -7.09%
0.46 0.67 0.26 0.65 0.18 3.43 1.45
Lab Lab Lab Lab Lab

13 15 17 19 25
4A*OES 4A*MS 4A*OES/MS 4A*OES/MS 4A*MS
33.6 32.4 23.0 26.4 25.1

33.5 30.1 23.8 26.0 25.8
35.5 30.3 24.4 23.6 24.4
35.1 31.8 28.4 25.8 25.6
35.0 31.6 24.2 24.2 27.7
37.3 31.3 23.8 25.0 28.2
35.0 31.3 24.6 25.1 26.1
35.1 31.5 24.0 25.4 25.7
1.4 0.9 1.9 1.1 1.5
3.91% 2.86% 7.82% 4.40% 5.73%
36.09% 21.56% -4.35% -2.22% 1.61%
1.42 0.88 0.19 0.00 0.14

07 08 09 10 11 12 13
15.0 15.0 15.6 10.0 16.0 7.7 16.9

15.0 14.0 15.8 10.0 16.0 9.2 16.4
15.0 15.0 16.1 10.0 17.0 7.8 16.6
15.0 15.0 15.8 11.0 17.0 8.0 16.9
16.0 15.0 15.5 6.0 17.0 8.4 16.3
16.0 14.0 15.8 10.0 17.0 9.8 16.6
15.3 14.7 15.7 9.5 16.7 8.5 16.6
15.0 15.0 15.8 10.0 17.0 8.2 16.6
0.516 0.516 0.185 1.761 0.516 0.845 0.242
3.37% 3.52% 1.17% 18.53% 3.10% 9.96% 1.45%
0.25% -4.11% 2.97% -37.89% 8.97% -44.53% 8.75%
0.18 0.61 0.67 5.90 1.76 7.94 1.72

07 08 09 10 11 12 13
32.0 33.0 33.6 37.0 34.0 29.0 35.9

31.0 30.0 31.7 33.0 30.0 28.0 36.7
29.0 31.0 31.5 34.0 34.0 27.0 36.8
30.0 29.0 29.2 34.0 30.0 25.0 34.9
34.0 31.0 29.6 34.0 35.0 26.0 37.8
29.0 30.0 28.3 36.0 30.0 23.0 35.5
30.8 30.7 30.7 34.7 32.2 26.3 36.3
30.5 30.5 30.5 34.0 32.0 26.5 36.3
1.9 1.4 2.0 1.5 2.4 2.2 1.1
6.29% 4.46% 6.44% 4.34% 7.47% 8.20% 2.91%
1.97% 1.42% 1.40% 14.65% 6.38% -12.91% 19.89%
0.03 0.00 0.00 0.65 0.27 0.79 1.02

14 15 17 19 24 25
4A*MS 4A*MS 4A*OES/MS 4A*OES/MS 4A*MS 4A*MS
1.70 1.66 1.60 1.49 1.70 1.60

1.70 1.66 1.67 1.45 1.70 1.60
1.70 1.71 1.63 1.49 1.60 1.50
1.70 1.75 1.71 1.43 1.70 1.50
1.70 1.66 1.60 1.43 1.70 1.60
1.70 1.76 1.68 1.49 1.70 1.50
1.70 1.70 1.65 1.46 1.68 1.55
1.70 1.69 1.65 1.47 1.70 1.55
0.000 0.047 0.045 0.030 0.041 0.055
0.00% 2.76% 2.75% 2.06% 2.43% 3.53%
2.28% 2.28% -0.83% -11.93% 1.28% -6.74%
0.40 0.40 0.31 2.84 0.17 1.66

06 07 08 09 10 11 12
4A*OES/AAS Various [α] Various [β] 4A*OES/MS 4A*OES 4A*AAS 4A*AAS
see footer see footer
1.02 1.02 1.06 1.03 1.04 1.05 1.00
1.02 0.96 1.07 1.05 1.05 1.05 1.01
1.04 0.98 0.98 1.03 1.03 1.04 1.00
1.03 0.98 1.07 1.03 1.02 1.05 1.00
1.02 1.01 1.00 1.05 1.05 1.08 1.00
1.04 0.98 0.99 1.05 1.04 1.08 1.00
1.03 0.99 1.03 1.04 1.04 1.06 1.00
1.02 0.98 1.03 1.04 1.04 1.05 1.00
0.012 0.020 0.042 0.010 0.012 0.017 0.004
1.13% 2.05% 4.04% 0.96% 1.13% 1.61% 0.41%
2.28% -1.61% 2.45% 3.54% 3.53% 5.39% -0.13%
0.65 0.51 0.70 1.03 1.02 1.58 0.07
Lab Lab
17 25
4A*OES/MS 4A*MS
1.13 1.25
1.19 1.25
1.15 1.20
1.22 1.20
1.15 1.25
1.15 1.40
1.17 1.26
1.15 1.25
0.033 0.074
2.86% 5.85%
-3.81% 3.89%
1.05 0.56
Lab Lab
17 25
4A*OES/MS 4A*MS
0.57 0.60
0.58 0.60
0.56 0.60
0.61 0.60
0.57 0.65
0.57 0.70
0.58 0.63
0.57 0.60
0.018 0.042
3.04% 6.69%
-3.07% 5.05%
0.91 0.91
Lab Lab
17 25
4A*OES/MS 4A*MS
0.78 0.55
0.77 0.55
0.80 0.55
1.55 0.55
0.60 0.60
0.72 0.60
0.87 0.57
0.78 0.55
0.341 0.026
39.18% 4.56%
0.91 0.00

07 08 09 10 11 12 13
2.89 2.87 3.05 2.90 3.13 2.77 3.01

2.72 2.89 3.02 2.91 3.18 2.94 2.98
2.81 2.79 3.01 2.90 3.13 3.06 3.06
2.77 2.86 3.05 2.82 3.14 2.37 3.06
2.85 2.85 3.07 2.90 3.13 2.52 3.00
2.78 2.81 3.13 2.88 3.13 2.71 2.99
2.80 2.85 3.06 2.89 3.14 2.73 3.01
2.80 2.86 3.05 2.90 3.13 2.74 3.00
0.061 0.038 0.043 0.033 0.020 0.256 0.033
2.16% 1.33% 1.42% 1.15% 0.64% 9.40% 1.11%
-4.08% -2.66% 4.53% -1.29% 7.44% -6.65% 3.14%
0.64 0.26 1.65 0.10 2.42 0.67 1.28

07 08 09 11 12 13 14
20.0 20.0 23.6 26.0 17.1 21.0 23.6

20.0 20.0 24.0 26.0 19.4 20.8 24.0
20.0 20.0 24.1 27.0 17.1 20.9 23.5
20.0 20.0 24.3 27.0 15.3 20.3 23.6
20.0 20.0 23.6 26.0 17.4 20.1 23.7
20.0 20.0 24.0 26.0 19.5 20.6 23.2
20.0 20.0 23.9 26.3 17.6 20.6 23.6
20.0 20.0 24.0 26.0 17.3 20.7 23.6
0.000 0.000 0.291 0.516 1.601 0.359 0.261
0.00% 0.00% 1.22% 1.96% 9.08% 1.74% 1.10%
-9.96% -9.96% 7.73% 18.56% -20.62% -7.13% 6.25%
0.84 0.84 0.74 1.71 1.80 0.59 0.61
Lab Lab
17 25
4A*OES/MS 4A*MS
1.74 2.00
1.83 2.00
1.78 1.60
1.87 1.60
1.79 2.00
1.78 1.80
1.80 1.83
1.79 1.90
0.045 0.197
2.52% 10.73%
1.53% 3.51%
0.08 0.31
Lab Lab Lab Lab

14 15 17 25
4A*MS 4A*MS 4A*OES/MS PF*MS
8.70 1.37 1.90 < 20

8.80 1.26 0.70 < 20
8.00 1.23 0.80 < 20
8.20 1.28 0.20 < 20
8.50 1.31 1.10 < 20
8.20 1.34 0.70 < 20
8.40 1.30 0.90
8.35 1.30 0.75
0.316 0.052 0.569
3.76% 4.00% 63.25%
66.48% -74.27% -82.16%
0.67 1.09 1.23 NA

14 15 17 19 24 25
2.80 2.67 2.60 2.67 2.40 2.40
2.90 2.57 2.46 2.51 2.40 2.20
2.70 2.67 2.49 2.58 2.40 2.20
2.90 2.70 2.65 2.50 2.60 2.20
2.70 2.57 2.42 2.57 2.60 2.40
2.70 2.64 2.25 2.59 2.40 2.40
2.78 2.64 2.48 2.57 2.47 2.30
2.75 2.66 2.48 2.57 2.40 2.30
0.098 0.055 0.142 0.063 0.103 0.110
3.53% 2.09% 5.71% 2.44% 4.19% 4.76%
10.23% 4.42% -1.85% 1.79% -2.31% -8.91%
1.74 0.75 0.31 0.31 0.39 1.50
Lab Lab
17 25
4A*OES/MS 4A*MS
0.19 0.20
0.20 0.22
0.19 0.20
0.21 0.22
0.19 0.22
0.19 0.24
0.20 0.22
0.19 0.22
0.008 0.015
4.29% 6.95%
-6.99% 3.35%
3.09 0.11

12 13 14 15 17 19 24
4A*MS 4A*MS 4A*MS 4A*MS 4A*OES/MS 4A*OES/MS 4A*MS
12.0 10.3 11.9 12.2 12.4 10.1 11.5

14.0 10.1 12.0 11.9 12.1 9.6 11.4
11.9 10.0 11.7 12.0 11.8 9.7 11.5
8.9 10.6 11.8 12.3 11.8 9.7 11.4
10.9 10.4 11.5 12.0 12.1 9.8 11.7
11.8 10.5 11.8 12.2 12.8 9.9 11.5
11.6 10.3 11.8 12.1 12.2 9.8 11.5
11.9 10.3 11.8 12.1 12.1 9.7 11.5
1.641 0.223 0.164 0.168 0.383 0.162 0.110
14.18% 2.16% 1.39% 1.39% 3.15% 1.66% 0.95%
3.28% -8.01% 5.23% 7.97% 8.62% -12.64% 2.67%
0.26 1.15 0.50 0.85 0.93 1.72 0.18

07 08 09 11 12 13 14
4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*OES
0.630 0.600 0.627 0.670 0.710 0.636 0.632

0.600 0.590 0.621 0.670 0.770 0.648 0.650
0.610 0.600 0.607 0.670 0.800 0.643 0.634
0.610 0.600 0.617 0.660 0.660 0.640 0.627
0.630 0.600 0.614 0.650 0.680 0.644 0.629
0.610 0.590 0.627 0.650 0.680 0.639 0.633
0.615 0.597 0.619 0.662 0.717 0.642 0.634
0.610 0.600 0.619 0.665 0.695 0.642 0.632
0.012 0.005 0.008 0.010 0.056 0.004 0.008
1.99% 0.87% 1.24% 1.49% 7.83% 0.64% 1.29%
-1.26% -4.21% -0.65% 6.23% 15.06% 3.02% 1.81%
0.49 1.41 0.30 1.84 4.59 0.84 0.46

07 08 09 11 12 13 15
10.0 10.0 15.1 12.0 4.9 16.0 17.0

10.0 10.0 15.4 12.0 6.4 18.1 17.0
10.0 20.0 15.3 12.0 4.8 13.8 17.0
10.0 10.0 15.7 12.0 4.8 15.7 17.0
10.0 10.0 15.4 12.0 5.1 15.8 17.0
10.0 10.0 15.5 12.0 5.7 12.4 17.0
10.0 11.7 15.4 12.0 5.3 15.3 17.0
10.0 10.0 15.4 12.0 5.0 15.7 17.0
0.0 4.1 0.2 0.0 0.6 2.0 0.0
0.00% 34.99% 1.32% 0.00% 12.17% 12.89% 0.00%
-16.08% -2.09% 29.40% 0.71% -55.66% 28.31% 42.67%
0.34 0.34 1.26 0.25 1.79 1.22 1.73

12 13 14 15 16 17 18
4A*MS 4A*OES 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES
20.5 20.8 18.0 18.0 18.0 19.0 27.0

16.7 21.3 17.8 17.8 18.0 19.0 28.0
20.0 21.1 17.7 18.7 18.0 19.0 27.0
18.7 21.1 17.8 18.2 18.0 19.0 27.0
18.4 21.0 17.3 17.9 18.0 19.0 27.0
21.0 21.2 17.3 18.9 18.0 18.0 27.0
19.2 21.1 17.7 18.2 18.0 18.8 27.2
19.4 21.1 17.8 18.1 18.0 19.0 27.0
1.594 0.169 0.288 0.444 0.000 0.408 0.408
8.30% 0.80% 1.63% 2.44% 0.00% 2.17% 1.50%
1.44% 11.22% -6.83% -3.74% -4.98% -0.58% 43.41%
0.24 1.49 0.82 0.43 0.58 0.02 5.60
Lab Lab
19 25
4A*OES/MS 4A*MS
0.098 0.100
0.100 0.120
0.101 0.100
0.099 0.120
0.094 0.100
0.111 0.120
0.101 0.110
0.100 0.110
0.006 0.011
5.66% 9.96%
1.78% 11.40%
0.00 0.75

07 08 09 10 11 12 13
800 800 813 750 900 1000 856
800 800 813 800 900 1100 857
800 800 805 800 900 1100 865
800 800 815 750 900 800 859
800 800 812 750 900 900 865
800 800 805 800 900 900 853
800 800 811 775 900 967 859
800 800 812 775 900 950 858
0 0 4 27 0 121 5
0.00% 0.00% 0.52% 3.53% 0.00% 12.53% 0.56%
-3.44% -3.44% -2.16% -6.46% 8.63% 16.68% 3.71%
0.51 0.51 0.23 1.19 2.18 3.98 1.08

07 08 09 10 11 12 13
142 137 134 131 151 124 141

131 136 135 131 146 123 141
137 138 135 131 150 151 146
136 137 137 128 143 111 143
141 135 136 129 141 115 143
136 132 133 131 148 111 141
137 136 135 130 147 123 143
137 137 135 131 147 119 142
4 2 2 1 4 15 2
2.89% 1.57% 1.13% 1.02% 2.69% 12.30% 1.37%
3.37% 2.36% 1.72% -1.91% 10.40% -7.69% 7.52%
0.26 0.10 0.00 0.57 1.38 2.17 0.92

07 08 09 10 11 12 14
5.00 6.00 6.08 6.00 7.00 5.77 6.60

5.00 6.00 6.25 5.00 7.00 6.52 6.70
5.00 7.00 6.27 4.00 7.00 6.07 6.30
5.00 5.00 6.03 5.00 7.00 5.10 6.60
6.00 6.00 6.21 5.00 6.00 5.34 6.30
5.00 5.00 6.37 5.00 8.00 5.71 6.50
5.17 5.83 6.20 5.00 7.00 5.75 6.50
5.00 6.00 6.23 5.00 7.00 5.74 6.55
0.408 0.753 0.127 0.632 0.632 0.508 0.167
7.90% 12.90% 2.04% 12.65% 9.04% 8.82% 2.57%
-14.64% -3.63% 2.44% -17.40% 15.65% -4.98% 7.39%
2.24 0.67 0.19 2.16 1.60 0.87 0.89

07 08 09 11 12 13 14
0.440 0.410 0.414 0.430 0.480 0.424 0.421

0.420 0.400 0.416 0.440 0.520 0.431 0.435
0.420 0.390 0.416 0.430 0.540 0.435 0.427
0.420 0.410 0.420 0.440 0.430 0.440 0.423
0.430 0.410 0.414 0.440 0.440 0.427 0.421
0.420 0.410 0.411 0.430 0.450 0.426 0.422
0.425 0.405 0.415 0.435 0.477 0.431 0.425
0.420 0.410 0.415 0.435 0.465 0.429 0.422
0.008 0.008 0.003 0.005 0.045 0.006 0.005
1.97% 2.07% 0.73% 1.26% 9.44% 1.40% 1.24%
-0.78% -5.45% -3.10% 1.55% 11.28% 0.51% -0.84%
0.23 1.57 0.89 0.45 3.25 0.15 0.24

12 14 15 17 19 23 25
4A*MS 4A*MS 4A*MS 4A*OES/MS 4A*OES/MS 4A*OES 4A*MS
4.30 7.10 7.65 6.50 7.66 6.00 8.50

4.30 7.40 7.24 6.80 7.94 6.00 8.00
3.50 7.60 7.16 6.90 7.54 7.00 7.50
4.20 7.60 7.72 7.50 7.34 6.00 8.00
3.50 7.20 7.62 6.50 7.39 6.00 8.50
4.10 7.20 7.35 6.20 7.77 7.00 8.00
3.98 7.35 7.46 6.73 7.61 6.33 8.08
4.15 7.30 7.49 6.65 7.60 6.00 8.00
0.382 0.217 0.237 0.450 0.231 0.516 0.376
9.58% 2.95% 3.17% 6.69% 3.04% 8.15% 4.66%
-43.85% 3.61% 5.11% -5.09% 7.20% -10.72% 13.94%
4.99 0.22 0.39 0.73 0.62 1.35 1.36
Lab Lab
17 25
4A*OES/MS 4A*MS
10.3 11.9
10.4 12.0
10.7 11.6
10.3 11.7
10.7 13.4
11.0 13.0
10.6 12.3
10.6 12.0
0.3 0.7
2.65% 6.09%
-7.18% 7.75%
0.88 0.50

07 08 09 10 11 12 13
117 113 108 143 113 111 107

111 113 108 157 114 131 108
114 92 109 159 114 112 109
112 111 109 144 112 86 107
116 111 107 143 113 100 109
113 110 107 141 112 108 109
114 108 108 148 113 108 108
114 111 108 144 113 109 108
2 8 1 8 1 15 1
2.04% 7.47% 0.75% 5.38% 0.79% 13.56% 0.81%
1.78% -3.14% -3.49% 32.18% 1.04% -3.47% -3.21%
0.45 0.00 0.74 7.30 0.28 0.77 0.67

07 08 09 11 12 14 16
540 530 587 522 594 519 300

510 520 566 579 675 523 100
530 510 549 518 611 515 200
520 520 549 522 469 500 200
540 520 534 526 545 519 < 100
530 500 531 525 635 516 200
528 517 553 532 588 515 200
530 520 549 524 603 518 200
12 10 21 23 73 8 71
2.21% 2.00% 3.80% 4.36% 12.34% 1.56% 35.36%
-1.09% -3.27% 3.44% -0.40% 10.12% -3.52% -62.56%
0.00 0.56 1.18 0.27 2.06 0.48 15.93

07 08 09 10 11 12 13
2020 2010 1914 1550 2029 2045 1952
1915 2020 1903 1790 1984 2243 2007
1995 2030 1936 1680 1976 2398 1993
1945 2000 1927 1540 1929 1845 1990
2000 1980 1935 1670 1946 1953 1996
1950 1960 1953 1640 1968 2014 1990
1971 2000 1928 1645 1972 2083 1988
1973 2005 1931 1655 1972 2029 1992
40 26 18 93 34 202 19
2.04% 1.30% 0.92% 5.63% 1.75% 9.71% 0.94%
3.29% 4.82% 1.05% -13.79% 3.35% 9.16% 4.18%
0.31 0.53 0.00 2.08 0.32 0.67 0.44
Lab Lab
17 25
4A*OES/MS 4A*MS
3.00 2.92
3.17 3.00
3.14 2.72
3.53 3.00
3.05 3.14
3.14 3.28
3.17 3.01
3.14 3.00
0.187 0.191
5.89% 6.34%
-1.69% -6.70%
0.29 0.65

14 15 17 19 24 25
23.5 23.4 26.0 21.1 21.2 23.2

25.2 23.6 25.5 20.7 21.6 24.6
24.1 23.5 25.7 20.7 21.2 22.2
23.9 23.7 25.4 20.6 20.6 23.2
24.0 23.4 25.9 20.8 21.4 23.6
23.2 24.1 26.8 21.3 21.4 23.4
24.0 23.6 25.9 20.9 21.2 23.4
24.0 23.5 25.8 20.8 21.3 23.3
0.685 0.286 0.504 0.290 0.344 0.774
2.86% 1.21% 1.95% 1.39% 1.62% 3.31%
1.49% -0.17% 9.53% -11.61% -10.14% -1.12%
0.08 0.08 0.87 1.21 1.06 0.17
Lab Lab Lab

14 15 25
4A*MS 4A*MS 4A*MS
< 50 < 10 < 100

< 50 < 10 < 100
< 50 10 < 100
< 50 20 < 100
< 50 10 < 100
< 50 10 < 100
13
10
5
40.00%
227.03%
NA 2.45 NA

07 08 09 10 11 12 13
3.82 3.69 3.69 3.63 3.76 4.28 3.56

3.60 3.70 3.55 3.66 3.69 4.77 3.55
3.74 3.93 3.53 3.62 3.69 4.59 3.50
3.68 3.65 3.60 3.54 3.83 3.39 3.54
3.76 3.65 3.63 3.61 3.77 3.97 3.54
3.70 3.62 3.73 3.61 3.78 4.37 3.49
3.72 3.71 3.62 3.61 3.75 4.23 3.53
3.72 3.67 3.62 3.62 3.77 4.33 3.54
0.075 0.113 0.079 0.040 0.055 0.493 0.028
2.03% 3.06% 2.18% 1.10% 1.46% 11.67% 0.80%
0.25% -0.02% -2.30% -2.58% 1.24% 14.05% -4.83%
0.00 0.35 0.61 0.67 0.24 3.29 1.21

07 08 09 10 11 12 13
228 210 197 220 234 59 152

212 210 202 210 234 64 149
216 213 203 210 226 50 146
212 208 200 220 231 50 155
214 210 197 200 232 58 151
215 208 199 220 231 68 146
216 210 200 213 231 58 150
215 210 200 215 232 58 150
6 2 2 8 3 7 4
2.78% 0.87% 1.24% 3.83% 1.27% 12.73% 2.38%
5.49% 2.40% -2.52% 4.11% 12.89% -71.76% -26.79%
0.46 0.27 0.23 0.44 1.31 7.14 2.65

07 08 09 11 12 13 14
4.00 4.00 4.10 5.00 3.80 4.29 4.00

4.00 4.00 4.37 4.00 4.10 4.16 4.00
4.00 4.00 4.23 4.00 4.20 4.44 4.00
4.00 4.00 4.41 4.00 3.30 4.14 4.00
4.00 4.00 4.29 4.00 3.50 4.29 4.00
4.00 4.00 4.33 4.00 3.70 4.18 4.00
4.00 4.00 4.29 4.17 3.77 4.25 4.00
4.00 4.00 4.31 4.00 3.75 4.24 4.00
0.000 0.000 0.113 0.408 0.344 0.112 0.000
0.00% 0.00% 2.63% 9.80% 9.15% 2.64% 0.00%
-1.02% -1.02% 6.17% 3.11% -6.79% 5.19% -1.02%
0.00 0.00 1.71 0.98 1.37 1.48 0.00

12 14 15 17 18 19 21
4A*MS 4A*MS 4A*MS 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES
65 60 58 64 71 46 97
73 61 59 68 69 46 82
62 58 58 66 84 46 87
52 59 59 68 73 46 87
61 62 57 66 72 45 72
66 59 57 66 81 46 75
63 60 58 66 75 46 83
64 60 58 66 73 46 85
7 1 1 2 6 0 9
10.94% 2.46% 1.97% 2.27% 8.04% 1.07% 10.91%
5.08% -0.46% -3.41% 10.35% 24.77% -23.62% 38.63%
0.35 0.00 0.18 0.67 1.57 1.44 2.44
Lab Lab
17 25
4A*OES/MS 4A*MS
2.00 2.30
2.00 2.20
2.00 2.10
2.00 2.30
2.00 2.40
2.10 2.30
2.02 2.27
2.00 2.30
0.041 0.103
2.02% 4.56%
-5.56% 6.15%
0.65 0.96

12 14 15 16 17 18 19
4A*MS 4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS
12.7 13.6 12.5 < 15 12.1 < 20 11.4

13.1 13.4 13.0 < 15 12.0 < 20 10.9
12.8 12.8 13.0 < 15 11.8 < 20 11.2
11.7 13.4 12.7 < 15 12.7 < 20 11.1
11.9 12.9 12.2 < 15 11.5 < 20 11.0
12.4 13.1 12.4 < 15 12.0 < 20 11.3
12.4 13.2 12.6 12.0 11.1
12.6 13.3 12.6 12.0 11.1
0.543 0.316 0.338 0.397 0.175
4.37% 2.40% 2.68% 3.30% 1.57%
-3.42% 2.54% -1.89% -6.66% -13.46%
0.82 0.00 0.61 NA 1.26 NA 2.19

07 08 09 11 12 13 14
4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*OES 4A*MS
533 504 524 397 225 499 555

461 514 536 402 281 501 566
500 539 541 418 237 486 601
512 483 531 399 230 495 477
454 485 527 379 230 497 546
508 498 526 407 245 493 507
495 504 531 400 241 495 542
504 501 529 401 233 496 551
31 21 7 13 21 5 44
6.24% 4.13% 1.26% 3.21% 8.56% 1.06% 8.10%
7.73% 9.72% 15.58% -12.82% -47.48% 7.81% 18.07%
0.25 0.35 0.62 0.72 2.45 0.26 0.74
Lab Lab Lab Lab Lab

15 17 19 24 25
4A*MS 4A*OES/MS 4A*OES/MS 4A*MS 4A*MS
0.65 0.56 0.72 0.40 0.50

0.67 0.36 0.74 0.30 0.50
0.67 0.43 0.67 0.30 0.40
0.64 0.54 0.66 0.40 0.50
0.67 0.44 0.68 0.40 0.50
0.68 0.26 0.70 0.40 0.50
0.66 0.43 0.69 0.37 0.48
0.67 0.44 0.69 0.40 0.50
0.015 0.112 0.031 0.052 0.041
2.27% 25.98% 4.47% 14.08% 8.45%
0.67 0.39 0.81 0.69 0.15
Lab Lab Lab

17 19 25
4A*OES/MS 4A*OES/MS 4A*MS
0.24 0.22 0.24

0.24 0.21 0.22
0.24 0.22 0.20
0.26 0.21 0.20
0.24 0.21 0.24
0.24 0.22 0.26
0.24 0.21 0.23
0.24 0.21 0.23
0.008 0.004 0.024
3.36% 2.06% 10.69%
5.14% -8.47% -2.06%
0.67 0.60 0.00
Lab Lab Lab Lab Lab

13 14 15 17 25
4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*MS
26 60 62 42 53
25 63 67 43 52
26 57 62 44 46
26 59 58 46 53
26 60 62 43 51
26 61 60 43 50
26 60 62 43 51
26 60 62 43 52
0 2 3 2 3
1.73% 3.26% 4.84% 3.75% 5.03%
-53.91% 7.03% 9.90% -22.89% -9.77%
2.78 0.52 0.67 1.16 0.30

08 09 12 13 14 15 17
4A*OES 4A*OES/MS 4A*MS 4A*MS 4A*MS 4A*MS 4A*OES/MS
< 20 6.14 2.10 6.33 5.90 6.95 5.20

< 20 6.24 2.70 6.60 6.54 6.90 5.00
< 20 6.41 1.70 6.69 6.32 6.99 5.40
< 20 6.33 2.00 6.74 6.36 7.11 6.00
< 20 6.26 2.20 6.92 6.23 7.08 5.30
< 20 6.27 2.30 6.74 6.09 7.13 4.70
6.28 2.17 6.67 6.24 7.03 5.27
6.27 2.15 6.72 6.28 7.04 5.25
0.089 0.333 0.199 0.223 0.094 0.437
1.42% 15.35% 2.98% 3.58% 1.33% 8.29%
6.35% -63.28% 13.02% 5.75% 19.08% -10.75%
NA 0.65 3.85 1.08 0.61 1.47 0.46

07 08 09 11 12 13 14
0.200 0.190 0.209 0.170 0.181 0.194 0.190

0.190 0.190 0.213 0.170 0.170 0.190 0.200
0.200 0.200 0.210 0.160 0.185 0.195 0.201
0.200 0.190 0.214 0.170 0.166 0.195 0.195
0.200 0.200 0.210 0.170 0.162 0.193 0.194
0.200 0.190 0.211 0.170 0.174 0.192 0.193
0.198 0.193 0.211 0.168 0.173 0.193 0.195
0.200 0.190 0.210 0.170 0.172 0.193 0.195
0.004 0.005 0.002 0.004 0.009 0.002 0.004
2.06% 2.67% 0.91% 2.43% 5.09% 1.08% 2.03%
3.80% 1.18% 10.39% -11.90% -9.46% 1.03% 2.28%
0.24 0.01 0.84 1.17 0.95 0.01 0.11

12 13 14 15 17 18 19
4A*MS 4A*MS 4A*MS 4A*MS 4A*OES/MS 4A*OES 4A*OES/MS
4.59 3.26 4.22 4.29 4.16 < 20 4.21
5.20 3.29 4.31 4.34 4.48 < 20 4.07
4.96 3.25 4.08 4.14 4.27 < 20 4.26
4.10 3.30 4.24 4.45 4.26 < 20 4.17
4.22 3.29 4.08 4.49 4.26 < 20 4.13
4.29 3.31 4.19 4.32 4.33 < 20 4.25
4.56 3.28 4.19 4.34 4.29 4.18
4.44 3.29 4.21 4.33 4.27 4.19
0.441 0.023 0.092 0.124 0.107 0.073
9.66% 0.71% 2.19% 2.87% 2.48% 1.75%
9.01% -21.51% 0.08% 3.71% 2.63% -0.08%
0.52 3.98 0.01 0.69 0.32 NA 0.01
Lab
25
4A*MS
0.100
0.080
0.100
0.100
0.100
0.120
0.100
0.100
0.013
12.65%
13.40%
2.89

11 12 13 14 15 17 18
4A*OES 4A*MS 4A*MS 4A*MS 4A*MS 4A*OES/MS 4A*OES
< 10 3.00 2.93 2.66 2.83 2.06 < 20

< 10 3.30 2.92 2.77 2.76 2.20 < 20
< 10 3.20 3.16 2.64 2.82 2.50 < 20
< 10 2.70 2.87 2.65 2.88 2.04 < 20
< 10 2.80 2.84 2.55 2.80 2.12 < 20
< 10 2.80 2.83 2.61 2.84 2.15 < 20
2.97 2.92 2.65 2.82 2.18
2.90 2.89 2.65 2.83 2.14
0.242 0.123 0.072 0.040 0.168
8.16% 4.20% 2.73% 1.42% 7.72%
9.66% 8.07% -2.17% 4.30% -19.48%
NA 1.32 1.18 0.13 0.87 3.16 NA

07 08 09 11 12 13 14
33.0 31.0 34.0 35.0 28.0 32.0 32.0

30.0 32.0 33.0 35.0 31.0 30.9 33.0
32.0 31.0 36.2 33.0 31.0 32.8 31.0
32.0 31.0 34.8 34.0 26.0 30.0 31.0
32.0 31.0 34.3 34.0 28.0 30.8 32.0
31.0 31.0 33.9 34.0 29.0 30.3 33.0
31.7 31.2 34.4 34.2 28.8 31.1 32.0
32.0 31.0 34.1 34.0 28.5 30.9 32.0
1.033 0.408 1.098 0.753 1.941 1.075 0.894
3.26% 1.31% 3.20% 2.20% 6.73% 3.45% 2.80%
-1.00% -2.57% 7.41% 6.81% -9.86% -2.67% 0.04%
0.06 0.12 0.99 0.92 0.92 0.13 0.17

07 08 09 11 12 13 14
< 10 10.0 14.9 13.0 16.0 12.8 15.9

< 10 10.0 14.7 12.0 16.8 12.3 16.7
< 10 20.0 15.4 13.0 16.0 13.6 15.6
< 10 10.0 15.3 13.0 15.3 13.4 15.8
< 10 10.0 15.2 13.0 16.3 13.5 15.2
< 10 10.0 15.1 11.0 17.0 12.9 15.8
11.7 15.1 12.5 16.2 13.1 15.8
10.0 15.2 13.0 16.2 13.1 15.8
4.1 0.3 0.8 0.6 0.5 0.5
34.99% 1.66% 6.69% 3.79% 3.98% 3.11%
-16.72% 7.82% -10.77% 15.88% -6.62% 13.03%
NA 1.49 0.14 1.17 0.30 0.94 0.14

12 13 14 15 16 17 18
4A*MS 4A*MS 4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*OES
6.30 6.33 5.80 6.00 < 10 5.60 5.00

7.00 6.42 5.80 5.00 < 10 6.10 5.00
6.60 6.45 5.70 6.00 < 10 5.90 5.00
5.60 6.27 5.70 6.00 < 10 6.10 5.00
5.80 6.21 5.70 6.00 < 10 5.70 5.00
5.80 6.13 5.70 6.00 < 10 5.80 5.00
6.18 6.30 5.73 5.83 5.87 5.00
6.05 6.30 5.70 6.00 5.85 5.00
0.546 0.124 0.052 0.408 0.207 0.000
8.82% 1.96% 0.90% 7.00% 3.52% 0.00%
9.63% 11.76% 1.65% 3.43% 4.02% -11.35%
2.17 2.67 0.28 0.70 NA 0.84 2.80
Lab Lab Lab

17 19 25
4A*OES/MS 4A*OES/MS 4A*MS
0.60 0.61 0.80

0.60 0.56 0.70
0.60 0.62 0.70
0.70 0.57 0.70
0.60 0.60 0.80
0.60 0.60 0.75
0.62 0.59 0.74
0.60 0.60 0.73
0.041 0.023 0.049
6.62% 3.94% 6.63%
1.19% -2.64% 21.70%
0.00 0.67 3.61

07 08 09 10 11 12 13
0.963 0.928 0.979 0.883 0.922 0.998 0.915

0.902 0.923 0.998 0.871 0.925 0.966 0.920
0.940 0.917 0.993 0.854 0.927 0.990 0.925
0.928 0.924 0.996 0.851 0.918 0.907 0.922
0.964 0.916 0.988 0.860 0.917 0.945 0.914
0.931 0.897 0.992 0.871 0.922 0.972 0.911
0.938 0.918 0.991 0.865 0.922 0.963 0.918
0.936 0.920 0.993 0.866 0.922 0.969 0.917
0.023 0.011 0.007 0.012 0.004 0.033 0.005
2.50% 1.20% 0.67% 1.40% 0.42% 3.47% 0.57%
1.99% -0.24% 7.77% -5.94% 0.24% 4.72% -0.20%
0.84 0.09 3.27 2.49 0.11 1.99 0.08

12 13 14 15 16 17 18
4A*MS 4A*OES 4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*OES
72 76 83 92 70 75 82
80 77 86 87 74 77 84
75 76 84 87 77 77 76
63 75 86 87 76 76 80
67 75 82 87 74 75 82
86 74 84 87 73 76 80
74 75 84 88 74 76 81
73 75 84 87 74 76 81
8.6 1.0 1.5 2.0 2.4 0.8 2.7
11.66% 1.27% 1.75% 2.32% 3.31% 1.08% 3.39%
-5.68% -3.22% 7.70% 12.59% -5.14% -2.92% 3.40%
0.44 0.15 1.15 1.60 0.37 0.11 0.64
13 14 15 16 17 18 19
4A*MS 4A*MS 4A*OES 4A*AAS 4A*OES/MS 4A*AAS 4A*AAS
281 297 292 298 - 307 290

307 301 294 297 - 308 301
298 268 289 281 - 312 306
287 321 295 296 - 308 303
293 296 295 284 - 311 310
299 309 288 293 - 311 304
294 298 292 292 310 302
295 299 293 295 310 304
9 18 3 7 2 7
3.10% 5.93% 0.95% 2.48% 0.67% 2.24%
-1.08% 0.28% -1.84% -2.02% 4.03% 1.62%
0.00 1.09 0.24 0.30 NA 1.63 1.13

14 15 16 17 18 19 23
4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES
4.03 4.19 3.65 3.88 3.87 4.04 3.66

4.15 4.19 3.67 3.88 3.84 3.98 3.33
4.05 4.15 3.72 3.94 3.86 3.99 3.06
3.99 4.17 3.54 3.87 3.87 3.96 3.88
4.02 4.20 3.57 3.97 3.84 4.01 3.74
4.05 4.13 3.71 3.85 3.83 3.99 3.77
4.05 4.17 3.64 3.90 3.85 3.99 3.57
4.04 4.18 3.66 3.88 3.85 3.99 3.70
0.054 0.027 0.074 0.046 0.017 0.029 0.313
1.34% 0.65% 2.02% 1.19% 0.45% 0.73% 8.77%
1.68% 4.79% -8.48% -2.08% -3.25% 0.32% -10.24%
0.55 1.26 1.79 0.32 0.59 0.24 1.10

15 16 17 18 19 21 23
4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*OES
1772 1608 1809 1682 1765 1686 1224

1570 1677 1944 1709 1768 1714 1261
1664 1691 1953 1687 1779 1625 1540
1715 1621 1962 1714 1773 1636 1249
1763 1628 1908 1660 1780 1404 1304
1791 1659 2061 1688 1756 1609 1185
1712 1647 1940 1690 1770 1612 1294
1739 1644 1949 1688 1771 1631 1255
84 33 82 20 9 109 127
4.88% 2.02% 4.22% 1.16% 0.52% 6.79% 9.81%
-4.90% -8.52% 7.71% -6.15% -1.70% -10.46% -28.15%
0.42 0.83 1.02 0.56 0.05 0.79 3.40
Lab Lab Lab Lab Lab

17 18 21 23 25
4A*OES/MS 4A*OES 4A*OES 4A*OES PF*MS
1018 643 1452 237 10900

1001 487 1498 118 11200
991 525 820 33 11100
1009 625 768 774 11300
1027 746 1034 376 11000
1018 619 664 369 11400
1011 608 1039 318 11150
1014 622 927 303 11150
13 92 359 261 187
1.30% 15.12% 34.51% 82.25% 1.68%
-59.64% -75.74% -58.49% -87.31% 345.29%
0.34 0.62 0.32 0.83 6.77

15 16 17 18 19 21 23
0.86 0.70 1.20 <3 0.75 2.00 <1

0.80 0.70 1.30 <3 0.71 2.00 <1
0.87 0.70 1.30 <3 0.53 <2 <1
0.82 0.70 1.30 <3 0.64 <2 <1
0.82 0.60 1.20 <3 0.64 <2 <1
0.82 0.70 1.30 <3 0.61 <2 <1
0.83 0.68 1.27 0.65 2.00
0.82 0.70 1.30 0.64 2.00
0.027 0.041 0.052 0.077 0.000
3.26% 5.97% 4.08% 11.92% 0.00%
17.11% -3.77% 78.37% -8.84% 181.64%
1.17 0.33 5.55 NA 0.69 12.93 NA

14 15 16 17 18 19 21
4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES
153 152 126 138 156 143 131

154 152 133 138 161 143 123
143 152 134 143 160 145 128
154 154 129 190 165 144 122
148 154 127 143 158 141 108
157 149 127 150 164 145 124
152 152 129 150 161 143 123
154 152 128 143 161 144 124
5 2 3 20 3 1 8
3.34% 1.14% 2.62% 13.25% 2.14% 1.02% 6.47%
1.67% 2.04% -13.30% 0.78% 7.70% -3.81% -17.77%
0.00 0.04 1.67 0.69 0.67 0.61 1.95

14 15 16 17 18 19 23
0.323 0.330 0.290 0.310 0.310 0.322 0.290

0.333 0.330 0.290 0.310 0.300 0.313 0.270
0.327 0.330 0.300 0.310 0.300 0.307 0.230
0.322 0.330 0.290 0.310 0.300 0.310 0.310
0.322 0.330 0.290 0.320 0.300 0.312 0.290
0.321 0.330 0.290 0.310 0.300 0.307 0.300
0.325 0.330 0.292 0.312 0.302 0.312 0.282
0.323 0.330 0.290 0.310 0.300 0.311 0.290
0.005 0.000 0.004 0.004 0.004 0.006 0.029
1.39% 0.00% 1.40% 1.31% 1.35% 1.78% 10.15%
2.15% 3.78% -8.27% -1.98% -5.13% -1.93% -11.42%
0.19 0.61 2.49 0.88 1.69 0.86 2.47
14 15 16 17 18 19 21
4A*MS 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES
54 54 51 57 73 52 48
56 55 54 56 75 49 53
54 55 54 56 74 50 45
56 55 51 112 75 50 46
54 55 52 57 73 50 39
55 53 53 60 75 50 45
55 55 53 66 74 50 46
55 55 53 57 75 50 46
0.8 0.8 1.4 22.5 1.0 0.8 4.6
1.46% 1.54% 2.63% 33.94% 1.33% 1.64% 9.91%
2.44% 1.58% -2.15% 23.42% 38.24% -6.33% -14.26%
0.00 0.13 0.70 0.59 5.43 1.41 2.14

14 15 16 17 18 19 21
4A*MS 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES
15.8 16.0 13.0 14.5 12.0 14.7 16.0

16.3 16.0 14.0 14.9 12.0 15.2 16.0
15.5 16.2 14.0 14.8 12.0 14.5 15.0
15.5 16.0 13.0 66.1 12.0 14.2 17.0
15.4 15.9 13.0 15.6 12.0 15.1 14.0
15.7 15.8 13.0 16.1 12.0 14.7 15.0
15.7 16.0 13.3 23.7 12.0 14.7 15.5
15.6 16.0 13.0 15.3 12.0 14.7 15.5
0.329 0.147 0.516 20.796 0.000 0.380 1.049
2.09% 0.92% 3.87% 87.87% 0.00% 2.58% 6.77%
2.65% 4.56% -12.82% 54.74% -21.54% -3.73% 1.34%
0.47 0.96 2.19 0.00 3.77 0.54 0.38

14 15 16 17 18 19 21
32.0 34.0 25.0 19.0 11.0 21.4 36.0

46.0 33.0 31.0 14.0 15.0 22.9 37.0
33.0 37.0 33.0 16.0 16.0 20.9 36.0
32.0 32.0 36.0 18.0 14.0 20.1 37.0
37.0 37.0 39.0 16.0 14.0 22.0 33.0
42.0 34.0 32.0 14.0 12.0 18.9 36.0
37.0 34.5 32.7 16.2 13.7 21.0 35.8
35.0 34.0 32.5 16.0 14.0 21.1 36.0
5.9 2.1 4.8 2.0 1.9 1.4 1.5
15.85% 6.01% 14.57% 12.63% 13.62% 6.70% 4.11%
22.36% 14.09% 8.03% -46.54% -54.80% -30.46% 18.50%
1.16 0.70 0.37 2.65 3.11 1.76 1.05

13 14 15 16 17 18 19
4A*OES 4A*OES 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS
1.01 0.99 1.01 0.87 0.93 0.98 0.96

1.00 0.99 0.98 0.89 0.92 0.99 0.94
1.02 0.97 0.98 0.90 0.94 0.98 0.94
1.02 0.98 1.02 0.85 0.91 0.98 0.94
1.00 0.97 1.00 0.86 0.94 0.98 0.95
1.00 0.99 1.00 0.89 0.90 0.98 0.96
1.01 0.98 1.00 0.88 0.92 0.98 0.95
1.01 0.98 1.00 0.88 0.93 0.98 0.95
0.009 0.011 0.015 0.020 0.014 0.004 0.007
0.92% 1.14% 1.53% 2.25% 1.52% 0.46% 0.75%
0.64% -2.16% -0.58% -12.59% -7.85% -2.33% -5.21%
0.16 0.67 0.20 3.78 2.37 0.72 1.58
14 15 16 17 18 19 21
2.87 3.00 2.49 2.84 3.11 2.99 2.76

2.97 2.98 2.53 2.83 3.12 2.98 2.73
2.89 2.98 2.58 2.87 3.08 2.99 2.68
2.85 2.96 2.43 2.80 3.09 2.98 2.70
2.86 2.99 2.44 2.90 3.06 2.84 2.30
2.90 2.94 2.56 2.78 3.09 2.79 2.65
2.89 2.98 2.51 2.84 3.09 2.93 2.64
2.88 2.98 2.51 2.84 3.09 2.98 2.69
0.043 0.022 0.062 0.044 0.021 0.091 0.169
1.50% 0.73% 2.48% 1.56% 0.69% 3.10% 6.42%
-1.12% 1.79% -14.29% -2.94% 5.78% 0.18% -9.79%
0.00 0.92 3.36 0.34 1.98 0.75 1.55
Lab Lab Lab Lab Lab

15 17 19 24 25
4A*OES 4A*OES/MS 4A*OES/MS 4A*MS 4A*MS
23.0 21.2 21.9 22.2 23.4

23.0 22.7 21.0 22.2 22.6
23.0 21.5 21.6 22.4 21.6
22.0 22.3 20.9 22.4 22.8
23.0 21.3 21.0 22.4 23.4
21.0 21.9 21.5 22.6 23.6
22.5 21.8 21.3 22.4 22.9
23.0 21.7 21.3 22.4 23.1
0.837 0.595 0.380 0.151 0.746
3.72% 2.73% 1.78% 0.67% 3.26%
1.30% -1.78% -3.97% 0.70% 3.10%
0.16 0.11 0.31 0.11 0.33
Lab
25
4A*MS
10.3
10.3
9.6
10.1
10.2
10.2
10.1
10.2
0.256
2.53%
-9.65%
1.24

15 16 17 18 19 21 23
4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*OES
0.620 0.610 0.630 0.580 0.620 1.280 0.610

0.630 0.610 0.630 0.580 0.606 1.340 0.590
0.620 0.620 0.640 0.580 0.611 1.370 0.560
0.630 0.600 0.630 0.570 0.603 1.340 0.620
0.630 0.610 0.650 0.560 0.613 1.600 0.600
0.630 0.630 0.620 0.570 0.615 1.400 0.610
0.627 0.613 0.633 0.573 0.611 1.388 0.598
0.630 0.610 0.630 0.575 0.612 1.355 0.605
0.005 0.010 0.010 0.008 0.006 0.111 0.021
0.82% 1.68% 1.63% 1.42% 1.01% 8.00% 3.57%
0.61% -1.53% 1.68% -7.95% -1.85% 122.90% -3.94%
0.09 0.57 0.42 2.57 0.67 36.02 1.32

16 17 18 19 23 25
4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS
9.1 12.3 < 20 10.7 7.0 13.1

9.2 12.6 < 20 10.9 5.0 13.9
8.3 13.2 < 20 10.8 6.0 13.1
7.3 16.1 < 20 10.2 7.0 13.8
8.8 12.7 < 20 9.4 6.0 15.2
7.8 12.1 < 20 9.8 6.0 15.1
8.4 13.2 10.3 6.2 14.0
8.6 12.7 10.4 6.0 13.9
0.8 1.5 0.6 0.8 0.9
9.00% 11.28% 5.89% 12.21% 6.62%
-29.36% 10.50% -13.60% -48.25% 17.77%
0.80 0.42 NA 0.25 1.47 0.85
Lab Lab Lab

19 24 25
4A*OES/MS 4A*OES 4A*MS
16.9 20.0 18.5

16.6 20.0 18.5
16.6 20.0 17.5
16.5 20.0 18.5
16.6 20.0 19.5
16.7 20.0 18.5
16.7 20.0 18.5
16.6 20.0 18.5
0.139 0.000 0.632
0.84% 0.00% 3.42%
-12.09% 5.58% -2.34%
1.49 0.76 0.25

14 15 16 17 18 19 23
815 900 800 900 900 830 800
846 900 800 900 800 800 800
827 900 800 900 900 820 700
811 900 800 900 800 810 800
822 900 800 900 900 790 800
824 900 800 900 800 810 800
824 900 800 900 850 810 783
823 900 800 900 850 810 800
12 0 0 0 55 14 41
1.48% 0.00% 0.00% 0.00% 6.44% 1.75% 5.21%
-0.52% 8.63% -3.44% 8.63% 2.60% -2.23% -5.45%
0.14 2.18 0.51 2.18 0.83 0.24 0.96

14 15 16 17 18 19 21
142 143 124 134 200 141 171

150 141 123 130 200 141 170
148 142 126 129 100 142 167
143 142 121 132 100 140 168
146 143 122 131 100 135 145
146 144 123 129 100 139 167
146 143 123 131 133 140 165
146 143 123 131 100 140 168
3 1 2 2 52 2 10
2.05% 0.74% 1.40% 1.48% 38.73% 1.76% 5.93%
9.90% 7.39% -7.18% -1.41% 0.48% 5.13% 24.09%
1.30 0.90 1.41 0.50 4.18 0.65 4.02

15 16 17 18 19 23 24
4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS
6.17 10.00 7.09 6.00 6.23 6.00 6.50

5.95 11.00 6.96 6.00 5.99 6.00 6.50
6.10 12.00 7.43 6.00 6.13 6.00 6.00
6.21 12.00 62.80 6.00 6.12 6.00 6.00
5.85 6.00 10.90 6.00 6.10 6.00 6.50
6.05 9.00 7.97 6.00 6.15 6.00 6.00
6.06 10.00 17.19 6.00 6.12 6.00 6.25
6.08 10.50 7.70 6.00 6.13 6.00 6.25
0.136 2.280 22.391 0.000 0.079 0.000 0.274
2.24% 22.80% 130.24% 0.00% 1.29% 0.00% 4.38%
0.03% 65.21% 184.02% -0.88% 1.10% -0.88% 3.25%
0.15 9.13 4.59 0.28 0.00 0.28 0.31

15 16 17 18 19 23 24
0.430 0.420 0.430 0.420 0.418 0.390 0.450

0.440 0.410 0.430 0.420 0.409 0.380 0.460
0.430 0.420 0.430 0.420 0.415 0.370 0.440
0.430 0.410 0.430 0.420 0.410 0.420 0.450
0.430 0.410 0.440 0.420 0.409 0.390 0.450
0.440 0.430 0.420 0.410 0.416 0.390 0.440
0.433 0.417 0.430 0.418 0.413 0.390 0.448
0.430 0.415 0.430 0.420 0.413 0.390 0.450
0.005 0.008 0.006 0.004 0.004 0.017 0.008
1.19% 1.96% 1.47% 0.98% 0.96% 4.29% 1.68%
1.16% -2.73% 0.39% -2.34% -3.62% -8.95% 4.67%
0.33 0.79 0.11 0.67 1.04 2.58 1.34
14 15 16 17 18 19 21
4A*OES 4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES
112 108 106 106 97 107 98

116 110 113 111 101 107 104
111 110 112 111 99 107 97
109 109 104 161 99 110 98
115 108 99 120 98 102 85
116 109 99 125 100 109 95
113 109 106 122 99 107 96
114 109 105 116 99 107 98
3 1 6 20 1 3 6
2.59% 0.65% 5.77% 16.48% 1.43% 2.51% 6.49%
1.18% -2.74% -5.67% 9.38% -11.48% -4.15% -14.02%
0.32 0.57 1.23 0.60 2.54 0.89 2.66

17 18 19 21 23 24 25
4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*OES 4A*OES 4A*OES
492 600 607 572 230 550 550

505 600 571 553 250 550 500
489 500 673 540 480 550 550
505 500 541 530 240 550 500
511 600 484 421 230 550 500
499 600 499 525 230 550 500
500 567 562 524 277 550 517
502 600 556 535 235 550 500
8 52 71 53 100 0 26
1.69% 9.11% 12.56% 10.12% 36.12% 0.00% 5.00%
-6.36% 6.09% 5.29% -1.99% -48.20% 2.97% -3.27%
1.36 1.86 0.58 0.76 14.18 1.06 0.56

14 15 16 17 18 19 21
1808 2022 1759 1902 1719 1683 1624
1863 2021 1856 1854 1764 1811 1635
1819 1991 1851 1899 1739 1738 1549
1815 2003 1771 1935 1760 1762 1564
1783 2028 1781 1860 1723 1739 1347
1820 1957 1792 1977 1744 1725 1532
1818 2004 1802 1905 1742 1743 1542
1817 2012 1787 1901 1742 1738 1557
26 27 42 46 18 42 104
1.43% 1.33% 2.31% 2.44% 1.06% 2.43% 6.74%
-4.72% 5.01% -5.58% -0.19% -8.73% -8.66% -19.19%
0.81 0.56 0.93 0.17 1.37 1.36 2.55
14 15 16 17 19 23 24
4A*OES 4A*OES PF*OES 4A*OES/MS 4A*OES/MS 4A*OES 4A*OES
3.61 3.60 N.A. - 3.82 3.60 3.98

3.67 3.58 N.A. - 3.70 3.50 3.95
3.56 3.53 N.A. - 3.83 3.30 4.02
3.51 3.57 N.A. - 3.72 3.60 4.12
3.65 3.61 N.A. - 3.63 3.60 4.04
3.62 3.48 N.A. - 3.74 3.60 4.07
3.60 3.56 3.74 3.53 4.03
3.62 3.58 3.73 3.60 4.03
0.060 0.050 0.074 0.121 0.061
1.66% 1.39% 1.99% 3.43% 1.52%
-2.83% -3.89% 0.88% -4.70% 8.70%
0.73 0.99 NA NA 0.15 0.88 2.01

14 15 16 17 18 19 21
197 204 177 216 187 224 168

210 209 190 223 206 215 170
205 208 193 214 115 218 167
208 211 187 230 121 219 166
204 212 188 211 133 216 139
205 210 187 212 158 221 161
205 209 187 218 153 219 162
205 210 188 215 146 218 167
5 3 5 7 37 3 12
2.31% 1.35% 2.89% 3.40% 24.15% 1.51% 7.16%
-0.06% 1.99% -8.74% 6.22% -25.17% 6.77% -21.02%
0.02 0.22 0.75 0.65 2.49 0.70 1.85

15 16 17 18 19 23 24
4.00 3.20 4.80 <5 4.03 6.00 5.00

4.00 3.40 5.30 <5 3.87 5.00 5.00
4.00 3.40 5.10 <5 4.18 3.00 5.00
4.00 3.30 5.40 <5 3.91 6.00 5.00
4.00 3.20 4.80 <5 3.74 6.00 5.00
4.00 3.30 5.30 <5 3.90 6.00 5.00
4.00 3.30 5.12 3.94 5.33 5.00
4.00 3.30 5.20 3.90 6.00 5.00
0.000 0.089 0.264 0.149 1.211 0.000
0.00% 2.71% 5.16% 3.79% 22.71% 0.00%
-1.02% -18.34% 26.61% -2.57% 31.98% 23.73%
0.00 4.12 6.57 NA 0.37 0.00 5.88
Lab Lab
24 25
4A*MS 4A*MS
70 55
70 55
70 50
70 55
70 55
70 55
70 54
70 55
0 2
0.00% 3.77%
16.45% -9.89%
1.05 0.59
Lab Lab Lab Lab
21 23 24 25
4A*OES 4A*OES 4A*MS 4A*MS
29.0 14.0 13.1 13.0

30.0 13.0 12.9 14.0
27.0 13.0 12.9 13.0
25.0 14.0 13.4 14.0
22.0 15.0 13.6 14.0
26.0 14.0 13.5 14.0
26.5 13.8 13.2 13.7
26.5 14.0 13.3 14.0
2.881 0.753 0.308 0.516
10.87% 5.44% 2.33% 3.78%
105.85% 7.46% 2.80% 6.16%
14.16 0.67 0.04 0.50

15 16 17 18 19 21 23
516 239 380 414 416 387 326

517 247 385 427 370 376 282
512 229 377 436 442 356 283
517 209 382 424 394 356 349
510 231 381 405 379 304 314
526 224 371 396 391 342 325
516 230 379 417 399 354 313
516 230 381 419 392 356 320
5 13 5 15 26 29 26
1.06% 5.67% 1.28% 3.56% 6.59% 8.22% 8.41%
12.40% -49.95% -17.39% -9.19% -13.20% -23.02% -31.80%
0.47 2.49 0.94 0.55 0.74 1.21 1.63
Lab Lab Lab Lab Lab
18 19 23 24 25
4A*OES 4A*OES/MS 4A*OES 4A*MS 4A*MS
< 20 5.25 3.00 6.70 5.60

< 20 5.44 3.00 5.60 5.60
< 20 5.07 3.00 5.10 5.20
< 20 4.65 3.00 6.80 5.30
< 20 4.75 4.00 7.90 6.20
< 20 5.48 4.00 5.70 6.20
5.11 3.33 6.30 5.68
5.16 3.00 6.20 5.60
0.349 0.516 1.026 0.431
6.83% 15.49% 16.28% 7.58%
-13.46% -43.51% 6.76% -3.69%
NA 0.63 2.57 0.67 0.00

15 16 17 18 19 21 23
0.190 0.120 0.160 0.200 0.169 0.121 0.190

0.180 0.130 0.160 0.200 0.166 0.118 0.190
0.180 0.130 0.160 0.200 0.171 0.115 0.180
0.180 0.120 0.170 0.210 0.166 0.114 0.190
0.180 0.120 0.160 0.200 0.166 0.097 0.190
0.180 0.120 0.160 0.200 0.168 0.111 0.190
0.182 0.123 0.162 0.202 0.168 0.113 0.188
0.180 0.120 0.160 0.200 0.167 0.114 0.190
0.004 0.005 0.004 0.004 0.002 0.008 0.004
2.25% 4.19% 2.53% 2.02% 1.23% 7.40% 2.17%
-4.92% -35.45% -15.39% 5.54% -12.25% -41.06% -1.44%
0.54 3.29 1.48 0.40 1.20 3.65 0.23
Lab Lab Lab

21 24 25
4A*OES 4A*MS 4A*MS
<2 3.80 4.20
<2 3.90 4.00
<2 4.00 3.70
<2 4.00 4.00
<2 4.20 4.10
<2 4.00 4.20
3.98 4.03
4.00 4.05
0.133 0.186
3.34% 4.62%
-4.78% -3.58%
NA 0.88 0.66
Lab Lab Lab Lab

19 23 24 25
4A*OES/MS 4A*OES 4A*MS 4A*MS
2.52 < 20 2.70 2.60

2.48 < 20 2.70 2.50
2.58 < 20 2.70 2.50
2.64 < 20 2.70 2.50
2.59 < 20 2.70 2.60
2.60 < 20 2.80 2.50
2.57 2.72 2.53
2.59 2.70 2.50
0.058 0.041 0.052
2.26% 1.50% 2.04%
-5.06% 0.42% -6.36%
0.57 NA 0.27 0.77

15 16 17 18 19 21 23
30.0 28.0 35.0 33.0 30.3 31.0 31.0

31.7 30.0 35.0 33.0 30.7 30.0 30.0
30.6 30.0 35.0 32.0 30.5 29.0 31.0
30.9 28.0 35.0 36.0 30.1 29.0 31.0
30.5 27.0 35.0 32.0 29.9 25.0 30.0
30.4 27.0 35.0 35.0 30.2 29.0 31.0
30.7 28.3 35.0 33.5 30.3 28.8 30.7
30.5 28.0 35.0 33.0 30.2 29.0 31.0
0.558 1.366 0.000 1.643 0.283 2.041 0.516
1.82% 4.82% 0.00% 4.90% 0.94% 7.08% 1.68%
-4.13% -11.42% 9.42% 4.73% -5.33% -9.86% -4.13%
0.29 1.10 1.21 0.69 0.42 0.66 0.29

15 16 17 18 19 23 24
4A*MS 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES 4A*MS
14.7 23.0 22.2 < 20 16.4 9.0 16.5

14.3 24.0 21.8 < 20 17.0 11.0 14.5
14.4 25.0 22.5 < 20 16.0 8.0 15.0
14.2 36.0 24.3 < 20 16.4 8.0 16.0
14.5 26.0 23.4 < 20 15.6 9.0 17.0
14.5 26.0 20.1 < 20 16.3 10.0 16.0
14.4 26.7 22.4 16.3 9.2 15.8
14.5 25.5 22.4 16.3 9.0 16.0
0.2 4.7 1.4 0.5 1.2 0.9
1.16% 17.70% 6.41% 2.86% 12.75% 5.88%
2.99% 90.36% 59.79% 16.13% -34.56% 13.03%
0.41 3.67 2.72 NA 0.31 2.48 0.14
Lab Lab Lab Lab

19 23 24 25
5.57 5.00 5.80 5.60

5.43 5.00 5.60 5.60
5.50 4.00 5.50 5.30
5.51 5.00 5.50 5.50
5.42 5.00 5.80 5.60
5.64 5.00 5.80 5.60
5.51 4.83 5.67 5.53
5.51 5.00 5.70 5.60
0.084 0.408 0.151 0.121
1.52% 8.45% 2.66% 2.19%
-2.28% -14.30% 0.47% -1.89%
0.65 2.80 0.00 0.36

14 15 16 17 18 19 21
4A*OES 4A*OES 4A*OES 4A*OES/MS 4A*OES 4A*OES/MS 4A*OES/AAS
0.928 0.929 0.858 0.863 0.926 0.914 0.866

0.944 0.913 0.889 0.868 0.928 0.906 0.840
0.912 0.926 0.896 0.870 0.914 0.897 0.834
0.899 0.899 0.856 0.869 0.918 0.909 0.851
0.931 0.922 0.860 0.867 0.908 0.915 0.838
0.923 0.890 0.874 0.865 0.915 0.925 0.843
0.923 0.913 0.872 0.867 0.918 0.911 0.845
0.926 0.918 0.867 0.867 0.917 0.911 0.841
0.016 0.015 0.017 0.003 0.008 0.009 0.011
1.70% 1.69% 1.95% 0.31% 0.83% 1.02% 1.35%
0.36% -0.69% -5.20% -5.72% -0.16% -0.97% -8.09%
0.16 0.28 2.17 2.39 0.06 0.40 3.39
Lab Lab Lab Lab

19 23 24 25
82 72 76 71
80 69 78 70
81 68 77 66
80 76 78 70
81 73 79 72
81 74 76 72
81 72 77 70
81 73 78 71
0.8 3.0 1.2 2.2
0.99% 4.21% 1.57% 3.18%
3.72% -7.71% -0.87% -10.06%
0.67 0.68 0.13 0.96
20 21 22 23 24 25
AD*AAS 4A*OES 4A*MS 4A*OES 4A*OES 4A*MS
298 303 294 288 259

298 303 294 296 259
298 293 296 296 241
298 297 293 292 252
299 251 290 291 292 259
297 290 286 294 286 254
298 289 288 294 292 254
298 295 288 294 292 257
1 19 3 2 4 7
0.23% 6.74% 0.98% 0.56% 1.40% 2.77%
0.11% -2.71% -3.19% -1.29% -1.96% -14.62%
0.38 0.31 0.67 0.07 0.28 4.04
Lab Lab
24 25
4A*OES 4A*OES
4.06 4.08
4.05 4.04
3.89 4.10
3.96 4.10
4.04 4.12
4.00 4.12
4.00 4.09
4.02 4.10
0.065 0.030
1.64% 0.74%
0.47% 2.82%
0.27 0.81
Lab Lab
24 25
4A*MS 4A*MS
1660 1650
1660 1640
1690 1530
1690 1610
1680 1700
1660 1690
1673 1637
1670 1645
15 62
0.90% 3.78%
-7.07% -9.11%
0.67 0.90
Lab Lab
24 25
4A*MS 4A*MS
1.00 0.70
1.00 0.70
1.00 0.60
1.00 0.60
1.00 0.70
1.00 0.60
1.00 0.65
1.00 0.65
0.000 0.055
0.00% 8.43%
40.82% -8.47%
2.86 0.66
Lab Lab Lab

23 24 25
4A*OES 4A*MS 4A*MS
135 134 162

133 136 160
131 135 146
141 139 154
134 141 166
136 137 162
135 137 158
135 137 161
3 3 7
2.52% 1.90% 4.55%
-9.50% -8.16% 6.14%
1.25 1.10 0.50
Lab Lab
24 25
4A*OES 4A*OES
0.330 0.330
0.330 0.330
0.320 0.340
0.320 0.330
0.320 0.330
0.310 0.330
0.322 0.332
0.320 0.330
0.008 0.004
2.34% 1.23%
1.16% 4.31%
0.07 0.74
Lab Lab Lab
23 24 25
4A*OES 4A*MS 4A*MS
56 48 55
55 48 55
52 49 53
57 47 54
56 47 54
56 48 54
55 48 54
56 48 54
1.8 0.5 0.8
3.27% 1.15% 1.41%
3.04% -11.47% 0.18%
0.29 2.11 0.34
Lab Lab Lab

23 24 25
4A*OES 4A*MS 4A*OES
14.0 15.0 20.0

14.0 14.0 15.0
15.0 14.0 15.0
15.0 14.0 15.0
15.0 14.0 15.0
15.0 15.0 20.0
14.7 14.3 16.7
15.0 14.0 15.0
0.516 0.516 2.582
3.52% 3.60% 15.49%
-4.11% -6.28% 8.97%
0.61 1.00 0.21
Lab Lab Lab

23 24 25
4A*OES 4A*OES PF*OES
18.0 30.0 < 50

24.0 30.0 < 50
29.0 30.0 < 50
19.0 30.0 < 50
17.0 30.0 < 50
20.0 30.0 < 50
21.2 30.0
19.5 30.0
4.5 0.0
21.43% 0.00%
-30.00% -0.79%
1.74 0.12 NA
Lab Lab Lab Lab

21 23 24 25
0.98 1.00 1.00 1.03

0.96 1.00 1.02 1.03
0.96 1.01 1.02 1.04
0.97 0.99 1.02 1.02
0.82 0.98 1.03 1.02
0.94 1.00 1.01 1.02
0.94 0.99 1.02 1.03
0.96 1.00 1.02 1.03
0.061 0.011 0.010 0.008
6.47% 1.12% 1.02% 0.80%
-6.42% -0.86% 1.37% 2.36%
1.22 0.28 0.38 0.68
Lab Lab Lab
23 24 25
4A*OES 4A*OES PF*OES
2.87 3.20 3.07

2.76 3.20 3.04
2.64 3.09 3.09
2.86 3.16 3.09
2.87 3.16 3.04
2.87 3.10 3.05
2.81 3.15 3.06
2.87 3.16 3.06
0.095 0.048 0.023
3.36% 1.51% 0.76%
-3.80% 7.84% 4.81%
0.26 2.53 1.73
Lab Lab
24 25
4A*OES PF*OES
0.650 0.600
0.650 0.700
0.620 0.700
0.630 0.700
0.640 0.600
0.630 0.700
0.637 0.667
0.635 0.700
0.012 0.052
1.90% 7.75%
2.22% 7.03%
0.59 1.24
Lab Lab
24 25
4A*OES PF*OES
900 1200
900 1100
800 1100
800 1200
900 1200
800 1200
850 1167
850 1200
55 52
6.44% 4.43%
2.60% 40.82%
0.83 9.38
Lab Lab Lab

23 24 25
4A*OES 4A*OES 4A*OES
133 122 114

130 136 116
123 128 114
138 128 116
134 130 124
136 132 126
132 129 118
134 129 116
5 5 5
4.02% 3.62% 4.46%
-0.28% -2.54% -10.83%
0.32 0.67 1.99
Lab
25
4A*MS
6.50
6.50
6.00
6.50
6.50
6.50
6.42
6.50
0.204
3.18%
6.01%
0.70
Lab
25
4A*OES
0.460
0.460
0.460
0.460
0.460
0.460
0.460
0.460
0.000
0.00%
7.39%
2.13
Lab Lab Lab
23 24 25
112 120 120

110 120 115
106 115 120
113 120 115
111 120 120
110 115 120
110 118 118
111 120 120
2 3 3
2.20% 2.18% 2.18%
-1.35% 5.80% 5.80%
0.26 1.36 1.36
Lab Lab Lab

23 24 25
4A*OES 4A*MS 4A*MS
1996 1810 2120
1970 1790 2080
1905 1790 1970
2019 1880 2050
2007 1860 2140
2005 1850 2080
1984 1830 2073
2001 1830 2080
42 38 60
2.11% 2.10% 2.89%
3.96% -4.09% 8.66%
0.52 0.72 1.07
Lab
25
PF*OES
3.80
3.76
3.84
3.76
3.80
3.78
3.79
3.79
0.030
0.80%
2.23%
0.47
Lab Lab
23 25
4A*OES 4A*MS
204 170
204 160
196 158
208 163
201 160
203 171
203 164
204 162
4 6
1.97% 3.38%
-1.10% -20.13%
0.08 1.98
Lab
25
4A*OES
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
0.000
0.00%
-1.02%
0.00
Lab Lab
24 25
4A*MS PF*MS
566 530
581 530
610 530
532 530
594 530
585 530
578 530
583 530
27 0
4.64% 0.00%
25.88% 15.42%
1.11 0.62
Lab Lab
24 25
4A*OES PF*OES
0.230 0.210
0.230 0.210
0.215 0.210
0.225 0.210
0.225 0.210
0.225 0.210
0.225 0.210
0.225 0.210
0.005 0.000
2.43% 0.00%
17.75% 9.90%
1.50 0.79
Lab Lab
24 25
4A*OES 4A*OES
35.0 35.0
35.0 35.0
35.0 35.0
35.0 30.0
35.0 35.0
35.0 35.0
35.0 34.2
35.0 35.0
0.000 2.041
0.00% 5.97%
9.42% 6.81%
1.21 0.92
Lab
25
4A*MS
15.5
15.0
14.0
14.5
15.5
15.5
15.0
15.3
0.6
4.22%
7.08%
0.18
Lab Lab Lab
23 24 25
0.930 0.936 0.934

0.919 0.951 0.914
0.884 0.936 0.923
0.947 0.920 0.915
0.941 0.941 0.917
0.934 0.927 0.914
0.926 0.935 0.920
0.932 0.936 0.916
0.023 0.011 0.008
2.45% 1.15% 0.86%
0.68% 1.69% -0.02%
0.67 0.71 0.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
298
10
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
3.98
11.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1801
12
Indicative
1.00
ppm
1.00
1.00
1.0
3.0
16.0
< 20
9.0
Indicative
1.00
ppm
0.00
0.00
1
4
16
2504
10
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.71
13.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
149
14
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.318
15.000
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
54
16
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
25.7
17.0
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
15.3
18.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
30.2
19.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.66
20.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
1.00
21.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.21
22.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.59
23.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
<1
24.00
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
2.92
25.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
22.2
26.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
1.77
27.00
Indicative
1.00
ppm
2.00
2.00
1.00
7.00
16.00
5.05
9.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.53
28.00
Indicative
1.00
ppm
2.00
2.00
1.00
4.00
16.00
<1
10.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.21
29.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
11.2
30.0
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.623
31.000
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
11.9
32.0
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
18.9
33.0
Certified
1.00
ppm
3.00
3.00
1.000
#N/A
16.000
0.099
34.000
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
828
35
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
133
36
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
6.05
37.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.428
38.000
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
7.09
39.00
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
11.4
40.0
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
112
41
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
534
42
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
1908
43
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
3.23
44.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
23.6
45.0
Indicative
1.00
ppb
0.00
0.00
1
7
16
4
9
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
3.71
46.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
205
47
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
4.04
48.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
60
49
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.14
50.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
12.9
51.0
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
459
52
Certified
1.00
ppm
2.00
2.00
1.00
6.00
16.00
<1
53.00
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
0.23
54.00
Certified
1.00
ppm
0.00
0.00
1
#N/A
16
56
55
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
5.90
56.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.191
57.000
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
4.18
58.00
Indicative
1.00
ppm
3.00
3.00
1.000
4.000
16.000
0.088
10.000
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
2.71
59.00
Certified
1.00
ppm
1.00
2.00
1.0
#N/A
16.0
32.0
60.0
Certified
1.00
ppm
1.00
1.00
1.0
#N/A
16.0
14.0
61.0
Certified
1.00
ppm
2.00
3.00
1.00
#N/A
16.00
5.64
62.00
Certified
1.00
ppm
2.00
2.00
1.00
#N/A
16.00
0.61
63.00
Certified
1.00
wt.%
3.00
3.00
1.000
#N/A
16.000
0.920
64.000
Certified
1.00
ppm
0.00
1.00
1
#N/A
16
78
65
Analytical results for C in OREAS 603 (Indicative Value 0.068 wt.%)
C Round Replicate Lab Lab
No No 02 21
IRC IRC
1 1 0.070 0.066
1 2 0.070 0.063
1 3 0.070 0.065
1 4 0.070 0.067
1 5 0.070 0.067
1 6 0.070 0.067
Mean 0.070 0.066
Median 0.070 0.066
Std Dev. 0.000 0.001
Rel.Std.Dev. 0.00% 2.22%
PDM3 3.11% -3.11%

No No 01 05 06 07
IRC IRC IRC IRC
1 1 4.07 4.04 3.89 3.87

1 2 4.05 4.04 3.94 3.89
1 3 3.91 4.08 3.87 3.92
1 4 4.06 4.04 3.90 3.92
1 5 4.06 4.05 3.87 3.98
1 6 3.95 4.03 3.91 3.95
Mean 4.02 4.05 3.90 3.92
Median 4.06 4.04 3.90 3.92
Std Dev. 0.069 0.018 0.027 0.040
Rel.Std.Dev. 1.71% 0.43% 0.68% 1.01%
PDM3 1.18% 1.94% -1.84% -1.21%
Z-Score (Absolute) 0.32 0.37 0.47 0.33
09 11 12 14 17 18 19
IRC IRC IRC IRC IRC IRC IRC
3.92 3.90 4.19 3.90 3.85 4.43 3.95

3.94 3.86 4.22 3.88 3.73 4.37 3.87
3.95 3.89 4.22 3.89 3.80 4.36 3.94
3.95 3.86 4.16 3.73 4.10 4.44 3.89
3.93 3.88 4.21 3.76 4.19 4.42 4.05
3.95 3.87 4.23 3.91 4.42 4.40 3.98
3.94 3.88 4.21 3.85 4.02 4.40 3.95
3.94 3.88 4.22 3.89 3.98 4.41 3.95
0.014 0.016 0.026 0.079 0.267 0.036 0.065
0.35% 0.42% 0.62% 2.05% 6.65% 0.82% 1.64%
-0.76% -2.35% 5.92% -3.14% 1.14% 10.93% -0.58%
0.23 0.59 1.26 0.76 0.19 2.38 0.19
Lab Lab Lab Lab Lab
21 22 24 25 26
IRC IRC IRC IRC IRC
4.38 4.21 3.76 4.17

4.39 4.19 3.68 4.18
4.55 4.21 3.84 4.11
4.51 4.17 3.67 4.19
3.97 3.79 4.23 3.90 4.15
4.43 3.69 4.20 3.64 4.14
4.37 3.74 4.20 3.75 4.16
4.41 3.74 4.21 3.72 4.16
0.206 0.071 0.020 0.104 0.029
4.72% 1.89% 0.49% 2.77% 0.71%
10.13% -5.79% 5.84% -5.58% 4.71%
2.64 1.35 1.24 1.31 0.99
Indicative
1.00
wt.%
3.00
3.00
1.000
10.000
16.000
0.068
16.000
Certified
1.00
wt.%
2.00
3.00
1.00
#N/A
16.00
3.97
126.00

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Table 1.

Abbreviations used for OREAS 603

Batch & Limits

one sigma standard deviation

4-acid (HF-HNO3-HClO4-HCl) digest with AAS finish

- Outlying individual values

- Outlying laboratory batch data sets and superfluous limit values

Laboratory Name and Location

Accurassay, Thunder Bay, Ontario, Canada

294 278 291

301 292 303

300 289 297

4.06 3.91 4.03

Constituent Unit Value Constituent Unit Value Constituent

ppm < 0.01

Constituent Unit Value Constituent Unit Value Constituent

Laser Ablation ICP-MS

Certified Absolute Standard Deviations Relative Standard Deviat

11.18% 16.76% 270 299

5.47% 8.20% 283 312

8.80% 13.20% 278 308

8.12% 12.19% 3.77 4.17

Analytical results for Au in OREAS 603 (Certified Value 5.18 ppm)

Analytical results for Pd in OREAS 603 (Indicative Value 754 ppb)

Analytical results for Pt in OREAS 603 (Indicative Value 144 ppb)

Lab Lab Lab Lab Lab Lab Lab

4.98 5.09 5.04 5.27 4.97 5.14 5.10

Lab Lab Lab Lab Lab Lab Lab

5.30 5.24 5.44 5.08 5.26 5.16 5.38

5.20 5.20 5.28 4.73 4.57 5.27 5.21

5.13 5.41 4.96

Analytical results for Al in OREAS 603 (Certified Value 0.58 wt.%)

Analytical results for As in OREAS 603 (Certified Value 1766 ppm)

Analytical results for Au in OREAS 603 (Certified Value 5.08 ppm)

Analytical results for B in OREAS 603 (Certified Value < 10 ppm)

Analytical results for Ba in OREAS 603 (Indicative Value 686 ppm)

Analytical results for Bi in OREAS 603 (Certified Value 151 ppm)

Analytical results for Ca in OREAS 603 (Certified Value 0.237 wt.%)

Analytical results for Cd in OREAS 603 (Certified Value 55 ppm)

Analytical results for Ce in OREAS 603 (Certified Value 13 ppm)

Analytical results for Co in OREAS 603 (Certified Value 15.2 ppm)

Analytical results for Cr in OREAS 603 (Certified Value 29.2 ppm)

Analytical results for Cs in OREAS 603 (Certified Value 0.74 ppm)

Analytical results for Cu in OREAS 603 (Certified Value 1.01 wt.%)

Analytical results for Dy in OREAS 603 (Certified Value 0.56 ppm)

Analytical results for Er in OREAS 603 (Certified Value 0.22 ppm)

Analytical results for Eu in OREAS 603 (Certified Value 0.25 ppm)

Analytical results for Fe in OREAS 603 (Certified Value 2.85 wt.%)

Analytical results for Ga in OREAS 603 (Certified Value 6.58 ppm)

Analytical results for Gd in OREAS 603 (Certified Value 0.86 ppm)

Analytical results for Ge in OREAS 603 (Indicative Value 1.35 ppm)

Analytical results for Hf in OREAS 603 (Certified Value 0.46 ppm)

Analytical results for Hg in OREAS 603 (Certified Value < 4 ppm)

Analytical results for Ho in OREAS 603 (Certified Value 0.096 ppm)

Analytical results for In in OREAS 603 (Certified Value 11.7 ppm)

Analytical results for K in OREAS 603 (Certified Value 0.093 wt.%)

Analytical results for La in OREAS 603 (Certified Value < 10 ppm)

Analytical results for Li in OREAS 603 (Certified Value 4.62 ppm)

Analytical results for Lu in OREAS 603 (Certified Value 26 ppb)