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Designation: F 1 – 03

Standard Specification for


Nickel-Clad and Nickel-Plated Steel Strip for Electron Tubes1
This standard is issued under the fixed designation F 1; the number immediately following the designation indicates the year of original
adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A superscript
epsilon (e) indicates an editorial change since the last revision or reapproval.

1. Scope 4.2 The material when fully annealed shall be capable of


1.1 This specification covers steel strip, nickel-clad or being bent flat upon itself without cracking, chipping, or
nickel-plated on both sides, for use in electron tubes. separating. This test shall be made with 0.5-in. (13-mm) wide
1.2 The values stated in inch-pound units are to be regarded samples taken both lengthwise and crosswise to the grain of the
as the standard. The metric equivalents of inch-pound units strip. Examination shall be made under 103 magnification.
may be approximate. 5. Thickness of Cladding or Plating
2. Referenced Documents 5.1 Nickel Cladding— The nickel cladding on each side
2.1 ASTM Standards: 2 shall conform to one of the following thickness requirements:
B 487 Test Method for Measurement of Metal and Oxide 5.1.1 Type I—A thickness of 10 6 1 % of the total thickness
Coating Thickness by Microscopical Examination of a of the strip.
Cross Section 5.1.2 Type II—A thickness of 15 6 1 % of the total
E 30 Test Methods for Chemical Analysis of Steel, Cast thickness of the strip.
Iron, Open-Hearth Iron, and Wrought Iron3 5.2 Nickel Plating— The nickel plating on each side shall
E 39 Test Methods for Chemical Analysis of Nickel3 conform to one of the following thickness requirements:
F 155 Test Method for Temper of Strip and Sheet Metals for 5.2.1 Type I—A thickness of 0.00012 in. (0.0030 mm), min.
Electronic Devices (Spring-Back Method)4 5.2.2 Type II—A thickness of 0.00025 in. (0.0064 mm),
F 239 Specification for Nickel Alloy Cathode Sleeves for min.
Electron Devices5 5.3 The thickness of the plating or cladding shall be
determined by metallographic examination of a transverse
3. Chemical Analysis section as described in Test Method B 487, or by any method
3.1 The chemical analysis of the steel shall be in accordance agreed upon by the producer and the consumer.
with Methods E 30. NOTE 1—A metallographic technique may be found in the Symposium
3.2 The chemical analysis of the nickel shall be made in on Methods of Metallographic Specimen Preparation.6
accordance with Methods E 39.
6. Temper
4. Bonding of Cladding or Plating 6.1 The temper of the strip shall conform to limits agreed
4.1 The nickel cladding may be bonded to the steel base by upon by the producer and the consumer, and shall be deter-
any process that will permit conformance to the requirements mined in accordance with Test Method F 155.
of this specification, except that no other material shall be
employed as a bonding agent. In the preparation of nickel- 7. Dimensions, Mass and Permissible Variations
plated steel no underplate shall be applied and no brighteners 7.1 Thickness—The thickness of the material shall conform
shall be used in the electroplating bath. to the following tolerances:
Thickness Tolerance,
Thickness, in. (mm) in. (mm)
Under 0.010 (0.25) 60.0005 (0.013)
1
This specification is under the jurisdiction of ASTM Committee F01 on 0.010 to 0.020 (0.25 to 0.50), incl 60.0008 (0.0203)
Electronics and is the direct responsibility of Subcommittee F01.03 on Metallic
Materials. The thickness shall be measured 0.375 in. (9.5 mm) from the
Current edition approved Dec. 1, 2003. Published January 2004. Originally edge on 1-in. (25.4-mm) or wider strip, or at any point on
approved in 1957. Last previous edition approved in 1994 as F 1–94 (2000).
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
narrower strip.
contact ASTM Customer Service at [email protected]. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3 6
Discontinued; see 1994 Annual Book of ASTM Standards, Vol 03.05. H. S. Link, “Mechanical Polishing of Metallographic Specimens,” Symposium
4
Discontinued, see 1983 Annual Book of ASTM Standards, Vol 10.04. on Methods of Metallogrpahic Specimen Preparation, ASTM STP 285, ASTTA,
5
Discontinued; see 1990 Annual Book of ASTM Standards, Vol 10.04. ASTM, 1961, pp. 8–11.

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.

1
F 1 – 03
7.2 Width—For strip less than 3.0 in. (76 mm) wide and less TABLE 2 Chemical Requirements of Nickel
than 0.020 in. (0.5 mm) thick, the width tolerance shall be6 Composition,%
0.005 in. (0.13 mm). Element UNS N02233 UNS N02205 UNS N02253
7.3 Edgewise Bow shall be a maximum of 0.5 in. (13 mm) Grade 1 A Grade 2 Grade 3 A
in 8 ft (2.4 m). Nickel (plus 99.0 99.0 99.9
7.4 Edge—The edge shall be such as would result from a cobalt), min
B C
Carbon, max 0.10 0.10 0.02
standard slitting operation. Copper, max 0.10 0.10 0.01
7.5 Burr—The burr shall not exceed one half the strip Iron, max 0.10 0.10 0.05
thickness or 0.0025 in. (0.064 mm) whichever is smaller, as Magnesium 0.10 max 0.01–0.08 0.005 max
Manganese, 0.30 0.30 0.003
measured in accordance with the procedure described in the max
Appendix. Silicon, max 0.10 0.10 0.005
Sulfur, max 0.005 0.005 0.003
8. Workmanship, Finish, and Appearance Titanium 0.005 max 0.005 max 0.005 max
Cobalt, max ... ... 0.10
8.1 The surface shall be as smooth and free of dirt, oxide, Chromium, ... ... 0.005
pits, scratches, seams, slivers, streaks, stains, scale, blisters, max
A
edge cracks, trimming burrs, and other defects, as best com- B
Duplicates chemistry of cathode Grade 23 in Specification F 239.
For rerolling, 0.15 max % carbon is allowed.
mercial practice will permit. Examination shall be made at C
Carbon of 0.02 % available in request.
103 magnification.
9. Coiling and Spooling
9.1 Each coil or spool shall have only one continuous length 11. Rejection
of strip, free from joints of any kind, unless otherwise agreed. 11.1 Any spools or coils not conforming to the specified
9.2 The strip shall be so coiled that the normal curvature is requirements may be rejected. If 15 % of the spools or coils in
not reversed. any shipment do not conform to the specified requirements, the
entire shipment may be rejected.
10. Chemical Requirements
10.1 The base metal shall be an aluminum-deoxidized 12. Product Marking
low-carbon steel conforming to the requirements as to chemi- 12.1 Each coil or spool shall be marked plainly as follows:
cal composition as prescribed in Table 1. 12.1.1 Name of material,
10.2 The nickel plating shall conform to the following 12.1.2 Name of manufacturer,
requirements as to chemical composition: 12.1.3 Lot or manufacturer’s identification number,
Nickel plus cobalt, min, % 99.95 12.1.4 Gross, tare, and net weight,
10.3 The nickel cladding shall conform to the requirements 12.1.5 Thickness and width of strip,
of Table 2, Grades 1, 2, or 3 as required. 12.1.6 Shipping date, and
12.1.7 Inspector’s number or designation.
TABLE 1 Chemical Requirements of Steel Strip
Low-Carbon Steel A
13. Packaging
Element
Composition, % 13.1 The packaging shall be adequate to protect the spools
Iron 99.1 min or coils from contamination and damage during shipment. If a
Carbon, max 0.11 protective coating is used, it shall be completely removable by
Manganese, max 0.50
Phosphorus, max 0.040 trichloroethylene degreasing.
Sulfur, max 0.050
Others 0.10 max, each,
0.20 total
14. Keywords
A
The material intended is AISI Grade 1008 (or lower carbon) aluminum- 14.1 electron tubes; electroplated nickel; nickel-clad steel
deoxidized steel. strip; steel strip; UNS N02205; UNS N02233; UNS N02253

2
F 1 – 03
APPENDIX

(Nonmandatory Information)

X1. PROCEDURE FOR MEASURING BURR ON STRIP

X1.1 Apparatus micrometer until the reading settles. Then open the anvils and
X1.1.1 The instrument used to measure the burr on strip insert the edge of the strip. Close the anvils and take the
shall be a bench micrometer with a dial indicator and an reading. The difference between the body and edge reading is
adjustable anvil pressure or equivalent. The anvil diameter the height of the burr.
shall be 0.25 in. (6.4 mm) and the pressure used shall be 200
to 250 g.
X1.2 Procedure
X1.2.1 Measure the body thickness of strip as close to the
edge as possible. Jog the specimen between the anvils of the

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