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24.1.1.11 Standard test pack as described in 26.1.
24.1.2 Procedure
24.1.2.1 Connect the needle valve to the steam pipe
as shown in figure 7.
24.1.2.2 Assemble the apparatus as shown in figure 7 and then locate it in a position which will allow the free
drainage of condensate through the rubber tubing.
24.1.2.3 Fill the container with cold de-aerated water (water which has been boiled for 5 min and then cooled),
until it flows through the overflow pipe.
24.1.2.4 Fill the burette with cold de-aerated water, invert it and place it in the container ensuring that no air is
introduced into the burette.
24.1.2.5 With the steam sampling pipe out of the container, open the needle valve and purge all air from the pipe.
Place the sampling pipe in the container and add more cold de-aerated water until it flows through
the overflow pipe.
24.1.2.6 Position the graduated cylinder under the container overflow and locate the steam sampling pipe within
the funnel. Adjust the needle valve to allow a
continuous sample of steam into the funnel sufficient to cause a small amount of 'steam hammer' to be heard.
Ensure that the steam entering the funnel is discharged so that the non-condensable gases are
collected in the burette.
24.1.2.7 Close the needle valve, after first noting the 'open' position.
24.1.2.8 Place the standard test pack above the nominal geometric centre of the horizontal plane of the usable
space supported at a distance of
between 100 mm and 200 mm above the sterilizer chamber base.
For sterilizers of one sterilization module the method shall be modified such that the standard test pack is supported
above the base of the sterilizer chamber.
24.1.2.9 Start a sterilization cycle and ensure that the graduated cylinder is empty and the container is filled with
water. When the steam supply to the sterilizer chamber commences, re-open the needle valve to
allow a continuous sample of steam into the funnel sufficient to cause a small amount of 'steam hammer to be
heard.
24.1.2.10 Allow the steam sample to condense in the funnel and the non-condensable gases to rise to the top of
the burette. Collect the overspill formed by the condensate and the water displaced by the gases in the graduated
cylinder. Close the needle valve when the temperature of the water in the container is between 70 °C and 75 °C.
Record the volume (7b) of water displaced from the burette and the volume (Fc) of water collected in the graduated
cylinder.
NOTE. A sequence of tests should be undertaken to determine whether the level of non-condensable gases in the steam is variable.
NOTE. If the connection to the steam pipe is less than 300 mm from the pitot connection, (see figure 9) reproducibility of the test can be
affected.
Figure 7. Diagrammatic representation of the apparatus for the measurement of non-condensable

gases
24.1.2.11 Calculate the concentration of non-
condensable gases as a percentage as follows:
where
V\) is the volume of water displaced from the burette, in millilitres;
Vc is the volume of water collected in the graduated cylinder, in millilitres.
24.1.2.12 Check that the result complies with the requirements specified in 13.3.2.
24.2 Dryness
NOTE 1. A continuous supply of dry saturated steam is required for steam sterilization. Excess moisture carried in suspension can cause
damp loads, while too little cannot prevent the steam from becoming superheated during expansion into the sterilizer chamber. The
accurate measurement of the percentage of moisture content in the steam is difficult and the traditional methods where constant steam flow
is required are not suitable for sterilizers. The test method described should be regarded not as measuring the true content of moisture in
the steam, but as a method by which the provision of acceptable steam quality can be demonstrated.
NOTE 2. An alternative procedure to the one described in 24.2 can be used providing it has been calibrated against this standard.
24.2.1 Apparatus
24.2.1.1 Pitot tube constructed as shown in figure 8 and fitted with a sensing tube having a nominal bore to suit the
pressure in the steam pipe from which the sample is to be taken.
24.2.1.2 Dewar flask of 11 nominal capacity.
24.2.1.3 Gland for inserting a temperature sensor into the steam pipe.
24.2.1.4 Thermometric recording instrument as described in 26.4 but having a scale range which includes 0 °C
to 200 °C.
24.2.1.5 Two temperature sensors as described in 26.3.
24.2.1.6 Rubber stopper, fitted with two 6 mm (nominal) outside diameter pipes for insertion into the Dewar flask.
Nominal lengths of insertion of the pipes 25 mm and 150 mm respectively. Rubber tubing, self-draining, having a
length of (450 ± 50) mm and a bore suitable for connection to the pitot tube and the longer of the tubes in the rubber
stopper.
24.2.1.7 Balance, capable of weighing a load of at least 2 kg and with an accuracy of at least ± 0,1 g.
24.2.1.8 Standard test pack as described in 26.1.
24.2.2 Procedure
24.2.2.1 Carry out a steam quality test for non-condensable gases in accordance with 24.1. If the values are not
within the limits specified in 13.3.2 the
fault shall be corrected before carrying out this test.
24.2.2.2 Fit the pitot tube concentrically within the steam service pipe as shown in figure 9.
24.2.2.3 Fit the temperature sensor entry gland to the steam service pipe and locate one of the temperature sensors
at the nominal axial centre of the pipe.
24.2.2.4 Connect the rubber tube to the longer of the pipes in the stopper and then place the stopper in the neck of
the Dewar flask, weigh the whole assembly and record the mass (rae).
24.2.2.5 Where the sterilizer has a number of sterilization cycles, select the textile cycle with a sterilization
temperature of 134 °C.
24.2.2.6 Cany out a sterilization cycle with the sterilizer chamber empty.
24.2.2.7 Remove the stopper and tube assembly and place (650 ± 50) ml of water at a temperature not exceeding 27
°C into the Dewar flask. Replace the stopper and tube assembly, weigh the whole assembly
and record the mass (ms).
24.2.2.8 Support the Dewar flask close to the pitot tube connection point and in a position which is protected from
excess heat and draughts.
24.2.2.9 Place the standard test pack as described in 26.1 in the sterilizer chamber.
24.2.2.10 Introduce the second temperature sensor through the shorter of the pipes in the stopper and into the
Dewar flask.
24.2.2.11 Note the temperature of the fluid in the Dewar flask (Ti).
24.2.2.12 Carry out a sterilization cycle. When the steam valve connected to the sterilizer chamber first opens,
attach the rubber tube to the pitot tube connection point, ensuring free drainage of condensate
into the Dewar flask.
24.2.2.13 Note the temperature of the steam {T3).
24.2.2.14 When the temperature of the water in the Dewar flask is approximately 80 CC, disconnect the rubber tube
from the pitot tube connection; agitate the flask so that the contents are thoroughly mixed and
then note Hie temperature of the fluid (T^).
24.2.2.15 Weigh the Dewar flask complete with water, condensate, stopper and tube (m£).
24.2.2.16 Calculate the dryness value of the steam from the equation:
where
L is the latent heat of dry saturated steam at
temperature T^ in kilojoules per kilogram; me is the mass of the Dewar flask and stopper,
pipes and tube, in kilograms; ms is the mass of the Dewar flask, water charge,
stopper, pipes and tube, in kilograms; mf is the mass of the flask, water charge,
condensate, stopper, pipes and tube in
kilograms;
Dimensions in millimetres
1 Suitable fitting for locating a temperature sensor into the tube
2 Nylon socket, fit into the tube
Figure 10. Expansion tube

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24.1.1.11 Standard test pack as described in 26.1.

Figure 7. Diagrammatic representation of the apparatus for the measurement of non-condensable

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