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    Banyu Idzhar
    The document describes the results of a titration experiment to determine the concentration of H3PO4. It includes a table with the volume of NaOH added, measured pH values, and pH differentials. It then shows the calculations to determine the concentration of H3PO4 from the titration curve, found to be 1.5 M. It also provides an overview of the experimental procedure and materials used, which involved titrating 5 mL of H3PO4 solution with NaOH while monitoring pH with a meter.

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    Perhitungan

    Uploaded by

    Banyu Idzhar
    11 views4 pages
    The document describes the results of a titration experiment to determine the concentration of H3PO4. It includes a table with the volume of NaOH added, measured pH values, and pH differentials. It then shows the calculations to determine the concentration of H3PO4 from the titration curve, found to be 1.5 M. It also provides an overview of the experimental procedure and materials used, which involved titrating 5 mL of H3PO4 solution with NaOH while monitoring pH with a meter.

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    The document describes the results of a titration experiment to determine the concentration of H3PO4. It includes a table with the volume of NaOH added, measured pH values, and pH differentials. It then shows the calculations to determine the concentration of H3PO4 from the titration curve, found to be 1.5 M. It also provides an overview of the experimental procedure and materials used, which involved titrating 5 mL of H3PO4 solution with NaOH while monitoring pH with a meter.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    11 views4 pages

    Perhitungan

    Uploaded by

    Banyu Idzhar
    The document describes the results of a titration experiment to determine the concentration of H3PO4. It includes a table with the volume of NaOH added, measured pH values, and pH differentials. It then shows the calculations to determine the concentration of H3PO4 from the titration curve, found to be 1.5 M. It also provides an overview of the experimental procedure and materials used, which involved titrating 5 mL of H3PO4 solution with NaOH while monitoring pH with a meter.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    of 4

    2

    No. Volume (ml) pH


    2
    1 0 0,85
    2-1 = 0,002 2-1 = 0
    2 5 0,86
    3-2 = 0,002 3-2 = 0
    3 10 0,87
    4-3 = 0,002 4-3 = 0
    4 15 0,88
    5-4 = 0,006 5-4 = 8.10-4
    5 20 0,91
    6-5 = 0,012 6-5 = 1,2.10-3
    6 25 0,97
    7-6 = 0,004 7-6 = -1,6.10-3
    7 30 0,99
    8-7 = 0,0028 8-7 = 4,8.10-4
    8 35 1,004
    9-8 = 0,004 9-8 = 2,4.10-4
    9 40 1,024
    10-9 = 0,0024 10-9 = 4.10-4
    10 45 1,036
    11-10 = 0,0044 11-10 = 4.10-4
    11 50 1,058

    PERHITUNGAN

    Diferensial H3PO4 :

    7 6 0,97 0,91 0,06


    = = = = 0,012
    7 6 30 25 5
    2 0,012 0,06 0,06
    = = = 1,2.103
    2 5 5
    Konsentrasi H3PO4 :

    = [ + ]
    = .
    (10 )2
    =

    (10 )2
    =

    (100,97 )2
    =
    7,5.103
    101,94
    =
    7,5.103
    101,06
    =
    7,5
    11,48
    =
    7,5
    = 1,5

    BAB III
    METODE KERJA

    3.1. Alat
    Adapun alat yang digunakan dalam praktikum titrasi potensiometri ialah erlenmeyer,
    pipet volume, magnetic stiring, hot plategelas ukur, pipet ukur.
    3.2. Bahan
    Adapun bahan yang digunakan dalam praktikum titrasi potensiometri ialah aquadest,
    NaOH dan H3PO4.
    3.3. Prosedur Kerja

    Siapkan alat dan bahan yang akan digunakan. Pipet H3PO4 sebanyak 5 ml kedalam labu ukur,
    encerkan hingga batas 100 ml. Masukkan larutan dan magnetic stiring ke dalam erlenmeyer.
    Letakkan erlenmeyer diatas hot plate untuk menghubungkan magnetic stiring. Hubungkan
    larutan dengan pH meter yang telah dihubungkan dengan sumber arus. Nyalakan hot plate agar
    magnetic stiring mulai mengaduk. Pipet NaOH ke dalam pipet volume hingga pada tanda batas.
    Lakukan titrasi dengan menambahkan NaOH secara berkala hingga total 50 ml dan ukur pH
    dengan menggunakan pH meter. Lakukan titrasi sampai terkumpul jumlah titik yang cukup
    untuk membuat titrasi. Gambarkan kurva dan tentukan letak titik ekuivalen menggunakan
    metode penentuan, serta hitung konsentrasi larutan H3PO4.

    LAMPIRAN I
    DOKUMENTASI HASIL ANALISA

    Pengenceran Asam Fosfat Persiapan Titrasi Titrasi Potensiometri

    Data yang dikumpulkan


    Titrasi Selesai
    LAMPIRAN II
    SKEMA KERJA SECARA UMUM
    POTENSIOMETRI

    SAMPEL

    Ambil 5 ml dan diencerkan dalam labu ukur


    sampai batas 100 ml.

    Masukkan ke dalam erlenmeyer.

    Masukkan magnetic stiring dan pH meter.

    Isi pipet volume dengan NaOH hingga 30 ml,


    Lakukan titrasi hingga 50 ml.

    Amati perubahan pH pada meter pH meter.

    Buat kurva titrasi potensiometri dan


    hitunglah konsentrasi H3PO4.

    HASIL
    PENGAMATAN

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