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    Uncertainty Budget Tables

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    Jepri Purwanto
    The document provides examples of uncertainty budget tables for various measurement standards and procedures, including air density, mass, length, and volume. Each table lists the components that contribute to measurement uncertainty, such as standards uncertainty, process uncertainty, environmental factors like temperature and pressure, and device properties. References are provided for estimating the standard uncertainty of each component. The document aims to demonstrate how to construct comprehensive uncertainty budgets.

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    © All Rights Reserved
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    Uncertainty Budget Tables

    Uploaded by

    Jepri Purwanto
    233 views11 pages
    The document provides examples of uncertainty budget tables for various measurement standards and procedures, including air density, mass, length, and volume. Each table lists the components that contribute to measurement uncertainty, such as standards uncertainty, process uncertainty, environmental factors like temperature and pressure, and device properties. References are provided for estimating the standard uncertainty of each component. The document aims to demonstrate how to construct comprehensive uncertainty budgets.

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    The document provides examples of uncertainty budget tables for various measurement standards and procedures, including air density, mass, length, and volume. Each table lists the components that contribute to measurement uncertainty, such as standards uncertainty, process uncertainty, environmental factors like temperature and pressure, and device properties. References are provided for estimating the standard uncertainty of each component. The document aims to demonstrate how to construct comprehensive uncertainty budgets.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    233 views11 pages

    Uncertainty Budget Tables

    Uploaded by

    Jepri Purwanto
    The document provides examples of uncertainty budget tables for various measurement standards and procedures, including air density, mass, length, and volume. Each table lists the components that contribute to measurement uncertainty, such as standards uncertainty, process uncertainty, environmental factors like temperature and pressure, and device properties. References are provided for estimating the standard uncertainty of each component. The document aims to demonstrate how to construct comprehensive uncertainty budgets.

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    © All Rights Reserved
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    of 11

    EXAMPLES OF UNCERTAINTY BUDGET TABLES

    AIR DENSITY
    SOP 2

    BUOYANCY CORRECTIONS (NISTIR 6969)


    Equation 1. OIML R 111

    u 2 u 2

    x
    u a [m s (a n )]2 4s 4x
    u m s s
    s
    s x
    x

    2
    bc

    Equation 2. SOP 2 Magnitude of Air Buoyancy Correction

    MABC m0 (

    )( a n )

    Component
    Description
    Standard uncertainty for air density
    ua
    ue
    Standard uncertainty for air density
    equation
    ut
    Standard uncertainty for temperature
    urh
    up
    us
    ux

    Reference

    CIPM Air density paper,


    e.g., 0.0012 mg/cm3
    HB 143 accuracy guideline,
    0.5 C; SOP 2 (NISTIR 6969)
    Standard uncertainty for relative humidity HB 143 accuracy guideline,
    5 %; SOP 2 (NISTIR 6969)
    Standard uncertainty for pressure
    HB 143 accuracy guideline,
    65 Pa; SOP 2 (NISTIR 6969)
    Calibration report, e.g., 0.008 %
    Standard uncertainty for density of
    (0.00064 g/cm3)
    standard (s)
    Standard uncertainty for density of
    Mfg. estimate, 0.05 g/cm3
    unknown (x)

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Page 1 of 11

    MASS
    SOP 3 (DOUBLE SUBSTITUTION, EQUAL ARM) (NISTIR 6969)
    SOP 4 (DOUBLE SUBSTITUTION) (NISTIR 6969)
    SOP 5 (THREE IN ONE) (NISTIR 6969)
    SOP 6 (TRANSPOSITION) (NISTIR 6969)
    SOP 7 (SINGLE SUBSTITUTION) (NISTIR 6969)

    Cx = Cs + d + disparity (bias/drift) + unrelated corrections


    Mx = Ms + d + a (Vx Vs) + disparity (bias/drift) + unrelated corrections
    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for the process

    ubc
    ua
    ue

    ut
    urh
    up
    us
    ux
    ud

    uba
    usens
    uresol
    uecc load
    umag
    uo

    Reference
    Calibration report, divide by k
    Measurement assurance process;
    control charts

    Standard uncertainty for buoyancy


    correction
    Standard uncertainty for air density
    Standard uncertainty for air density equation CIPM Air density paper
    (Davis/Giacomo, 1992), e.g.,
    0.0012 mg/cm3
    Standard uncertainty for temperature
    HB 143 accuracy guideline,
    0.5 C; SOP 2 (NISTIR 6969)
    Standard uncertainty for relative humidity
    HB 143 accuracy guideline,
    5 %; SOP 2 (NISTIR 6969)
    Standard uncertainty for pressure
    HB 143 accuracy guideline,
    65 Pa; SOP 2 (NISTIR 6969)
    Standard uncertainty for density of standard Calibration report, e.g.,
    e.g., 0.008 % (0.00064 g/cm3)
    (s)
    Standard uncertainty for density of
    Mfg. Estimate, 0.05 g/cm3
    unknown (x)
    Standard uncertainty for disparity due to
    Rectangular distribution and
    drift/bias
    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)
    Standard uncertainty of the balance
    Typically not used if sp is used.
    Standard uncertainty due to sensitivity of
    OIML R111-1
    balance
    Standard uncertainty due to digital
    OIML R111-1
    resolution of balance
    Standard uncertainty due to eccentric
    OIML R111-1
    loading
    Standard uncertainty due to magnetism
    OIML R111-1
    Standard uncertainty for other factors

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Page 2 of 11

    SOP 8 (MODIFIED SUBSTITUTION) (NISTIR 6969)

    Cx = Cs + d + disparity (bias/drift) + unrelated corrections


    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for the process
    ubc
    Standard uncertainty for buoyancy
    correction
    Standard uncertainty for air density
    ua
    ue
    Standard uncertainty for air density equation

    ut

    Standard uncertainty for temperature

    urh

    Standard uncertainty for relative humidity

    up

    Standard uncertainty for pressure

    us
    ux
    ud

    uba
    usens
    uresol
    uecc load
    umag
    uo

    Standard uncertainty for density of standard


    (s)
    Standard uncertainty for density of
    unknown (x)
    Standard uncertainty for disparity due to
    drift/bias
    Standard uncertainty of the balance
    Standard uncertainty due to sensitivity of
    balance
    Standard uncertainty due to digital
    resolution of balance
    Standard uncertainty due to eccentric
    loading
    Standard uncertainty due to magnetism
    Standard uncertainty for other factors

    Reference
    Calibration report, divide by k
    Measurement assurance process
    Possibly: uncorrected systematic
    error

    CIPM Air density paper


    (Davis/Giacomo, 1992), e.g.,
    0.0012 mg/cm3
    HB 143 accuracy guideline,
    0.5 C; SOP 2 (NISTIR 6969)
    HB 143 accuracy guideline,
    5 %; SOP 2 (NISTIR 6969)
    HB 143 accuracy guideline,
    65 Pa; SOP 2 (NISTIR 6969)
    Calibration report, e.g., 0.008 %
    (0.00064 g/cm3)
    Mfg. Estimate, 0.05 g/cm3
    Rectangular distribution and
    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)
    Typically not used if sp is used.
    OIML R111
    OIML R111
    OIML R111
    OIML R111

    QUESTION: CAN ubc BE ASSUMED TO BE NEGLIGIBLE, AT THIS LEVEL?


    OR IS IT SAFER TO EVALUATE IT AND THEN DECIDE THE
    NEGLIGIBILITY OF IT AND HAVE IT DOCUMENTED?

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Page 3 of 11

    SOP 28 (ADVANCED WEIGHING DESIGNS) (NISTIR 5672)

    Mx = Ms + d + a (Vx Vs) + disparity (bias/drift) + unrelated corrections


    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for the process

    ubc
    ua
    ue

    ut
    urh
    up
    uCO2
    ucce
    us
    ux
    ud

    uba
    usens
    uresol
    uecc load
    umag
    uo

    Reference
    Calibration report, divide by k
    Measurement assurance process;
    control charts

    Standard uncertainty for buoyancy


    correction
    Standard uncertainty for air density
    Standard uncertainty for air density equation CIPM Air density paper
    (Davis/Giacomo, 1992), e.g.
    0.0012 mg/cm3
    Standard uncertainty for temperature
    HB 143 accuracy guideline,
    0.5 C; SOP 2 (NISTIR 6969)
    Standard uncertainty for relative humidity
    HB 143 accuracy guideline,
    5 %; SOP 2 (NISTIR 6969)
    Standard uncertainty for pressure
    HB 143 accuracy guideline,
    65 Pa; SOP 2 (NISTIR 6969)
    Standard uncertainty for carbon dioxide
    determination
    Standard uncertainty for cubical coefficient
    of expansion
    Standard uncertainty for density of standard Calibration report, e.g., 0.008 %
    (0.00064 g/cm3)
    (s)
    Standard uncertainty for density of
    Mfg. Estimate, 0.05 g/cm3
    unknown (x)
    Standard uncertainty for disparity due to
    Rectangular distribution and
    drift/bias
    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)
    Standard uncertainty of the balance
    Typically not used if sp is used.
    Standard uncertainty due to sensitivity of
    OIML R111
    balance
    Standard uncertainty due to digital
    OIML R111
    resolution of balance
    Standard uncertainty due to eccentric
    OIML R111
    loading
    Standard uncertainty due to magnetism
    OIML R111
    Standard uncertainty for other factors

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Page 4 of 11

    LENGTH
    SOP 10 (RIGID RULE) (NBS Handbook 145)

    Lx = Ls + d + disparity (bias/drift) + unrelated corrections


    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for the process

    ugr
    ud

    Standard uncertainty for graduated reticle


    Standard uncertainty for disparity due to
    drift/bias

    ures

    Standard uncertainty due to resetting of the


    rules
    Standard uncertainty for other factors

    uo

    Reference
    Calibration report, divide by k
    Measurement assurance process;
    range charts

    Rectangular distribution and


    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)

    SOP 11 (BENCH METHOD) (NBS Handbook 145)


    SOP 23 (PI TAPES) (NBS Handbook 145)

    Lx = Ls + d + Ln [(t 20) ( - )] + disparity (bias/drift) + unrelated corrections


    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for the process

    ugr
    utc
    ut
    ulce (,)
    utw
    ud

    ures
    uo

    Standard uncertainty for graduated reticle


    Standard uncertainty for temperature
    correction
    Standard uncertainty for temperature

    Reference
    Calibration report, divide by k
    Measurement assurance process;
    range charts

    HB 143 accuracy guideline,


    0.05 C

    Standard uncertainty for linear coefficient of


    expansion
    Standard uncertainty for tension weights
    Standard uncertainty for disparity due to
    Rectangular distribution and
    drift/bias
    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)
    Standard uncertainty due to resetting of the
    tape
    Standard uncertainty for other factors

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Page 5 of 11

    SOP 12 (TAPE TO TAPE)

    Lx = Ls + d + disparity (bias/drift) + unrelated corrections


    Component
    us
    sp
    ugp
    uss
    ud

    Description
    Standard uncertainty for standards
    Standard uncertainty for the process
    Standard uncertainty for graph paper
    Standard uncertainty for spring scales
    Standard uncertainty for disparity due to
    drift/bias

    ures

    Standard uncertainty due to resetting of the


    tapes
    Standard uncertainty for other factors

    uo

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Reference
    Calibration report, divide by k
    Measurement assurance process

    Rectangular distribution and


    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)

    Page 6 of 11

    VOLUME - GRAVIMETRIC
    SOP 13 (MECHANICAL BALANCE)
    SOP 14 (ELECTRONIC BALANCE)
    SOP 15 (EQUAL ARM BALANCE)
    1
    1 (t t ref )
    Vtref M F M E M S M R 1 a

    s w
    a

    1
    1 (t t ref )
    Vtref O3 O2 O1 M S 1 a
    s w a

    Vx = d(F E) + a (Vx Vs) + [1 - (t tref)] + bias/drift + other corrections


    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for the measuring
    process to determine mass difference
    between filled and empty container;
    recorded in volume units on charts to be
    converted to grams by dividing a Z constant
    of 1.003; represents all weighing operations
    ubc
    Standard uncertainty for buoyancy
    correction
    Standard uncertainty for air density
    ua
    ue
    Standard uncertainty for air density equation

    us
    ux
    utc
    ut

    uw

    ut

    Standard uncertainty for temperature

    urh

    Standard uncertainty for relative humidity

    up

    Standard uncertainty for pressure


    Standard uncertainty for density of standard
    (s)
    Standard uncertainty for density of
    unknown (x)
    Standard uncertainty for temperature
    correction
    Standard uncertainty for temperature

    ucce (,) Standard uncertainty for cubical coefficient


    of expansion
    Standard uncertainty for density of water

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Reference
    Calibration report, divide by k
    Measurement assurance process;
    control chart or range chart and
    d2*

    CIPM Air density paper


    (Davis/Giacomo, 1992),
    0.0012 mg/cm3
    HB 143 accuracy guideline,
    0.5 C; SOP 2 (NISTIR 6969)
    HB 143 accuracy guideline,
    5 %; SOP 2 (NISTIR 6969)
    HB 143 accuracy guideline,
    65 Pa; SOP 2 (NISTIR 6969)
    Calibration report, e.g., 0.008 %
    (0.00064 g/cm3)
    Mfg. Estimate, 0.05 g/cm3

    HB 143 accuracy guideline,


    0.05 C
    NBS Report 10 081,
    5 x 10-6 /F (0.000009 / C)

    Page 7 of 11

    ue

    ut

    Standard uncertainty for water density


    equation and uncorrected systematic error
    due to air-free vs air-saturated water
    densities
    Standard uncertainty for temperature

    uread men
    ud

    Standard uncertainty for reading meniscus


    Standard uncertainty for disparity due to
    drift/bias

    uba

    Standard uncertainty of the balance


    Standard uncertainty due to sensitivity of
    balance
    Standard uncertainty due to digital
    resolution of balance
    Standard uncertainty due to eccentric
    loading
    Standard uncertainty due to magnetism
    Standard uncertainty for other factors

    usens
    uresol
    uecc load
    umag
    uo

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Metrologia, Patterson/Morris
    (1994), 7 ppm (0.000007 g/cm3)

    HB 143 accuracy guideline,


    0.1 C, SOPs
    (ASTM E694); GMP 3
    Rectangular distribution and
    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)
    Typically not used if sp is used.
    OIML R111-1
    OIML R111-1
    OIML R111-1
    OIML R111-1

    Page 8 of 11

    VOLUME TRANSFER
    SOP 16 (FLASKS)

    Vx = VsP + VsB + V [1 + ( - ) (t tref)] + disparity (bias/drift) + unrelated corrections


    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for the process

    utc
    ut

    ud

    Standard uncertainty for temperature


    correction
    Standard uncertainty for temperature

    ucce (,) Standard uncertainty for cubical coefficient


    of expansion
    Standard uncertainty for disparity due to
    drift/bias

    uread men
    udrain
    utime piece
    uo

    Standard uncertainty for reading meniscus


    Standard uncertainty due to drain time
    Standard uncertainty for time piece
    Standard uncertainty for other factors

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Reference
    Calibration report, divide by k
    Measurement assurance process;
    control chart or range chart and
    d2*

    HB 143 accuracy guideline,


    0.05 C; SOPs
    NBS Report 10 081,
    5 x 10-6 /F (0.000009 / C)
    Rectangular distribution and
    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)
    (ASTM E694)

    Page 9 of 11

    SOP 18 (GRADUATED NECK)

    Vx = Vs + disparity (bias/drift) + unrelated corrections


    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for the process

    ud

    Standard uncertainty for disparity due to


    drift/bias

    uread men
    udrain
    utime piece
    uo

    Standard uncertainty for reading meniscus


    Standard uncertainty due to drain time
    Standard uncertainty for time piece
    Standard uncertainty for other factors

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Reference
    Calibration report, divide by k
    Measurement assurance process;
    control chart or range chart and
    d2*
    Rectangular distribution and
    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)
    (ASTM E694); GMP 3

    Page 10 of 11

    SOP 19 (LARGE NECK)


    Vx

    w s Vs 1 t t ref
    w x 1 t t ref


    disparity (bias / drift ) unrelated corrections

    Component
    Description
    us
    Standard uncertainty for standards
    sp
    Standard uncertainty for standards
    utc
    Standard uncertainty for temperature
    correction
    ut
    Standard uncertainty for temperature

    uw

    ucce (,) Standard uncertainty for cubical coefficient


    of expansion
    Standard uncertainty for density of water
    ue
    Standard uncertainty for water density
    equation
    ut
    Standard uncertainty for temperature

    ud

    Standard uncertainty for disparity due to


    drift/bias

    uread men
    udrain
    utime piece
    uo

    Standard uncertainty for reading meniscus


    Standard uncertainty due to drain time
    Standard uncertainty for time piece
    Standard uncertainty for other factors

    SOP 29 Job Aid UNCERTAINTY BUDGET TABLE EXAMPLES.doc

    Reference
    Calibration report, divide by k
    Measurement assurance process

    HB 143 accuracy guideline,


    0.05 C
    NBS Report 10 081,
    5 x 10-6 /F (0.000009 / C)
    Metrologia, Patterson/Morris
    (1994), 7 ppm (0.000007 g/cm3)
    HB 143 accuracy guideline,
    0.05 C
    Rectangular distribution and
    reasons, 0.577 d, 0.29 d;
    SOP 29 (NISTIR 6969)
    (ASTM E694)

    Page 11 of 11

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