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    Faculty of Chemical Engineering

    Uploaded by

    Arif Hanafi
    1) The document summarizes an experiment on the titration of acids and bases to determine the molarity of sodium hydroxide (NaOH) and calculate the percentage of potassium hydrogen phthalate (KHP) in unknown samples. 2) Standardization of NaOH was performed by titrating it against KHP and calculating molarity. Unknown samples were then titrated against the standardized NaOH to determine their KHP percentage. 3) The KHP percentage in the unknown samples was found to be 52.75%, 46.60%, and 49.90% respectively. The molarity of NaOH was determined to be 1.0 mol.

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    © All Rights Reserved
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    Faculty of Chemical Engineering

    Uploaded by

    Arif Hanafi
    90 views5 pages
    1) The document summarizes an experiment on the titration of acids and bases to determine the molarity of sodium hydroxide (NaOH) and calculate the percentage of potassium hydrogen phthalate (KHP) in unknown samples. 2) Standardization of NaOH was performed by titrating it against KHP and calculating molarity. Unknown samples were then titrated against the standardized NaOH to determine their KHP percentage. 3) The KHP percentage in the unknown samples was found to be 52.75%, 46.60%, and 49.90% respectively. The molarity of NaOH was determined to be 1.0 mol.

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    1) The document summarizes an experiment on the titration of acids and bases to determine the molarity of sodium hydroxide (NaOH) and calculate the percentage of potassium hydrogen phthalate (KHP) in unknown samples. 2) Standardization of NaOH was performed by titrating it against KHP and calculating molarity. Unknown samples were then titrated against the standardized NaOH to determine their KHP percentage. 3) The KHP percentage in the unknown samples was found to be 52.75%, 46.60%, and 49.90% respectively. The molarity of NaOH was determined to be 1.0 mol.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    90 views5 pages

    Faculty of Chemical Engineering

    Uploaded by

    Arif Hanafi
    1) The document summarizes an experiment on the titration of acids and bases to determine the molarity of sodium hydroxide (NaOH) and calculate the percentage of potassium hydrogen phthalate (KHP) in unknown samples. 2) Standardization of NaOH was performed by titrating it against KHP and calculating molarity. Unknown samples were then titrated against the standardized NaOH to determine their KHP percentage. 3) The KHP percentage in the unknown samples was found to be 52.75%, 46.60%, and 49.90% respectively. The molarity of NaOH was determined to be 1.0 mol.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    of 5

    FACULTY OF CHEMICAL ENGINEERING

    Universiti Teknologi MARA (UiTM) Terengganu


    Kampus Bukit Besi,
    Bukit Besi, Dungun, TERENGGANU

    TECHNICAL/EXECUTIVE REPORT : CHEMICAL ENGINEERING


    Lab No. :
    Topic :

    Module :

    Titration of Acids and Bases

    Mark :
    Date :

    Participant
    *Please cancel which
    is not necessary.

    Instructor

    Course : Chemical Engineering


    No.

    Semester : 1

    Name

    Ezzanie Balqhis bt Basir

    Nurul Nazirah Bt Abdul Rahman

    3/8/2016
    Group

    10

    :
    Matrix No.

    Signatu

    201680069
    4
    201680062
    6

    Sir Rafie

    Objective :
    1
    2

    To determine molarity of standard sodium hydroxide (NaOH)


    To calculate percentage of potassium hydrogen phthalate (KHP) in an unknown
    acidic sample.

    Demonstrate effective team role and responsibility in the task execution.

    Abstract :

    re

    The experiment is briefly about titration of acids and bases.There are two acids
    that were used in this experiment which is potassium hydrogen phthalate (KHP)
    and unknown acid.The base that was used in this experiment is sodium
    hydroxide solution (NaOH).

    The standardization of sodium hydroxide solution (NaOH) are carried out first by
    measuring the weight of weighing paper and potassium hydrogen phthalate
    (KHP) separately.Once the weighing paper and the potassium hydrogen
    phthalate (KHP) are measured,record the reading of mass of both weighing paper
    and hydrogen phthalate (KHP).After that,pour the sodium hydroxide solution
    (NaOH) into the burette until it is full.Mix the potassium hydrogen phthalate
    (KHP) with distilled water in the conical flask until it is dilute.Add 3 drops of
    phenolphthalein into the conical flask.Slowly,add the sodium hydroxide solution
    (NaOH) drop by drop into the conical flask containing dilute potassium hydrogen
    phthalate solution (KHP).

    Observe the changes colour of phenolphthalein from pink colour turns to


    colourless once the sodium hydroxide solution (NaOH) are added into the conical
    flask.

    When the phenolphthalein in the conical flask show changes in colour from pink
    to colourless once the sodium hydroxide solution (NaOH) are added drop by
    drop,it shows that the end point of neutralization between sodium hydroxide
    solution (NaOH) and potassium hydrogen phthalate (KHP).

    Part 1:Standardization of NaOH solution


    Data/Results
    /Calculation:

    No
    1
    2
    3
    4
    5
    6
    7

    Measureme
    nts
    Mass of
    weighing
    paper+KHP
    Mass of
    weighing
    paper
    Mass of KHP
    used
    Final burette
    reading
    Initial
    burette
    reading
    mL of NaOH
    used
    Molarity of
    NaOH

    0.7140g

    0.6670g

    0.5580g

    0.1440g

    0.1440g

    0.1440g

    0.5700g

    0.5230g

    0.4140g

    37.0mL

    33.0mL

    22.0mL

    0.0mL

    0.0mL

    0.0Ml

    20.0mL

    20.0mL

    20.0mL

    1.0 mol

    1.0 mol

    1.0 mol

    0.7144g

    0.6370g

    0.5170g

    0.1440g

    0.1440g

    0.1440g

    0.5704g

    0.4930g

    0.3730g

    37.5mL

    32.5mL

    25.5mL

    0.0mL

    0.0mL

    0.0mL

    20.0mL

    20.0mL

    20.0Ml

    1.1535

    1.1323

    0.8327

    52.75%

    46.60%

    49.90%

    Part 2:Analysis of unknown acidic solution


    No
    1

    2
    3
    4
    5
    6
    7
    8
    Discussion:

    Measureme
    nts
    Mass of
    weighing
    paper+unkn
    own
    Mass of
    weighing
    paper
    Mass of
    unknown
    used
    Final burette
    reading
    Initial
    burette
    reading
    mL of NaOH
    used
    Mass of KHP
    in unknown
    Percent of
    KHP in
    unknown
    The percentage of KHP

    in the sample is 52.75%,46.60% and

    49.90%
    2

    Compute the standard deviation (SD) of the results

    Compute the average deviation from the mean to the test the
    result.Explain the test result.

    There is no effects of NaOH molarity to percentage of KHP in


    unknown sample

    The effects of wrong titration techniques to the experiment results


    is no consistency in the reading of the experiment.

    Conclusion:

    The molarity of the standard sodium hydroxide solution (NaOH) is


    1.0 mol

    The percentage of potassium hydrogen phthalate (KHP) in an


    unknown acidic sample is 52.75%,46.60% and 49.90%

    References:

    Approval

    https://www.coursehero.com

    Chemistry textbook

    Example report at http://ichemey.org

    Authorize Person
    Technician
    Instructor

    Initial

    Date

    Stamp

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