Designation: C 240 97

AMERICAN SOCIETY FOR TESTING AND MATERIALS

100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM

Standard Test Methods of

Testing Cellular Glass Insulation Block1

This standard is issued under the fixed designation C 240; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.

1. Scope
1.1 These test methods cover the testing of cellular glass
insulation block for density, water absorption, compressive
strength, flexural strength at ambient temperature; preparation
for chemical analysis; and thermal conductivity measurements.
1.2 The values stated in SI are generally to be regarded as
the standard. The SI dimensions are to be used for material
supplied in metric sizes. The inch dimensions are to be used for
material supplied in inch sizes.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2.2 ISO Standard:

ISO 3951 Sampling Procedure and Charts for Inspection by
Variables for Percent Defective4
2.3 Military Standard:
MIL-I-24244 Specification Insulation Materials with Special Corrosion, Chloride, and Fluoride Requirements5
2.4 Other Standard:
NRC 1.36 Nonmetallic Thermal Insulation for Austenitic
Stainless Steel6
3. Terminology
3.1 DefinitionsTerminology C 168 shall be considered as
applying to the terms considered in these test methods.
4. Significance and Use
4.1 From a general standpoint, these test methods outline
the particular points which have to be taken into account when
applying ASTM standard test methods to the case of cellular
glass insulating block.

2. Referenced Documents
2.1 ASTM Standards:
C 165 Test Method for Measuring Compressive Properties
of Thermal Insulations2
C 168 Terminology Relating to Thermal Insulating Materials2
C 177 Test Method for Steady-State Heat Flux Measurements and Thermal Transmission Properties by Means of
the Guarded Hot Plate Apparatus2
C 203 Test Methods for Breaking Load and Flexural Properties of Block-Type Thermal Insulation2
C 303 Test Method for Density of Preformed Block-Type
Thermal Insulation2
C 390 Criteria for Sampling and Acceptance of Preformed
Thermal Insulation Lots2
C 518 Test Method for Steady-State Heat Flux Measurements and Thermal Transmission Properties by Means of
the Heat Flow Meter Apparatus2
C 871 Test Methods for Chemical Analysis of Thermal
Insulation Materials for Leachable Chloride, Fluoride,
Silicate, and Sodium Ions2
D 226 Specification for Asphalt-Saturated Organic Felt
Used in Roofing and Waterproofing3

5. Test Methods
5.1 General Sample PreparationAll tests have to be run
on dry specimens. In case of need, the sample must be
unpacked and stored in a dry place in such a way that all
surfaces are exposed to the ambient air for at least one day
before testing.
5.2 DensityDetermine the density in accordance with Test
Method C 303. Preferably, the density shall be measured on a
full block, 450 by 600 mm (18 by 24 in.) by full thickness.
5.2.1 It should be noted that density is interesting as such for
calculation of insulated equipment load and because it has
some influence on the other important properties of cellular
glass. But it should not be considered in itself as a criterion for
acceptance in the case of cellular glass.
5.3 Water Absorption:
5.3.1 ScopeThis test method covers the determination of
water absorption of cellular glass insulating blocks by measuring the amount of water retained as a result of complete
immersion for a prescribed time interval. Surface blotting is
used to correct for the water absorbed on the cut surface cells.

1
These methods are under the jurisdiction of ASTM Committee C-16 on
Thermal Insulation and are the direct responsibility of Subcommittee C16.32 on
Mechanical Properties.
Current edition approved September 10, 1997. Published June 1998. Originally
published as C 240-50 T. Last previous edition C 240-91.
2
Annual Book of ASTM Standards, Vol 04.06.
3
Annual Book of ASTM Standards, Vol 04.04.

4
Available from American National Standards Institute, 11 W. 42nd St., 13th
Floor, New York, NY 10036.
5
Available from Standardization Documents Order Desk, Bldg. 4, Section D,
700 Robbins Ave., Philadelphia, PA 19111-5094.
6
Available from Director of Regulatory Standards, US Atomic Energy Commission, Washington, DC 20545.

C 240
abrasive surface to produce the required flat surface.
5.4.2 The test specimens shall preferably be one half block
300 by 450 mm (12 by 18 in.) by nominal received thickness.
Alternates include a quadrant 225 by 300 mm (9 by 12 in.) or
a full block 450 by 600 mm (18 by 24 in.) by nominal received
thickness. A quadrant specimen shall be taken from any one of
four equal area quadrants of the preformed block. The minimum acceptable specimen size is 200 by 200 mm (8 by 8 in.).
The report shall include the specimen size.
5.4.3 Cap both bearing surfaces of the specimens as follows:
Coat one surface with molten Type III or Type IV asphalt
(preheated to 177, + 28, 14C (350, + 50, 25F)), completely filling the surface cells with a small excess. Such a
coating application rate is approximately 1.0 kg/m2(0.20 lb/ft2)
6 25%. Immediately press the hot coated block onto a precut
piece of felt or paper laying on a flat surface. This is to prevent
the asphalt surface from sticking to the compression platten
during the test. A lightweight kraft paper is suitable, although
traditionally a Type 1 roofing felt paper, commonly called a
No. 15 asphalt felt, per Specification D 226 has been used.

5.3.2 Significance and UseThis test method provides a

means of measuring the water absorption of cellular glass
insulating blocks under isothermal conditions as a result of
direct immersion in liquid water. It is intended for use in
product evaluation and quality control.
5.3.3 Equipment and Materials:
5.3.3.1 Balance, with about 1500 g capacity and at least 0.1
g sensitivity.
5.3.3.2 Immersion Tank, equipped with inert specimen supports and top surface weights such as stainless steel.
5.3.3.3 Synthetic Sponge, at least 100 by 180 by 40 mm (4
by 7 by 1.5 in.). Sponges found acceptable to use include
cellulosic sponges and fine-pored absorbent synthetic plastic
sponges.
5.3.3.4 Test Room, with temperature of 21 6 3C (70 6
5F) and relative humidity of 50 6 10 %.
5.3.3.5 Distilled Water.
5.3.4 Procedure:
5.3.4.1 Carefully measure the thickness, width, and length
to the nearest 1 mm of a cellular glass block, preferably 50 by
300 by 450 mm (2 by 12 by 18 in.) and calculate the volume
and exposed surface area.
5.3.4.2 Weigh the specimen to the nearest 0.1 g (W1), then
submerge it horizontally under 25 mm (1 in.) of water
maintained at 21 6 3C (70 6 5F). Inert top surface weights
are required to keep it submerged. After submerging it for 2 h,
set the specimen on end on a damp cotton bath towel to drain
for 10 min. After the 10 min, remove the excess surface water
by hand with a damp sponge for 1 min per large face and 1 min
for the four sides. Wring out the sponge before and once in
between for each face and pass at least two times on each
surface. Blot each face of the specimen equally by compressing
the sponge by at least 10 % of its thickness. Weigh the
specimen immediately (W2) to the nearest 0.1 g.
5.3.5 Calculation of ResultsCalculate the weight of water
absorbed (W 2 W1) and express it as a function of the exterior
surface of the sample (g/cm 2). Water absorption can also be
expressed as a function of volume percent, absorbed water
volume divided by specimen volume; or as a function of
weight percent, weight of water absorbed (W2 W1) divided
by the dry specimen weight (W1). Such ways of expressing the
results should be strictly limited to direct comparison of results
on specimens of identical sizes.
5.3.6 Precision and BiasThe precision as determined in
inter-laboratory tests is given in Research Report RR C161007.7 The repeatability or single-laboratory operator precision
is 60.00060 g/cm2 or 60.030 volume % (61S). The reproducibility or multilaboratory operator precision is 60.00071
g/cm2 or 60.035 volume %. Due to a lack of a standard, no
statement can be made regarding bias.
5.4 Compressive StrengthDetermine the compressive
strength in accordance with Test Method C 165 Procedure A,
with the following test parameters and specimen preparation
techniques:
5.4.1 Each of the two parallel bearing surfaces of the
specimens shall be plane. If necessary, rub them on a suitable

NOTE 1A hot asphalt capping is used to simulate field applied

systems, which require a high load bearing insulation product, ranging
from roof applications to cryogenic storage tank base applications.
Uncapped material or different cappings will give different values.

Properly capped surfaces should be approximately plane and

parallel. Set the specimens on edge, exposing both capped
surfaces to room temperature for a minimum of 15 min to
allow the asphalt to harden before testing.
5.4.4 The number of specimens to be tested and the sampling plan shall conform to Criteria C 390 where applicable.
For the purpose of inspection by users representative or
independent third party, the number of specimens shall conform to ISO 3951 inspection level S-4, 10.0 % AQL using the
S method.
5.4.5 Compress the specimen until failure. The deformation
at failure will vary, depending on the thickness of insulation
and the thickness of the capping materials. Record the loads at
the failure point or definite yield point. The compressive
strength is calculated from this load divided by the specimen
cross sectional area in accordance with Test Method C 165.
5.4.6 The rate of loading will depend on the type of
equipment used. With a hydraulic test machine use a constant
load rate of 2200 N/s (500 lbf/s) for half block specimen. With
a screw driven machine use a crosshead speed of 0.1 mm/min.
(0.01 in./min.) per cm (in.) of specimen thickness, within a
tolerance of 625 %. Another alternate testing procedure is to
reach the failure within 30 to 90 s [nominal 16kPa/s (2.3
psi/s)].
5.4.7 Due to the sample preparation, with the inclusion of
felts and asphalt, the method described in Test Method C 165
to determine compressive modulus of elasticity does not apply
for cellular glass as a material by itself.
NOTE 2It has been found extremely convenient to employ a partially
submerged roll (see Fig. 1) for applying the asphalt.

5.5 Flexural StrengthDetermine flexural strength in accordance with Test Method C 203, Method I or Method II,
Procedure A, preferably with a test specimen 25 mm thick by

Supporting data from interlaboratory tests are available from ASTM Headquarters. Request RR: C16-1007.

C 240
from several pieces of cellular glass. Joints are prohibited in
the central measuring area and their number should be minimized in the guard area.
5.6.4 The number of specimens to be tested and the sampling plan shall conform to Criteria C 390 where applicable.
For the purpose of inspection by users representative or
independent third party, the number of specimens shall conform to ISO 3951 inspection level S-3, 10.0 % AQL using the
S method.
5.7 Specimen Preparation for Chemical AnalysisWhen
specified in the purchase order or contract, the following
chemical analysis results shall be furnished to the purchaser.
5.7.1 Chemical Analysis for Leachable Chloride, (Fluoride), Silicate, and Sodium IonsDetermine leachable chloride, (fluoride), silicate and sodium ions in accordance with
Test Methods C 871, MIL-I-24244, or NRC 1.36, with the
following exceptions or additions. The test specimen may be
prepared for leaching by either of the following equivalent
methods:
5.7.1.1 Method ABreak about 300 g of the sample into
small size pieces about 13 mm (12 in.) or less. Comminute in
a nominal 4-L (1-gal) mill one-third to one-half full of
appropriate media for about 10 min. Screen out
the 200 + 325 mesh fraction of about 50 g, wash on the finer
screen with 400 to 600 mL of cp methanol using a wash bottle,
and dry on the screen to constant weight at 100 to 110C (212
to 230F). An appropriate grinding media is flint pebbles or
alumina pebbles.
5.7.1.2 Method BBreak about 150 g of the sample into
small size pieces about 13 mm (12 in.) or less. Comminute
using either a manual or motorized mortar and pestle or a
blender, and concurrently screen out the 200 + 325 mesh
fraction until about 50 g is accumulated. Wash the fraction on
the finer screen with 400 to 600 mL of cp methanol, using a
wash bottle, and dry on the screen to constant weight at 100 to
110C (212 to 230F).

FIG. 1 Application of Hot Asphalt to Specimen Surfaces

100 mm wide by 300 mm long ( 1 in. thick by 4 in. wide by 12

in. long ).
5.5.1 Measure the distance between the supports from
center to center of the bearing bars.
5.5.2 The number of specimens to be tested and the sampling plan shall conform to Criteria C 390 where applicable.
For the purpose of inspection by users representative or
independent third party, the minimum number of specimens
shall conform to ISO 3951 inspection level S-3, 10.0 % AQL
using the S method.
5.6 Thermal ConductivityDetermine the thermal conductivity in accordance with Test Method C 177 or Test Method
C 518. In the case of cellular glass, the following points
deserve special attention:
5.6.1 To achieve flatness and parallelism of the surface as
required by Test Method C 177 or Test Method C 518, the
following method is suggested:
5.6.1.1 By sawing from the original block, prepare a specimen with the required dimensions, its thickness being 2 or 3
mm greater than the final thickness should be.
5.6.1.2 Place the specimen on a flat metal plate slightly
larger than the specimen itself and put two machined metal
bars on the metal plate near two opposite sides of the specimen.
Insert a uniform sheet of paper with a thickness about 14 mm
(0.01 in.) between the flat base plate and the metal bars but not
under the sample. The metal bars are as thick as the final
thickness of the specimen and machined so that their top and
bottom surfaces are flat and parallel. Alternatively to machined
bars, one can use cold-rolled steel bars. These bars generally
are sufficiently flat and uniform in thickness.
5.6.1.3 Using a third straight metal bar long enough to lap
metal bars on each side, carefully rub off the upper face of the
specimen until scraping bar just contacts thickness bars.
5.6.1.4 Turn the specimen upside down and place it back on
the flat metal plate and put the two metal bars on the metal
plate near two opposite sides of the specimen, this time without
the sheet of paper under each metal bar.
5.6.1.5 Repeat the rubbing operation described in 5.6.1.3.
5.6.1.6 If the specimens have to be shipped, provide adequate protection.
5.6.2 Due to the rigid nature of the material and its open cell
surface, it is preferable to have the thermocouples mounted in
the surface of the plates and not adhered to the surface of the
specimens.
5.6.3 For maximum accuracy, it is recommended that the
temperature difference between the hot and cold surfaces of the
specimens is such that the temperature gradient in the specimen
equals or exceeds 900 K m1(40 F/in.). Avoid specimens made

NOTE 3Alternatively, the sized fraction may be washed in a specially

made small screen by dunking repeatedly into a container of methanol. In
any case, the screens should be washed first with methanol.

5.7.2 All of the other chemical requirements of Test Methods C 871, MIL-I-24244, and NRC 1.36 are to be followed.
6. Report
6.1 The report shall include the following information:
6.1.1 Density, flexural strength and thermal conductivity
shall be reported as designated in the appropriate method.
6.1.2 Water absorption, in g/cm2.
6.1.3 Compressive strength in accordance with Test Method
C 165, except that the dimensions of the test specimens shall
also be recorded.
6.1.4 Chemical analysis results, if required, as specified in
purchase order.
7. Keywords
7.1 breaking load; breaking strength; cellular materials;
compressive strength; flexural strength; thermal insulating
materials-glass; water absorption

C 240
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